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Stress-Relief Cracking of a Welded Alloy Steel Tube 焊接合金钢管的应力释放开裂
Pub Date : 2019-06-01 DOI: 10.31399/asm.fach.process.c0091009
A thick-walled tube that was weld fabricated for use as a pressure vessel exhibited cracks. Similar cracking was apparent at the weld toes after postweld stress relief or quench-and-temper heat treatment. The cracks were not detectable by nondestructive examination after welding, immediately prior to heat treatment. Multiple-pass arc welds secured the carbon-steel flanges to the Ni-Cr-Mo-V alloy steel tubes. Investigation (visual inspection, metallographic analysis, and evaluation of the fabrication history and the analysis data) supported the conclusion that the tube failed as a result of stress-relief cracking. Very high residual stresses often result from welding thick sections of hardenable steels, even when preheating is employed. Quenched-and-tempered steels containing vanadium, as well as HSLA steels with a vanadium addition, have been shown to be susceptible to this embrittlement. Manufacturers of susceptible steels recommend use of these materials in the as-welded condition.
焊接制造的厚壁管作为压力容器出现裂纹。在焊后应力消除或调质热处理后,焊缝脚趾处也出现了类似的裂纹。焊接后,热处理前的无损检测无法检测到裂纹。多道弧焊将碳钢法兰固定在Ni-Cr-Mo-V合金钢管上。调查(目视检查、金相分析以及对制造历史和分析数据的评估)支持了该管因应力释放开裂而失效的结论。焊接可淬硬钢的厚段时,即使采用预热,残余应力也常常很高。含有钒的调质钢,以及添加钒的HSLA钢,已被证明易受这种脆化的影响。易感钢的制造商建议在焊接状态下使用这些材料。
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引用次数: 0
Failure of a Brazed Joint in a Type 321 Stainless Steel Assembly Due to Inadequate Cleaning 由于清洗不当,321型不锈钢组件中的钎焊接头失效
Pub Date : 2019-06-01 DOI: 10.31399/asm.fach.process.c0047745
A 321 stainless steel radar coolant-system assembly fabricated by torch brazing with AWS type 3A flux, failed at the brazed joint when subjected to mild handling before installation, after being stored for about two years. It was revealed by visual examination of the failed braze that the filler metal had not covered all mating surfaces. Lack of a metallurgical bond between the brazing alloy and stainless steel and instead mechanical bonding of the filler metal to an oxide layer on the stainless steel surface was revealed by examination of the broken joint at the cup. It was indicated by the thickness of the oxide layer that the steel surface was not protected from oxidation by the flux during torch heating. It was concluded that the failure was caused by lack of a metallurgical bond between the brazing alloy and the stainless steel. Components made of 347 stainless steel (better brazeability) brazed with a larger torch tip (wider heat distribution) and AWS type 3B flux (better filler-metal flow) were recommended for radar coolant-system assembly.
使用AWS 3A型焊剂钎焊制造的321不锈钢雷达冷却系统组件,在安装前经过轻微处理后,在储存约两年后,在钎焊接点发生故障。通过对失效钎焊的目视检查发现,填充金属没有覆盖所有配合表面。焊接合金和不锈钢之间缺乏冶金结合,取而代之的是填充金属与不锈钢表面氧化层的机械结合,这是通过检查杯处的断裂接头发现的。氧化层的厚度表明,在焊枪加热过程中,焊剂没有保护钢的表面不被氧化。结果表明,失效是由于钎焊合金与不锈钢之间缺乏冶金结合造成的。雷达冷却系统组件推荐采用347不锈钢(更好的钎焊性)和AWS 3B型焊剂(更好的填料-金属流动)钎焊,焊头更大(热分布更广)。
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引用次数: 0
Brittle Fracture of Rocket-Motor Case That Originated at Delayed Quench Cracks 由延迟淬火裂纹引起的火箭发动机壳体脆性断裂
Pub Date : 2019-06-01 DOI: 10.31399/asm.fach.process.c0046044
A rocket-motor case made of consumable-electrode vacuum arc remelted D-6ac alloy steel failed during hydrostatic proof-pressure testing. Close visual examination, magnetic-particle inspection, and hardness tests showed cracks that appeared to have occurred after austenitizing but before tempering. Microscopic examinations of ethereal picral etched sections indicated that the cracks appeared before or during the final tempering phase of the heat treatment and that cracking had occurred while the steel was in the as-quenched condition, before its 315 deg C (600 deg F) snap temper. Chemical analysis of the cracked metal showed a slightly higher level of carbon than in the component that did not crack. X-ray diffraction studies of material from the fractured dome showed a very low level of retained austenite, and chemical analysis showed a slightly higher content of carbon in the metal of the three cracked components. Bend tests verified the conclusion that the most likely mechanism of delayed quench cracking was isothermal transformation of retained austenite to martensite under the influence of residual quenching stresses. Recommendations included modifying the quenching portion of the heat-treating cycle and tempering in the salt pot used for quenching, immediately after quenching.
消耗性电极真空电弧重熔D-6ac合金钢火箭发动机外壳在静压试验中失效。近距离目视检查、磁粉检查和硬度测试显示,裂纹似乎是在奥氏体化之后、回火之前出现的。空灵的picral蚀刻截面的显微检查表明,裂纹出现在热处理的最后回火阶段之前或期间,并且裂纹发生在钢处于淬火状态时,在315摄氏度(600华氏度)的快速回火之前。对断裂金属的化学分析显示,其碳含量略高于未断裂金属。对断裂圆顶材料的x射线衍射研究表明,残留的奥氏体含量非常低,化学分析表明,三个断裂部件的金属碳含量略高。弯曲试验验证了延迟淬火开裂最可能的机制是残余淬火应力作用下残余奥氏体向马氏体的等温转变。建议包括修改热处理循环的淬火部分,并在淬火后立即在盐锅中回火。
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引用次数: 0
Premature Engine Failure Due to Improper Surface Finish Caused by Carbon Flotation 碳浮选引起的表面光洁度不当导致发动机过早故障
Pub Date : 2019-06-01 DOI: 10.31399/asm.fach.process.c0089646
Nodular cast iron crankshafts and their main-bearing inserts were causing premature failures in engines within the first 1600 km (1000 mi) of operation. The failures were indicated by internal noise, operation at low pressure, and total seizing. Concurrent with the incidence of engine field failures was a manufacturing problem: the inability to maintain a similar microfinish on the cope and drag sides of a cast main-bearing journal. Investigation supported the conclusion that the root cause of the failure was carbon flotation due to the crankshafts involved in the failures showing a higher-than-normal carbon content and/or carbon equivalent. Larger and more numerous cope side graphite nodules broke open, causing ferrite caps or burrs. They then became the mechanism of failure by breaking down the oil film and eroding the beating material. A byproduct was heat, which assisted the failure. Recommendations included establishing closer control of chemical composition and foundry casting practices to alleviate the carbon-flotation form of segregation. Additionally, some nonmetallurgical practices in journal-finishing techniques were suggested to ensure optimal surface finish.
球墨铸铁曲轴及其主轴承嵌套在发动机运行的最初1600公里(1000英里)内就会导致发动机过早失效。故障表现为内部噪声、低压运行和全卡死。与发动机现场故障发生率同时发生的是一个制造问题:无法在铸造主轴承轴颈的处理和拖动侧保持类似的微光洁度。调查结果表明,故障的根本原因是由于曲轴的碳含量和/或碳当量高于正常水平而导致的碳浮选。更大和更多的石墨侧结核破裂,造成铁氧体帽或毛刺。然后,它们通过破坏油膜和侵蚀跳动的材料而成为失效的机制。副产品是热,它加剧了故障。建议包括建立更严格的化学成分控制和铸造工艺,以减轻碳浮选形式的偏析。此外,还提出了一些非冶金工艺,以确保最佳的表面光洁度。
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引用次数: 0
Stress-Corrosion Cracking of a Brazed Joint in a Type 321 Stainless Steel Pressure-Tube Assembly 321型不锈钢压力管组件中钎焊接头的应力腐蚀开裂
Pub Date : 2019-06-01 DOI: 10.31399/asm.fach.process.c0047749
A type 321 stainless steel (AMS 5570) pressure-tube assembly that contained a brazed reinforcing liner leaked during a pressure test. Fluorescent liquid-penetrant inspection revealed a circumferential crack extended approximately 180 deg around the tube parallel to the fillet of the brazed joint. The presence of multiple origin cracks was indicated on the inside surface of a fractured portion of the crack surface. The cracks had originated adjacent to the braze joining the tube and the reinforcing liner and propagated through the wall to the outer surface. The residues on the inner surface of the tube were identified as fluorides from the brazing flux by chemical analysis. The nature of the crack, potential for corrosion due to residual fluorides and residual swaging stress in the tube prior to brazing, confirmed that failure of the tube end was due to stress-corrosion cracking. Stress relief treatment of tube before brazing and immediate cleaning of brazing residual fluorides was recommended to avoid failure.
321型不锈钢(AMS 5570)压力管组件,包含钎焊增强衬垫,在压力测试中泄漏。荧光液体渗透检查显示,在与钎焊接头圆角平行的管周围有一个圆周裂纹,延伸约180度。在裂纹表面断裂部分的内表面存在多源裂纹。裂纹起源于连接钢管和加强衬板的钎焊附近,并通过墙体传播到外表面。通过化学分析,确定了焊管内表面的残留物为钎焊助焊剂中的氟化物。裂纹的性质,由于残余氟化物和钎焊前管内残余的挤压应力造成的潜在腐蚀,证实了管端失效是由于应力腐蚀开裂造成的。建议在钎焊前对焊管进行应力消除处理,并立即清除钎焊残余氟化物,以避免钎焊失败。
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引用次数: 0
Fracture of a Cast Steel Bracket 铸钢支架断裂
Pub Date : 2019-06-01 DOI: 10.31399/asm.fach.process.c0090974
A cast steel bracket manufactured in accordance with ASTM A 148 grade 135/125 steel failed in railroad maintenance service. Ancillary property requirements included a 285 to 331 HB hardness range and minimum impact energy of 27 J (20 ft·lbf) at -40 deg C (-40 deg F). The conditions at the time of failure were characterized as relatively cold. Investigation (visual inspection, chemical analysis, and unetched 119x and 2% nital etched 119x SEM images) supported the conclusion that the bracket failed through brittle overload fracture due to a number of synergistic factors. The quenched-and-tempered microstructure contained solidification shrinkage, inherently poor ductility, and type II Mn-S inclusions that are known to reduce ductility. The macro and microscale fracture features confirmed that the casting was likely in low-temperature service at the time of failure. The composition and mechanical properties of the casting did not satisfy the design requirements. Recommendations included exerting better composition control, primarily with regard to melting, deoxidation, and nitrogen control. Better deoxidation practice was recommended to generate the more desirable Mn-S inclusion morphology, and reevaluation of the casting design was suggested to minimize shrinkage.
根据ASTM a148等级135/125钢制造的铸钢支架在铁路维修服务中失败。辅助性能要求包括285至331 HB的硬度范围,在-40℃(-40℉)下的最小冲击能为27 J (20 ft·lbf)。失效时的条件特征是相对寒冷。调查(目视检查、化学分析、未蚀刻的119x和2%初始蚀刻的119x SEM图像)支持了支架由于许多协同因素而导致脆性过载断裂的结论。淬火回火组织包含凝固收缩、固有的低延展性和II型Mn-S夹杂物,这些夹杂物已知会降低延展性。宏观和微观尺度的断裂特征证实了铸件在失效时可能处于低温使用状态。铸件的成分和力学性能不符合设计要求。建议包括实施更好的成分控制,主要是关于熔化、脱氧和氮控制。建议进行更好的脱氧操作以产生更理想的Mn-S夹杂物形态,并建议重新评估铸件设计以尽量减少收缩。
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引用次数: 0
Fractures of Electro-Galvanized Cylinderhead Screws 电镀锌圆柱头螺钉断裂
Pub Date : 2019-06-01 DOI: 10.31399/asm.fach.process.c9001178
F. Naumann, F. Spies
Eight cylinderhead screws cracked after a short running time in motors. They were made of Fe-0.45C-1Cr steel, had rolled threads, were heat treated to 110 kg/sq mm tensile strength, and were electrolytically galvanized. All fractured at the root of the thread. The surfaces of fracture were fine-grained and had not spread by rubbing. Because the screws were electrolytically galvanized, failure resulted from “delayed fracture.” Experience has shown that this type of fracture is seen on production parts made of high-strength steels, which absorbed hydrogen during pickling or during a galvanic surface treatment. Such parts will rupture below the elastic limit during continuous stressing. This often occurs only after the expiration of a certain time period, and preferably at locations of stress concentrations such as changes in cross section or threads. As a rule, the hydrogen cannot be verified analytically because most of it escapes again after prolonged storage at room temperature or short heating at 100 to 200 deg C.
发动机运行时间不长,8颗气缸盖螺钉断裂。它们由Fe-0.45C-1Cr钢制成,螺纹轧制,热处理至110 kg/sq mm抗拉强度,并进行电解镀锌。都是从线的根部断裂的。断口表面晶粒细小,未因摩擦而扩散。由于螺钉是电解镀锌的,因此导致“延迟断裂”。经验表明,这种类型的断裂出现在由高强度钢制成的生产部件上,这些部件在酸洗或电表面处理过程中吸收了氢。这类部件在连续受力过程中会在弹性极限以下发生断裂。这通常只发生在某一特定时间段届满之后,并且最好发生在应力集中的位置,例如截面或螺纹的变化。通常,氢不能用分析方法验证,因为在室温下长时间储存或在100至200℃下短时间加热后,大部分氢会再次逸出。
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引用次数: 0
Intergranular Cracking in an Air Bottle Because of Torch Overheating Before Welding 焊前焊枪过热引起的气瓶晶间裂纹
Pub Date : 2019-06-01 DOI: 10.31399/asm.fach.process.c0047632
An air bottle, machined from a solid block of aluminum alloy 2219-T852, displayed liquid-penetrant crack indications after assembly welding. The air bottle was machined to rough shape, a 3.8 mm (0.15 in.) wall thickness cylindrical cup with a 19 mm (3/4 in.) wall thickness integral boss on one side. After annealing, hot spinning, annealing a second time, and tack welding a port fitting, the assembly was torch preheated to 120 to 150 deg C (250 to 300 deg F). The port fitting was then welded in place. Final full heat treatment to the T62 temper was followed by machining, testing, and inspection. The crack indications were found only on one side of the boss and on the lower portion of the hot-spun dome region. The metallographic specimens revealed triangular voids and severe intergranular cracks. The cracks displayed the glossy surfaces typical of melted and resolidified material. The localized cracks in the air bottle were from grain-boundary eutectic melting caused by local torch overheating used in preparation for assembly welding of a port fitting. A change in design was scheduled to semiautomatic welding without the use of preheating for the joining of the port fitting for the dome opening.
一个由2219-T852铝合金实心块加工而成的空气瓶,在装配焊接后显示出渗透液体的裂纹迹象。空气瓶被加工成粗糙的形状,一个3.8毫米(0.15英寸)壁厚的圆柱形杯,一侧有一个19毫米(3/4英寸)壁厚的整体凸台。在退火、热纺丝、第二次退火和钉焊端口配件后,将组件火炬预热到120至150摄氏度(250至300华氏度)。然后将端口配件焊接到位。最后对T62回火进行全面热处理,然后进行加工、试验和检查。裂纹迹象仅在凸台的一侧和热纺圆顶区域的下部发现。金相试样显示出三角形空洞和严重的晶间裂纹。裂缝显示出熔化和再凝固材料的典型光滑表面。气瓶的局部裂纹是由于焊接过程中焊枪局部过热引起的晶界共晶熔化造成的。设计上的一个变化是在不使用预热的情况下进行半自动焊接,以连接圆顶开口的端口配件。
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引用次数: 0
Boiler Tube Cracked During Bending 锅炉管在弯曲时开裂
Pub Date : 2019-06-01 DOI: 10.31399/asm.fach.process.c9001194
F. Naumann, F. Spies
A seamless hot-drawn boiler tube NW 300 of 318 mm OD and 9 mm wall thickness made of steel 15Mo3 was bent with sand filling after preheating allegedly to 1000 deg C. In the process it had cracked repeatedly in the drawn fiber. The composition corresponded to specifications, but exceptionally high copper content was noticeable. Microstructural examination showed the damage was due to overheating and burning during preheating and bending. Furthermore, crack formation was promoted by precipitation of metallic copper that had penetrated into the austenitic grain boundaries under the influence of tensile stresses that arose during bending. This phenomenon is known as “solder brittleness.”
一种外径318 mm、壁厚9 mm、材质为15Mo3钢的nw300无缝热拔锅炉管,据称预热至1000℃后进行填砂弯曲,在拉伸纤维中出现多次开裂现象。成分与规格相符,但铜含量明显异常高。显微组织检查表明,损伤是由于预热和弯曲过程中的过热和燃烧造成的。此外,在弯曲过程中产生的拉伸应力的影响下,渗入奥氏体晶界的金属铜的析出促进了裂纹的形成。这种现象被称为“焊料脆性”。
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引用次数: 0
Improper Fabrication Rotating Blades Results in Premature Failure 旋转叶片制造不当导致过早失效
Pub Date : 2019-06-01 DOI: 10.31399/asm.fach.process.c9001150
Fred W. Tatar
A number of rotating blades in a diffuser at a sugar beet processing plant fabricated from rectangular bars cut from rolled carbon-manganese steel plate fractured brittlely. However, apparently identical blades underwent significant plastic deformation without fracture. Inspection of both fractured and bent blades revealed similar preexisting cracks at the toes of bar attachment welds. Metallographic examination of the bent and the fractured bars revealed they had been cut parallel and transverse, respectively, to the rolling direction of the steel plate. Due to the combined effects of the low fracture toughness of the plate on planes parallel in the rolling direction, the presence of the preexisting cracks, and the relatively large section thickness of the bars, the bars whose lengths were transverse to the rolling direction fractured brittlely when subjected to impact loads. Had the poor transverse properties of thick-section plate been recognized, and all the bars properly cut with respect to the rolling direction, the premature fractures would not have occurred.
甜菜加工厂的扩散器中若干旋转叶片发生脆性断裂,这些叶片是由轧制的碳-锰钢板切割成的矩形棒材制成的。然而,显然相同的叶片发生了明显的塑性变形而没有断裂。对断裂和弯曲叶片的检查显示,在棒材连接焊缝的脚趾处存在类似的预先存在的裂缝。对弯曲和断裂的棒材进行金相检查,发现它们分别与钢板轧制方向平行和横向切割。由于轧制方向平行平面上板的断裂韧性较低,预先存在的裂纹的存在,以及棒材截面厚度较大等综合作用,长度与轧制方向横向的棒材在冲击载荷作用下脆性断裂。如果认识到厚截面板的横向性能差,并根据轧制方向正确切割所有棒材,就不会发生过早断裂。
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引用次数: 0
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ASM Failure Analysis Case Histories: Processing Errors and Defects
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