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Free vibration and mechanical behavior of treated woven jute polymer composite 经处理的编织黄麻聚合物复合材料的自由振动和力学性能
Q3 Materials Science Pub Date : 2023-09-15 DOI: 10.17212/1994-6309-2023-25.3-137-151
Savendra Singh, Chetan Hirwani
Introduction: Recently, the use of natural fibers have been increased to replace the use of synthetic fibers to save our environment from waste disposal problems, natural fibers have a lower level of mechanical properties. The purpose of work: This study examines the effect of treating the surface and deeper layers of jute fiber on the mechanical behavior and characteristics of free vibrations of a composite material based on it. The methods of investigation: due to the uniform distribution of stresses in the WARP and WEFT directions, four-layer basket weave jute fibers were used in this study. Result and discussion: the mechanical and free vibration properties of composite materials are significantly improved when NaOH is applied to jute fibers because it eliminates the weak matrix material lignin and makes the fibers stiffer and stronger. However, increasing the percentage of NaOH and soaking time for the fibers in NaOH solution have little effect on these properties. The highest value of tensile strength and tensile modulus are found 50 ± 1.17 MPa and 1.94 ± 0.23 GPa respectively seen in case of basket weave jute fiber composite with 1 hour treatment. Tensile strength and tensile modulus increase about 12 % and 40 % over the stokes value, respectively. Similarly the value of flexural strength and flexural modulus are found 95 ± 1.17 MPa and 3.99 ± 0.23 GPa respectively in case of basket weave jute fiber composite with 1 hour treatment. It also shows the highest value of fundamental frequency 77.837 Hz.The presence of an O-H bond in the composite, as revealed by FTIR study, gives it a hydrophilic character and limits its use in humid environments. The fiber to matrix ratio is shown in SEM images.
简介:近年来,天然纤维的使用越来越多,以取代合成纤维的使用,以拯救我们的环境免于废物处理的问题,天然纤维具有较低水平的机械性能。工作目的:本研究考察了黄麻纤维表面和深层处理对基于它的复合材料的机械行为和自由振动特性的影响。研究方法:由于应力在WARP和WEFT方向上分布均匀,本研究采用四层篮编黄麻纤维。结果与讨论:在黄麻纤维中加入NaOH后,复合材料的力学性能和自由振动性能明显改善,因为NaOH消除了弱基质材料木质素,使纤维变得更硬、更强。然而,增加NaOH的比例和在NaOH溶液中的浸泡时间对纤维的这些性能影响不大。篮织黄麻复合材料经1小时的拉伸强度和拉伸模量最高,分别为50±1.17 MPa和1.94±0.23 GPa。拉伸强度和拉伸模量分别比斯托克斯值提高约12%和40%。篮织黄麻复合材料经1小时处理后,其抗弯强度和抗弯模量分别为95±1.17 MPa和3.99±0.23 GPa。它还显示了基频77.837 Hz的最大值。FTIR研究表明,复合材料中O-H键的存在使其具有亲水性,限制了其在潮湿环境中的使用。纤维与基体的比率显示在SEM图像中。
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引用次数: 0
Experimental studies of high-speed grinding rails modes 高速磨削导轨模态试验研究
Q3 Materials Science Pub Date : 2023-09-15 DOI: 10.17212/1994-6309-2023-25.3-19-35
Andrey Ilinykh, Aleksandr Pikalov, Vladimir Miloradovich, Marina Galay
Introduction. Rails’ grinding in the conditions of a railway track is a priority for extending its life cycle due to the timely removal of tread surface defects and formation of required transverse profile. Today, 14 RSHP-48 rail grinding trains are used in Russia. At the same time, most rail grinding trains are ending its service life. Therefore, the development of a fundamentally new rail grinding train with increased efficiency is an urgent task. Siberian transport university is working together with the Kaluga plant “Remputmash” to create a new rail grinding train named RSHP 2.0. The rail grinding train RSHP 2.0 is based on the technology of high-speed rail grinding, which is based on increasing working speed of rail grinding train by increasing rotational speed of grinding wheels and setting the angle of attack. The aim of this work is to study rails’ grinding modes on a specially designed installation URSH, which implements the technology of high-speed grinding rails by increasing speed of grinding wheels rotation up to 5,000 rpm. Research methods. Grinding wheel speed control was carried out by IT-5-ChM “Termit” electronic tachometer and “Megeon 18005” laser tachometer. The angle of attack of grinding wheel was measured by digital, three-axis accelerometer-inclinometer ATst 90. The force of pressing grinding wheel to the rail was evaluated by strain-resistive sensors M50-0.5-C3. The measurement of head rail transverse profile before and after grinding and evaluation of metal removal were carried out by a PR-03 rail profiler. The width of grinding track was controlled by ShTsTs-I-300-0.01 caliper. The surface roughness of rail sample after machining was measured by TR 200 portable instrument. Results and discussion. Based on research results of CRS, the parameters of the working equipment of designed grinding rail train, which implements the technology of high-speed rail grinding, the influence of grinding modes on the formation of the quality parameters of the machined rail surface are established, and the optimal values of the forces of pressing the grinding wheel to the rail are determined.
介绍。在铁路轨道条件下,钢轨磨削是延长钢轨寿命的首要任务,因为它能及时消除胎面缺陷,形成所需的横向轮廓。今天,俄罗斯使用了14辆RSHP-48轨道磨削列车。与此同时,大多数钢轨磨削列车正在结束其使用寿命。因此,开发一种全新、高效的钢轨磨削列车是一项紧迫的任务。西伯利亚交通大学正在与卡卢加“Remputmash”工厂合作,创造一种名为RSHP 2.0的新型轨道磨削列车。钢轨磨削列车RSHP 2.0是基于高速钢轨磨削技术,通过提高砂轮转速和设置攻角来提高钢轨磨削列车的工作速度。本研究的目的是在一个特殊设计的URSH装置上研究钢轨的磨削方式,该装置通过将砂轮转速提高到5000转/分来实现高速磨削钢轨技术。研究方法。采用IT-5-ChM“Termit”电子转速表和“Megeon 18005”激光转速表对砂轮转速进行控制。采用数字式三轴加速度-倾角仪atst90测量砂轮迎角。采用应变式传感器M50-0.5-C3测量砂轮对导轨的压紧力。利用PR-03型钢轨廓形仪对磨削前后的头轨横廓形进行了测量,并对金属去除率进行了评价。采用ShTsTs-I-300-0.01卡尺控制磨削轨迹宽度。用tr200便携式仪器测量了加工后钢轨样品的表面粗糙度。结果和讨论。基于CRS的研究成果,设计了实现高速铁路磨削技术的磨削轨道列车的工作设备参数,建立了磨削方式对加工轨道表面质量参数形成的影响,确定了砂轮对轨道的压紧力的最优值。
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引用次数: 0
Structure and properties of HEA-based coating reinforced with CrB particles CrB颗粒增强hea基涂层的结构与性能
Q3 Materials Science Pub Date : 2023-09-15 DOI: 10.17212/1994-6309-2023-25.3-87-103
Alexey Ruktuev, Aleksandr Yurgin, Vladislav Shikalov, Arina Ukhina, Ivan Chakin, Evgeny Domarov, Gleb Dovzhenko
Introduction. Currently, a new class of materials, namely high-entropy alloys, is an active area of research. One of the areas of its application is the fabrication of protective coatings with high performance properties. The high-entropy alloy of CoCrFeNiMn composition is characterized by high ductility, which is retained both at elevated and cryogenic temperatures, as well as high thermal stability and, thus, can be considered as promising materials for protective coatings formation. At the same time, its disadvantages are low hardness and strength. It is known that the reinforcement of the CoCrFeNiMn high-entropy alloy with hardening particles is an effective way to improve the mechanical properties of coatings. It is assumed that the addition of hardening boride particles affects positively on the mechanical characteristics of the alloy. The aim of this work is to study the structural and phase states and wear resistance of coatings based on a CoCrFeNiMn high-entropy alloy reinforced with CrB particles. Coatings obtained by the method of non-vacuum electron-beam surfacing of powder mixtures with different mass ratios of CoCrNiMn metal powders to the CrB powder (100:0, 95:5, 90:10, 80:20, 70:30) are studied in this work. To investigate the structure and phase composition of the coatings, such methods as optical microscopy, scanning electron microscopy and X-ray diffraction analysis were applied. To study the elemental composition, energy-dispersive X-ray analysis was used. The mechanical properties were evaluated based on the microhardness measuring results. The wear resistance of the coatings was determined under conditions of dry sliding friction during reciprocating motion. Results and discussion. The addition of CrB powder to the surfacing mixture led to the formation of eutectic structures. When 5 wt. % CrB was added, a hypoeutectic structure is formed in the coating. An increase in the amount of CrB leads to the formation of coatings with a hypereutectic structure containing primary borides. The main phases found in the coatings are the fcc solid solution, and (Cr,Mn,Fe)2B, (Ni,Co,Mn)2B, CrB borides. All the studied coatings are characterized by an adhesive wear mechanism. The addition of 20 % and 30 % CrB to the surfacing mixture composition results in the wear resistance increase of the high-entropy alloy-based coatings by 3.6 and 6.1 times, respectively.
介绍。目前,一类新的材料,即高熵合金,是一个活跃的研究领域。其应用领域之一是制造具有高性能的保护涂层。CoCrFeNiMn组成的高熵合金具有高延展性,在高温和低温下都能保持高的延展性,以及高的热稳定性,因此可以被认为是有前途的保护涂层材料。同时,它的缺点是硬度和强度低。研究表明,用硬化颗粒增强CoCrFeNiMn高熵合金是提高涂层力学性能的有效途径。认为硬化硼化物颗粒的加入对合金的力学性能有积极的影响。研究了CrB颗粒增强CoCrFeNiMn高熵合金涂层的组织、相态和耐磨性。研究了不同质量比的CoCrNiMn金属粉末与CrB粉末(100:0,95:5,90:10,80:20,70:30)的粉末混合物采用非真空电子束堆焊方法制备的涂层。采用光学显微镜、扫描电镜和x射线衍射分析等方法对涂层的结构和相组成进行了研究。为了研究元素组成,采用了能量色散x射线分析。根据显微硬度测试结果评价了材料的力学性能。在往复运动干滑动摩擦条件下测定了涂层的耐磨性。结果和讨论。在堆焊混合物中加入CrB粉末可形成共晶结构。当加入5 wt. % CrB时,涂层中形成亚共晶结构。随着CrB含量的增加,形成了含有初生硼化物的过共晶涂层。涂层中的主要相为fcc固溶体和(Cr,Mn,Fe)2B、(Ni,Co,Mn)2B、CrB硼化物。所研究的涂层均具有粘附磨损机理。在堆焊混合物中添加20%和30%的CrB,可使高熵合金基涂层的耐磨性分别提高3.6倍和6.1倍。
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引用次数: 0
Study of energy dissipation and rigidity of welded joints obtained by pressure butt welding 压力对接焊接接头的耗能和刚度研究
Q3 Materials Science Pub Date : 2023-09-15 DOI: 10.17212/1994-6309-2023-25.3-104-116
Anatoly Maytakov, Alexey Grachev, Anatoly Popov, Sergey Li, Nadezhda Vetrova, Konstantin Plotnikov
Introduction. When studying the energy dissipation associated with internal friction in a weld, it is extremely important to choose a measurement technique, since the reliability and integrity of the data obtained depends on it. At the same time, it is necessary to investigate the change in internal friction depending on the presence of defects in the weld. Of the variety of methods for non-destructive testing of joints obtained by pressure welding, only ultrasonic is currently used. However, lightly oxidized lacks of welding penetration are not detected, which can be detected only in the presence of other defects accompanying it. Compounds of dissimilar materials are not controlled by ultrasound at all. Therefore, the development of non-destructive testing methods for such compounds is very relevant. The purpose of the work: to find a procedure for testing the quality of a welded joint in metals and alloys that will be a quick and simple alternative to the known methods of non-destructive testing, by measuring the energy dissipation in the weld of the sample by the static hysteresis loop method. The method of investigation is non-destructive quality control of the welded joint in metals and alloys by measuring the energy dissipation in the weld of the sample by the static hysteresis loop method. Results and discussion. It is established that with an increase in the lacks of welding penetration, the energy dissipation increases at the same values of the torque amplitude under static loading conditions. The rigidity of the qualitative welded joints remains constant, and the joints with lacks of welding penetration decrease with increasing torque amplitude. The relationship of strength with stiffness and damping ability obtained by the static hysteresis loop method is preserved for various structural states of the sample material.
介绍。在研究与焊缝内摩擦相关的能量耗散时,选择一种测量技术是非常重要的,因为所获得的数据的可靠性和完整性取决于它。同时,有必要研究内摩擦的变化取决于焊缝中缺陷的存在。在压力焊接获得的接头的各种无损检测方法中,目前只使用超声波。然而,不能检测到轻度氧化缺乏焊透,只有在伴随其他缺陷的情况下才能检测到。不同材料的化合物根本不受超声波的控制。因此,开发此类化合物的无损检测方法具有十分重要的意义。这项工作的目的是:寻找一种测试金属和合金焊接接头质量的程序,该程序将是一种快速和简单的替代已知的无损检测方法,通过静态滞后回线法测量样品焊缝中的能量耗散。研究方法是采用静滞回线法测量试样焊缝中的能量耗散,对金属和合金焊接接头进行无损质量控制。结果和讨论。结果表明,在静加载条件下,当扭矩幅值相同时,随着焊透缺失量的增加,能量耗散增大。定性焊接接头刚度保持不变,焊透不足的接头刚度随扭矩幅值的增大而减小。静力滞回线法得到的强度与刚度和阻尼能力的关系在不同结构状态下都保持不变。
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引用次数: 0
The concept of microsimulation of processes of joining dissimilar materials by plastic deformation 塑性变形连接异种材料过程的微观模拟概念
Q3 Materials Science Pub Date : 2023-09-15 DOI: 10.17212/1994-6309-2023-25.3-36-49
Denis Salikhyanov, Nikolay Michurov
Introduction. Bond strength between dissimilar materials is the most important characteristic of laminated composites, which determines the success of its development for industrial use. In order to develop the theory of joining materials by plastic deformation, it is proposed to perform computer simulation of joint deformation of representative volumes of dissimilar materials on a microscale and compare the parameters of the stress-strain state with the previously presented theoretical mechanism. The aim of this work is to analyze the stress-strain state of dissimilar materials under plastic deformation on a microscale and to establish the location of the onset of fracture of surface oxide films. To achieve this aim, the following tasks of the work are formulated: 1) to study the surface profiles of dissimilar materials to be bonded by plastic deformation; 2) to simulate by the finite element method (FE) the plastic deformation of contact surfaces of dissimilar materials on a microscale; 3) to study the stages of joint deformation of dissimilar materials on a microscale and verify of the theoretical mechanism. Research methodology. The study of three-dimensional topography and roughness was carried out on a Veeco Wyko NT1100 Optical Profiling System. Deform-3D FE simulation package was chosen as the main research tool. Aluminum alloys AMg3 and D16 were chosen as the materials under study. Results and discussion. In this work, computer FE simulating of the joint deformation of the surface layers of AMg3 and D16 alloys on a microscale was performed, an analysis of the surface profiles of materials after various types of processing was carried out, the parameters of the stress-strain state were studied and compared with the parameters of the theoretical mechanism. Based on the results of the comparison, the adequacy of the proposed theoretical mechanism was assessed, and the practical difficulties of theoretical simulation of the joint deformation of dissimilar materials on the microscale were noted. Microscale FE simulation made it possible to study the flow of plastic deformation in the near-surface layers of materials, as well as to identify areas of the most probable fracture of surface oxide films and, consequently, areas of primary bonding of dissimilar materials.
介绍。不同材料之间的结合强度是层压复合材料最重要的特性,它决定了层压复合材料工业开发的成功与否。为了进一步发展塑性变形连接材料理论,提出了在微观尺度上对不同材料的典型体的连接变形进行计算机模拟,并将应力-应变状态参数与已有的理论机制进行比较。本工作的目的是在微观尺度上分析不同材料在塑性变形下的应力-应变状态,并确定表面氧化膜断裂的起始位置。为了实现这一目标,制定了以下工作任务:1)研究塑性变形粘合的不同材料的表面轮廓;2)采用有限元法模拟不同材料接触面在微尺度上的塑性变形;3)在微观尺度上研究不同材料节理变形的阶段,验证理论机理。研究方法。在Veeco Wyko NT1100光学仿形系统上进行了三维形貌和粗糙度的研究。本文选择Deform-3D有限元仿真包作为主要研究工具。选用铝合金AMg3和D16作为研究材料。结果和讨论。在微观尺度上对AMg3和D16合金表层的接头变形进行了计算机有限元模拟,分析了材料经过各种加工后的表面轮廓,研究了应力-应变状态参数,并与理论机理参数进行了比较。基于对比结果,评价了所提出的理论机制的充分性,并指出了在微观尺度上理论模拟不同材料接头变形的实际困难。微尺度有限元模拟可以研究材料近表层的塑性变形流动,也可以确定表面氧化膜最可能断裂的区域,从而确定不同材料的主要结合区域。
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引用次数: 0
Rationalization of modes of HFC hardening of working surfaces of a plug in the conditions of hybrid processing 杂化加工条件下插头工作面HFC硬化方式的合理化
Q3 Materials Science Pub Date : 2023-09-15 DOI: 10.17212/1994-6309-2023-25.3-63-86
Vadim Skeeba, Nikita Vakhrushev, Kristina Titova, Aleksey Chernikov
Introduction. The development of a cluster of hybrid metalworking systems in the machine tool industry is associated with a number of positive consequences. First, such systems help reduce production costs by optimizing the use of resources and energy. This is especially true in the face of increased competition and a trend towards savings. Secondly, hybrid systems enable the production of quality products with increased efficiency. By integrating various functions in one process equipment, metalworking processes become more efficient and precise. This reduces the amount of defective products and improves the quality of the final ones. In addition, hybrid metalworking systems have autonomous functionality, which is especially important in flexible engineering production, where rapid changeover and adaptation to various production tasks is required. Thus, hybrid metalworking systems represent an important step in the development of modern mechanical engineering, helping to reduce costs, increase efficiency and ensure high product quality. The purpose of this work is to increase efficiency and reduce energy consumption during surface-thermal hardening of machine parts through the use of concentrated energy sources under integral processing conditions. Theory and Methods. To achieve this purpose, studies were carried out on the possible structural composition and layout of hybrid equipment integrating mechanical and surface-thermal processes. When developing the theory and methods, the main provisions of the structural synthesis and components of metalworking systems were taken into account. Theoretical research is based on the application of system analysis, geometric theory of surface formation and design of metalworking machines. The experiments were carried out on a modernized multi-purpose machining center MS 032.06, equipped with an additional energy source, which was a microwave thyristor-type generator SHF-10 with an operating frequency of 440 kHz, which implements high-energy heating by high-frequency currents. Structural studies were carried out using optical and scanning microscopy. The stress-strain state of the surface layer of the part was evaluated by mechanical and X-ray methods for determining residual stresses. The microhardness of the hardened surface layer of the parts was evaluated on a Wolpert Group 402MVD instrument. Results and discussion. An original method for conducting structural-kinematic analysis for pre-project studies of hybrid metalworking equipment is presented. Methodological recommendations were developed for the modernization of metal-cutting machine tools, allowing high-energy heating with high-frequency currents (HEH HFC) on a standard machine tool system and creating high-tech technological equipment with enhanced functionality. It has been experimentally confirmed that the introduction of the proposed hybrid machine into production in combination with recommendations for the appointment of high-frequency elec
介绍。在机床工业中,混合金属加工系统集群的发展带来了许多积极的后果。首先,这种系统通过优化资源和能源的使用,有助于降低生产成本。面对日益激烈的竞争和储蓄趋势,这一点尤其正确。其次,混合系统能够以更高的效率生产高质量的产品。通过在一个工艺设备中集成各种功能,金属加工过程变得更加高效和精确。这减少了次品的数量,提高了最终产品的质量。此外,混合金属加工系统具有自主功能,这在需要快速转换和适应各种生产任务的柔性工程生产中尤为重要。因此,混合金属加工系统代表了现代机械工程发展的重要一步,有助于降低成本,提高效率并确保高产品质量。本工作的目的是通过在整体加工条件下使用集中的能量源,提高机械零件表面热硬化的效率,降低能耗。理论与方法。为了实现这一目的,对机械和表面热过程相结合的混合设备可能的结构组成和布局进行了研究。在发展理论和方法时,考虑到金属加工系统的结构综合和组成的主要规定。理论研究是基于系统分析、表面形成的几何理论和金属加工机械设计的应用。实验在现代化多用途加工中心MS 032.06上进行,该加工中心附加能量源为工作频率为440 kHz的微波晶闸管型发生器SHF-10,利用高频电流实现高能加热。使用光学显微镜和扫描显微镜进行结构研究。采用机械法和x射线法测定残余应力,评价了零件表层的应力-应变状态。采用Wolpert Group 402MVD仪对零件表面硬化层的显微硬度进行了测定。结果和讨论。提出了一种用于混合金属加工设备工程前期研究的结构-运动学分析方法。为金属切削机床的现代化制定了方法建议,允许在标准机床系统上使用高频电流(HEH HFC)进行高能加热,并创建具有增强功能的高科技技术设备。实验证实,将所提出的混合机床引入生产,并结合建议指定高频电力单元进行冲孔类零件的整体加工,可以将表面硬化生产率提高36-40倍,并将能源成本降低6倍。
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引用次数: 0
Analysis of mechanical behavior and free vibration characteristics of treated Saccharum munja fiber polymer composite 处理过的糖蜜纤维高分子复合材料力学性能及自由振动特性分析
Q3 Materials Science Pub Date : 2023-09-15 DOI: 10.17212/1994-6309-2023-25.3-117-125
Savendra Singh, Chetan Hirwani
Introduction. With increasing environmental concern nowadays, researchers are studying new alternating materials that can meet the society needs and are extracted from renewable and biodegradable resources. The various natural fibers have been investigated by researchers to replace synthetic ones. The purpose of the work. In present study, treated saccharum munja fibers considered as reinforcement material in Particulate (PC), Short and Random (SRC) and in Unidirectional (UDC) form along with AW106 Resin and HV953. The paper assesses the mechanical properties of Munya fibers (Saccharum munja). Initial six natural frequencies along with corresponding damping factors are measured to analyze the possibility of using a composite material. Research methods. A compression molding machine was used to form laminated composite materials. Surface treatment of fibers removes the dust, lignin and hemicellulose, which improves mechanical and free vibration properties. Results and Discussion. Tensile and flexural test shows the highest value of strength 170 MPa and 143 MPa in case of UDC composite, and the lowest in the case of PC. Addition of munja fiber to epoxy matrix enhances the fiber matrix adhesion bonding. The PC composite shows better value of damping than SRC and UDC composite. The highest natural frequency 43, 233, 298, 849, 918 and 1,440 Hz obtained in case of UDC irrespective of all modes. The results of the free vibration analysis show that Saccharum Munja fiber composite may be used as structural material. Analysis of variance (ANOVA) shows that the experimental results output in case of tensile and flexural teste are significant.
介绍。随着人们对环境问题的日益关注,研究人员正在研究从可再生和可生物降解的资源中提取的满足社会需求的新型交替材料。研究人员已经研究了各种天然纤维来取代合成纤维。工作的目的。本研究将处理后的甘蔗纤维与AW106树脂和HV953作为增强材料,分别以颗粒(PC)、短随机(SRC)和单向(UDC)三种形态进行了研究。本文对芒草纤维的力学性能进行了评价。测量了初始六个固有频率以及相应的阻尼因子,以分析使用复合材料的可能性。研究方法。采用压缩成型机对层压复合材料进行成型。纤维表面处理去除灰尘、木质素和半纤维素,提高机械和自由振动性能。结果和讨论。拉伸和弯曲试验表明,UDC复合材料的强度最高为170 MPa和143 MPa, PC复合材料的强度最低。在环氧树脂基体中加入紫花纤维,增强了纤维基体的粘结性。PC复合材料比SRC和UDC复合材料表现出更好的阻尼值。最高固有频率43,233,298,849,918和1,440赫兹,在UDC的情况下,无论所有模式。自由振动分析结果表明,糖蜜纤维复合材料可作为结构材料。方差分析(ANOVA)表明,拉伸试验和弯曲试验的实验结果具有显著性。
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引用次数: 0
Synthesis of Ti–Fe intermetallic compounds from elemental powders mixtures 从元素粉末混合物中合成Ti-Fe金属间化合物
Q3 Materials Science Pub Date : 2023-09-15 DOI: 10.17212/1994-6309-2023-25.3-126-136
Gennady Pribytkov, Anton Baranovskiy, Victoria Korzhova, Irina Firsina, Vladimir Krivopalov
Introduction. Intermetallic compounds Fe2Ti and FeTi are of practical application as hydrogen accumulators (FeTi) or as magnetic materials (Fe2Ti). Due to the peculiarities of the double equilibrium diagram, the production of these intermetallic compounds by casting is difficult. Therefore, powder metallurgy methods are widely used combined with preliminary mechanical activation of the powder mixtures. The aim of the work is to investigate the possibility of obtaining single-phase compounds from powder mixtures of titanium and iron of target compositions. Research methods. Mechanically activated powder mixtures, products of combustion and subsequent annealing were studied by X-ray phase analysis, optical metallography, and scanning electron microscopy using elemental composition determination by energy-dispersive X-ray spectroscopy. Research methodology. Powder mixtures were mechanically activated for 20 minutes in an Activator 2S planetary ball mill with an intensity of 40 g and a ball/mixture ratio of 20. The mechanically activated mixtures were heated in a sealed reactor in argon media at an average rate of 85 C°/min. Results and discussion. At a temperature of about 500 °C, thermographs of thermocouples placed in a mechanically activated mixture showed a sharp rise (thermal explosion), indicating an exothermic reaction in the mixture. The rise for the 2Fe + Ti composition turned out to be more pronounced than that for the Fe + Ti composition. X-ray diffraction analysis showed that the main reaction product is the Fe2Ti compound for both mixtures. The predominant formation of Fe2Ti is explained by the greater negative enthalpy of Fe2Ti formation of compared to FeTi (−87.45 and −40.58 kcal/mol, respectively). Conclusion. High-temperature annealing of thermal explosion products did not make it possible to obtain single-phase target products. The content of secondary phases and unreacted reagents changed little after annealing. Based on the obtained results, it was concluded that the thermodynamic factor (the enthalpy of formation of the intermetallic compound) is the main one that determines the phase composition of the synthesis products in powder mixtures of titanium and iron.
介绍。金属间化合物Fe2Ti和FeTi作为储氢剂(FeTi)或磁性材料(Fe2Ti)具有实际应用价值。由于双平衡图的特殊性,用铸造法生产这些金属间化合物是困难的。因此,粉末冶金方法与粉末混合物的初步机械活化相结合得到了广泛的应用。这项工作的目的是研究从目标成分的钛和铁的粉末混合物中获得单相化合物的可能性。研究方法。采用x射线相分析、光学金相学和扫描电子显微镜对机械活化的粉末混合物、燃烧产物和随后的退火进行了研究,并用能量色散x射线能谱法测定元素成分。研究方法。粉末混合物在Activator 2S行星球磨机中机械活化20分钟,活化强度为40 g,球料比为20。机械活化的混合物在氩气介质中以85℃/min的平均速率在密封反应器中加热。结果和讨论。在大约500℃的温度下,放置在机械激活混合物中的热电偶的热像图显示出急剧上升(热爆炸),表明混合物中发生了放热反应。结果表明,2Fe + Ti组分的上升比Fe + Ti组分的上升更为明显。x射线衍射分析表明,两种混合物的主要反应产物均为Fe2Ti化合物。与FeTi相比,Fe2Ti的负焓更大(分别为- 87.45 kcal/mol和- 40.58 kcal/mol),从而解释了Fe2Ti的主要形成。结论。热爆炸产物的高温退火不能得到单相目标产物。退火后二次相和未反应试剂的含量变化不大。根据所得结果,认为热力学因素(金属间化合物的生成焓)是决定钛铁混合粉末中合成产物物相组成的主要因素。
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引用次数: 0
Simulation of the rolling process of a laminated composite AMg3/D16/AMg3 层合复合材料AMg3/D16/AMg3轧制过程模拟
Q3 Materials Science Pub Date : 2023-09-15 DOI: 10.17212/1994-6309-2023-25.3-6-18
Denis Salikhyanov, Nikolay Michurov
Introduction. Over the past decades, laminated composites based on aluminum alloys have been increasingly used in the aerospace and automotive industries. Laminated composites are usually produced by accumulative roll bonding, which results in the metallurgical bonding of initially prepared sheets. Hence, the main task of accumulative roll bonding is to obtain a reliable bond between materials. However, at present, the process of joining similar or dissimilar materials by plastic deformation is still a poorly understood phenomenon. In this regard, in recent years, methods of finite element modeling of the processes of joining materials have begun to develop intensively. The purpose of the work is to establish a relationship between stress-strain state parameters and the formation of a stable bond between aluminum alloys of different compositions. To achieve this goal, the following tasks are formulated: 1. Simulation of the laminated composite “AMg3/D16/AMg3” rolling process using data corresponding to physical experiments carried out at the Institute of Engineering Science of the Ural Branch of the Russian Academy of Sciences; 2. Selection and analysis of the most important stress-strain state parameters of the laminated composite “AMg3/D16/AMg3” rolling process. Research methods. Process simulation system Deform-3D was chosen as the main research tool. Results and Discussion. An analysis of the coordinate grid distortion and velocity vectors of material flow of layers revealed that the deformation is distributed inhomogeneously in the cross section after rolling: the outer layers flow more intensively compared to the middle layer. The maximum scatter of strain intensity ei in the cross section, observed at a maximum reduction ratio of 75%, is 12%. This allows one to accept for analytical calculations in the first approximation the assumption of deformation uniformity. A relationship is established between the beginning of the formation of a bond between composite layers and the threshold expansion of the contact surface and normal pressure at the interlayer boundary. In the final part of the study, future directions for improving the approaches of simulation the laminated composites rolling processes are proposed.
介绍。在过去的几十年中,基于铝合金的层压复合材料在航空航天和汽车工业中得到了越来越多的应用。层压复合材料通常是通过累积轧制结合生产的,这导致了初始制备的板材的冶金结合。因此,累积辊粘合的主要任务是在材料之间获得可靠的粘合。然而,目前,通过塑性变形连接相似或不同材料的过程仍然是一个知之甚少的现象。在这方面,近年来,材料连接过程的有限元建模方法开始得到大力发展。本工作的目的是建立应力-应变状态参数与不同成分铝合金之间形成稳定结合之间的关系。为实现这一目标,制定了以下任务:利用俄罗斯科学院乌拉尔分院工程科学研究所的物理实验数据,对层压复合材料“AMg3/D16/AMg3”轧制过程进行了模拟;2. 层压复合材料“AMg3/D16/AMg3”轧制过程中最重要应力-应变状态参数的选择与分析研究方法。选择过程仿真系统Deform-3D作为主要研究工具。结果和讨论。通过对各层物料流动坐标网格畸变和速度矢量的分析,发现轧制后物料在截面上的变形分布不均匀,外层物料的流动强度大于中间层。当最大折减比为75%时,截面应变强度ei的最大散射值为12%。这就允许人们在第一次近似中接受变形均匀性假设的解析计算。建立了复合材料层间键合的开始与接触面的阈值膨胀和层间边界的法向压力之间的关系。最后,对层合复合材料轧制过程模拟方法的改进方向进行了展望。
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引用次数: 0
Economical crankshaft design through topology analysis for C type gap frame power press SNX-320 通过对SNX-320型C型间隙架动力压力机的拓扑分析,设计出经济型曲轴
Q3 Materials Science Pub Date : 2023-09-15 DOI: 10.17212/1994-6309-2023-25.3-50-62
Darshan Tratiya, Manojkumar Sheladiya, Ghanshyam Acharya, Shailee Acharya
Introduction. The presses are powered machines having stationary beds and slides (rams) which have controlled sliding motion towards and away from the beds, guided by the frames. Metal can be worked in power press in a wide verity of ways like punching, shearing, forming, etc. Crankshaft is one of the basic components for power transmission, which transmits rotary motion to sliding motion in the mechanical power press. It is around this element that all stresses and deformations are concentrated. The purpose of the study: rationalization of the design of the crankshaft, taking into account the strength characteristics of the frame, connection screws, tie rods. The methods include two stages of crankshaft design development: 1) modelling in parametric cad software; 2) FE analysis in Ansys-22R1. The existing as well as the improved design of the crankshaft was investigated by the FE method with topology analysis. Topology is part of FE analysis as well as Generative design. Result and Discussion. The design of the crankshaft, including the bearing assembly, depends largely on the maximum pressure that will be generated at the bottom of the stroke, and this is carefully considered when designing other parts of the presses. Based on the results of the topology analysis of the crankshaft structure, it was found that an increase in the strength of this structural element is possible by adding additional material in the area of potential destruction. During the study, it was possible to develop a rational design of the crankshaft with improved mechanical properties compared to the existing one, which will increase the service life of the crankshaft, preventing its failure.
介绍。压力机是有动力的机器,有固定的床和滑块(滑块),滑块在机架的引导下,可以控制进出床的滑动运动。在动力压力机上,金属可以用多种方式加工,如冲孔、剪切、成形等。曲轴是动力传动的基本部件之一,在机械动力压力机中起着将旋转运动转化为滑动运动的作用。所有的应力和变形都集中在这个元素周围。研究目的:合理设计曲轴,兼顾车架、连接螺钉、拉杆的强度特性。该方法包括曲轴设计开发的两个阶段:1)在参数化cad软件中建模;2) Ansys-22R1的有限元分析。采用拓扑分析的有限元方法对曲轴的现有设计和改进设计进行了研究。拓扑学是有限元分析和生成设计的一部分。结果与讨论。曲轴的设计,包括轴承组件,在很大程度上取决于将在冲程底部产生的最大压力,在设计压力机的其他部件时仔细考虑了这一点。根据曲轴结构的拓扑分析结果,发现通过在潜在破坏区域添加附加材料可以提高该结构元件的强度。在研究过程中,有可能开发出一种合理的曲轴设计,与现有曲轴相比,其力学性能得到改善,这将增加曲轴的使用寿命,防止其失效。
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引用次数: 0
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Obrabotka Metallov-Metal Working and Material Science
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