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The Roman amphitheatre in Mérida, Spain ˗Augustan or Flavian? Radiocarbon dating results on mortar carbonate 西班牙msamrida的罗马圆形剧场——奥古斯都还是弗拉维安?灰浆碳酸盐放射性碳定年结果
IF 1.2 4区 地球科学 Q3 Earth and Planetary Sciences Pub Date : 2020-01-01 DOI: 10.2478/geochr-2020-0028
A. Lindroos, J. Heinemeier, Å. Ringbom, T. S. Daugbjerg, I. Hajdas
Abstract Four lime mortar samples from the Mérida amphitheatre in Spain were dated in 2001 and re-dated in 2019 with refined dating methods and focus on carbon dioxide that was released in late CO2 fractions when dissolved in phosphoric acid. The samples were difficult to date because they contained highly soluble, young carbonate contamination that dominated the carbon dioxide from the early stages of the reaction with the acid in the hydrolysis process. They were also rather hydraulic and rich in magnesium, which could have caused delayed hardening. However, there was very little dead carbon contamination so that late carbon dioxide fraction gave uniform 14C ages, pointing to a late 1st c. AD Flavian, or later age of the amphitheatre.
研究人员于2001年测定了西班牙msamrida圆形剧场的4个石灰砂浆样本的年代,并于2019年用精确的测年方法重新测定了样本的年代,重点研究了溶解在磷酸中以后期二氧化碳组分释放的二氧化碳。这些样品很难确定年代,因为它们含有高度可溶的年轻碳酸盐污染物,这些污染物主要是在水解过程中与酸反应的早期阶段产生的二氧化碳。它们还具有很强的水力和丰富的镁,这可能会导致延迟硬化。然而,几乎没有死碳污染,因此晚期二氧化碳馏分给出了统一的14C年龄,指向公元1世纪晚期的弗拉维安,或更晚的圆形剧场。
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引用次数: 1
A Tree-Ring chronology from Allerød–YD transition from Koźmin (Central Poland) 来自Koźmin(波兰中部)的allero ød - yd转变的树轮年代学
IF 1.2 4区 地球科学 Q3 Earth and Planetary Sciences Pub Date : 2020-01-01 DOI: 10.2478/geochr-2020-0025
M. Krąpiec, E. Szychowska-Krąpiec, J. Barniak, T. Goslar, P. Kittel, D. Michczyńska, A. Michczyński, N. Piotrowska, A. Rakowski, Damian Wiktorowski
Abstract Subfossil trunks of pine (Pinus sylvestris L.) from the Late Weichselian were discovered in the site Koźmin in the Koło Basin, central Poland (Dzieduszyńska et al., 2014a). Another part of organic sediments with trunks was excavated in the frame of the research project. Altogether 224 samples from Koźmin were analysed dendrochronologically; they represented generally young trees, 40 to 70 years old. Based on the most convergent sequences, the chronology 2KOL_A1 was produced, 210 years in length. With the wiggle-matching method, it was dated to ca. 13065–12855 cal BP. Dendrochronological dating of trunks buried in organic sediments, most of which occurred in situ, revealed that tree deaths occurred successively, over more than 100 years. That could have been due to unfavourable climatic conditions, as well as extreme events, e.g. strong winds.
摘要在波兰中部Koło盆地的Koßmin遗址发现了晚魏氏时代的松(Pinus sylvestris L.)的亚化石树干(Dzieduszyńska et al.,2014a)。另一部分带树干的有机沉积物是在研究项目的框架内挖掘出来的。共对来自科罗兹明的224个样本进行了树木年代分析;它们通常代表40至70年树龄的幼树。根据最收敛的序列,产生了长达210年的2KOL_A1年表。使用摆动匹配方法,其年代为约13065–12855 cal BP。对埋藏在有机沉积物中的树干进行树木年代测定,其中大多数发生在原位,表明树木死亡连续发生,超过100年。这可能是由于不利的气候条件以及强风等极端事件造成的。
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引用次数: 4
Increase in 14C dating accuracy of prehistoric skeletal remains by optimised bone sampling: Chronometric studies on eneolithic burials from Mikulin 9 (Poland) and Urziceni-Vada Ret (Romania) 通过优化骨骼采样提高史前骨骼遗骸的14C定年精度:对Mikulin 9(波兰)和Urziceni-Vada Ret(罗马尼亚)新石器时代墓葬的时间测定研究
IF 1.2 4区 地球科学 Q3 Earth and Planetary Sciences Pub Date : 2020-01-01 DOI: 10.2478/geochr-2020-0026
T. Chmielewski, Agata Hałuszko, T. Goslar, Olivia Cheronet, T. Hajdu, Tamás Szeniczey, Cristian Virag
Abstract In this research, sampling optimisation and modelling based thereon follow from the assumption that each human skeleton can be treated as a set of heterochronous carbon reservoirs capable of supplying at least an elementary sequence consisting of two 14C dates corresponding to the moment of birth (otic capsule) and that of demise (ribs), as well as an anthropologically defined lag between them. Two case studies demonstrate that the approach can raise the precision of 14C dates related to the death of the individuals. The benefits and main issues of this sampling strategy as well as the involved bioarchaeological conflict potential are taken under discussion.
摘要在这项研究中,采样优化和基于此的建模遵循的假设是,每个人类骨骼都可以被视为一组异时碳库,能够提供至少一个由两个14C日期组成的基本序列,这两个日期对应于出生时刻(耳膜)和死亡时刻(肋骨),以及它们之间的人类学定义的滞后。两个案例研究表明,该方法可以提高与个体死亡相关的14C日期的准确性。讨论了这种采样策略的好处和主要问题,以及所涉及的生物考古冲突的可能性。
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引用次数: 4
Chronostratigraphy of Late Glacial aeolian activity in SW Poland – A case study from the Niemodlin Plateau 波兰西南部晚冰期风成活动的年代地层学——以涅莫德林高原为例
IF 1.2 4区 地球科学 Q3 Earth and Planetary Sciences Pub Date : 2020-01-01 DOI: 10.2478/geochr-2020-0015
P. Moska, Z. Jary, R. Sokołowski, G. Poręba, Jerzy Raczyk, M. Krawczyk, J. Skurzyński, P. Zieliński, A. Michczyński, K. Tudyka, G. Adamiec, N. Piotrowska, Fatima Pawełczyk, Michał Łopuch, A. Szymak, Kamila Ryzner
Abstract The stratigraphy of Late Pleniglacial and Late Glacial fluvio-to-aeolian succession was investigated in two sites located at the Niemodlin Plateau, SW Poland. Lithofacial analysis was used for the reconstruction of sedimentary environments. An absolute chronology for climatic change and the resulting environmental changes were determined based on optically stimulated luminescence (OSL – nine samples) and radiocarbon (three samples) dating methods. Four phases of changes in sedimentary environments were established. The first depositional phase correlates with the Last Permafrost Maximum (24−17 ka) based on the type and size of the periglacial structures, which aggraded under continuous permafrost conditions. During 17.5−15.5 ka (upper Late Pleniglacial), a stratigraphic gap was detected, owing to a break in the deposition on the interfluve area. The second depositional phase took place during 15.5−13.5 ka. During this phase, the first part of the dune formation (Przechód site) and fluvio-aeolian cover (Siedliska site) was deposited. The sedimentary processes continued throughout the entire Bølling interstadial and Older Dryas. In the third phase (Allerød interstadial), soil formation took place. At the Siedliska site, palaeosol represented Usselo soil type, whereas at the Przechód site, there was a colluvial type of soil. The last phase (Younger Dryas) is represented by the main phase of dune formation in both sites. After the Younger Dryas, no aeolian activity was detected. High compliance with both absolute dating methods was noticed.
摘要对波兰西南部涅莫德林高原的两个地点进行了晚更冰期和晚冰期河流-风成演替的地层学研究。采用岩面分析对沉积环境进行了重建。基于光激发发光(OSL - 9个样品)和放射性碳(3个样品)测年方法,确定了气候变化和由此导致的环境变化的绝对年表。确定了沉积环境的4个变化阶段。根据冰缘构造的类型和大小,第一个沉积阶段与最后的永久冻土最大值(24 ~ 17 ka)相关,在连续的永久冻土条件下,冰缘构造发生了累积。在17.5 ~ 15.5 ka(晚更新世上部)期间,由于间隔区沉积断裂,发现了一个地层缺口。第二期沉积发生在15.5 ~ 13.5 ka。在这一阶段,第一部分沙丘形成(Przechód地点)和河流-风成覆盖物(Siedliska地点)沉积。沉积过程贯穿了整个b.o lling间冰期和古仙女木期。在第三阶段(allerr ød间隔期),土壤形成。在Siedliska遗址,古土壤为Usselo土壤类型,而在Przechód遗址,古土壤为崩塌型土壤。最后阶段(新仙女木期)是两个地点沙丘形成的主要阶段。在新仙女木期之后,没有发现风成活动。注意到这两种绝对测年方法的一致性很高。
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引用次数: 11
Age of sediments on Danube terraces of the Pest Plain (Hungary) based on optically stimulated luminescence dating of quartz and feldspar 匈牙利佩斯平原多瑙河阶地沉积物的光学激发发光法测定石英和长石的年代
IF 1.2 4区 地球科学 Q3 Earth and Planetary Sciences Pub Date : 2020-01-01 DOI: 10.2478/geochr-2020-0021
E. Thamó‐Bozsó, G. Csillag, J. Füri, A. Nagy, Á. Magyari
Abstract The numerical ages available for the sediments on the Danube terraces in the Pest Plain are scarce. In this study, we present quartz OSL and K feldspar post-IR IRSL290 ages for the sandy fluvial, aeolian and slope sediments collected from Danube terraces IIb, III and V. The feldspar post-IR IRSL290 ages without residual dose subtraction are older than the quartz OSL ages, except for one sample, but the two sets of ages are overlapping within one or two sigma errors. In the bleaching experiment under natural sunlight during summer, an unbleachable component ranging from 2.5±0.7 Gy to 5.2±0.3 Gy after 30 h exposure to bright sunshine is observed and it corresponds to 3−8% of the measured K feldspar post-IR IRSL290 equivalent doses. These facts indicate that residual dose subtraction would be necessary before age calculation, in most cases. The saturated fluvial gravelly sand of terrace V of the Danube is older than ~ 296 ka based on feldspar post-IR IRSL290 measurements. This age does not contradict the traditional terrace chronology and the earlier published age data of this terrace. The other studied sediments on the surface of the terraces V, III and IIb deposited much later than the formation of these terraces. They infer aeolian activity and fluvial sedimentation of small streams during the MIS 3 and MIS 2 periods. The age of the dated dune sands with coeval aeolian sediments in Hungary indicate the cold and dry periods with strong wind activity of the Late Weichselian.
摘要佩斯平原多瑙河阶地沉积物的可用数字年龄很少。在这项研究中,我们提出了从多瑙河阶地IIb、III和V采集的沙质河流、风成岩和斜坡沉积物的石英OSL和钾长石IR后IRSL290年龄。除一个样品外,没有残余剂量减法的长石IR后IRCL290年龄比石英OSL年龄老,但两组年龄在一个或两个西格玛误差内重叠。在夏季自然阳光下的漂白实验中,在明亮的阳光下暴露30小时后,观察到范围在2.5±0.7 Gy至5.2±0.3 Gy的不可漂白成分,其相当于红外IRSL290后测得的钾长石等效剂量的3−8%。这些事实表明,在大多数情况下,在计算年龄之前需要减去剩余剂量。根据长石后IR IRSL290测量,多瑙河V阶地的饱和河流砾砂年龄大于~296 ka。这一年龄与传统的阶地年表和早期公布的该阶地的年龄数据并不矛盾。其他研究的阶地V、III和IIb表面沉积物的沉积时间比这些阶地的形成晚得多。他们推断了MIS 3和MIS 2时期的风成活动和小河流的河流沉积。匈牙利具有同时代风成沉积物的年代确定的沙丘沙的年龄表明了晚魏克塞利亚具有强风活动的寒冷和干燥时期。
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引用次数: 0
Status of the AMS graphitization system in the dendrochronological laboratory at AGH-UST, Kraków 克拉科夫AGH-UST树状实验室AMS石墨化系统的现状
IF 1.2 4区 地球科学 Q3 Earth and Planetary Sciences Pub Date : 2020-01-01 DOI: 10.2478/geochr-2020-0024
Damian Wiktorowski, M. Krąpiec, A. Rakowski, A. Cherkinsky
Abstract A new system for the preparation of graphite samples for radiocarbon (14C) measurement using an accelerator mass spectrometer (AMS) has been built in the Dendrochronological Laboratory at AGH-UST, Kraków. This system consists of three independent components. The first is the equipment for mechanical and chemical sample pre-treatment. The second is the vacuum line for sample sealing and the purification of CO2. The third and central part of this system is a graphitization line, where graphite is produced from CO2. In the first stage, chemical sample preparation was carried out to remove impurities. IAEA and NIST OxII standard materials were converted to CO2 without pre-treatment. In the next step, samples were combusted to CO2. The resulting CO2 was released under vacuum and cryogenically purified for subsequent graphitization. The performance of the system was tested with NIST OxII, IAEA standards (IAEA C5, C6 and C7) and background samples. The test confirms good reproducibility of results obtained for the samples prepared using this system. The results of the 49 samples of NIST Ox-II, IAEA standards and blank samples were presented in this article.
摘要在克拉科夫AGH-UST的树状结构实验室建立了一个使用加速器质谱仪(AMS)制备用于放射性碳(14C)测量的石墨样品的新系统。该系统由三个独立组件组成。第一种是用于机械和化学样品预处理的设备。第二个是用于样品密封和CO2纯化的真空管线。该系统的第三个也是中心部分是石墨化线,石墨是由二氧化碳生产的。在第一阶段,进行化学样品制备以去除杂质。IAEA和NIST OxII标准材料在未经预处理的情况下转化为CO2。在下一步中,将样品燃烧成二氧化碳。将得到的CO2在真空下释放并低温纯化以用于随后的石墨化。该系统的性能用NIST OxII、IAEA标准(IAEA C5、C6和C7)和背景样品进行了测试。该测试证实了使用该系统制备的样品所获得的结果具有良好的再现性。本文介绍了49个NIST Ox II、IAEA标准样品和空白样品的结果。
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引用次数: 0
Dendrochronological dating of St. George’s Orthodox Church in Drohobych, Ukraine 乌克兰德罗霍比奇圣乔治东正教教堂的年代学
IF 1.2 4区 地球科学 Q3 Earth and Planetary Sciences Pub Date : 2020-01-01 DOI: 10.2478/geochr-2020-0023
M. Krąpiec, E. Szychowska-Krąpiec, L. Tymoshenko, R. Myska
Abstract St. George’s Orthodox Church in Drohobych is a wooden monument of sacral architecture, recently registered in the UNESCO World Heritage List. However, clear, unequivocal written sources about the origins of the structure are lacking. Absolute dating was attempted with the dendrochronological method, and it was carried out in a noninvasive way due to the status and value of the object. Construction elements of the church were documented with over 40 macrophotographs. The studies were made for selected elements, displaying distinct perpendicular or tangential cross sections. Most of the elements examined represented fir wood. It turned out that the wood used for the construction of this church was contemporaneous and most likely represented a single construction phase. The 124-year chronology based on correlated curves covers the period 1464–1598 AD. Construction elements with the outermost rings retained indicate that the timber was harvested in the 1590s. In most cases, the outermost rings were lacking, which allowed only for dating terminus post quem. The youngest preserved rings (1598 AD) from the church wood apparently reveal the dates of both the wood harvesting and the structure’s construction. Such a dating may indicate that the church mentioned in the sources as purchased in Nadiyevo in 1657 AD could be the basis for the rebuilding of Drohobych St. George’s Orthodox Church, only adapted to the new conditions. The church later underwent renovation, consisting in reconstruction of the dome in 1821 AD.
摘要Drohobich的圣乔治东正教堂是一座骶骨建筑的木制纪念碑,最近被联合国教科文组织列入世界遗产名录。然而,缺乏关于该结构起源的明确、明确的书面资料。绝对年代测定是用树状年代测定法进行的,由于对象的地位和价值,它是以一种非侵入性的方式进行的。教堂的建筑元素被记录在40多张宏观照片中。这些研究是针对选定的元素进行的,显示了不同的垂直或切向横截面。所检查的大多数元素都代表杉木。事实证明,用于建造这座教堂的木材是同时代的,很可能代表了一个单一的建造阶段。基于相关曲线的124年年表涵盖了公元1464年至1598年。保留最外圈的建筑元素表明木材是在1590年代收获的。在大多数情况下,最外层的环都是缺失的,这只允许在quem后进行定年。教堂木材中保存最年轻的戒指(公元1598年)显然揭示了木材采集和建筑的日期。这样的年代测定可能表明,资料中提到的公元1657年在纳迪耶沃购买的教堂可能是重建Drohobich圣乔治东正教会的基础,只是适应了新的条件。教堂后来进行了翻修,包括在公元1821年重建圆顶。
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引用次数: 1
Establishing a common standardised growth curve for single-aliquot OSL dating of quartz from sediments in the Jilantai area of North China 吉林台地区沉积物中石英单等分OSL测年通用标准化生长曲线的建立
IF 1.2 4区 地球科学 Q3 Earth and Planetary Sciences Pub Date : 2020-01-01 DOI: 10.2478/geochr-2020-0017
Zhenjun Li, Xuesong Mou, Yuxin Fan, Qingsong Zhang, Guangliang Yang, Hui Zhao
Abstract Establishing a common standardised growth curve (SGC) can substantially reduce the instrumental time for equivalent-dose (De) measurements in optically stimulated luminescence (OSL) dating. Several studies have indicated that different samples have different dose–response curves (DRCs) and therefore that it is difficult to construct a common SGC, although an SGC has been proposed in some cases. In this study, our aims were to construct a regional SGC based on small aliquots of sedimentary quartz from more than 100 samples from different sedimentary environments in the Jilantai Basin in North China and to investigate the applicability of different methods of establishing an SGC for the area. The precision of the De values of aliquots which were obtained using the SGC was compared with those obtained using the single-aliquot regenerative (SAR) protocol. Our results indicate the following: (1) for establishing an SGC using the regenerative normalisation (Re-SGC) method, selecting a suitable re-normalisation dose that is close to double the characteristic saturation dose, 2D0, can reduce the inter-aliquot/inter-sample variation in the form of DRCs within a larger dose range. (2) A common regional SGC can be established for the Jilantai area using the Re-SGC and least-squares normalisation (LS-SGC) methods, which provides reliable dating results within the 200 Gy De range.
摘要建立一个通用的标准化生长曲线(SGC)可以大大减少光激发发光(OSL)测年中等效剂量(De)测量的仪器时间。一些研究表明,不同的样品具有不同的剂量-反应曲线(DRCs),因此很难构建一个共同的SGC,尽管在某些情况下已经提出了SGC。本研究旨在利用冀兰台盆地不同沉积环境下100多个样品的沉积石英小等分,构建区域SGC,并探讨不同方法在该地区的适用性。比较了用SGC法获得的等分De值与用单等分再生法获得的等分De值的精度。结果表明:(1)采用再生正规化(Re-SGC)方法建立SGC时,选择合适的再正规化剂量,即接近特征饱和剂量的两倍(2D0),可以在较大的剂量范围内减少相同/样品间的dc变化。(2)利用Re-SGC和最小二乘归一化(LS-SGC)方法,可以在吉兰台地区建立一个共同的区域SGC,在200 Gy De范围内提供了可靠的测年结果。
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引用次数: 0
Schmidt hammer exposure dating for brick masonry 施米特锤曝光测定砖砌体的年代
IF 1.2 4区 地球科学 Q3 Earth and Planetary Sciences Pub Date : 2020-01-01 DOI: 10.2478/geochr-2020-0030
L. Debailleux
Abstract This research investigates the validity of the Schmidt hammer exposure dating (SHED) technique as a complementary means to date monuments according to the evaluation of the brick decay from masonry exposed to climatic conditions. The degree of surface weathering, I5 (%) is calculated as an indicator of the ageing effect and compared to the absolute age of the churches constructed between 1600 and 1795. This paper discusses the results obtained with such a method and the use of the technique within the framework of historical research. Tests were done on exterior church walls built between the 17th and 19th centuries. All the churches were located within the limited geographical area of Hainaut, in the south of Belgium. Results indicate that SHED provides encouraging results for buildings constructed between 1790 and 1895, with a linear correlation (R2>0.8) between surface weathering of brick façades and their ages. However, the weathering indices show high variability of values for the period 1750−1790, which may confirm that the variable qualities of bricks were in use during this period of time because of the different production techniques. As such, the results highlight the probable influence of the entire manufacturing and construction process and technical improvements in traditional brick-making.
摘要:本研究考察了施密特锤暴露测年(SHED)技术作为一种补充手段的有效性,根据砖石暴露在气候条件下的砖衰变的评估来确定纪念碑的年代。表面风化程度,I5(%)被计算为老化效应的指标,并与建于1600年至1795年之间的教堂的绝对年龄进行比较。本文在历史研究的框架内讨论了这种方法所获得的结果以及该技术的使用。测试是在17世纪到19世纪之间建造的教堂外墙上进行的。所有的教堂都位于比利时南部Hainaut有限的地理区域内。结果表明,SHED对1790 ~ 1895年间建造的建筑物提供了令人鼓舞的结果,砖砌体表面风化与它们的年龄呈线性相关(R2 >.8)。然而,风化指数显示1750 - 1790年间的数值变化很大,这可能证实了由于不同的生产技术,在这段时间内使用了不同质量的砖。因此,结果突出了整个制造和施工过程以及传统制砖技术改进的可能影响。
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引用次数: 1
Estimation of the durations of breaks in deposition – Speleothem case study 沉积中断持续时间的估计——Speleothem案例研究
IF 1.2 4区 地球科学 Q3 Earth and Planetary Sciences Pub Date : 2020-01-01 DOI: 10.2478/geochr-2020-0022
J. Pawlak, H. Hercman, P. Sierpień, P. Pruner, M. Gąsiorowski, A. Mihevc, N. Zupan Hajna, P. Bosák, M. Błaszczyk, B. Wach
Abstract Speleothems provide one of the most continuous terrestrial archives. However, due to changing conditions in temperature/humidity or the chemistry of percolating water, sedimentation breaks (hiatuses) and erosional events are possible and are commonly recorded in speleothems. Sedimentation breaks with durations longer than the resolution of the studied record should be considered in potential speleothem age-depth models. The most classic and reliable solution to the problem is the independent construction of age-depth models for the parts of speleothems separated by the hiatuses. However, in some cases, it is not possible to obtain a sufficient number of dating results for reliable age-depth model estimation. In such cases, the problem can be solved by the application of other sources of chronological information. Here, based on a few speleothem examples, an alternative approach – oxygen isotopic stratigraphy – is used to estimate the chronology for the parts of speleothems where there is not enough chronological information for classic age-depth models. As a result, the deposition break duration can be estimated.
摘要Speleothem提供了最连续的陆地档案之一。然而,由于温度/湿度或渗透水化学性质的变化,沉积中断(间断)和侵蚀事件是可能的,并且通常记录在洞穴中。在潜在洞穴年龄深度模型中,应考虑持续时间超过研究记录分辨率的沉积断裂。该问题最经典、最可靠的解决方案是独立构建由裂缝分隔的洞穴部分的年龄深度模型。然而,在某些情况下,不可能获得足够数量的测年结果来进行可靠的年龄深度模型估计。在这种情况下,可以通过应用其他按时间顺序排列的信息来源来解决这个问题。在这里,基于一些洞穴的例子,使用了一种替代方法——氧同位素地层学——来估计洞穴中没有足够的年代信息用于经典年龄深度模型的部分的年代。结果,可以估计沉积中断持续时间。
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引用次数: 2
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Geochronometria
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