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Erratum: Post-IR IRSL dating of K-feldspar from last interglacial marine terrace deposits on the kamikita coastal plain, northeastern Japan 勘误:日本东北部神喜多海岸平原末次间冰期海相阶地沉积物中钾长石的后ir IRSL定年
IF 1.2 4区 地球科学 Q3 Earth and Planetary Sciences Pub Date : 2018-01-01 DOI: 10.1515/geochr-2015-0100
Kazumi Ito, T. Tamura, S. Tsukamoto
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引用次数: 0
Koonalda Cave, Nullarbor Plain, South Australia – issues in optical and radiometric dating of deep karst caves 南澳大利亚纳拉伯平原的库纳尔达洞——深溶洞的光学和辐射测年问题
IF 1.2 4区 地球科学 Q3 Earth and Planetary Sciences Pub Date : 2017-12-29 DOI: 10.1515/geochr-2015-0081
K. Walshe
Abstract Koonalda Cave is located on the Nullarbor Plain of South Australia and is one of 17 deep karst caves in this region. In 2014, the cave was listed as a National Heritage Place in recognition of its significant archaeological and cultural heritage features. It In order to understand the antiquity of and complex human activity in this site a range of dating methods have been applied including typologic, radiometric and luminescence. Each has been challenged and the chronology of this highly significant site has relied on contextual data from other sites. This paper presents an overview of the archaeology recorded at Koonalda Cave, the issues in dating sites in deep karst systems and emphasises the urgent need to resolve these issues so that a reliable chronology can be presented for Koonalda Cave.
库纳尔达洞穴位于南澳大利亚的纳拉伯平原,是该地区17个深溶洞之一。2014年,该洞穴因其重要的考古和文化遗产特征而被列为国家遗产。为了了解这个遗址的古代和复杂的人类活动,人们采用了一系列的测年方法,包括类型学、放射学和发光学。每一个都受到了挑战,这个高度重要的遗址的年表依赖于其他遗址的背景数据。本文综述了库纳尔达洞的考古记录和深部岩溶系统测年存在的问题,强调迫切需要解决这些问题,以便为库纳尔达洞提供可靠的年代学。
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引用次数: 2
Luminescence dating of Holocene beach-ridge sands on the Yumigahama Peninsula, western Japan 日本西部羽滨半岛全新世海滩脊砂的发光年代测定
IF 1.2 4区 地球科学 Q3 Earth and Planetary Sciences Pub Date : 2017-12-29 DOI: 10.1515/geochr-2015-0076
T. Tamura, Kazumi Ito, Takahiko Inoue, T. Sakai
Abstract We applied infrared stimulated luminescence (IRSL50) and post-infrared (post-IR) IRSL150 dating to K-feldspar sand obtained from Holocene beach ridges on the Yumigahama Peninsula, Japan, to investigate the rate of progradation of the beach, which has been affected by 17–18th century iron mining in a local river catchment. All samples showed higher equivalent doses for the post-IR IRSL signal. Fading tests indicated that IRSL yielded relatively high g-values (11–13%/decade), while post-IR IRSL yielded negative g-values (–5 to –8%/decade). The corrected IRSL age of the oldest sample, 8.1 ± 1.3 ka, was slightly overestimated with respect to its expected age of 5–6.7 ka. The corrected age is highly dependent on the g-value, which if slightly inaccurate would have caused the overestimate. The uncorrected post-IR IRSL ages were underestimated, and we consider that the post-IR IRSL signal faded. However, given the negative g-values, application of an appropriate fading correction was not feasible. The corrected IRSL ages of the younger samples, coupled with an assumption of residual dose, roughly agreed with the historical shoreline changes, indicating that the rate of shoreline progradation increased markedly during the recent period of mining-related enhanced sediment discharge.
摘要我们将红外激发发光(IRSL50)和后红外(post-IR)IRSL150测年法应用于从日本Yumighama半岛全新世海滩山脊获得的钾长石砂,以研究当地河流流域17-18世纪铁矿开采对海滩进积速率的影响。所有样品都显示出较高的IR后IRSL信号等效剂量。衰落测试表明,IRSL产生相对较高的g值(11-13%/10年),而IR后的IRSL产生负g值(-5%--8%/年)。最老样本的校正IRSL年龄为8.1±1.3 ka,相对于其预期年龄(5–6.7 ka)略有高估。校正后的年龄高度依赖于g值,如果稍有不准确,就会导致高估。未校正的IR后IRSL年龄被低估了,我们认为IR后的IRSL信号减弱了。然而,考虑到负g值,应用适当的衰落校正是不可行的。较年轻样本的校正IRSL年龄,加上残留剂量的假设,与历史海岸线变化大致一致,表明在最近与采矿相关的沉积物流量增加期间,海岸线前积速率显著增加。
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引用次数: 4
Post-IR IRSL dating of K-feldspar from last interglacial marine terrace deposits on the Kamikita coastal plain, northeastern Japan 日本东北部神喜多海岸平原末次间冰期海相阶地沉积物中钾长石的ir - IRSL定年
IF 1.2 4区 地球科学 Q3 Earth and Planetary Sciences Pub Date : 2017-12-29 DOI: 10.1515/geochr-2015-0077
Kazumi Ito, T. Tamura, S. Tsukamoto
Abstract To establish a suitable luminescence dating protocol for marine terrace deposits in Japan, we tested the applicability of K-feldspar post-infrared (IR) infrared stimulated luminescence (IRSL) (pIRIR) dating using a marine isotope stage (MIS) 5e terrace deposit from the Kamikita coastal plain (NE Japan), where independent age control from a tephra is available. One of the most commonly used pIRIR signals, measured at 290°C with the first IR stimulation temperature at 50°C (pIRIR50/290), faded with a mean g2days value of 1.94 ± 0.19%/decade. In contrast, the pIRIR signal with a higher first IR stimulation temperature of 200°C (pIRIR200/290) had a much lower fading rate (g2days = 0.16 ± 0.49%/decade). The average fading-uncorrected and -corrected pIRIR200/290 ages of MIS 5e subtidal sediments obtained from two sampling sites were 126 ± 3 ka and 132 ± 2 ka, which is in good agreement with the independent age control. We conclude that is it is now possible to use pIRIR protocol to estimate the ages of not only marine terraces formed during MIS 5 substages (5a, 5c) but also of older marine terraces, for which age evidence is limited.
摘要为了建立适合日本海相阶地沉积的发光测年方案,我们利用日本东北部神喜多海岸平原5e阶地沉积的海洋同位素阶段(MIS)测试了k -长石后红外(IR)红外激发发光(IRSL) (pIRIR)测年的适用性,该阶段具有独立的tephra年龄控制。最常用的pIRIR信号之一,在290°C下测量,第一次红外刺激温度为50°C (pIRIR50/290),其平均g2days值为1.94±0.19%/decade。相比之下,首次红外刺激温度为200℃(pIRIR200/290)的pIRIR信号的衰落率要低得多(g2days = 0.16±0.49%/decade)。两个采样点获得的MIS 5e潮下沉积物未校正和校正后的平均pIRIR200/290年龄分别为126±3 ka和132±2 ka,与独立年龄控制相吻合。我们的结论是,现在不仅可以使用pIRIR协议来估计MIS 5亚阶段(5a, 5c)形成的海洋阶地的年龄,还可以估计年龄证据有限的更老的海洋阶地的年龄。
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引用次数: 12
Application of different protocols and age-models in OSL dating of earthen mortars 不同协议和年龄模型在土砂浆OSL定年中的应用
IF 1.2 4区 地球科学 Q3 Earth and Planetary Sciences Pub Date : 2017-12-29 DOI: 10.1515/geochr-2015-0072
L. Panzeri, M. Cantù, M. Martini, E. Sibilia
Abstract In this study, OSL dating was applied to earthen mortars, consisting in a quartz-rich aggregate dispersed in silty-clayey matrix. The samples were taken from two independently dated structures in Cremona, Northern Italy (Palazzo Raimondi, 1495–1499 AD and Palazzo Soldi, 1770–1790 AD). The evaluation of the equivalent dose (De) was attempted with both the multigrain and the single grain protocols using the 150–250 μm quartz fraction. The reliability and effectiveness of the various statistical methods in identifying the well-bleached samples were tested. The use of the multi-grain technique gave unreliable results, due to the high amount of poorly bleached grains. With the single-grain technique, more promising results were obtained: in particular, the un-log MAM3 and IEU models allowed an accurate evaluation of the mortar expected age in most cases, even if the precision is still relatively low.
摘要在本研究中,OSL测年被应用于土砂浆,该砂浆由分散在粉质粘土基质中的富含石英的骨料组成。样本取自意大利北部克雷莫纳的两个独立年代的建筑(雷蒙迪宫,公元1495–1499年和索尔迪宫,1770–1790年)。使用150–250μm石英粒级,尝试使用多颗粒和单颗粒方案评估等效剂量(De)。测试了各种统计方法在识别良好漂白样品方面的可靠性和有效性。由于大量漂白不良的颗粒,多颗粒技术的使用给出了不可靠的结果。使用单颗粒技术,获得了更有希望的结果:特别是,在大多数情况下,即使精度仍然相对较低,非对数MAM3和IEU模型也可以准确评估砂浆的预期使用寿命。
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引用次数: 9
Variation of OSL residual doses in terms of coarse and fine grain modern sediments along the Hungarian section of the Danube 多瑙河匈牙利段粗粒和细粒现代沉积物中OSL残留剂量的变化
IF 1.2 4区 地球科学 Q3 Earth and Planetary Sciences Pub Date : 2017-12-29 DOI: 10.1515/geochr-2015-0079
O. Tóth, G. Sipos, T. Kiss, Tamás Bartyik
Abstract Reliable OSL dating of fluvial sediments requires an assessment of incomplete bleaching and consequent residual dose in samples. A well-established way of this is determining the equivalent dose of modern samples from similar sedimentary environments as in the case of palaeo-samples. Meanwhile, relatively low, or close to zero doses are also greatly affected by the thermal transfer phenomenon, which can also lead to a palaeodose overestimation. The present study attempts to quantify both factors in coarse and fine grain modern sediments along the Hungarian section of the Danube River, with the aim of determining their significance when dating both young and palaeo-sediments. Investigations were performed at 30 sites along a 417 km long river section with varying morphological and erosive character. The studied samples were deposited during the record flood of 2013, mobilising and relocating a vast amount of sediment in the system. Tests have shown that thermal transfer can be minimized successfully by choosing preheat temperatures below 200°C, however it remains a significant factor when dating young or modern sediments. Based on equivalent dose measurements, coarse grain samples proved to be relatively well bleached, and residual doses showed only a minor spatial variation. Although in terms of fine grain samples residual doses were obviously much higher, results can enhance the reliability of dates retrieved later from fine grain palaeo-samples. In the meantime, the higher spatial variability of fine grain residual doses may also allow the assessment of the erosive character of different river reaches.
摘要河流沉积物的可靠OSL年代测定需要评估样品中的不完全漂白和由此产生的残留剂量。一种公认的方法是确定来自类似沉积环境的现代样品的等效剂量,就像古样品一样。同时,相对较低或接近零的剂量也受到热传递现象的极大影响,这也可能导致古剂量的高估。本研究试图量化多瑙河匈牙利段粗粒和细粒现代沉积物中的这两个因素,目的是确定它们在确定年轻沉积物和古沉积物年代时的意义。在417公里长的河段上的30个地点进行了调查,这些河段具有不同的形态和侵蚀特征。所研究的样本是在2013年创纪录的洪水期间沉积的,调动和重新定位了系统中的大量沉积物。测试表明,通过选择低于200°C的预热温度,可以成功地将热传递降至最低,但在确定年轻或现代沉积物的年代时,这仍然是一个重要因素。根据等效剂量测量,粗粒样品被证明是相对良好的漂白,残留剂量仅显示出微小的空间变化。尽管就细粒样品而言,残留剂量明显高得多,但结果可以提高后来从细粒古样品中检索到的日期的可靠性。同时,细粒残留剂量的较高空间变异性也可以评估不同河段的侵蚀特性。
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引用次数: 13
OSL chronostratigraphy for loess deposits from Tyszowce – Poland 波兰Tyszowce黄土沉积的OSL年代学
IF 1.2 4区 地球科学 Q3 Earth and Planetary Sciences Pub Date : 2017-11-30 DOI: 10.1515/geochr-2015-0074
P. Moska, G. Adamiec, Z. Jary, A. Bluszcz
Abstract The presented work concerns a loess profile located in Tyszowce, in the eastern part of Poland on the Volyn Upland, close to the Ukrainian border. The investigated loess formation is well preserved and is characterised by clear stratigraphic units providing an opportunity to refine the loess chronostratigraphy in Poland. In the paper, we present luminescence ages of loess from the last glacial cycle in SE Poland (up to about 100 ka) together with seven radiocarbon ages. Twenty-one samples were collected and dated using infrared (post-IR IRSL) and blue light stimulated luminescence dating. Two fractions were used, namely polymineral fine grains (4–11 μm) and medium sized quartz grains (45–63 μm). The obtained luminescence ages show very good agreement of both methods in relation to loess deposits, however for the fossil soil units the post-IR IRSL method yields older ages. Radiocarbon dates also confirm luminescence chronostratigraphy for younger units. Moreover, the luminescence results are supported by detailed analyses of grain size distribution, carbonate content and magnetic susceptibility variations allowing to create a comprehensive picture of chronological evolution of this site.
提出的工作涉及位于Tyszowce的黄土剖面,在波兰东部的沃林高地,靠近乌克兰边境。所研究的黄土地层保存完好,地层单元清晰,为完善波兰的黄土年代地层提供了机会。本文给出了波兰东南部末次冰期(约100 ka)黄土的发光年龄和7个放射性碳年龄。采用红外(post-IR IRSL)和蓝光激发发光测年法对21个样品进行了测年。采用多矿物细颗粒(4 ~ 11 μm)和中等尺寸石英颗粒(45 ~ 63 μm)两组。两种方法所得的发光年龄在黄土沉积物中具有很好的一致性,但对于化石土壤单元,ir后的IRSL方法所得的年龄更大。放射性碳测年也证实了较年轻单位的发光年代地层。此外,发光结果还得到了粒度分布、碳酸盐含量和磁化率变化的详细分析的支持,从而形成了该遗址年代学演变的全面图景。
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引用次数: 12
Some novel features of post-500°C heating blue stimulated OSL emission of fired natural quartz 烧制天然石英500°C后加热蓝色激发OSL发射的一些新特性
IF 1.2 4区 地球科学 Q3 Earth and Planetary Sciences Pub Date : 2017-11-23 DOI: 10.1515/geochr-2015-0078
D. Koul, A. Soni, D. Datta
Abstract In this study, some novel features of the post 500°C blue stimulated optically stimulated luminescence (OSL) of fired geological quartz are reported. Different observations (i) pulse annealing and (ii) impact of bleaching on high temperature TL glow peak suggested 510°C (heating rate of 2°C/s) TL peak trap to be responsible for the observed emission. The dosimetric properties of this emission were seen to make its applicability for dose assessment till kGy range. The signal was seen to be easily bleachable, reaching background value within 100 s with blue light at 125°C. The signal qualified all the tests (i) reproducibility, (ii) negligible recuperation and (iii) accuracy of dose recovery needed for reliable assessment of the radiation dose with modified Single aliquot regenerative (SAR) protocol. Considering the bleachability and high dynamic dose range of this signal, it has the potential to stretch the upper dose limit of dating by one order of magnitude than possible with conventional OSL, corresponding to 325°C TL trap. So, combining all the results, the signal reported here could be very useful for dosimetric applications involving measurement of high radiation dose, like dating.
摘要本文报道了地质石英燃烧后500℃蓝激光激发光(OSL)的一些新特征。不同的观测结果(1)脉冲退火和(2)漂白对高温TL发光峰的影响表明510°C(升温速率为2°C/s) TL峰陷阱是造成观测到的发光的原因。该辐射的剂量学性质使其适用于kGy范围内的剂量评估。该信号很容易漂白,在125°C的蓝光下,在100秒内达到背景值。该信号通过了以下所有测试:(i)可重复性、(ii)可忽略不计的恢复和(iii)剂量恢复的准确性,这些测试是使用改进的单一当量再生(SAR)方案可靠评估辐射剂量所需的。考虑到该信号的可漂白性和高动态剂量范围,它有可能比常规OSL延长一个数量级的测年上限,相当于325°C TL陷阱。因此,综合所有的结果,这里报告的信号对于包括测量高辐射剂量的剂量学应用非常有用,比如测年。
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引用次数: 0
Coarse versus fine-grain quartz optical dating of the sediments related to the 1985 Ms7.1 Wuqia earthquake, northeastern margin of the Pamir salient, China 1985年帕米尔凸起东北缘乌恰7.1级地震沉积物的粗粒石英与细粒石英光学测年
IF 1.2 4区 地球科学 Q3 Earth and Planetary Sciences Pub Date : 2017-11-23 DOI: 10.1515/geochr-2015-0075
Huili Yang, Jie Chen, N. Porat, Tao Li, Wenqiao Li, Weipeng Xiao
Abstract Optical dating of earthquake related sediments were investigated including one modern sample and three samples from a trench excavated across the 1985 Ms7.4 Wuqia Earthquake surface rupture. The results indicated that equivalent dose (De) values vary with grain size and the method used for De determination. The residual dose of the modern sample is 0.1 ka ( 0.2−0.1+0.2 $begin{array}{} 0.2_{-0.1}^{+0.2} end{array} $ Gy) for the quartz single grain measurements. Only 1.5–3.6% of the grains have a detectable OSL signal. Single grain quartz ages are similar to the expected ages. Fine grain quartz results overestimate the De values and are much older than single grain quartz and coarse grain quartz small aliquot standardized growth curve (SA-SGC) ages. Single grain quartz OSL dating may be optimal for dating earthquake related deposits, but SA-SGC can save measurement time and has potential for dating some poorly bleaching samples.
摘要研究了与地震有关的沉积物的光学测年,包括一个现代样品和三个1985年乌恰7.4级地震地表破裂期间挖掘的沟渠样品。结果表明,等效剂量(De)值随晶粒尺寸和De测定方法的不同而变化。现代样品的残余剂量为0.1ka(0.2−0.1+0.2$bbegin{array}{}0.2_{-0.1}^{+0.2}end{array}$Gy),用于石英单颗粒测量。只有1.5-3.6%的晶粒具有可检测的OSL信号。单颗粒石英的年龄与预期年龄相似。细粒石英的结果高估了De值,并且比单粒石英和粗粒石英小等分试样标准化生长曲线(SA-SGC)的年龄要老得多。单颗粒石英OSL测年可能是地震相关矿床测年的最佳方法,但SA-SGC可以节省测量时间,并有可能对一些漂白不良的样品进行测年。
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引用次数: 6
U-Pb geochronology, Sr-Nd geochemistry, petrogenesis and tectonic setting of Gandab volcanic rocks, northeastern Iran 伊朗东北部Gandab火山岩U-Pb年代学、Sr-Nd地球化学、岩石成因及构造背景
IF 1.2 4区 地球科学 Q3 Earth and Planetary Sciences Pub Date : 2017-11-16 DOI: 10.1515/geochr-2015-0061
A. E. Harsini, S. A. Mazaheri, S. Saadat, J. Santos
Abstract This paper addresses U-Pb geochronology, Sr-Nd geochemistry, petrogenesis and tectonic setting in the Gandab volcanic rocks. The Gandab volcanic rocks belong to the Sabzevar zone magmatic arc (northeastern Iran). Petrographically, all the studied volcanic rocks indicate porphyritic textures with phenocrysts of plagioclase, K-feldespar, hornblende, pyroxene, and magnetite which are embedded in a fine to medium grained groundmass. As well, amygdaloidal, and poikilitic textures are seen in some rocks. The standard chemical classifications show that the studied rocks are basaltic trachy andesite, trachy andesite, trachyte, and trachy dacite. Major elements reveal that the studied samples are metaluminous and their alumina saturation index varies from 0.71 to 1.02. The chondrite-normalized rare earth element and mantle-normalized trace element patterns show enrichment in light rare earth elements (LREE) relative to heavy rare earth elements (HREE) and in large ion lithophile elements (LILE) relative to high field strength elements (HFSE). As well they show a slightly negative Eu anomaly (Eu/Eu* = 0.72 – 0.97). The whole-rock geochemistry of the studied rocks suggests that they are related to each other by fractional crystallization. LA-MC-ICP-MS U-Pb analyses in zircon grains from two volcanic rock samples (GCH-119 and GCH-171) gave ages ranging of 5.47 ± 0.22 Ma to 2.44 ± 0.79 Ma, which corresponds to the Pliocene period. In four samples analysed for Sr and Nd isotopes 87Sr/86Sr ratios range from 0.704082 to 0.705931 and εNd values vary between +3.34 and +5. These values could be regarded to as representing mantle derived magmas. Taking into account the comparing rare earth element (REE) patterns, an origin of the parental magmas in enriched lithospheric mantle is suggested. Finally, it is concluded that Pliocene Gandab volcanic rocks are related to the post-collision environment that followed the Neo-Tethys subduction.
本文论述了甘达布火山岩的U-Pb地质年代学、Sr-Nd地球化学、岩石成因和构造环境。Gandab火山岩属于Sabzevar带岩浆弧(伊朗东北部)。从岩石学角度来看,所有研究的火山岩都显示出含斜长石、钾长石、角闪石、辉石和磁铁矿斑晶的斑状结构,这些斑晶嵌入细粒至中等粒度的岩体中。此外,在一些岩石中还可以看到杏仁状和尖晶状结构。标准化学分类表明,所研究的岩石为玄武质管安质岩、管安山岩、管安岩和管英安岩。主要元素表明,所研究的样品为金属铝,其氧化铝饱和度指数在0.71至1.02之间。球粒陨石归一化稀土元素和地幔归一化微量元素模式显示,相对于重稀土元素(HREE),轻稀土元素(LREE)富集,相对于高场强元素(HFSE),大离子亲石元素(LILE)富集。此外,它们还显示出轻微的负Eu异常(Eu/Eu*=0.72–0.97)。所研究岩石的全岩地球化学表明,它们通过分级结晶相互关联。来自两个火山岩样品(GCH-119和GCH-171)的锆石颗粒的LA-MC-ICP-MS U-Pb分析给出的年龄范围为5.47±0.22 Ma至2.44±0.79 Ma,对应于上新世。在四个分析Sr和Nd同位素的样品中,87Sr/86Sr比值在0.704082至0.705931之间,εNd值在+3.34至+5之间变化。这些数值可以被视为代表地幔衍生的岩浆。考虑到稀土元素(REE)模式的比较,提出了富集岩石圈地幔母岩浆的起源。最后得出结论,上新世甘达布火山岩与新特提斯俯冲后的碰撞后环境有关。
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引用次数: 2
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Geochronometria
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