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A portable calorimeter for measuring the calorific value of natural gas 一种测量天然气热值的便携式量热计
IF 0.1 Pub Date : 2021-09-29 DOI: 10.24027/2306-7039.3.2021.241253
L. Prysyazhnyuk, I. Petryshyn, B. Dolishnii, L. Ropyak
Abstract Natural gas quality assessment is a relevant issue. A critical analysis of calorimeter designs for measuring the calorific value of natural gas was carried out. The most common methods for determining the calorific value of natural gas are as follows: direct by gas calorimeters; indirect by gas chromatographs; indirect, based on correlations. The advantages of isoperibolic calorimeters of measuring calorific value of natural gas directly in the consumer’s conditions are substantiated. The design of a portable calorimeter containing a thermostated shell, calorimetric tank, Peltier element with tank, circulating pump, gas burner, thermostat systems, metered supply of natural gas and air, fuel ignition, sensors, combustion analyzer and control and measurement unit, was developed. The geometric dimensions of the calorimetric tank are optimized, materials and technologies of manufacturing parts are specified. The metrological analysis of the developed portable calorimeter was carried out. A method for measuring the calorific value of natural gas directly in the conditions of household consumers and transport enterprises was developed. The results of testing the prototype calorimeter in the laboratory confirmed its high performance and metrological characteristics, and the deviation of the measurement of the calorific value of natural gas from that determined using a gas chromatograph was 0.6%.
天然气质量评价是一个相关问题。对测量天然气热值的量热计设计进行了严格的分析。测定天然气热值最常用的方法有:直接用气体量热计测定;间接气相色谱法;间接的,基于相关性。证实了等循环量热仪在消费者条件下直接测量天然气热值的优点。设计了一种便携式量热计,包括恒温外壳、量热罐、带罐的珀尔梯元件、循环泵、燃气燃烧器、恒温系统、天然气和空气计量供应、燃料点火、传感器、燃烧分析仪以及控制和测量单元。优化了量热罐的几何尺寸,规定了制造零件的材料和工艺。对研制的便携式量热仪进行了计量分析。提出了一种在家庭消费者和运输企业条件下直接测量天然气热值的方法。样品量热仪在实验室的测试结果证实了其高性能和计量特性,天然气热值测量与气相色谱仪测定的偏差为0.6%。
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引用次数: 1
Qualimetric assessment of metrological characteristics of household gas meters during periodic verification 定期检定时家用燃气表计量特性的质量评定
IF 0.1 Pub Date : 2021-07-02 DOI: 10.24027/2306-7039.2.2021.236086
Орест Євгенович Середюк, Олександр Криницький, Василь Романів, Деніс Середюк, Анна Григорівна Винничук
Informative parameters for statistical estimation of operational error of SAMGAS, METRIX, PREMAGAS household gas meters (HGM) are formulated. These are the values of the measured volume during the verification period of operation and the experimentally determined error of the meter during operation at three normalized flow rates: minimum, maximum and 20% of the maximum. Six ranges of variation of the HGM error at the minimum flow rate were selected to form statistical samples of meters. According to the proposed algorithm, the change in the weighted average HGM error for three normalized flow rates from the measured volume is quantified, taking into account the number of HGMs and their error ranges. It is proposed to apply the concept of generalized weighted average error of HGM, which reflects the operational error of HGMs during their operation in the entire range of consumption when measuring gas volumes up to 60 thousand cubic meters.
制定了SAMGAS、METRIX、PREMAGAS家用燃气表(HGM)运行误差统计估计的信息性参数。这些是在运行验证期间测量的体积值,以及在三种标准化流速(最小、最大和最大的20%)下运行期间仪表的实验确定的误差。选择最小流速下HGM误差的六个变化范围来形成流量计的统计样本。根据所提出的算法,在考虑HGM的数量及其误差范围的情况下,量化了来自测量体积的三个归一化流速的加权平均HGM误差的变化。建议应用HGM广义加权平均误差的概念,该概念反映了HGM在测量高达6万立方米的天然气体积时在整个消耗范围内运行时的操作误差。
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引用次数: 0
Procedure of hydrogen and mixture impact assessment on the changes of mechanical parameters and errors of household gas meters 氢气和混合物对家用燃气表机械参数和误差变化的影响评估程序
IF 0.1 Pub Date : 2021-07-02 DOI: 10.24027/2306-7039.2.2021.236083
I. Petryshyn, D. Serediuk, Yuriy Pelikan, Oleksandr Bas, Roman Manulyak
The article describes the method of conducting representative research to determine the effect of pure gaseous hydrogen and a mixture of hydrogen and natural gas (methane) on the performance and metrological characteristics of household gas meters. The experimental research has been carried out in two stages. 84 membrane and rotary meters have been selected for research. The main aspect of the need for such research is the safety of meters. Before the start of the tests and after each stage, the metrological characteristics of all gas meters on the reference prover are determined. At the first stage, a set of static tests is performed, according to which the internal and external short-term and long-term (42 days) tightness of gas meters are checked. A prototype of the installation layout has been developed to conduct experiments on determining the tightness. The second stage is to conduct a dynamic series of tests. Gas meters are assembled according to the developed scheme and installed for testing on the model of the gas distribution network system. It is recommended to use a drum-type meter as a reference gas meter. The criterion for determining the effect of hydrogen and gas meter is the established change in metrological characteristics after the study.
本文描述了进行代表性研究的方法,以确定纯气态氢气以及氢气和天然气(甲烷)的混合物对家用燃气表性能和计量特性的影响。实验研究分两个阶段进行。选择了84个膜式和旋转式流量计进行研究。需要进行此类研究的主要方面是电表的安全性。在测试开始之前和每个阶段之后,确定参考校准仪上所有气量计的计量特性。在第一阶段,进行了一组静态测试,根据这些测试检查燃气表的内部和外部短期和长期(42天)密封性。已经开发了安装布局的原型,以进行确定密封性的实验。第二阶段是进行一系列动态测试。燃气表根据开发的方案进行组装,并安装在燃气分配网络系统的模型上进行测试。建议使用鼓型气量计作为参考气量计。确定氢气和燃气表效果的标准是研究后计量特性的既定变化。
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引用次数: 0
Synthesis of a linear static function for grain moisture meter with capacitive sensors 电容式谷物水分计线性静态函数的综合
IF 0.1 Pub Date : 2021-07-02 DOI: 10.24027/2306-7039.2.2021.236098
О. В. Заболотний, Віталій Заболотний, Микола Дмитрович Кошовий
Moisture content is a grain quality factor, a parameter which changes during the processes of storage and processing and determines consumer properties of different food products. OIML organization in its international recommendation OIML R59 “Moisture Meters for Cereal Grain and Oilseeds” restricts maximal permissible value of moisture meters uncertainty to not more than 3% of relative full scale error. Main task of the research is in receiving linear static function for the grain moisture meter with four capacitive sensors. Method of Least Squares and general linear regression instruments had been used for that purpose. Analyzing the graphs of modified static function for different moist substances it was possible to say that it happened to be far more effective than initial static function and the static function received from a first-order polynomial after the LS method implementation. Root mean estimator was calculated for initial static function, the static function received with the LS method and static function, received after general linear regression implementation as an integral difference between nominal and calculated values of moisture content. Corresponding root mean estimator values were 1.3062%, 1.1616% and 0.4158%, that proves the effectiveness of a static function modified with the general linear regression instruments.Keywords: moisture content measurement; capacitive moisture meter; reference channel; capacitive sensor; linear static function
水分含量是粮食的一个品质因子,是在储存和加工过程中变化的参数,它决定了不同食品的消费特性。OIML组织在其国际建议OIML R59《谷物和油籽用湿度计》中限制湿度计不确定度的最大允许值不超过相对满量程误差的3%。研究的主要任务是接收四电容式谷物水分计的线性静态函数。为此,使用了最小二乘法和一般线性回归工具。通过对不同湿性物质的修正静态函数图的分析,可以发现LS方法实施后,修正静态函数的效果远远优于初始静态函数和从一阶多项式得到的静态函数。对初始静态函数、LS法得到的静态函数和一般线性回归后得到的静态函数进行均方根估计,作为含水率标称值与计算值之间的积分差。相应的根均值估计值分别为1.3062%、1.1616%和0.4158%,证明了用一般线性回归工具修正静态函数的有效性。关键词:含水率测量;电容式湿度计;参考通道;电容式传感器;线性静态函数
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引用次数: 1
Method of kurtosis in estimating the measurement uncertainty during calibration of the electrical resistance measures using a potentiometer 用电位器校准电阻测量时估计测量不确定度的峰度方法
IF 0.1 Pub Date : 2021-07-02 DOI: 10.24027/2306-7039.2.2021.236078
Ігор Петрович Захаров, Олеся Анатоліївна Боцюра, Валерій Семеніхін
Calibration of electrical resistance measures is considered by the indirect method, which is realized through measuring the voltage drop across the series-connected reference and calibrated resistors. The biases of the estimates of the measurand and the combined standard uncertainty due to the nonlinearity of the measurement model were calculated. The distribution laws of the input quantities in the calculation of the expanded uncertainty were taken into account by the kurtosis method. An example of measurement uncertainty evaluating during calibration of single-size electrical resistance measure R331 with a nominal resistance of 1000 Ω by comparing its value using a potentiometer R345 with the value of the calibrated reference standard is considered. Estimates of the measurand and its standard and expanded uncertainties obtained using the proposed method showed good agreement with the estimates obtained using the Monte Carlo method.
电阻测量的校准采用间接方法,通过测量串联的参考电阻和校准电阻之间的压降来实现。计算了由于测量模型的非线性所引起的测量值估计偏差和联合标准不确定度。在计算扩展不确定性时,采用峰度法考虑了输入量的分布规律。以标称电阻为1000 Ω的单尺寸电阻测量器R331为例,通过电位器R345与校准的参考标准值进行比较,评定测量不确定度。用该方法得到的测量值及其标准不确定度和扩展不确定度的估计值与用蒙特卡罗方法得到的估计值一致。
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引用次数: 0
The mathematical model of the system-oriented measuring instrument 面向系统的测量仪器的数学模型
IF 0.1 Pub Date : 2021-07-02 DOI: 10.24027/2306-7039.2.2021.236057
Олег Величко, Олег Грабовський
Modern measuring instruments (MIs) are designed to obtain complete and reliable measuring information. To perform this important function, MIs must be of appropriate quality and must be reliably assessed. Using mathematical models simulate the operation of technical systems in order to decide on the optimization of its characteristics. As a result of the analysis of the model, the specific features of the studied processes and certain quantitative regularities are established. This allows to predict the processes in the system over time and determine their quantitative characteristics. The article presents the results of mathematical modeling of system-oriented measuring instruments as a system and its software as a subsystem using the apparatus of general systems theory. Such models with its graphical interpretation allow obtaining the necessary and useful information about the properties of the MIs as a technical system. The performed modeling makes it possible to describe the functioning of the MIs and to obtain a certain assessment of quality indicators.
现代测量仪器(MI)旨在获得完整可靠的测量信息。为了履行这一重要职能,MI必须具有适当的质量,并且必须进行可靠的评估。利用数学模型模拟技术系统的运行,以决定其特性的优化。通过对模型的分析,确定了研究过程的具体特征和一定的定量规律。这允许预测系统中随时间变化的过程,并确定其定量特征。本文介绍了利用一般系统理论的仪器,将面向系统的测量仪器作为一个系统及其软件作为一个子系统进行数学建模的结果。这种具有图形解释的模型允许获得关于作为技术系统的MI的特性的必要和有用的信息。所执行的建模使得描述MI的功能和获得质量指标的特定评估成为可能。
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引用次数: 1
Reliable instrumental metering of natural gas is the key to Ukraine’s energy independence 可靠的天然气仪表计量是乌克兰能源独立的关键
IF 0.1 Pub Date : 2021-07-02 DOI: 10.24027/2306-7039.2.2021.236084
Аліна Коваленко
By virtue of geographical and historic factors, Ukraine has been playing an important role in oil and natural gas deliveries to European energy markets. Such status is basically attributed to the fact that West and Central European countries, while being rather big consumers of natural hydrocarbons, have shortage in their own energy resources. On the other hand, major natural gas and oil reserves are concentrated in the Russian Federation, Caspian region and the Gulf area. Currently Ukraine has become a major juncture in the transit of gas and oil from Russia and Kazakhstan to European markets. The expected increase in consumption of natural hydrocarbon resources, as well as their uneven distribution make Ukraine, owing to its suitable geographical location and the developed gas and oil network, an “energy bridge” between the exporting countries and consumers in the industrialized Europe. In the article the author considers the modern gas supply system of Ukraine. The author carried out a study on the technical feasibility of calibration of flow meters on the environment of natural gas under pressure. Currently in Ukraine calibration is performed only in the air. This does not make it possible to reduce the error in the instrumentation of natural gas. Given the volume of natural gas consumption in the country (about 20 billion m3/year), this leads to huge non-production losses, negative impact on economic performance and inflated cost for end users. The European experience was analyzed: PTB, DNV, PIGSAR, SICK, INOTECH. Modernization of the gas industry of Ukraine is proposed.
由于地理和历史因素,乌克兰在向欧洲能源市场输送石油和天然气方面一直发挥着重要作用。这主要是由于西欧和中欧国家虽然是天然碳氢化合物的大消费国,但他们自己的能源短缺。另一方面,主要的天然气和石油储备集中在俄罗斯联邦、里海地区和海湾地区。目前,乌克兰已成为俄罗斯和哈萨克斯坦向欧洲市场输送天然气和石油的重要枢纽。预计天然碳氢化合物资源的消费将会增加,而且这种资源的分布不均衡,这使乌克兰由于其适当的地理位置和发达的天然气和石油网络而成为出口国和工业化欧洲消费者之间的“能源桥梁”。本文对乌克兰的现代天然气供应系统进行了思考。对天然气承压环境下流量计标定的技术可行性进行了研究。目前在乌克兰,校准只在空中进行。这并不能减少天然气仪器的误差。鉴于该国的天然气消费量(约200亿立方米/年),这会导致巨大的非生产损失,对经济效益产生负面影响,并导致最终用户的成本膨胀。分析了欧洲的经验:PTB、DNV、PIGSAR、SICK、INOTECH。提出了乌克兰天然气工业的现代化。
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引用次数: 0
About continuity and discreteness of quantities: examples from physics and metrology 关于量的连续性和离散性:来自物理学和计量学的例子
IF 0.1 Pub Date : 2021-07-02 DOI: 10.24027/2306-7039.2.2021.236054
F. Pavese
The VIM3 defines a quantity as a “property of a phenomenon, body, or substance”, leaving the characteristics of the term ‘quantity’, related to the chosen characteristics of the relevant properties. The question is: does necessarily a property also necessarily refer to the possible granularity of a phenomenon, body, or substance?Take, for example, for the quantity “mass”: it does not always have to take into account whether or not a phenomenon, body, or substance is subdivided into discrete entities? It depends of the frame of the analysis and also on the chosen measurement unit. In other cases, like temperature, the macroscopic properties are related to the statistical properties of granular substances like atoms and molecules are, so the present meaning of ‘temperature’ is generally lost at the numerical level where the entity’s statistics become meaningless. Yet another case is quantum physics. The paper illustrates the issue and possible solutions under development.Keywords: continuous; granular; quantity; magnitude; quanta; integer number; real number; counting; function
VIM3将量定义为“现象、物体或物质的特性”,留下“量”一词的特征,与相关特性的选定特征相关。问题是:一个性质是否也必然指一种现象、物体或物质的可能粒度?以“质量”为例:它并不总是需要考虑一个现象、物体或物质是否被细分为离散的实体?这取决于分析的框架,也取决于所选择的测量单位。在其他情况下,如温度,宏观性质与原子和分子等颗粒物质的统计性质有关,因此“温度”的当前含义通常在数值水平上消失,实体的统计变得毫无意义。另一个例子是量子物理学。本文阐述了这一问题以及正在制定的可能解决方案。关键词:连续;由颗粒构成的量巨大量子;整数;实数;计数;作用
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引用次数: 1
Comparative analysis of the accuracy requirements of the equipment for determining the mean integral refractive index of air using different realizations of the gradient method 比较分析了不同梯度法实现下空气平均积分折射率测定设备的精度要求
IF 0.1 Pub Date : 2021-07-02 DOI: 10.24027/2306-7039.2.2021.236075
P. Neyezhmakov, A. Prokopov, Tatiana Panasenko, A. Shloma
The speed of propagation of electromagnetic waves in the Earth’s atmosphere differs from the speed of their propagation in a vacuum, which is one of the main factors that have a significant impact on the accuracy of long distance measurement. This influence is taken into account in long distance measurement with the correction for the mean integral group refractive index of air, which depends on such meteorological parameters as temperature, atmospheric pressure and relative air humidity.The purpose of this work is to compare the accuracy requirements for equipment designed to measure temperature, pressure, and relative humidity required to determine the above correction by the gradient method using the Euler-Maclaurin quadrature formula (hereafter, the Euler-Maclaurin method) and the formula based on Hermite interpolation polynomials (hereafter, the Hermite method). The requirements for the uncertainty of measurements carried out with the sensors of meteorological parameters, allowing to find the mean integral group refractive index of air, providing length measurements of the baselines of up to 5 km with an expanded uncertainty of not more than 1 mm, are established.Keywords: atmosphere; mean integral group refractive index of air; laser long distance measurement
电磁波在地球大气层中的传播速度与在真空中的传播速率不同,这是对远距离测量精度产生重大影响的主要因素之一。在对空气的平均积分群折射率进行校正的长距离测量中考虑了这种影响,该折射率取决于温度、大气压力和相对空气湿度等气象参数。本工作的目的是比较设计用于测量温度、压力和相对湿度的设备的精度要求,这些设备需要通过使用Euler-Maclaurin求积公式(以下简称Euler-Mclaurin方法)的梯度法和基于Hermite插值多项式的公式(以下称Hermite方法)来确定上述校正。确定了利用气象参数传感器进行测量的不确定度要求,从而能够找到空气的平均积分群折射率,提供5公里以下基线的长度测量,扩展不确定度不超过1毫米。关键词:大气;空气的平均积分群折射率;激光远距离测量
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引用次数: 0
Immersion ultrasonic transducers 浸入式超声波换能器
IF 0.1 Pub Date : 2021-07-02 DOI: 10.24027/2306-7039.2.2021.236076
Ортаголі Хакімов
The principles of operation and design of immersion ultrasonic transducers developed by the authors for excitation and reception of elastic vibrations in moving filament-like and plane-parallel materials, in particular, polymer fibbers and films, with an adjustable angle of input (reception) of probing signals into moving controlled object – polymer fibbers and films at normal and high temperatures. The technical characteristics of the installation are given in which the converters developed by us are used, namely, sounding base (distance from the emitter to the receivers), the duration of the probing pulses, the frequency of filling and the duration of the probing pulses, the speed of the controlled object, the combined standard measurement uncertainties of the difference Δt of the propagation times of ultrasonic waves from the emitter to the first and second signal receivers, relative combined standard uncertainties of measurements of attenuation coefficient and velocity of propagation of ultrasonic waves.
作者开发的浸入式超声波换能器的工作原理和设计用于激励和接收移动的丝状和平面平行材料中的弹性振动,特别是聚合物纤维和薄膜,在常温和高温下,具有可调节的探测信号输入(接收)角度,可进入移动的受控对象——聚合物纤维和薄膜。给出了使用我们开发的转换器的设备的技术特征,即探测基准(从发射器到接收器的距离)、探测脉冲的持续时间、填充频率和探测脉冲的时间、受控对象的速度、,超声波从发射器到第一和第二信号接收器的传播时间差Δt的组合标准测量不确定度,超声波的衰减系数和传播速度的测量的相对组合标准不确定度。
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引用次数: 0
期刊
Ukrainian Metrological Journal
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