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Electrothermal superhydrophobic epoxy nanocomposite coating for anti-icing/deicing 防冰/除冰用电热超疏水环氧纳米复合涂层
IF 2.3 4区 材料科学 Q2 Chemistry Pub Date : 2023-04-26 DOI: 10.1007/s11998-023-00762-x
Jiayu Fan, Zhu Long, Jin Wu, Peng Gao, Yun Wu, Pengxiang Si, Dan Zhang

Wind power, as a new type of green energy, can be converted into electric energy through wind turbines. However, the extremely cold and harsh weather makes the blade surface easy to freeze, which seriously affects the capacity of wind power. In this study, a bilayer epoxy-based nanocomposite coating that consists of an electrothermal and superhydrophobic layer has been developed for anti-icing/deicing. The electrothermal layer consists of epoxy/silver-coated copper (Ag–Cu) and epoxy/multi-walled carbon nanotubes (MWCNTs) nanocomposites. Epoxy/Ag–Cu coating showed high electrical conductivity, which can quickly generate heat under voltage. Epoxy/MWCNTs coating exhibited high thermal conductivity, which conducts heat to the whole surface. The superhydrophobic layer was fabricated by epoxy/SiO2/hexadecyltrimethoxysilane (HDTMS) nanocomposite, which covered the top of electrothermal layer. The designed bilayer epoxy nanocomposite coating displayed electrical power consumption (0.2 W), super hydrophobicity (static and dynamic water contact angle of 156.3° and 3°, respectively), low ice adhesion (0.01 MPa), long icing time (312 s), short deicing time (41 s), and good wear, acid, alkali, and salt resistance, making it promising for industrial application on wind turbine blades.

风能作为一种新型的绿色能源,可以通过风力发电机将其转化为电能。然而,极端寒冷恶劣的天气使叶片表面容易结冰,严重影响风电容量。在这项研究中,开发了一种由电热层和超疏水层组成的双层环氧基纳米复合涂层,用于防冰/除冰。电热层由环氧/镀银铜(Ag-Cu)和环氧/多壁碳纳米管(MWCNTs)纳米复合材料组成。环氧/ Ag-Cu涂层具有高导电性,在电压作用下能快速发热。环氧/MWCNTs涂层表现出高导热性,将热量传导到整个表面。采用环氧树脂/SiO2/十六烷基三甲氧基硅烷(HDTMS)纳米复合材料制备了超疏水层,覆盖在电热层的顶部。所设计的双层环氧纳米复合涂层具有电耗(0.2 W)、超疏水性(静、动水接触角分别为156.3°和3°)、低冰附着(0.01 MPa)、长结冰时间(312 s)、短除冰时间(41 s)、良好的耐磨性、耐酸、耐碱、耐盐性等特点,在风力发电机叶片上具有良好的工业应用前景。
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引用次数: 1
Optical properties of polymer-based coatings containing metallic particles: effect of particle shape and binder 含金属颗粒聚合物基涂层的光学性能:颗粒形状和粘结剂的影响
IF 2.3 4区 材料科学 Q2 Chemistry Pub Date : 2023-04-24 DOI: 10.1007/s11998-023-00766-7
Kuilong Song, Ming Xie, Qing Ai

Polymer-based coatings containing metallic microparticles are a kind of functional material with effective spectral selectivity. The spectral radiative transfer model of polymer-based coatings is built based on geometrical optics, and the spectral radiative characteristics of the coatings were investigated by Monte Carlo ray-tracing method. The coatings consist of aluminum particles with different shapes as fillers and four kinds of polymer resins as binders, respectively. After verifying the reliability of the method, the effect of particle shape and binder on the infrared emission properties in the range of 8–14 μm is systematically investigated. The results demonstrate that adding flake particles into the coating can obtain lowest infrared emissivity, which is at most 86.79% lower than the coating containing spherical particles when the volume fraction is 30%. The mean emissivity of Al/acrylic resin, Al/polyetherimide (PEI), Al/polymethyl methacrylate, and Al/polystyrene (PS) composite coatings is 0.46, 0.48, 0.41, and 0.22, respectively. Al/PS composite coating has the minimum mean infrared emissivity among these four kinds of polymer-based coatings, which is 54.2% lower than Al/PEI composite coating. The method proposed in this work will provide theoretical guidance for experimental research.

含有金属微粒的聚合物基涂层是一种具有有效光谱选择性的功能材料。基于几何光学建立了聚合物基涂层的光谱辐射传递模型,采用蒙特卡罗射线示踪方法研究了涂层的光谱辐射特性。该涂层分别由不同形状的铝颗粒作为填料和四种聚合物树脂作为粘合剂组成。在验证了该方法的可靠性后,系统地研究了颗粒形状和粘结剂对8 ~ 14 μm范围内红外发射性能的影响。结果表明:当涂层体积分数为30%时,片状颗粒的红外发射率比球形颗粒的红外发射率低86.79%;Al/丙烯酸树脂、Al/聚醚酰亚胺(PEI)、Al/聚甲基丙烯酸甲酯和Al/聚苯乙烯(PS)复合涂层的平均发射率分别为0.46、0.48、0.41和0.22。在四种聚合物基涂料中,Al/PS复合涂料的平均红外发射率最小,比Al/PEI复合涂料低54.2%。本文提出的方法将为实验研究提供理论指导。
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引用次数: 0
Traditional science in pigments and recipe of painting woodcarving in medieval Assam, India 中世纪印度阿萨姆邦的传统颜料科学和木雕绘画配方
IF 2.3 4区 材料科学 Q2 Chemistry Pub Date : 2023-04-24 DOI: 10.1007/s11998-023-00765-8
Asadulla A. Ali, Robin K. Dutta

A painting tradition of medieval Assam, popularly known as Hengul-Hāitāl, has been studied with an aim of restoring and conserving centuries-old woodcarvings and Sāncipat manuscripts for preserving in ordinary open conditions at villages and Vaishnavite monasteries. The pigments, their combinations for producing various shades and the resulting colors have been characterized using various physicochemical techniques. The study unravels some interesting traditional science, such as, using red Hengul (cinnabar), yellow Hāitāl (yellow orpiment) and blue Nīl (Indigo or Prussian blue) as primary colors to produce any desired shade, inclusion of either or both of Hengul and Hāitāl in every shade to repel fungi and insects, applying Kharimāti (a clay) as a wood-primer for better painting effects, choosing of Bael gum as a robust non-staining natural adhesive and finally varnishing with Lā (a natural lac) to protect the pigments from natural erosion and protect the woodcarving from humidity and contaminating hands touching them. The findings provide clues to develop an appropriate method of restoration of partially worn-out woodcarvings for preserving them in ordinary open conditions, based on the traditional method of preparation.

中世纪阿萨姆邦的绘画传统,通常被称为Hengul-Hāitāl,已经被研究,目的是恢复和保存数百年的木雕和Sāncipat手稿,以便在村庄和毗什纳维修道院的普通开放条件下保存。颜料,它们的组合产生不同的色调和所产生的颜色已经用各种物理化学技术进行了表征。这项研究揭示了一些有趣的传统科学,例如,使用红色的Hengul(朱砂),黄色的Hāitāl(黄色的香料)和蓝色的n l(靛蓝或普鲁士蓝)作为原色来产生任何想要的色调,在每种色调中加入Hengul和Hāitāl中的一种或两种都可以击退真菌和昆虫,使用Kharimāti(粘土)作为木材底漆以获得更好的绘画效果。选择Bael胶作为一种坚固的不染色的天然粘合剂,最后用lha(一种天然紫胶)进行清漆,以保护颜料免受自然侵蚀,保护木雕免受潮湿和接触它们的手的污染。这一发现为开发一种适当的修复方法提供了线索,该方法可以在传统的准备方法的基础上,将部分磨损的木雕保存在普通的开放条件下。
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引用次数: 1
Preparation and characterization of carbon black coated membranes for the treatment of saline water by membrane distillation 膜蒸馏处理盐水用炭黑包覆膜的制备与表征
IF 2.3 4区 材料科学 Q2 Chemistry Pub Date : 2023-04-14 DOI: 10.1007/s11998-023-00759-6
Mohamed E. A. Ali, Shimaa Elbakry, Moustafa Aboelfadl, Hosam Shawky, Qilin Li, Francois Perreault

Membrane distillation (MD) is a promising approach to address water scarcity due to its capacity to achieve high water recovery in desalination. However, high energy consumption and decline in permeate flux are key issues of MD desalination. Nanophotonic materials like carbon black (CB) have been used to improve MD performance and reduce energy consumption in the presence of sunlight. In this article, we investigated different coating procedures for the formation of a uniform layer of CB particles on polytetrafluoroethylene (PTFE) and polyvinylidene fluoride membranes. The coated membranes were manufactured and characterized using Fourier-transform infrared spectroscopy and scanning electron microscopy. Contact angle measurements demonstrated an increase in hydrophilicity after CB was added. Both types of membranes exhibited an increase in permeate flux and salt rejection with the addition of CB, with the PTFE membrane coated with 0.5% of CB having the highest water flux, reaching 14.6 L/m2 h (LMH) compared to a commercial control having a flux of 8.0 LMH. The effects of different parameters on the performance of the hydrophilic CB-coated PTFE membrane were examined. The results demonstrated that the CB coating developed can be advantageous to improve the performance of MD membranes.

膜蒸馏(MD)是一种很有前途的解决水资源短缺的方法,因为它能够在海水淡化中实现高水回收率。然而,高能耗和渗透通量下降是MD脱盐的关键问题。像炭黑(CB)这样的纳米光子材料已经被用来提高光电二极管的性能,并在阳光下降低能耗。在本文中,我们研究了在聚四氟乙烯(PTFE)和聚偏氟乙烯膜上形成均匀的CB颗粒层的不同涂覆工艺。制备了涂层膜,并用傅里叶变换红外光谱和扫描电镜对其进行了表征。接触角测量表明,加入丁基苯后,亲水性有所提高。两种类型的膜都表现出随着CB的添加而增加的渗透通量和盐的截留,其中涂有0.5% CB的PTFE膜的水通量最高,达到14.6 L/m2 h (LMH),而商业控制的通量为8.0 LMH。考察了不同工艺参数对亲水cb包覆PTFE膜性能的影响。结果表明,所开发的CB涂层有利于提高MD膜的性能。
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引用次数: 0
Comparison of bio-based epoxide-diamine coatings prepared with acyclic and cyclic aliphatic diamines 无环和环脂肪二胺制备生物基环氧二胺涂料的比较
IF 2.3 4区 材料科学 Q2 Chemistry Pub Date : 2023-03-27 DOI: 10.1007/s11998-022-00756-1
Ilknur Babahan-Bircan, Jomin Thomas, Mark D. Soucek

As replacements for bisphenol-A, new bio-based and reactive epoxy-amine coatings have been investigated in this study. Bio-based precursor, epoxy-functionalized tung oil (ETO) was synthesized using glycidyl methacrylate (GMA) and tung oil via a Diels–Alder reaction according to our previous work. The new ETO-diamine-cured systems were prepared with the equivalent molar ratio at room temperature. ETO was cured with acyclic aliphatic (Jeffamine D400) and cyclic aliphatic (Epicure 3300) amines, at four temperatures ranging from 25 to 150°C. The coatings were then compared in terms of their thermal and mechanical properties. The cured coatings were analyzed by IR, thermogravimetric analysis (TGA), and gel content tests. TGA analysis showed that the epoxide-diamine polymers demonstrated thermal stability up to 170°C. The mechanical properties of the films were investigated by pendulum hardness, pencil hardness, cross-hatch adhesion, pull-off adhesion, impact resistance, reverse resistance, and chemical resistance testing. While all the cured systems exhibited good pencil hardness, cross-hatch adhesion, impact resistance, and reverse resistance properties, the epoxide-acyclic diamine system demonstrated greater pendulum hardness and notable pull-off adhesion at 150°C. The research demonstrates the potential for greener and more reactive tung oil-based epoxide coatings with enhanced properties.

作为双酚a的替代品,研究了新的生物基活性环氧胺涂层。在前人的基础上,以甲基丙烯酸缩水甘油酯(GMA)和桐油为原料,通过Diels-Alder反应合成了生物基环氧功能化桐油(ETO)。在室温条件下,以当量摩尔比制备了新的eto -二胺固化体系。ETO用无环脂肪族胺(Jeffamine D400)和环脂肪族胺(Epicure 3300)在25 ~ 150℃四种温度下固化。然后比较了涂层的热性能和机械性能。通过红外光谱(IR)、热重分析(TGA)和凝胶含量测试对固化后的涂层进行了分析。TGA分析表明,环氧二胺聚合物的热稳定性可达170℃。通过摆硬度、铅笔硬度、十字口附着力、拉脱附着力、抗冲击性、抗反转性和耐化学性测试,考察了薄膜的力学性能。所有固化体系均表现出良好的铅笔硬度、交叉口附着力、抗冲击性和抗反向性能,而环氧化合物-无环二胺体系在150℃时表现出更高的摆硬度和显著的拉脱附着力。该研究表明,具有增强性能的桐油基环氧化物涂料具有更环保、更活泼的潜力。
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引用次数: 1
Effect of polytetrafluoroethylene (PTFE) emulsion impregnation coating on filtration performance and thermal property of polyphenylene sulfide (PPS) needle felt 聚四氟乙烯(PTFE)乳液浸渍涂层对聚苯硫醚(PPS)针刺毡过滤性能和热性能的影响
IF 2.3 4区 材料科学 Q2 Chemistry Pub Date : 2023-03-22 DOI: 10.1007/s11998-022-00755-2
Chao Lv, Ruiqing Shen, Yang Yang, Rui Shu, Guodong Li, Jingxian Liu

Polytetrafluoroethylene (PTFE) emulsion is widely used as a coating material in the impregnation process for preparing polyphenylene sulfide (PPS) needle felts due to its excellent chemical stability and good mechanical properties. However, the effect of emulsion impregnation coating on the filtration performance of needle felts is still under debate. Moreover, in industrial applications with high temperatures, the service life of needle felts is directly affected by their thermal stability, but the pyrolysis and kinetic properties of PPS needle felt after PTFE emulsion impregnation post-processing have rarely been quantitatively investigated. In this study, the PPS fiber/PTFE emulsion (PPS/PTFE) composite needle felt was fabricated by a direct impregnation process. The pressure drop characteristic and mechanical collection efficiency of PPS needle felt and PPS/PTFE composite needle felt were comprehensively evaluated. It was found that the PTFE emulsion impregnation coating not only increases the pressure drop, but also decreases the collection efficiency. More specifically, for particles having a size below 2.5 μm, the decrement of collection efficiency further increases with the decrease of particle size, but the mechanical collection efficiency of PPS/PTFE composite needle felt for particles having larger size is almost the same as that of PPS needle felt. Three emulsion impregnation coating distribution models were inferred to systematically explain this experimental phenomenon. Additionally, the thermal degradation process of PPS needle felt and PPS/PTFE composite needle felt was analyzed, and several typical pyrolysis kinetic parameters were also determined theoretically. It was confirmed that the PTFE emulsion impregnation coatings can enhance the thermal stability of PPS needle felts. This work provides new insight into the rational application of the direct impregnation process as well as emulsion impregnation coating in the industrial filtration field.

聚四氟乙烯(PTFE)乳液由于其优异的化学稳定性和良好的力学性能,在聚苯硫醚(PPS)针毡浸渍工艺中被广泛用作涂层材料。然而,乳化浸渍涂层对针刺毡过滤性能的影响仍存在争议。此外,在高温工业应用中,针刺毡的热稳定性直接影响其使用寿命,但聚四氟乙烯乳液浸渍后处理后PPS针刺毡的热解和动力学性能的定量研究很少。采用直接浸渍法制备了PPS纤维/聚四氟乙烯乳液(PPS/PTFE)复合针刺毡。综合评价了PPS针刺毡和PPS/PTFE复合针刺毡的压降特性和机械收集效率。结果表明,PTFE乳液浸渍涂层不仅增大了压降,而且降低了收集效率。更具体地说,对于粒径小于2.5 μm的颗粒,随着粒径的减小,收集效率的衰减量进一步增大,但PPS/PTFE复合针刺毡对粒径较大的颗粒的机械收集效率与PPS针刺毡基本相同。推导了三种乳液浸渍涂层分布模型,系统地解释了这一实验现象。此外,还分析了PPS针刺毡和PPS/PTFE复合针刺毡的热降解过程,并从理论上确定了几种典型的热解动力学参数。结果表明,聚四氟乙烯乳液浸渍涂层能提高PPS针毡的热稳定性。本研究为直接浸渍工艺及乳液浸渍涂料在工业过滤领域的合理应用提供了新的思路。
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引用次数: 0
Investigation of EMI and UV–IR shielding properties of wool and cotton/elastane nanocomposite fabrics 羊毛和棉/弹性纳米复合织物的电磁干扰和紫外-红外屏蔽性能研究
IF 2.3 4区 材料科学 Q2 Chemistry Pub Date : 2023-03-20 DOI: 10.1007/s11998-022-00753-4
İlhami İlhan, Mehmet Esen, Muharrem Karaaslan, Banu Yılmaz Akyürek

In this study, the electromagnetic interference (EMI) and ultraviolet–infrared (UV–IR) shielding behavior of wool (WO) and cotton/elastane (CO/EL) nanocomposite fabrics have been investigated. The study aims to investigate the EMI and UV–IR shielding performance of the CO/EL and wool-based fabrics coated with carbon (C), graphite (Gr), and indium (In) nanocomposite layers. To produce nanocomposite fabric samples, these three materials were used in different compositions and the coating processes were carried out by electron cyclotron resonance (ECR) and thermal evaporation methods. Subsequently, the EMI and UV–IR measurements were performed for the coated fabric samples, and the results have been analyzed. In this study, it has been proven for the first time that the ECR coating method can be used for coating fabrics as a textile material. Finally, it is found that the C+Gr(grid filled)+In wool sample and the carbon-coated CO/EL sample have widely exhibited a significant positive effect on increasing the EMI shielding performance in the range of 18–43 and 12–18 GHz frequencies, respectively. In addition, the results show that the C+Gr(grid)+C-coated CO/EL fabric has significant potential to increase the UV–IR shielding performance.

本文研究了羊毛(WO)和棉/弹性(CO/EL)纳米复合织物的电磁干扰(EMI)和紫外-红外(UV-IR)屏蔽性能。该研究旨在研究涂覆碳(C)、石墨(Gr)和铟(In)纳米复合层的CO/EL和羊毛基织物的EMI和UV-IR屏蔽性能。采用电子回旋共振(ECR)和热蒸发法对三种材料进行涂层处理,制备纳米复合织物样品。随后,对涂层织物样品进行了EMI和UV-IR测量,并对结果进行了分析。在本研究中,首次证明了ECR涂层方法可以作为纺织材料用于涂层织物。最后,发现C+Gr(栅格填充)+In羊毛样品和碳包覆CO/EL样品分别在18-43 GHz和12-18 GHz频率范围内对提高电磁干扰屏蔽性能有显著的正向影响。此外,结果表明,C+Gr(栅格)+C涂层CO/EL织物具有显著的提高UV-IR屏蔽性能的潜力。
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引用次数: 1
Preparation and characterization of organic–inorganic hybrid coatings for improving the insulation properties of electrical steel 提高电工钢绝缘性能的有机-无机杂化涂层的制备与表征
IF 2.3 4区 材料科学 Q2 Chemistry Pub Date : 2023-03-15 DOI: 10.1007/s11998-022-00751-6
Bong-Gu Kim, Hyun-Hee Choi, Hye-Yeong Park, Min Serk Kwon, Yun-Ki Byeun, Sung Kang, Yeon-Gil Jung, Jung-Hun Son, SeungCheol Yang

Phosphate has been used as a coating agent in various fields, such as electrical steel (ES), because of its excellent electrical insulation and corrosion resistance. Although the insulating properties of a phosphate coating can significantly improve the iron loss of the ES sheet, a new coating material to enhance the performance of the ES sheet further should be developed. In this study, we synthesized organic–inorganic hybrid coating agents with superior insulation compared to that of the conventional phosphate coating agent. Inorganic particles with excellent insulating properties (SiO2, TiO2, and Cr2O3) and silane coupling agents were used as starting materials. The good surface modification of inorganic particles by silane coupling agents with appropriate solvent content in the coating agent led to good dispersion stability of the coating agent. Homogeneous dispersion of the coating agent was attributed to the good surface roughness of the hybrid materials coated on the ES. Finally, when the hybrid coating agent with optimized composition was applied to the ES, the insulation property of the hybrid coating (< 100 mA) was superior compared to that of the conventional phosphate coating (~ 200 mA), and corrosion resistance was also excellent.

磷酸盐由于其优异的电绝缘性和耐腐蚀性,已被用作各种领域的涂覆剂,如电工钢(ES)。尽管磷酸盐涂层的绝缘性能可以显著改善ES板的铁损,但仍需开发新的涂层材料来进一步提高ES板的性能。在本研究中,我们合成了有机-无机杂化包衣剂,与传统的磷酸盐包衣剂相比,它具有更好的绝缘性。以绝缘性能优良的无机颗粒(SiO2、TiO2和Cr2O3)和硅烷偶联剂为原料。涂覆剂中适当溶剂含量的硅烷偶联剂对无机颗粒进行了良好的表面改性,使涂覆剂具有良好的分散稳定性。涂覆剂分散均匀是由于涂覆在ES上的杂化材料具有良好的表面粗糙度。最后,将优化组合后的杂化涂覆剂应用于ES时,其绝缘性能(< 100 mA)优于常规磷酸盐涂层(~ 200 mA),耐腐蚀性能也很好。
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引用次数: 0
Robotic painting: mimicking human applicators 机器人绘画:模仿人类涂抹器
IF 2.3 4区 材料科学 Q2 Chemistry Pub Date : 2023-03-13 DOI: 10.1007/s11998-022-00750-7
Karan Bansal, Yayun Du, Eric Palan, Mohiuddin Quadir, Mohammad Khalid Jawed

Robotically assisted painting is widely used for spray and dip applications. However, use of robots for coating substrates using a roller applicator has not been systematically investigated. We showed for the first time, a generic robot arm-supported approach to painting engineering substrates using a roller with a constant force at an accurate joint step, while retaining compliance and thus safety. We optimized the robot design such that it is able to coat the substrate using a roller with a performance equivalent to that of a human applicator. To achieve this, we optimized the force, frequency of adjustment, and position control parameters of robotic design. A framework for autonomous coating is available at https://github.com/duyayun/Vision-and-force-control-automonous-painting-with-rollers; users are only required to provide the boundary coordinates of surfaces to be coated. We found that robotically- and human-painted panels showed similar trends in dry film thickness, coating hardness, flexibility, impact resistance, and microscopic properties. Color profile analysis of the coated panels showed non-significant difference in color scheme and is acceptable for architectural paints. Overall, this work shows the potential of robot-assisted coating strategy using roller applicator. This could be a viable option for hazardous area coating, high-altitude architectural paints, germs sanitization, and accelerated household applications.

机器人辅助绘画广泛应用于喷涂和浸渍应用。然而,使用机器人涂层基材使用滚轮涂抹器还没有系统的研究。我们首次展示了一种通用的机械臂支撑方法,使用具有恒定力的滚轮在精确的关节步骤上喷涂工程基材,同时保持顺应性和安全性。我们优化了机器人的设计,使其能够使用与人类涂布器性能相当的滚筒涂覆基材。为了实现这一目标,我们优化了机器人设计的力、调整频率和位置控制参数。自动涂层的框架可在https://github.com/duyayun/Vision-and-force-control-automonous-painting-with-rollers上获得;用户只需要提供要涂覆的表面的边界坐标。我们发现机器人和人类绘制的面板在干膜厚度,涂层硬度,柔韧性,抗冲击性和微观性能方面表现出相似的趋势。涂覆板的色彩分析显示,配色方案无显著差异,可用于建筑涂料。总的来说,这项工作显示了使用滚轮涂抹器的机器人辅助涂层策略的潜力。这可能是危险区域涂料,高海拔建筑涂料,细菌消毒和加速家庭应用的可行选择。
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引用次数: 1
Phosphaphenanthrene-modified zirconium phosphate nanosheets for improving fire resistance, smoke suppression and water tolerance of intumescent coatings 磷菲改性磷酸锆纳米片提高膨胀涂层的防火、抑烟和耐水性
IF 2.3 4区 材料科学 Q2 Chemistry Pub Date : 2023-03-13 DOI: 10.1007/s11998-022-00749-0
Cheng Wang, Siqi Huo, Guofeng Ye, Zhengping Fang, Hao Wang, Zhitian Liu

Developing intumescent fire-retardant coatings (IFRCs) combining superior smoke suppression and water resistance is crucial for their industrial applications. Herein, novel 9,10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide (DOPO)-decorated zirconium phosphate (ZrP-D) nanosheets are synthesized and employed in the IFRCs. The ZrP-D nanosheets feature multifunctionality, which simultaneously improve the fire resistance, smoke suppression, thermal stability and water tolerance of IFRCs. Notably, introducing 3wt% ZrP-D decreases the backside temperature of IFRC from 293.9 to 166.3°C by ~ 43.4% in fire resistance test, followed by 47.9%, 33.5% and 89.4% reductions in peak heat release rate, total heat release and total smoke release. Moreover, this IFRC exhibits improved thermal stability and water tolerance, of which char yield and water contact angle reach up to 64% and 82.7°, respectively. When exposed to high-temperature flame, the ZrP-D nanoplatelets mainly function in condensed phase, which significantly increases the expansion and compactness of residual char due to the barrier and catalytic charring effects, thus suppressing the heat release and smoke diffusion. This work provides a rational design for creating intumescent fire-retardant coatings combining smoke suppression and water resistance, thus possessing broad prospects in industry.

Graphical Abstract

开发具有优异抑烟性和耐水性的膨胀型阻燃涂料对其工业应用至关重要。本文合成了新型的9,10-二氢-9-氧-10-磷酸菲-10-氧化物(DOPO)修饰的磷酸锆(ZrP-D)纳米片,并将其应用于ifrc中。ZrP-D纳米片具有多种功能,可同时提高ifrc的耐火性、抑烟性、热稳定性和耐水性。值得注意的是,在防火测试中,引入3wt% ZrP-D后,IFRC的背面温度从293.9℃降至166.3℃,降低了43.4%,其次是峰值放热率、总放热率和总放烟率分别降低了47.9%、33.5%和89.4%。此外,该材料具有较好的热稳定性和耐水性,炭产率和水接触角分别达到64%和82.7°。ZrP-D纳米薄片在高温火焰下主要以缩合相作用,由于屏障和催化炭化作用,显著提高了残余炭的膨胀和致密性,从而抑制了热量的释放和烟雾的扩散。本工作为研制抑烟阻水型膨胀型阻燃涂料提供了合理的设计思路,具有广阔的工业应用前景。图形抽象
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引用次数: 1
期刊
Journal of Coatings Technology and Research
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