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Luminescence Dating of Lacustrine Sediments from Cuoe Lake on the Central Tibetan Plateau 青藏高原中部错湖湖相沉积物的发光测年
IF 1.2 4区 地球科学 Q3 Earth and Planetary Sciences Pub Date : 2020-07-22 DOI: 10.2478/geochr-2020-0002
Yandong Hou, H. Long, Lei Gao, Ji Shen
Abstract Luminescence dating technology has been used for chronological constraints on lacustrine sediments due to the ubiquitous materials (e.g., quartz and feldspar) as dosimeters, and a relatively long dating range, compared with the commonly used radiocarbon dating method. However, quartz dating on the Tibetan Plateau may suffer from dim and unstable luminescence signals. In the current study, we investigate a lake-related outcrop from the shore of Cuoe Lake on the central Tibetan Plateau. Both coarse-grained quartz and K-feldspar fractions were extracted, and OSL and post-IR IRSL signals were measured from these fractions, respectively. Combining the stratigraphy analysis and dating results, this study shows that: (1) quartz appears to be unsuitable for dating because of very dim natural signals and even anomalous fading (average g-value: 4.30 ± 2.51 %/decade). The suitability of the applied pIRIR protocol measured at 150°C (pIRIR150) for K-feldspar samples was confirmed by a set of luminescence tests; (2) compared with the luminescence-based chronology, the 14C age of shells from the same sediment layer yielded older age by ∼7 ka, which is likely attributed to hard water reservoir effect in Cuoe Lake; (3) the lake level reached its peak and maintained high-stand during the early Holocene (∼9.4–7.1 ka). This study highlights the applicability of K-feldspar luminescence dating when the counterpart quartz OSL is insensitive and encounters anomalous fading.
摘要与常用的放射性碳测年方法相比,发光测年技术广泛使用石英、长石等材料作为剂量计,且测年范围较长,因此被用于湖泊沉积物的年代限制。然而,青藏高原石英测年存在发光信号微弱、不稳定的问题。在本研究中,我们研究了青藏高原中部郭湖岸的一个与湖泊有关的露头。提取粗粒石英和钾长石组分,分别测量其OSL和ir后的IRSL信号。结合地层分析和测年结果表明:(1)石英的自然信号非常微弱,甚至出现异常衰减(平均g值为4.30±2.51% / 10年),不适合测年。在150°C下测量的pIRIR方案(pIRIR150)对k -长石样品的适用性通过一组发光测试得到证实;(2)与基于发光的年代学相比,同一沉积层壳的14C年代学结果显示,其年代学年龄要老约7 ka,这可能与错湖硬水储层效应有关;(3)全新世早期(~ 9.4 ~ 7.1 ka)湖泊水位达到顶峰并保持高位。该研究强调了钾长石发光定年在对应石英OSL不敏感和遇到异常褪色时的适用性。
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引用次数: 7
Timing of Holocene Lake Highstand in Jinchang Paleolake from the Northeast Tibetan Plateau Foreland 青藏高原东北部前陆金昌古湖泊全新世湖高水位定年
IF 1.2 4区 地球科学 Q3 Earth and Planetary Sciences Pub Date : 2020-07-22 DOI: 10.2478/geochr-2020-0004
H. Long, Hongyi Cheng, Linhai Yang, Lei Gao, Qian Liu
Abstract Lake shoreline beach ridges and their sediments have often been investigated as paleoenvironmental indicators in arid northern China. Robust chronology is crucial to utilize this archive for paleoenvironmental reconstruction and interpretation. In this study, we reported a robust chronology for the highest wave-built beach ridge around Jinchang paleolake at the northeast (NE) margin of the Tibetan Plateau, using a combined quartz and K-feldspar luminescence dating technique, together with radiocarbon dating. The consistent quartz and K-feldspar ages suggested the sufficient reset of luminescence signals before deposition for the investigated sediments. Both kinds of luminescence ages were in agreement with three independent 14C ages, further corroborating the robustness of these obtained luminescence ages. Our results demonstrated that the investigated beach ridge was formed around 8.5–6.9 ka, suggesting a distinct period of lake highstand which has been identified in other lakes nearby. This highstand event may implicate an increased regional moisture condition, which is likely caused by the increased Asian summer monsoon precipitation.
摘要在中国北方干旱地区,湖岸滩脊及其沉积物经常被作为古环境指标进行调查。稳健的年表对于利用该档案进行古环境重建和解释至关重要。在这项研究中,我们使用石英和钾长石发光测年技术以及放射性碳测年,报道了青藏高原东北(NE)边缘金昌古湖周围最高波浪建造的海滩山脊的有力年表。一致的石英和钾长石年龄表明,对于所研究的沉积物来说,沉积前的发光信号已经足够重置。两种发光年龄与三个独立的14C年龄一致,进一步证实了这些获得的发光年龄的稳健性。我们的研究结果表明,所调查的海滩山脊形成于8.5–6.9 ka左右,这表明附近其他湖泊中存在一个明显的湖泊高位期。这一高水位事件可能意味着区域湿度条件的增加,这可能是由亚洲夏季风降水增加引起的。
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引用次数: 0
CW-OSL, LM-OSL and TL Dating of Bricks from Karakorum, Mongolia: Insights from TL Spectra 蒙古喀喇昆仑地区砖的CW-OSL、LM-OSL和TL定年:来自TL光谱的启示
IF 1.2 4区 地球科学 Q3 Earth and Planetary Sciences Pub Date : 2020-07-22 DOI: 10.2478/geochr-2020-0003
S. Solongo, S. Tengis, G. Wagner, Hans Hüttel
Abstract In this study, we present results of luminescence dating using CW-OSL, LM-OSL and TL on heated quartz from the archaeological and historical site in Karakorum – the ancient capital of Mongolia, to test their convergence with the age control in the form of the Karakorum inscription 1346. The TL spectra conducted on quartz from red and grey coloured bricks appeared to be characteristic of the technological origin. Quartz TL from red bricks showed a UV emission band at ∼360 nm and a strong fast OSL component dominated signal. In contrast, blue emission detected in the TL spectra of grey coloured bricks, resulting possibly in the medium component dominated OSL signal. Finally, OSL and TL results gave dates from 1180±70 AD to 1360±70 consistent with the expected ages.
摘要在这项研究中,我们介绍了使用CW-OSL、LM-OSL和TL对蒙古古都喀喇昆仑考古和历史遗址的加热石英进行发光测年的结果,以测试它们与喀喇昆仑1346铭文形式的年龄控制的一致性。在红色和灰色砖的石英上进行的TL光谱似乎是技术起源的特征。来自红砖的石英TL显示出约360 nm的紫外线发射带和强烈的快速OSL成分主导信号。相反,在灰色砖的TL光谱中检测到蓝色发射,可能导致介质成分主导的OSL信号。最后,OSL和TL结果给出了从公元1180±70到1360±70的日期,与预期年龄一致。
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引用次数: 1
ESR Dating of Optically Bleached Quartz Grains: Assessing the Impact of Different Experimental Setups on Dose Evaluations 光学漂白石英颗粒的ESR定年:评估不同实验设置对剂量评估的影响
IF 1.2 4区 地球科学 Q3 Earth and Planetary Sciences Pub Date : 2020-07-18 DOI: 10.2478/geochr-2020-0005
V. Guilarte, M. Duval
Abstract In recent years, our investigation has been centred on improving the reliability and accuracy of the ESR method applied to quartz grains. As part of this ongoing investigation, we present an intra-laboratory study to evaluate the impact of different experimental setups on the ESR measurement precision and dose evaluation for ESR dating of optically bleached quartz grains. Repeated measurements of quartz samples have been performed at CENIEH, Spain, using two different Bruker spectrometers (EMXmicro and Elexsys E500) and resonators (standard rectangular ER4102ST and cylindrical Super High QE cavities). Their performance in terms of sensitivity, measurement repeatability and dose determination are presented in this study. This intra-laboratory work has allowed to evaluate the robustness of our protocol for ESR dating of quartz grains and to study the potential impact of different experimental setups on dose evaluation, which is essential for future standardization of the ESR dating method. Our results indicate that all the different experimental setups provide comparable precision of the ESR intensity measurements. Moreover, all the ESR dose estimates are within 1-sigma error, suggesting that it is possible to compare results obtained by different laboratories when similar analytical procedures are followed. Finally, the higher sensitivity achieved by the SHQE resonator appears to be of particular interest when dealing with samples showing low ESR signal intensities.
摘要近年来,我们的研究重点是提高应用于石英晶粒的ESR方法的可靠性和准确性。作为这项正在进行的研究的一部分,我们提出了一项实验室内研究,以评估不同实验装置对光学漂白石英颗粒ESR测年的ESR测量精度和剂量评估的影响。在西班牙CENIEH,使用两种不同的Bruker光谱仪(EMXmicro和Elexsys E500)和谐振器(标准矩形ER4102ST和圆柱形超高QE腔)对石英样品进行了重复测量。本研究介绍了它们在灵敏度、测量重复性和剂量测定方面的性能。这项实验室内的工作使我们能够评估石英颗粒ESR测年方案的稳健性,并研究不同实验设置对剂量评估的潜在影响,这对ESR定年方法的未来标准化至关重要。我们的结果表明,所有不同的实验装置都提供了相当精度的ESR强度测量。此外,所有ESR剂量估计值都在1西格玛误差范围内,这表明当遵循类似的分析程序时,可以比较不同实验室获得的结果。最后,当处理显示低ESR信号强度的样品时,SHQE谐振器实现的更高灵敏度似乎特别令人感兴趣。
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引用次数: 4
Applicability of OSL Dating to Fine-Grained Fluvial Deposits in the Mekong River Floodplain, Cambodia 柬埔寨湄公河漫滩细粒河流沉积物OSL测年的适用性
IF 1.2 4区 地球科学 Q3 Earth and Planetary Sciences Pub Date : 2020-06-03 DOI: 10.2478/geochr-2020-0006
Y. Ishii, T. Tamura, D. Collins, Bunnarin Ben
Abstract Optically stimulated luminescence (OSL) dating of fine-grained (4–11 μm) fluvial sediments is rarely attempted but is crucial for constraining the evolution of mud-dominated floodplains. This study investigated the applicability of OSL dating to fine-grained deposits in the Mekong River, Cambodia based on a very young (<600 yr) point-bar to riverbank succession and modern flood deposits. In succession, fine-grained quartz OSL provided the youngest ages, whereas age estimates by multi-grain sand-sized quartz OSL, and feldspar and polymineral infrared-stimulated luminescence are >200 years older than the fine-grained quartz OSL age estimates. Ages of fine-grained quartz OSL are concordant with the minimum ages obtained from the single-grain quartz OSL. These results are supported by the generally small residual doses (<0.1 Gy) measured in modern fine-grained flood-plain deposits. This indicates that fine-grained sediments in the Mekong River (Cambodia) are sufficiently bleached at deposition and can yield reliable quartz OSL ages for establishing the chronology of the floodplain. The sufficient bleaching of fine-grained quartz partly results from the long transport distance and may also occur in other large river systems.
摘要细粒(4–11μm)河流沉积物的光激发光(OSL)测年很少尝试,但对于限制泥质泛滥平原的演变至关重要。本研究调查了OSL测年法在湄公河细粒沉积物中的适用性,柬埔寨基于一个非常年轻的(比细粒石英OSL年龄估计值早200年)。细粒石英OSL的年龄与从单粒石英OSL获得的最小年龄一致。这些结果得到了现代细粒洪泛平原矿床中测得的通常较小的残余剂量(<0.1 Gy)的支持。这表明湄公河(柬埔寨)的细粒沉积物在沉积时充分漂白,可以产生可靠的石英OSL年龄,用于确定泛滥平原的年代。细粒石英的充分漂白部分是由于运输距离长,也可能发生在其他大型河流系统中。
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引用次数: 4
High Resolution Quartz OSL and K-feldspar post-IR IRSL Dating of Loess in the Central Shandong Mountains (Eastern China) 鲁中黄土的高分辨率石英OSL和钾长石红外光谱后定年
IF 1.2 4区 地球科学 Q3 Earth and Planetary Sciences Pub Date : 2020-05-30 DOI: 10.1515/geochr-2015-0113
Qiuyue Zhao, M. Ding, Shuzhen Peng, Luo Wang, Wei Zhang, Bo Song, Rui Zhou, Jun-sheng Yue, Dongdong Zheng
Abstract The loess sediments widely distributed in the Central Shandong Mountains are sensitive records of East Asian monsoon changes for situating in a key region connected to the Eurasian Plate and the Pacific Ocean. However, the detailed processes of palaeoclimatic changes are poorly understood for the lack of high-resolution chronology. In this study, the chronology of Heishan loess palaeosol sequence in the Central Shandong Mountains is investigated using quartz SAR OSL and K-feldspar post-IR infrared (IR) stimulated luminescence (post-IR IRSL) dating method. The quartz is sensitive, fast component dominated and saturate at ∼150 Gy (∼50 ka). The measured K-feldspar pIRIR290 De showed no dependency on the first IR stimulation temperature between 50°C and 260°C. The K-feldspar pIRIR290 ages are consistent with the stratigraphy up to ∼75 ka. In establishing the chronological sequence for the study section, quartz OSL ages <50 ka and the K-feldspar pIRIR290 ages >50 ka were selected. Derived sedimentation rates show two relatively rapid stages of ∼32.0 ± 5.5 cm/ka for the palaeosol (∼11–8 ka) and ∼54.8 ± 1.1 cm/ka for the loess (∼34–30 ka). An erosional hiatus of loess between ∼30 ka and ∼17 ka is identified. We conclude that the pIRIR290 of loess sediments is applicable for samples during ∼8–75 ka.
山东中部广泛分布的黄土沉积物是东亚季风变化的敏感记录,地处连接欧亚板块和太平洋的重要区域。然而,由于缺乏高分辨率的年表,人们对古气候变化的详细过程知之甚少。本研究采用石英SAR OSL和钾长石后红外(IR)激发发光(post-IR-IRSL)测年方法,对鲁中黑山黄土古土壤序列进行了年代测定。石英是敏感的,快速成分占主导地位,在~150 Gy(~50 ka)时饱和。测得的钾长石pRIR290-De不依赖于50°C至260°C之间的第一次IR刺激温度。钾长石pIRIR290年龄与高达~75ka的地层一致。在确定研究剖面的时间序列时,选择了50 ka的石英OSL。导出的沉积速率显示出两个相对快速的阶段,古土壤为~32.0±5.5 cm/ka(~11–8 ka),黄土为~54.8±1.1 cm/ka(约34–30 ka)。确定了约30 ka至约17 ka之间的黄土侵蚀间断。我们得出结论,黄土沉积物的pIRIR290适用于~8–75ka期间的样品。
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引用次数: 3
Assessing the Dating Potential of Violet Stimulated Luminescence Protocols 评估紫激发光协议的定年潜力
IF 1.2 4区 地球科学 Q3 Earth and Planetary Sciences Pub Date : 2020-05-26 DOI: 10.1515/geochr-2015-0115
Mariana Sontag-González, M. Frouin, Bo Li, J. Schwenninger
Abstract Violet stimulation is a new development in optical dating which has been suggested to extend the upper age limit of optically simulated luminescence (OSL) dating of quartz. Despite the reported advantage, few validation tests and applications have been published so far. The present study investigated the violet stimulated luminescence (VSL) using a single aliquot regenerative dose (SAR) protocol and a multiple aliquot additive dose (MAAD) protocol. Sedimentary quartz samples from four archaeological sites in Europe with independent age controls spanning 40–900 ka were used, including Grotte Mandrin (France), Brooksby Quarry (UK), Cueva Negra del Estrecho del Río Quípar (Spain) and Sima de las Palomas del Cabezo Gordo (Spain). The equivalent dose of a relatively young sample (∼40 ka) was successfully determined. However, significant underestimations were observed for older samples with higher doses. These findings indicate the need for further development of the measurement protocol to date high-dose natural samples.
摘要紫激发是光学测年的一个新进展,它被认为可以延长石英光学模拟发光测年的年龄上限。尽管报道了这种优势,但到目前为止,很少有验证测试和应用发表。本研究使用单等分再生剂量(SAR)方案和多等分添加剂量(MAAD)方案研究了紫激发光(VSL)。使用了来自欧洲四个考古遗址的沉积石英样品,这些遗址的独立年龄控制范围为40-900 ka,包括Grotte Mandrin(法国)、Brooksby Quarry(英国)、Cueva Negra del Estreco del Río Quípar(西班牙)和Sima de las Palomas del Cabezo Gordo(西班牙)。成功测定了相对年轻的样品(~40ka)的等效剂量。然而,对于具有较高剂量的较老样本,观察到明显的低估。这些发现表明,有必要进一步开发迄今为止高剂量天然样品的测量方案。
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引用次数: 5
Analyzing Statistical Age Models to Determine the Equivalent Dose and Burial Age Using a Markov Chain Monte Carlo Method 用马尔可夫链蒙特卡罗方法分析统计年龄模型以确定等效剂量和埋葬年龄
IF 1.2 4区 地球科学 Q3 Earth and Planetary Sciences Pub Date : 2020-05-02 DOI: 10.1515/geochr-2015-0114
Jun Peng
Abstract In optically stimulated luminescence (OSL) dating, statistical age models for equivalent dose (De) distributions are routinely estimated using the maximum likelihood estimation (MLE) method. In this study, a Markov chain Monte Carlo (MCMC) method was used to analyze statistical age models, including the central age model (CAM), the minimum age model (MAM), the maximum age model (MXAM), etc. This method was first used to obtain sampling distributions on parameters of interest in an age model using De distributions from individual sedimentary samples and subsequently extended to simultaneously extract age estimates from multiple samples with stratigraphic constraints. The MCMC method allows for the use of Bayesian inference to refine chronological sequences from multiple samples, including both fully and partially bleached OSL dates. This study designed easily implemented open-source numeric programs to perform MCMC sampling. Measured and simulated De distributions are used to validate the reliability of dose (age) estimates obtained by this method. Findings from this study demonstrate that estimates obtained by the MCMC method can be used to informatively compare results obtained by the MLE method. The application of statistical age models to multiple OSL dates with stratigraphic orders using the MCMC method may significantly improve both the precision and accuracy of burial ages.
摘要在光激发光(OSL)测年中,等效剂量(De)分布的统计年龄模型通常使用最大似然估计(MLE)方法进行估计。本研究采用马尔可夫链蒙特卡罗(MCMC)方法分析统计年龄模型,包括中心年龄模型(CAM)、最小年龄模型(MAM)、最大年龄模型(MXAM)等。该方法首先用于使用单个沉积样品的De分布来获得年龄模型中感兴趣参数的采样分布,随后扩展到同时从具有地层约束的多个样品中提取年龄估计值。MCMC方法允许使用贝叶斯推断来细化多个样本的时间序列,包括完全漂白和部分漂白的OSL日期。本研究设计了易于实现的开源数字程序来执行MCMC采样。测量和模拟的De分布用于验证通过该方法获得的剂量(年龄)估计的可靠性。这项研究的结果表明,通过MCMC方法获得的估计值可以用于信息比较通过MLE方法获得的结果。使用MCMC方法将统计年龄模型应用于具有地层顺序的多个OSL日期,可以显著提高埋葬年龄的精度和准确性。
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引用次数: 4
Variations of Thermally and Optically Stimulated Luminescence Sensitivity of Loess and Pedocomplex Samples from Southern Tajikistan, Central Asia 中亚塔吉克斯坦南部黄土和土壤复合体样品的热光敏感性变化
IF 1.2 4区 地球科学 Q3 Earth and Planetary Sciences Pub Date : 2020-04-29 DOI: 10.1515/geochr-2015-0118
Yuetian Li, Liping Zhou
Abstract To better understand the factors controlling the quartz luminescence sensitivity in loess deposits, samples from two loess sections in southern Tajikistan are investigated. Both pattern and amplitude in the variations of quartz luminescence sensitivity of these two sections are similar, showing higher values in pedocomplex units and lower values in the loess units. Similar trends of variation are found between the quartz luminescence sensitivity and climate proxies, including frequency-dependent magnetic susceptibility, median grain size and IRSL/[post-IR] OSL ratio. Laboratory experiments involving thermal activation and repeated bleaching/irradiation cycles reveal much larger sensitivity enhancement for samples with initial lower sensitivity from loess units than those from pedocomplex units with higher sensitivity. The observed systematic contrast in quartz luminescence sensitivity between the loess and pedocomplex units are interpreted as resulting from the differentiation of the weathering products from the source area and subsequent sensitization during the sedimentary transfer prior to deposition.
摘要为了更好地了解黄土沉积物中石英发光敏感性的控制因素,对塔吉克斯坦南部两个黄土剖面的样品进行了研究。两个剖面的石英发光灵敏度变化模式和幅度相似,均表现为土壤复合体单元较高,黄土单元较低。石英发光敏感性与气候指标(包括频率相关磁化率、中值粒度和IRSL/[后ir] OSL比)之间也存在类似的变化趋势。包括热活化和重复漂白/辐照循环在内的实验室实验表明,黄土单元中初始灵敏度较低的样品的灵敏度要比灵敏度较高的土壤复合体单元的样品的灵敏度提高得多。观测到的黄土与土壤复合体单元石英发光敏感性的系统对比可以解释为源区风化产物的分异和沉积转移过程中沉积前敏化的结果。
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引用次数: 5
Component Resolved Equivalent Dose Estimation Using TL Glow Curves of Travertine Samples from Anatolia, Turkey 使用土耳其安纳托利亚石灰华样品的TL发光曲线进行成分分解等效剂量估计
IF 1.2 4区 地球科学 Q3 Earth and Planetary Sciences Pub Date : 2020-04-29 DOI: 10.1515/geochr-2015-0116
E. Şahiner, G. Polymeris, M. Öztürk, Y. Kadıoğlu, N. Meriç
Abstract This study provides methodological aspects on the equivalent dose estimation for travertine samples, namely heated calcium carbonate, using the TL multiple-aliquot additive-dose approach. Large equivalent doses (EDs), within the range 750–1300 Gy, were calculated using the plateau method based on the NTL glow curve. Moreover, a component resolved TL glow-peak analysis was carried out, using the integrated intensity of the NTL glow peaks for the ED estimation after deconvolution based on the OTOR model. Three different TL peaks were used, termed P4, P5 and P6. The integrated intensity of TL glow peak P4 resulted in age overestimation (15–26%), compared to the age provided using the plateau method. This overestimation could be attributed to the fact that the temperature range of P4 does not coincide with the plateau region of each sample. Milder overestimation (8–14%) was noticed using the integrated intensity of TL glow peak P6, mostly due to the poor deconvolution resolution. Only the integrated intensity of TL glow peak P5 after deconvolution provides ED values compatible with those yielded using the plateau method, with good accuracy. The present study suggests not using the TL intensity (neither in terms of integrated intensity nor of peak height intensity) for ED estimation; instead it is highly recommended to use either the plateau method, or alternatively integrated intensity of TL peak P5 after deconvolution. Unfortunately, using the peak height of TL P5 is not recommended, due to overlapping with P6.
摘要:本研究对加热碳酸钙钙华样品的等效剂量估计进行了方法学方面的研究。基于NTL发光曲线,采用平台法计算了750 ~ 1300 Gy范围内的大等效剂量(EDs)。此外,基于OTOR模型,利用NTL发光峰的综合强度进行反卷积后的ED估计,进行了分量分解的TL发光峰分析。使用了三个不同的TL峰,分别称为P4、P5和P6。与使用平台法提供的年龄相比,TL发光峰P4的综合强度导致年龄高估(15-26%)。这种高估可能是由于P4的温度范围与每个样本的高原区域不一致。利用TL发光峰P6的综合强度发现了较轻微的高估(8-14%),主要是由于较差的反卷积分辨率。只有反褶积后的TL辉光峰P5的综合强度才能提供与平台法相匹配的ED值,且具有较好的精度。本研究建议不使用TL强度(无论是综合强度还是峰高强度)来估计ED;相反,强烈建议使用平台法,或者使用反褶积后TL峰P5的综合强度。不幸的是,由于与P6重叠,不建议使用TL P5的峰高。
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引用次数: 2
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Geochronometria
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