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Degradasi senyawa fenol secara fotokatalisis dengan menggunakan katalis C-doped TiO2 苯酚化合物通过使用c剂量TiO2催化剂进行光合作用的光合作用
Pub Date : 2019-06-28 DOI: 10.24960/JLI.V9I1.4675.51-57
Safni Safni, Vepilia Wulanda, K. Khoiriah, D. V. Wellia
Fenol merupakan senyawa kimia yang banyak digunakan dalam proses industri. Akan tetapi fenol dalam konsentrasi berlebihan dapat menimbulkan efek buruk terhadap kehidupan manusia dan lingkungan pada umumnya. Pada penelitian ini, fenol didegradasi secara fotolisis tanpa dan dengan menggunakan  katalis TiO 2 /C di bawah sinar UV (10 Watt, λ= 365 nm) dan sinar tampak (lampu philips LED 13 watt 1400 lux, λ= 465-640 nm). Larutan fenol yang telah didegradasi diukur dengan Spektrofotometer UV-Vis pada panjang gelombang 200-400 nm. Hasil karakterisasi XRD dan DRS UV-Vis memperlihatkan bahwa katalis modifikasi titania menggunakan unsur karbon berpotensi aktif pada sinar tampak. Aplikasi katalis TiO 2 /C mampu meningkatkan efisiensi dari degradasi fenol pada sistem fotolisis. Larutan fenol 8 mg/L terdegradasi sebanyak 38,98% dan 35,59% tanpa katalis dan meningkat menjadi 51,69% dan 66,10% dengan penambahan 5 mg katalis TiO 2 /C masing-masing di bawah sinar UV dan sinar tampak. ABSTRACT Phenol is a chemical compound that is widely used in industrial processes. However, phenol in excessive concentration can endanger human life and the environment. In this study, phenol was degraded without and using TiO 2 /C catalyst under UV-light (10 Watts, λ = 365 nm) and visible-light (13 watt Philips, lux= 1400, λ = 465-640 nm) photolysis. The degraded of phenol solution was measured by a UV-Vis spectrophotometer at a wavelength 200-400 nm. The results of XRD and DRS UV-Vis characterization show that the modified of titania catalyst using carbon potentially actives in visible-light. Application of TiO 2 /C catalyst can improve the efficiency of phenol degradation in photolysis system. Phenol solution with concentration 8 mg/L was degraded by 38.98% and 35.59% without catalyst and increased to be 51.69% and 66.10% in presence of 5 mg TiO 2 /C catalyst under UV-light and visible-light, respectively.
苯酚是一种在工业过程中广泛使用的化合物。然而,过多的浓度会对人类生活和环境产生不利的影响。在这个研究,不是didegradasi fotolisis没有和使用TiO 2 / C催化剂在紫外线下(10瓦,λ= 365 nm)和一束看起来勒克斯(飞利浦13 1400瓦的LED灯,λ= 465-640 nm)。苯酚溶液已被分解为在200-400 nm波长上用UV-Vis光谱仪检测。XRD和UV-Vis特性检测结果表明,titania的催化剂使用的是可见光中潜在的活性碳元素。催化二/C的应用可以提高光合系统苯酚退化的效率。如果没有催化剂,苯酚溶液降低了38.98%和3559%,增加到51.9%和66.10%,在紫外线和可见光下增加5毫克催化2 /C。苯酚是一种在工业加工中广泛使用的化学化合物。悬浮,极端集中的苯酚会危及人类生命和环境。In this study,苯酚用TiO是无国界degraded和2 / C下加泰罗尼亚UV-light(10瓦特,λ= 365 nm)和飞利浦visible-light(13瓦,lux = 1400,λ= 465-640 nm) photolysis。苯酚解决方案的降解是由一个uv - vite光谱仪在200-400 nm中提出的。XRD和DRS UV-Vis性格测定显示,catalyst采用了可见光中潜在的碳活动。ps 2 /C catalyst可以在photolysis系统中引入苯酚降解的efficition。8 mg/L分解的苯酚解决方案没有加注,增加到58.98%和35.9%
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引用次数: 1
Penapisan, isolasi, dan karakterisasi mikroalga yang berpotensi sebagai sumber biodiesel dari perairan Danau Kerinci, Jambi 皮尔逊、隔离和潜在的微藻特性是Kerinci lake Jambi的生物柴油来源
Pub Date : 2019-06-28 DOI: 10.24960/JLI.V9I1.4326.41-49
Riska Hernandi, Abdi Dharma, Armaini Armaini
Mikroalga menjadi sumber minyak nabati yang berpotensi sebagai bahan baku pembuatan biodiesel dengan kandungan lipid 30-70% dari berat biomassa kering dan komposisi asam lemak yang lengkap. Penelitian ini bertujuan untuk mempelajari keragaman spesies mikroalga dari perairan Danau Kerinci di Jambi, menganalisis kandungan lipid dan asam lemak isolat mikroalga. Mikroalga diisolasi dengan kombinasi teknik goresan, pengenceran berseri, dan mikropipet. Penentuan tingkat pertumbuhan dengan spektrofotometer UV-Vis. Penentuan berat biomassa kering secara gravimetri. Analisis kualitatif lipid dengan uji nile red menggunakan mikroskop flourescence . Analisis kuantitatif lipid dengan ekstraksi menggunakan n-heksana.  Analisis kandungan asam lemak dengan alat GC-MS. Terdapat 19 spesies mikroalga yang diidentifikasi dan 2 spesies berhasil ditapis dengan stres salinitas, yaitu MA1 ( Scenedesmus rubescens ) dan MA2 ( Galdieria sulphuraria ). MAI dan MA2 memiliki kandungan lipid yang lebih tinggi pada pupuk Growmore dibandingkan pada medium Bold’s Basal . MA1 memiliki kandungan lipid 31,95% pada medium Bold’s Basal dan 32,4% pada pupuk Growmore . MA2 memiliki kandungan lipid 28,72% pada medium Bold’s Basal dan 28,93% pada pupuk Growmore . Mikroalga MA1 dan MA2 dapat dijadikan sumber biodiesel dengan kandungan lipid dan asam lemak jenuh (C16:0, C18:0) yang tinggi. ABSTRACT Microalgae has been considered recently as a promising biomass feedstock with great potential for biodiesel production with 30-70% lipid content of the dry biomass weight and produces high fatty acid. This research investigated the diversity of microalgae species from waters of Lake Kerinci in Jambi and analysis of the lipid content and fatty acid of microalgae. The isolation was done by agar plate, serial dilution, and micropipette method. The growth rate of the isolated microalgae was determined by UV-Vis spectrophotometer. Dry biomass weight was determined gravimetrically. Nile red staining performed on the isolates to observe the potential of lipid content. Lipids were extracted using n-hexane. Fatty acid analysis by GC-MS. From the results of identification, there were 19 species of microalgae and 2 species were screened with salinity stress. Based on identification of the both isolates, it is known that MA1 isolate is Scenedesmus rubescens and MA2 is Galdieria sulphuraria. MAI and MA2 had higher lipid content in Growmore agrolyzer than Bold’s Basal medium. MA1 had lipid content 31.95% in Bold’s Basal medium and 32.4% in Growmore agrolyzer, MA2 had lipid content 28.72% in Bold’s Basal medium and 28.93 % in Growmore agrolyzer. MA1 and MA2 was a potential as a biodiesel source with high lipid content and saturated fatty acids (C16:0, C18:0).
微藻是一种潜在的生物柴油燃料来源,其脂含量为干生物量的30%和完整脂肪酸成分。该研究的目标是研究Jambi Kerinci lake water的微藻种类多样性,分析微藻类的脂质和分离酸。微藻是由划痕、系列放松和微管技术混合而成的。用UV-Vis光谱仪确定增长率。重力测定干生物质量。用flourescence显微镜对红外试验中的脂质分析。定量脂分析采用n-heksana提取。GC-MS设备对脂肪酸进行分析。已鉴定出19种微藻,其中2种已被盐碱化,即MA1 (Scenedesmus rubescens)和MA2 (sulphuraria画廊)。麦和马二兄弟在Growmore化肥中所含的脂质比Bold玄武岩中所含的脂质还要高。MA1的腰椎中有395%的脂肪,Growmore肥料中有32.4%的脂肪。MA2的脂肪含量是2872%,Bold玄武岩中283%,Growmore肥料中283%。微藻MA2和MA2可作为高脂和饱和脂肪酸的生物柴油来源(C16:0, C18:0)。微藻被认为是一种潜在的生物燃料生产,对生物柴油生产有30%到70%的粘性。这项研究研究的微algae特种物来自Jambi的Kerinci Lake的分支,并分析了纳米algae的上皮和脂肪酸。孤立是通过车牌、舷窗和微皮质方法完成的。自隔离微生物的增长速度是由UV-Vis光谱仪决定的。干洗重量是重力确定的。尼尔红不锈钢在孤立中表现出来,观察了潜在的粘性。Lipids正在使用n-hexane。GC-MS的Fatty acid分析。从鉴定结果来看,有19个微生物被发现,2个物种被盐碱化。根据对两种异体的识别,我们知道一种分离体是scenecrisis rubescens和MA2是sulphuraria的露天看台。MAI和MA2拥有高强度的脂肪酶,比Bold的玄武岩中更强。MA1有粘性脂肪酸31. Bold玄武岩中95%的介质和32.4%的介质在Growmore agrolyzer中,MA2有粘性脂肪酸28.72%在Bold玄武岩中,28.93 %在Growmore agrolyzer中。MA1和MA2是一种潜在的美国生物柴油资源,上皮和均匀的脂肪acids (C16:0, C18:0)。
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引用次数: 3
Pengaruh penyalut maltodekstrin terhadap produk mikrokapsul minyak jahe dengan teknik spray drying maltodexrin与姜黄喷雾技术对姜黄油微胶囊的影响
Pub Date : 2019-06-28 DOI: 10.24960/JLI.V9I1.4664.1-7
Fitriana Djafar, M. D. Supardan
Penelitian ini bertujuan untuk membuat mikrokapsul minyak jahe dengan menggunakan teknik spray drying . Bahan penyalut yang digunakan adalah maltodekstrin. Variabel penelitian yang dipelajari adalah konsentrasi maltodekstrin yaitu 10, 20 dan 30 (%-b/v) dan rasio minyak jahe terhadap maltodekstrin yaitu 1:8, 1:10, 1:12 dan 1:14 (b/v). Variabel penelitian dengan rendemen tertinggi akan digunakan untuk mempelajari pengaruh variasi suhu inlet proses spray drying (160, 170, 180 dan 190 o C). Hasil analisis gas kromatografi-spektrofotometri massa menunjukkan bahwa ada lima komponen terbesar yang terdapat dalam minyak jahe yaitu benzene (28,62%), zingiberene (19,46%), β- bisabolene (13,48%), cyclohexane (12,59%) dan farnesene (5,83%). Rendemen produk mikrokapsul minyak jahe tertinggi diperoleh pada perlakuan konsentrasi maltodekstrin 30% dan rasio minyak jahe terhadap maltodekstrin 1:14 yaitu sebesar 37 gram. Hasil penelitian juga menunjukkan bahwa peningkatan suhu inlet spray drying memberikan pengaruh terhadap kadar air, kadar minyak total, kadar minyak di permukaan dan kadar minyak terperangkap mikrokapsul minyak jahe. Hasil analisis Scanning Electron Microscopy menunjukkan mikrostruktur produk mikrokapsul minyak atsiri jahe yang dihasilkan memiliki bentuk yang bervariasi.  ABSTRACT This study aims to make ginger oil microcapsules using spray drying technique. Maltodextrine was used as a coating material. The process variables studied were maltodextrin concentration 10, 20 and 30 (%-w/v) and ratio of ginger oil to maltodextrin 1:8, 1:10, 1:12 and 1:14 (w/v). The best process variable with the highest product yield will be used to investigate the effect of inlet temperature variations of spray drying process (160, 170, 180 and 190 o C). The results of gas chromatography-mass spectroscopy analysis showed that the five largest components contained in ginger oil were benzene (28.62%), zingiberene (19.46%), β-bisabolene (13.48%), cyclohexane (12.59%) and farnesene (5.83%). The highest yield of ginger essential oil microcapsule products was obtained 37 grams at maltodextrin concentration 30% and ratio of ginger oil to maltodextrin 1:14. The experimental results showed that the inlet temperature of spray drying affected the moisture content, total oil content, surface oil content, and trapped oil content of the ginger oil microcapsules products. Meanwhile, Scanning Electron Microscopy analysis results showed that the microstructure of ginger essential oil products from several research treatments generally have various shape.
这项研究的目的是用喷雾干燥技术制造姜黄油的微胶囊。使用的燃烧材料是maltodestrin。研究的变量是10、20和30 (%-b/v)的浓度和生姜油与maltodekstrin的比例为1:8、1:10、1:12和1:14 (b/v)。rendemen最高的研究变量将用于研究干喷雾过程(160进口温度变化的影响,170、180、190个o C)。kromatografi-spektrofotometri气体质量分析结果表明,有五个成分姜中最大的石油苯(28,62%)zingiberene(19,46%),β- bisabolene 13,48%), cyclohexane(12,59%)和farnesene(5,83%)。姜黄色油微胶囊的最高推荐产品是30%的浓度和姜油比37克。研究还发现,发胶内的温度上升会影响含水率、总石油水平、浮油水平和姜油微胶囊的作用。扫描电子显微扫描显示,从生姜中提取的微型胶囊产品的微结构各不相同。根据这项研究,用喷雾干燥技术制造姜油微胶囊。Maltodextrine就像一种涂料。10%、20和30 (%-w/v)和姜油浓度为maltodexrin 1:8、1:10、1:12和1:14 (w/v)。《最高广告收益最好的过程可变和进口效应》将习惯investigate variations of喷雾干的过程的温度(160、170、180和190个o C)气体。The results of chromatography-mass spectroscopy分析那里那五个人最大components有趣在姜油是苯(28 . 62%)、zingiberene(19 . 46%),β-bisabolene (48%), cyclohexane(12 13。5 59%)和farnesene(83%)。姜对石油的最终收购在maltodextrin集中销售的37克,30%的姜油排放到maltoxtrin 1:14。最近的实验表明,喷雾干燥的表面温度影响潜在的石油排放、总石油消耗、表面石油污染产品。虽然扫描电子显微分析结果显示,来自several研究项目的石油产品的微观结构通常有不同的形状。
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引用次数: 1
Pengaruh jenis pelarut dan kecepatan homogenizer terhadap karakteristik partikel katekin gambir 溶剂类型和同质速度对冈比亚微粒特性的影响
Pub Date : 2019-06-28 DOI: 10.24960/JLI.V9I1.5227.9-14
Gustri Yeni, S. Silfia, Yulia Helmi Diza
Penelitian ini bertujuan untuk mengetahui pengaruh jenis pelarut dan kecepatan homogenizer terhadap karakteristik partikel katekin gambir. Penelitian dilakukan dengan cara katekin gambir dilarutkan dengan variasi pelarut air, etanol 20%, campuran etanol 20% dan etil asetat (perbandingan 1:10) dan kecepatan homogenizer 500; 1.500; 2.000; dan 2.500 rpm. Karakteristik partikel hasil perlakuan diuji menggunakan particle size analyzer (PSA) diperoleh hasil bervariasi antara 2.148-3.354 nm. Proses pengadukan dengan kecepatan 2500 rpm dapat memperkecil ukuran partikel (2.148 nm), secara visual dilihat dari tingkat kejernihan larutan yang dihasilkan. Peningkatan kecepatan homogenizer menyebabkan terjadi kerusakan senyawa katekin yang ditandai dengan perubahan warna menjadi coklat, ditunjukkan dengan penurunan kadar katekin dari 84,32%  menjadi 75,91%. Sampel hasil perlakuan dikeringkan dengan spray dryer pada kondisi operasi suhu inlet 100 o C dan outlet 90 o C, tekanan vakum pada 15 Psi, terjadi penurunan ukuran partikel (209,45 nm). Sampel diuji menggunakan scanning electron microscope (SEM) menunjukkan morfologi katekin tidak simetris. Analisis ukuran partikel katekin dilanjutkan menggunakan software image-J dan diperoleh ukuran partikel antara 209,53-280,50 nm. ABSTRACT This study was aimed to determine the effect of solvent type and homogenizer speed on the particle characteristics of gambier catechins. The research was conducted by dissolving the gambir catechins with solvents variation of water, ethanol 20%, mixture of ethanol 20% and ethyl acetate (ratio 1:10) and homogenizer speed 500; 1,500; 2,000; and 2,500 rpm. The particle characteristics of the treatment were tested using a particle size analyzer (PSA) and obtained the results varied between 2,148-3,354 nm. The stirring process at a speed of 2500 rpm can reduce the particle size (2,148 nm), visually seen from the clarity level of the solution produced. Increasing the speed of the homogenizer caused damage to the catechin compound which was marked by a change in color became brown, indicated by a decrease in catechin content from 84.32% to 75.91%. The treated sample was dried with a spray dryer under operating conditions of inlet temperature 100 o C and outlet temperature 90 o C, vacuum pressure at 15 Psi particle size decreased (209.45 nm). Samples were tested using a scanning electron microscope (SEM) showed the symmetrical morphology of the catechins. The analysis of catechins particle size was continued using the image-J software and obtained the particle size between 209.53-280.50 nm.
本研究旨在确定溶剂类型和均匀速度对冈比亚介质颗粒特征的影响。研究是通过水溶剂、乙醇20%、乙醇20%和乙醇混合(比较1:10)和均匀适性500;1500;2000;每分钟2500转。使用粒子分析仪(PSA)测试出的颗粒特征,结果在2148 - 354 nm之间。以2500转/分钟的速度搅拌过程可以将颗粒的大小缩小到2148 nm,从溶液的清晰度可以看到。均质生成器速度的增加导致致癌物质的损伤,其颜色为棕色,从84.32%下降到75.91%。治疗方法的样本通过喷雾干燥在100 o - C和90 o - C出口,15 Psi的真空压力,粒子大小下降(209.45 nm)。该样本使用扫描电子显微镜(SEM)进行测试,显示不对称的肿瘤形态。katekin粒子大小分析继续使用imagej软件,获得粒子大小为209,53- 280.50 nm。这项研究已被证明能够确定solvent类型和均匀性的速度影响。这项研究是由水变量、乙醇20%、乙醇20%和乙醇乙醇混合(ratio 1:10)和恐同速度500;1500;2000;每分钟2500转。治疗的参与特征是使用一种成分分析仪(PSA)和发现在2,148-3,354 nm之间的可变结果结果检测。在2500转/小时的速度下,将大小的粒子还原为2.148 nm,从解决方案的清晰级别可见。增加对等基因的速度,以棕色为标记的变化,从84.32%到75.91%,由核核试验的法令决定。采集样本时,样本中含有一种喷雾dryer,在处理的条件下使用样本被试验使用一种扫描电子显微镜(SEM)揭示了该技术的共生形态。catechins particle的分析继续使用imagej软件和在20.53 -280 nm之间进行。
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引用次数: 5
Pembuatan minuman fungsional tablet effervescent dari bubuk ekstrak daun kacang tujuh jurai (Phaseolus lunatus, L.)
Pub Date : 2019-06-28 DOI: 10.24960/JLI.V9I1.4649.23-31
D. Sari
Penelitian ini bertujuan untuk mengetahui pengaruh penambahan bubuk ekstrak daun kacang tujuh jurai terhadap sifat fisik dan kimia tablet effervescent . Penelitian ini menggunakan Rancangan Acak Lengkap (RAL) dengan 5 perlakuan yaitu penambahan bubuk ekstrak daun kacang tujuh jurai masing-masing 10, 15, 20, 25, dan 30% dengan 3 kali ulangan. Pengamatan tablet effervescent meliputi pengamatan fisik : penampakan, waktu larut, kekerasan dan kerapuhan; pengamatan kimia : kadar air, pH larutan, kadar vitamin C, aktivitas antioksidan, kadar klorofil, dan warna. Hasil penelitian menunjukkan bahwa penambahan bubuk ekstrak daun kacang tujuh jurai berpengaruh nyata terhadap ketebalan tablet, waktu larut, kerapuhan, kadar air, vitamin C, aktivitas antioksidan, kadar klorofil dan warna tablet effervescent yang dihasilkan. Penambahan bubuk ekstrak daun kacang tujuh jurai tidak mempengaruhi ukuran diameter tablet effervescent, kekerasan dan pH. ABSTRACT This study was aimed to determine the effect of the addition of lima bean leaf extract powder on the physical chemical and properties of effervescent tablets. This study used a completely randomized design (CRD) with 5 treatments, the addition of lima bean leaf extract powder of 10, 15, 20, 25, and 30% with 3 replications, respectively. Tablet effervescent observations include physical observations: appearance, dissolution time, hardness and fragility; chemical observations: water content, pH of the solution, vitamin C level, antioxidant activity, chlorophyll content, and color. The results showed that the addition of lima bean leaf extract powder significantly affected tablet thickness, dissolution time, fragility, moisture content, vitamin C, antioxidant activity, chlorophyll content and effervescent tablet color produced. The addition of lima bean leaf extract powder did not affect the size of the effervescent tablet diameter, hardness and pH.
这项研究的目的是确定在片状颗粒的生理和化学性质中加入七种草甘膦酸盐的影响。这项研究采用了一种随机设计的方法,采用五种方法,即在每样产品中加入七种青豆提取物,每样产品10、15、20、25和30%,每三次重复。带氧片观察包括物理观察:视觉、时间、暴力和脆弱性;化学观察:含水率、溶液pH值、维生素C含量、抗氧化剂活性、叶绿素水平和颜色。研究表明,添加七朱砂提取物粉对药片的厚度、时间、脆性、含水率、维生素C、抗氧化剂活性、叶绿素水平和effervescent片的颜色产生了明显的影响。添加七朱雷叶提取物粉不会影响药片的直径、硬度和pH值。这项研究用了5次试验,加上5次bean leaf extract powder 10、15、20、25和30%的三种复制、崇敬。包括物理观测在内的发光观测:化学观察:水合作用,pH值,维生素C级,抗氧化剂活性,氯氧合酶,颜色。结果表明,五颗小豆叶排泄物的成分有明显的成分,有延迟的时间,脆弱的乳汁,维生素C,抗氧化剂活性,氯仿满足片生产。五颗豆叶extract powder的附录不影响食用药片直径、硬度和pH值的大小。
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引用次数: 3
Biosorben cangkang pensi (Corbicula moltkiana) sebagai penyerap zat warna metanil yellow ditinjau dari pH dan model kesetimbangan adsorpsi pH值和分级平衡模型
Pub Date : 2019-06-28 DOI: 10.24960/JLI.V9I1.4661.15-22
Rahmiana Zein, Putri Ramadhani, Hermansyah Aziz, Refilda Suhaili
Penelitian cangkang pensi ( Corbicula moltkiana ) sebagai penyerap zat warna metanil yellow telah dilakukan dengan sistem batch . Kondisi optimum penyerapan terjadi pada pH 4 dan konsentrasi awal 100 mg/L. Proses adsorpsi terjadi mengikuti model isoterm Langmuir dengan nilai R 2 adalah 0,886 pada monolayer dengan kapasitas adsorpsi maksimum (q max ) diperoleh 2,591 mg/g. Hasil analisis gugus fungsi cangkang pensi dengan FTIR menunjukkan adanya interaksi antara molekul zat warna metanil yellow dan gugus fungsi. Analisis morfologi permukaan cangkang pensi menggunakan SEM menunjukkan bahwa pori-pori cangkang pensi telah diisi oleh molekul zat warna metanil yellow . Cangkang pensi dapat digunakan sebagai bahan penyerap zat warna metanil yellow di dalam larutan.  ABSTRACT The study of the Pensi Shell (Corbicula moltkiana) to adsorb metanil yellow (MY)dyes  has been investigated. This study was determined by batch system. The optimum conditions of metanil yellow dyes adsorption occurred at pH 4 and initial concentration 100 mg/L. The adsorption process was properly described by Langmuir isotherm model which was indicated by the value of R 2 =0,886. This confirmed that the adsorption process was monolayer with maximum adsorption capacity (q max ) was 2,591 mg/g. Functional groups analysis by FTIR showed the interactions MY molecule on pensi shell functional groups. Analysis of morphology surface of pensi shell by SEM indicated that the pore was filled by MY molecules. Pensi shell could be used as adsorbent of metanil yellow dyes in aqueous solution.
潘西壳(moltkiana Corbicula)作为甲烷色物质吸收剂的研究已经与批化系统进行了。最佳吸收条件为pH 4和100毫克/L浓度。根据R 2的等价模型进行的adsorpsi是0.886,单层级最高可容纳能力为2,591 mg/g。FTIR - shell功能集的分析结果显示,甲烷色物质和星系团之间存在相互作用。pensi外壳表面的形态分析表明,pensi外壳的毛孔已经被颜色甲烷黄色的分子填充。pensi shell可以作为溶液中甲烷色物质的吸收剂。摘要对蛋壳的研究(moltkiana Corbicula)进行了后续调查。这项研究是由批次系统决定的。甲醇黄色dyes在pH 4和最初集中100毫克/L。地址处理程序由Langmuir isotherm所描述的按值R 2 = 0.886所列的模型所述。证实,与max q关系重大的调理程序是2591 mg/g。FTIR的有趣分析展示了我在shell functure中发现的分子类别的有趣之处。分析外壳的形态面,分析里面充满了我的分子。Pensi shell可以作为一种加入metanil的黄色dyes在水状解决方案。
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引用次数: 2
Pembuatan tablet effervescent berbahan aktif sediaan kering ekstrak daun senduduk dan bakteri asam laktat asal dadih Sijunjung sebagai minuman fungsional
Pub Date : 2019-06-28 DOI: 10.24960/JLI.V9I1.5273.59-67
Yulia Helmi Diza, Alfi Asben, Tuty Anggraini
Pembuatan tablet effervescent dengan bahan aktif ekstrak kering daun senduduk  dan sediaan kering bakteri asam laktat yang berasal dari dadih Kabupaten Sijunjung telah dilakukan melalui pencetakan langsung. Penelitian ini bertujuan untuk membuat sediaan minuman fungsional yang mengandung senyawa antioksidan dan bakteri baik yang mudah dan cepat disajikan. Bahan aktif yang digunakan adalah sediaan kering BAL asal dadih sebanyak 2%, 4% dan 6% dari bahan penyusun tablet dan ekstrak kering daun senduduk sebanyak 15% untuk semua perlakuan. Terhadap produk yang dihasilkan dilakukan pengujian total BAL, aktivitas antioksidan, total fenol, pH larutan, kadar air, waktu larut, kekerasan, dan uji kesukaan meliputi penampakan tablet, rasa, warna larutan dan aroma. Hasil penelitian menunjukkan bahwa total BAL yang tumbuh pada larutan tablet effervescent yang memenuhi syarat untuk pangan fungsional adalah perlakuan penambahan sediaan kering BAL 4% dan 6%, yaitu 4,04x10 6 kol/g, 1,72x10 7 kol/g, aktivitas antioksidan 52,20% dan 54,50% dengan total fenol 0,81 mg GAE/g dan 0,86 mg GAE/g. Dari hasil uji kesukaan diketahui bahwa perlakuan yang mempunyai rata-rata nilai kesukaan tertinggi adalah perlakuan dengan bahan aktif ekstrak kering senduduk 15% dan sediaan kering BAL 4% dengan pH 5,03, kadar air 9,34%, waktu larut 1,875 menit dan kekerasan 4,18 kg. ABSTRACT Making of effervescent tables with active ingredients of dried extracts of senduduk leaves and dried preparations of lactic acid bacteria from dadih Sijunjung have been done through direct compression. This study aims to make functional beverage preparations that contain antioxidant compounds and bacteria both easily and quickly served. The active ingredients used were dried LAB preparations from dadih as much as 2%, 4% and 6% of the constituent tablets and dried extracts of senduduk leaves as much as 15% for all treatments. The products were  tested of total LAB, antioxidant activity, total phenol, pH of the solution, moisture content, dissolution time, hardness, and test of preference included tablet appearance, taste, solution color, and flavour. The results showed that the total LAB that grown in the effervescent tablet solution met the requirements for functional food was the treatment of the addition of 4% and 6%  LAB dry dosage, namely 4.04x106 col/g, 1.72x107 col/g, antioxidant activity 52.20% and 54.50% with total phenol 0.81 mg GAE/g and 0.86 mg GAE/g. From the test results, it was known that the treatment that had the highest average value of preference was treatment with the active ingredient of dry extract of 15% and dry preparation of LAB 4%  with pH 5.03, moisture content 9.34%, soluble time 1.875 minutes, and hardness 4.18 kg .
由司喀什摄区活性提取物和干桶乳酸细菌制成的effervescent片已经通过直接印刷完成。这项研究的目的是使一种功能饮料储存起来,这种饮料既容易又容易地提供抗氧化剂和细菌。使用的活性成分是凝乳量,其来源为2%、4%和6%的片剂和干叶提取物占15%。对生产的产品进行了总测试、抗氧化剂活性、总苯酚、pH溶液、水溶液水平、溶剂、暴力和最喜欢的测试,包括药片的外观、味道、溶液颜色和气味。研究结果表明,在具有功用的effervescent食品溶液中生长的总电荷为4.4%和6%,即4.04x10次/g, 1,72x10 7次/g,抗氧化剂活性为52.20%和54.50%,总为0.81毫克/g, 0.86毫克/g。检测结果显示,最受欢迎的治疗方法是使用pH 5.03的主动提取物15%和4%的瓶装水,9.34%的水,溶解1.875分钟的时间和4.18公斤的硬度。从凝乳中提取的有害细菌和从凝乳中提取的潜在细菌的活性成分已被直接压缩。这项研究的条件使其具有有趣的准备作用,即抗氧化物化合物和细菌都容易吸收。实验用的活性成分包括从凝血实验室中提取的产品,如2%、4%和6%产品测试了完全的实验室、抗氧化剂活动、总苯酚、溶液pH值、污染、浪费时间、匮乏和测试包括片状珍珠、品味、色色和口味的预览。The results那里那个实验室总那个《数字化》《大都会冒泡solution平板requirements for functional食品治疗》是加法,4%和6%的实验室干dosage, namely 4 . 04x106坳g / g, 1 . 72x107坳,antioxidant活动52和54 20%。50%完全用苯酚0。81毫克GAE / g和0。86毫克GAE - g。从结果来看,据了解,最重要的参考资料所述,目前的治疗方法是接受15%的活性排版和4%的土壤排版,湿度为9,34%,解决时间1,875分钟,hardness为4.18公斤。
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引用次数: 2
Pemanfaatan modified cassava flour dan tepung tapioka sebagai bahan pengisi keju cedar olahan 改良的木薯粉和木薯淀粉作为加工雪松料料加料
Pub Date : 2018-12-28 DOI: 10.24960/JLI.V8I2.4050.61-66
Gunawan Priadi, Fitri Setiyoningrum, F. Afiati, R. Syarief
Ubi kayu merupakan sumber karbohidrat yang berpotensi sebagai bahan pengisi keju cedar olahan. Pengkajian terhadap karakteristik fisikokimia keju cedar olahan bertujuan untuk memperoleh model formula penambahan bahan pengisi berbasis ubi kayu dan mengetahui nilai kesukaan terhadap keju cedar olahan terpilih. Penelitian terdiri dari beberapa tahap yaitu pembuatan keju cedar olahan, karakterisasi keju olahan, penentuan model fomula penambahan bahan pengisi berbasis ubi kayu, verifikasi formula terpilih dan uji organoleptik terhadap produk dengan model formula terpilih. Pembuatan keju cedar olahan mengunakan rancangan acak lengkap dengan satu faktor. Penentuan model formula mengunakan respon permukaan historical data . Hasil penelitian menunjukan bahwa penambahan mocaf dan tapioka dengan variasi konsentrasi berpengaruh signifikan terhadap kadar lemak dan karbohidrat produk, sedangkan kadar air, kadar abu, kadar protein dan profil tekstur produk tidak dipengaruhi secara signifikan. Penambahan tapioka 3% (b/b) merupakan model formula terpilih keju cedar olahan dengan karakteristik kadar air 46,96 %; kadar protein 36,39 % (bk); kadar lemak 36,05 % (bk); kadar karbohidrat 5,09% (bk), nilai kekerasan 844,518 gF; daya adhesive 69,739 g/s; elastisitas 0,421; daya kohesif 0,424; kelengketan 358,697 gF; dan daya kunyah 151,244 gF serta nilai kesukaan keju cedar olehan formula terpilih cenderung netral. Mocaf dan tapioka dapat dijadikan bahan pengisi keju cedar olahan. Abstract Cassava is a potential source of carbohydrate as a filler for processed cedar cheese. Study of physicochemical characteristics of processed cheddar cheese was done to obtain the formula of the cassava based filler addition and preferential value of the selected formula. The research  consisted of some steps, i.e. processed cheddar cheese production, processed cheddar cheese characterization, determination of processed cheddar cheese formula model, verification of selected formula, and hedonic test on selected formula product. Preparation of processed cheddar cheese using randomized complete design with one factor, while the formula modeling using response surface with historical data method. The result showed that the use of modified cassava flour (mocaf) and tapioca with different concentration significantly influenced (p<0,05) to the increasing fat and decreasing carbohydrate content of the product, while the water, ash, protein and texture profile ore not significantly influenced. The addition of 3% tapioca (w/w) was selected as formula model with the characteristic water content 46.96%; protein 36.39% (db); fat 36.05% (db); carbohydrate 5.09% (db), hardness 844.518 gF; adhesiveness 69.739 g/s; springiness 0.421; cohesiveness 0.424; gumminess 358.697 gF; and chewiness 151.244 gF, with preferential value tend to be neutral. Mocaf and tapioca could be used as filler in processing processed cheddar cheese.
山药是一种潜在的碳水化合物,用于制作加工雪松奶酪。对精制雪松奶酪的生理特征的研究旨在获得一种以木薯为基础的填充香料的配方模型,并确定其对精制雪松奶酪的喜爱价值。该研究包括生产精制雪松芝士、加工芝士的描述、确定以甘薯为基础的填充填充模型、对选定的配方进行验证和有机化合物测试等。生产精制雪松奶酪是由一个因素的随机设计而成的。公式模型采用历史数据表面响应。研究表明,含油量和木薯淀粉的浓度变化对产品的脂肪和碳水化合物水平有显著影响,而该产品的含水率、灰烬水平、蛋白质和纹理剖面水平没有受到显著影响。木薯3%的加入(b/b)是一种精选的雪松芝士配方,其含水率为46.96 %;蛋白质含量为36.39 % (bk);脂肪含量为36.05 % (bk);碳水化合物浓度5.09% (bk),硬度844.518 gF;粘附力69.739 g/s;0,421弹性;内聚功率0.424;完整358.697 gF;151.244种咀嚼能力,gF和首选的香料杉木奶酪的得分往往是中性的。Mocaf和木薯可以作为加工雪松的填充物。不在场证明砂锅是一种潜在的资源。医生对过程切达干酪的研究完全是为了确定一种基于添加和优化配方的木薯配方。这项研究包括几种步骤,i。处理切达干酪的方法是用一个因素完成设计,而调制解调器公式的方法是用历史数据的方法。最近的结果表明,这种修改过的木薯粉(mocaf)和木薯粉的重要性受到了不同程度的影响(p< 0.05),而水、灰、蛋白质和农产品的成分并没有显著影响。3%的木薯粉是由characteristic water consult指定的公式46.96%;蛋白质36.39% (db);fat 36.05% (db);carbohydrate 59% (db), hardness 844,518 gF;adhesiveness 69739 g/s;springiness 0.421;cohesiveness 0.424;gumminess 358,697 gF;胸痛151244 gF,一般为中立。Mocaf和木薯卡可以作为加工切达干酪的填料使用。
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引用次数: 2
Pengaruh penggunaan ekstrak gambir sebagai antimikroba terhadap mutu dan ketahanan simpan cake bengkuang (Pachyrhizus erosus)
Pub Date : 2018-12-28 DOI: 10.24960/JLI.V8I2.4329.111-117
K. Kamsina, F. Firdausni
Gambir merupakan sari getah yang diekstraksi dari daun tanaman gambir dan mengandung senyawa katekin yang bersifat sebagai antimikroba.  Guna meningkatkan ketahanan simpan pangan dan meminilisir penggunaan antimikroba sintetis dilakukan penelitian ini dengan tujuan mengetahui pengaruh pemberian konsentrasi katekin terhadap nilai gizi dan ketahanan simpan cake bengkuang. Penelitian ini dilakukan dengan metoda Rancangan Acak Lengkap (RAL) dengan 5 perlakuan (persentase catechin) yaitu A (kontrol), B (0,010%), C (0,015%), D (0,020%) dan E   (0,025%) dengan 5 kali ulangan. Hasil perlakuan optimal didapatkan pada perlakuan D dengan nilai kadar air 21,55%, kadar abu 0,3805%, gula 15,765%, antioksidan 28,38% dan total fenolik 2,01%. Uji organoleptik warna, rasa, aroma, dan tekstur disukai dengan nilai berturut-turut 3,481; 3,593; 3,593; 3,333. Sedangkan untuk ketahanan simpan cake bengkuang sampai minggu ke-3 untuk kadar air 31,91 % dan mikroba (Angka lempeng total) 7,4 x 10 4 koloni/g dan memenuhi standard SNI 01-3840-1995 (Roti). Penggunaan ekstrak gambir sebagai antimikroba dalam menghambat pertumbuhan bakteri kuat dengan daya hambat bakteri Escherechia coli 11 mm dan Salmonella 15 mm. Abstract Gambier is a material that extracted from the leaves of gambier plants and contains catechin compounds which have antimicrobial characteristic. In order to improve the storage resistance of food and to minimize the use of synthetic antimicrobials, this study was carried out with the aim of knowing the effect of giving catechin concentrations on the nutritional value and storage resistance of yam cake. The method was conducted by a completely randomized design (CRD) with 5 treatments (percentage of catechin), namely A (control), B (0.010%), C (0.015%), D (0.020%) and E (0.025%) with 5 replications. The optimal result were obtained in treatment D with water content value 21.55%, ash content 0.3805%, sugar content 15.765%, antioxidant 28.38%, and total phenol 2.01%. Organoletic test of color, taste, flavor, and texture were preferred with value 3.481; 3.593; 3.593; 3.333 respectively. Whereas the resistance of jicama cake storage until the third week for water content 31.91% and microbes (total plate number) 7.4 x 10 4 colony/g and fulfilled the SNI standard 01-3840-1995 (Bread). The use of gambier extract as an antimicrobial in inhibit the growth of strong bacteria with inhibition of 15 mm for Salmonella bacteria and 11 mm for Escherechia coli.
冈比亚是一种从冈比亚植物的叶子中提取的树脂汁,含有一种耐微生物化合物。为了提高粮食存贮率,并将合成抗菌素的使用降至最低,本研究旨在确定草甘病浓度对营养价值的影响,以及工蚁蛋糕的保质性。这项研究是用五种随机设计方法完成的,即A(控制百分比)、B(0.010%)、C(0.020%)、D(0.020%)和E(0.025%),再重复5次。最佳治疗结果是D治疗,含水率为21.55%,含盐量为0.3805%,含糖量为15765%,抗氧化剂为2838%,总ph值为2.01%。连续3.481次的有机着色、味觉、香味和纹理测试;3,593;3,593;3,333。另一方面,为了保持蛋糕的存活率,直到第三周,涉及31.91 %的水和微生物,7.4×10 4个菌落/g,符合标准SNI 01-3840-1995(面包)。用冈比氏提取物作为抗菌素,用11毫米的大肠杆菌和15毫米沙门氏菌的抑制抑制抑制强大细菌的生长。甘菊是一种从甘菊植物的叶子中提取出来的材料,并接触有抗微生物特性的化合物。为了增加粮食供应阻力,并减少合成抗微生物药的使用,这项研究的目标是确定将营养价值集中在山药蛋糕的营养价值和储存阻力上的效果。方法是由五种配方的完全融合设计,namely a(控制),B (0.010%), C (0.020%), D(0.025%)和5种复制因子来控制的。最佳结果是接受水浸值为21.55%,灰受限为0.3805%,糖含量为15765%,抗氧化剂含量为28.38%,总苯酚含量为2.01%。颜色、口味、口味和文本的有机测试优先于价值3.481;3.593;3.593;3.333 respectively。在第三周的水饱率前,jicama蛋糕的反抗力量被储存了33.91%和微生物,这是7.4×10次殖民地/g,并填补了SNI标准01-3840-1995(面包)。用冈比耶排泄物作为一种抗微生物的药物,用15毫米的沙门氏菌抑制和11毫米的大肠杆菌抑制。
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引用次数: 4
Pengaruh waktu hidrolisis dan konsentrasi HCl terhadap karakteristik pati termodifikasi dari bengkuang (Pachyrrhizus erosus) 水解时间和HCl浓度对班贡(Pachyrrhizus erosus)特有的淀粉特性的影响
Pub Date : 2018-12-28 DOI: 10.24960/JLI.V8I2.4334.53-60
Gustri Yeni, S. Silfia, Wilsa Hermianti, Tri Wahyuningsih
Tepung bengkuang dapat dimanfaatkan sebagai penyalut tipis (enkapsulan) bahan aktif. Untuk memenuhi spesifikasi produk tersebut tepung bengkuang perlu dilakukan modifikasi. Tujuan dari penelitian ini adalah mempelajari pengaruh hidrolisis asam terhadap pati secara lambat untuk menghasilkan tepung termodifikasi dari bengkuang dengan karakteristik fisiko-kimia yang dapat dimanfaatkan sebagai  enkapsulan. Proses hidrolisis asam tepung bengkuang menggunakan variasi perlakuan waktu hidrolisis (24, 48, dan 72 jam) dan konsentrasi HCl (1%, 2%, dan 3%). Hasil penelitian menunjukkan perlakuan optimal diperoleh pada waktu hidrolisis 72 jam dan konsentrasi HCl 2% dengan nilai derajat polimerisasi (DP) 22,34 yang sudah memenuhi persyaratan jika digunakan sebagai matrik enkapsulan. Karakteritik dari tepung termodifikasi pada kondisi ini adalah kadar air 16,47%, kadar abu 1,17%, amilosa 31,01%, viskositas 155cP, kelarutan 80,83%, dan aktivitas antioksidan (IC 50 ) 148 μgml -1 . Morfologi granula tepung  hasil uji dengan mikroskop dan SEM bentuknya tidak terlalu banyak mengalami perubahan pada hidrolisis asam.  Abstract Jicama flour can be used as a thin coating (encapsulation) of an active ingredients. To meet the specifications of the product, jicama flour needs to be modified. The purpose of this study was to study the effect of acid hydrolysis on starch slowly to produce jicama modified flour with physico-chemical characteristics that could be used as an encapsulants. The process of acid hydrolysis of jicama flour using treatment variations of hydrolysis time (24, 48, and 72 hours) and HCl concentrations (1, 2, and 3%). The results showed that the optimal treatment was obtained at 72 hours hydrolysis and 2% HCl concentration with a polymerization degree (DP) of 22.34 which met the requirements if used as an encapsulation matrix. The characteristics of the modified flour in this condition were water content 16.47%, ash content 1.17%, amylose 31.01%, viscosity 155cP, solubility 80.83%, and antioxidant activity (IC 50 ) 148 μgml- 1 . The test results of flour granular morphology with microscopy and SEM did not change too much in acid hydrolysis.
磨成的面粉可以用作发酵剂。为了满足产品的规格,本品需要进行改装。这项研究的目的是研究酸溶酶对淀粉的缓慢影响,使淀粉产生一种具有可用于消化的物理化学特征的改良面粉。草甘膦酸盐的盐酸处理方法采用了刺激性化合物(24小时、48小时和72小时)和HCl浓度(1%、2%和3%)的变化。研究结果表明,在72小时的水解时间内获得了最佳治疗,聚合度为22.34的HCl 2%,如果将其作为导体,应符合条件。Karakteritik termodifikasi面粉的条件是说水位16,47%阿布1,17%水平,amilosa 31,01%,粘度155cP、80,83%溶解度和IC(50)抗氧化能力148μgml的录音。颗粒状颗粒样貌,通过显微镜和闪的作用,微酸水利发生了短暂的变化。Jicama洪水可以被用作一种激动人心的耕作。要了解产品的具体情况,jicama flour需要改进。这项研究的目的是研究一种缓慢地从粘附的生理特征中提取一种具有改性化学特性的酸性氢化水的效果。使用氢溶时间(24、48和72小时)和HCl浓度(1、2和3%)的摇匀水的过程。结果表明,最佳治疗方法是在72小时内结合2%的氢化和2%的氢化集中,与2234种多糖浓度(DP)结合,如果用作抑制矩阵,就会满足要求。《modified characteristics面粉在这雾是水满足16 . 47%,阿什内容1 . 17%,amylose 31 . 01%, viscosity 155cP、solubility 80。83%和IC antioxidant活动(50)148μgml - 1。微镜和SEM在酸性氢化中没有变化太多。
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引用次数: 5
期刊
JLI Jurnal Litbang Industri
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