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Direct material property determination: One‐dimensional formulation utilising full‐field deformation measurements 直接材料性能测定:利用全场变形测量的一维公式
IF 2.1 3区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2022-10-10 DOI: 10.1111/str.12427
Sreehari Rajan‐Kattil, M. Sutton, S. Sockalingam, F. Thomas, T. Weerasooriya, S. Alexander
A direct approach is described to determine the elastic modulus distribution in a nominally heterogeneous material subject to tensile/compression loading and primarily experiencing deformations in the axial direction. The formulation is developed for uniaxial applications using basic theoretical constructs, resulting in a computational framework that has a matrix form [A] {E} = {R}, where the [A] matrix components are known functions of measured axial strains and axial positions, {R} components are known functions of axial body forces, applied loads and reactions and {E} components are the unknown elastic moduli at discrete locations along the length of the specimen. For a series of one‐dimensional (1D) material property identification procedure with known axial strains at discrete locations and various levels of random noise, results are presented to demonstrate the accuracy and noise sensitivity of the methodology. Finally, experimental measurements for a heterogeneous bone specimen are compared to our 1D model predictions, demonstrating that the predictions are in very good agreement with independent estimates at each load level of interest along the length of the bone specimen.
描述了一种直接方法来确定承受拉伸/压缩载荷并主要经历轴向变形的标称非均质材料中的弹性模量分布。该公式是使用基本理论结构为单轴应用开发的,产生了矩阵形式[a]{E}的计算框架 = {R} ,其中[A]矩阵分量是测得的轴向应变和轴向位置的已知函数,{R}分量是轴向体力、施加的载荷和反作用力的已知函数;{E}分量是沿试样长度的离散位置处的未知弹性模量。对于一系列在离散位置具有已知轴向应变和不同水平随机噪声的一维(1D)材料特性识别程序,给出了结果,以证明该方法的准确性和噪声敏感性。最后,将异质性骨样本的实验测量值与我们的1D模型预测值进行了比较,表明这些预测值与沿着骨样本长度的每个感兴趣的载荷水平下的独立估计值非常一致。
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引用次数: 1
Image correlation technique for strain measurement of polycrystalline microstructures 多晶微结构应变测量的图像相关技术
IF 2.1 3区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2022-10-07 DOI: 10.1111/str.12428
Youssef A. F. Hafiz, Z. Stachurski, S. Kalyanasundaram
An image processing technique is proposed to measure the deformation of polycrystalline materials based on correlating the grains in reference and deformed SEM images. The advantage of this technique compared to the conventional subset‐based Digital Image Correlation (DIC) is that it can be applied when speckle patterning is not efficient or when studying boundary‐related mechanics is the objective. The technique is based on correlating grains by defining their boundaries rather than just subsets of image pixels. It reveals the anisotropy inherent in the polycrystals since it allows the analysis to specify each grain separately without averaging the results. The technique is applied by detecting the approximate grain boundaries edges and then refining their location with high accuracy. The correlation is performed between points calculated from each grain in the reference and deformed images as a Point Set Registration (PSR) problem. Finally, the displacements and strains are calculated from the resulting transformation matrix. A benchmark problem was developed to discuss the error over a strain range of 0.02 to 0.2 and showed that the resulting strains are reasonably accurate. Also, an in situ experiment was conducted to demonstrate the implementation of the technique using a specimen with fine‐grained Zirconia polycrystals. The technique successfully revealed the crack tip plastic zone, and strain mismatch between grains.
提出了一种基于参考图像和变形扫描电镜图像晶粒关联的多晶材料变形图像处理技术。与传统的基于子集的数字图像相关(DIC)技术相比,该技术的优势在于,它可以在散斑模式效率不高或以研究边界相关力学为目标时应用。该技术是基于通过定义颗粒边界来关联颗粒,而不仅仅是图像像素的子集。它揭示了多晶中固有的各向异性,因为它允许分析单独指定每个晶粒而不平均结果。该技术通过检测近似晶界边缘,然后高精度地细化其定位。作为点集配准(PSR)问题,从参考图像中的每个颗粒计算出的点与变形图像之间进行相关性。最后,根据得到的变换矩阵计算位移和应变。开发了一个基准问题来讨论在0.02到0.2应变范围内的误差,并表明得到的应变是相当准确的。此外,还进行了原位实验,利用细粒度氧化锆多晶样品来演示该技术的实现。该技术成功地揭示了裂纹尖端的塑性区和晶粒间的应变失配。
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引用次数: 2
Issue Information 问题信息
IF 2.1 3区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2022-09-01 DOI: 10.1002/vetr.966
No abstract is available for this article.
这篇文章没有摘要。
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引用次数: 0
Testing methodologies for the calibration of advanced plasticity models for sheet metals: A review 金属板材高级塑性模型校准的试验方法:综述
IF 2.1 3区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2022-07-19 DOI: 10.1111/str.12426
M. Rossi, A. Lattanzi, L. Morichelli, J. M. P. Martins, S. Thuillier, A. Andrade-Campos, S. Coppieters
Numerical simulations have become essential in engineering and manufacturing processes involving plasticity. The reliability and effectiveness of the simulations depend strongly on the accuracy of the adopted constitutive model. Accordingly, in recent years, an increasing interest is pointed towards experimental procedures and characterization methods that can be used to identify the constitutive parameters of advanced plasticity models, which allow to simulate properly the plastic behaviour of complex materials like, for instance, high strength steel. This paper provides a thorough review of the current state‐of‐the‐art, looking at both academia and industry. The available methodologies can be subdivided in two main areas: quasi‐homogeneous material tests with analytical or numerical post‐treatment of the experimental data and heterogeneous tests coupled with inverse methods for parameter identification. For each method, a brief description and references to norms and articles is provided, illustrating the advantages and the disadvantages.
数值模拟在涉及塑性的工程和制造过程中变得至关重要。模拟的可靠性和有效性在很大程度上取决于所采用的本构模型的准确性。因此,近年来,人们对实验程序和表征方法越来越感兴趣,这些方法可用于识别先进塑性模型的本构参数,从而能够正确模拟复杂材料(如高强度钢)的塑性行为。本文从学术界和工业界的角度对当前的技术状况进行了全面的回顾。可用的方法可细分为两个主要领域:对实验数据进行分析或数值后处理的准均质材料试验和与参数识别逆方法相结合的非均质试验。对于每种方法,都提供了对规范和文章的简要描述和参考,说明了其优点和缺点。
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引用次数: 9
Local strain distribution imaging using terahertz time‐domain spectroscopy 利用太赫兹时域光谱进行局部应变分布成像
IF 2.1 3区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2022-06-27 DOI: 10.1111/str.12425
Luis M. Reig Buades, S. Karmarkar, A. Dhiman, V. Tomar
In this work, terahertz time‐domain spectroscopy (THz TDS) was applied to monitor strain distribution as a function of mechanical loading through a passive composite sensor. The composite sensor was made up of strontium titanate (STO) particles. Strain distribution was measured by analysing the change in THz pulse amplitude while it passes through the composite sensor. The change in THz pulse amplitude is related to change in dielectric permittivity. The change in dielectric permittivity induced in the STO composite layer due to deformation leads to a change in the time of arrival (ToA) of the electromagnetic pulse (EMP) in THz band. This change in the sub‐millimetre domain is correlated to the strain and can be mapped for reproducing strain distribution around different geometries. The measurements of strain mapping are compared with finite element simulations and digital image correlation (DIC) measurements, showing similar strain contours.
在这项工作中,太赫兹时域光谱(THz TDS)通过被动复合传感器应用于监测应变分布作为机械载荷的函数。该复合传感器由钛酸锶(STO)颗粒组成。通过分析太赫兹脉冲通过复合传感器时振幅的变化来测量应变分布。太赫兹脉冲幅度的变化与介电常数的变化有关。在STO复合材料层中,由于变形引起介电常数的变化,导致电磁脉冲在太赫兹波段的到达时间(ToA)发生变化。亚毫米域的这种变化与应变相关,可以通过映射来再现不同几何形状周围的应变分布。将应变映射测量结果与有限元模拟和数字图像相关(DIC)测量结果进行了比较,得到了相似的应变轮廓。
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引用次数: 0
Evaluation of image registration for measuring deformation fields in soft tissue mechanics 软组织力学形变场测量中图像配准的评价
IF 2.1 3区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2022-06-15 DOI: 10.1111/str.12424
O. Lisický, S. Avril, Bastien Eydan, B. Pierrat, J. Burša
High‐fidelity biomechanical models usually involve the mechanical characterisation of biological tissues using experimental methods based on optical measurements. In most experiments, strains are evaluated based on displacements of a few markers and represents an average within the region of interest (ROI). Full‐field measurements may improve description of non‐homogeneous materials such as soft tissues. The approach based on non‐rigid image registration is proposed and compared with standard digital image correlation (DIC) on a set of samples, including (i) complex heterogeneous deformations with sub‐pixel displacement, (ii) a typical uniaxial tension test of aorta, and (iii) an indentation test on skin. The possibility to extend the ROI to the whole sample and the exploitation of a natural tissue pattern represents the main assets of the proposed method whereas the results show similar accuracy as standard DIC when analysing sub‐pixel deformations. Therefore, displacement and strain fields measurement based on image registration is very promising to characterise heterogeneous specimens with irregular shapes and/or small dimensions, which are typical features of soft biological tissues.
高保真生物力学模型通常涉及使用基于光学测量的实验方法对生物组织进行机械表征。在大多数实验中,应变是基于几个标记的位移来评估的,并且表示感兴趣区域(ROI)内的平均值。全场测量可以改善对非均质材料(如软组织)的描述。提出了基于非刚性图像配准的方法,并将其与一组样本上的标准数字图像相关(DIC)进行了比较,包括(i)具有亚像素位移的复杂非均匀变形,(ii)主动脉的典型单轴拉伸试验,以及(iii)皮肤压痕试验。将ROI扩展到整个样本和利用自然组织模式的可能性代表了所提出方法的主要资产,而在分析亚像素变形时,结果显示出与标准DIC相似的准确性。因此,基于图像配准的位移场和应变场测量非常有希望表征具有不规则形状和/或小尺寸的异质试样,这是软生物组织的典型特征。
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引用次数: 0
Measuring representative volume elements from high‐resolution grain‐scale strain fields 测量来自高分辨率晶粒尺度应变场的代表性体积元素
IF 2.1 3区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2022-06-02 DOI: 10.1111/str.12423
Renato B. Vieira, J. Lambros
Most crystalline materials present a highly heterogeneous response at the microscale, which can be affected by both internal factors (such as microstructural parameters) and external factors (such as loading). Relating microscale inhomogeneities to the macroscale response of a material requires the use of homogenisation techniques, usually based on the concept of a representative volume element (RVE)—the smallest volume of material that represents the global average response. In this work, we present a new and robust experimental method of measuring the size of a strain‐based RVE from high‐resolution grain‐scale strain fields obtained using digital image correlation (DIC). The proposed method is based on the statistical (stereological) nature of the RVE, which has been widely adopted in numerical studies, and involves dividing a strain field into randomly selected regions of varying sizes and statistically analysing the distributions of average strains within them. To validate the new method, we generate a large number of synthetic strain fields from a fractional Gaussian noise algorithm. The proposed stereological method is shown to be capable of producing reliable RVE measurements from a very large range of possible microscale strain fields while at the same time being robust in that it can produce RVE measurement results even in cases where other existing methods may be unable to do so. The proposed method has a low field‐of‐view requirement, only needing a field‐of‐view about 1.2 times as large as the RVE to produce reliable measurements. In addition, the stereological method offers significant flexibility since its statistical nature allows for control over how strict the RVE measurement should be in each case.
大多数晶体材料在微观尺度上表现出高度不均匀的响应,这可能受到内部因素(如微观结构参数)和外部因素(如负载)的影响。将微观尺度的不均匀性与材料的宏观尺度响应联系起来需要使用均匀化技术,通常基于代表性体积元素(RVE)的概念——代表全球平均响应的最小体积材料。在这项工作中,我们提出了一种新的、稳健的实验方法,从使用数字图像相关(DIC)获得的高分辨率晶粒尺度应变场中测量基于应变的RVE的大小。所提出的方法基于RVE的统计学(体视学)性质,该性质已在数值研究中广泛采用,包括将应变场划分为随机选择的不同大小的区域,并统计分析其中平均应变的分布。为了验证新方法,我们从分数高斯噪声算法中生成了大量的合成应变场。所提出的体视学方法被证明能够从很大范围的可能微尺度应变场中产生可靠的RVE测量结果,同时具有鲁棒性,因为即使在其他现有方法可能无法做到这一点的情况下,它也可以产生RVE测量结果,只需要一个大约是RVE 1.2倍大的视场就可以进行可靠的测量。此外,体视学方法提供了显著的灵活性,因为其统计性质允许控制在每种情况下RVE测量的严格程度。
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引用次数: 0
A generic topography reconstruction method based on multi‐detector backscattered electron images 一种基于多探测器背散射电子图像的通用地形重建方法
IF 2.1 3区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2022-05-29 DOI: 10.1111/str.12416
J. Neggers, E. Héripré, M. Bonnet, S. Hallais, S. Roux
Surface topographies can be reconstructed from backscattered electron (BSE) images captured from different detector orientations. This article presents a very general approach to this problem, in the spirit of photometric stereo methods, allowing for arbitrary BSE detector number (at least 3) and shapes. The general idea is to both determine the (non‐linear) model parameters and compute the surface topography so that the modelled images match at best the acquired ones. Three samples are used for validation of the measured topography with respect to atomic force microscopy (AFM) measurements. Root mean square (RMS) errors in the range of 10–35 nm, or 1–1.5% of total sampleheight, are obtained.
从不同的探测器方向捕获的背散射电子(BSE)图像可以重建表面形貌。本文提出了一个非常通用的方法来解决这个问题,在光度立体方法的精神,允许任意的BSE探测器数量(至少3)和形状。总体思路是确定(非线性)模型参数并计算表面形貌,以便建模图像最好与获取的图像匹配。三个样品用于验证测量形貌与原子力显微镜(AFM)测量。均方根误差(RMS)在10-35 nm范围内,或样品总高度的1-1.5%。
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引用次数: 0
Combined thermographic phosphor and digital image correlation (TP + DIC) for simultaneous temperature and strain measurements 用于同时测量温度和应变的热成像磷光体和数字图像相关(TP+DIC)组合
IF 2.1 3区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2022-05-17 DOI: 10.1111/str.12415
E. Jones, Amanda Jones, C. Winters
Thermographic phosphors (TP) are combined with stereo digital image correlation (DIC) in a novel diagnostic, TP + DIC, to measure full‐field surface strains and temperatures simultaneously. The TP + DIC method is presented, including corrections for nonlinear CMOS camera detectors and generation of pixel‐wise calibration curves to relate the known temperature to the ratio of pixel intensities between two distinct wavelength bands. Additionally, DIC is employed not only for strain measurements but also for accurate image registration between the two cameras for the two‐colour ratio method approach of phosphoric thermography. TP + DIC is applied to characterize the thermo‐mechanical response of 304L stainless steel dog bones during tensile testing at different strain rates. The dog bones are patterned for DIC with Mg3F2GeO4:Mn (MFG) via aerosol deposition through a shadow mask. Temperatures up to 425°K (150°C) and strains up to 1.0 mm/mm are measured in the localized necking region, with conservative noise levels of 10°K and 0.01 mm/mm or less. Finally, TP + DIC is compared to the more established method of combining infrared (IR) thermography with DIC (IR + DIC), with results agreeing favourably. Three topics of continued research are identified, including cracking of the aerosol‐deposited phosphor DIC features, incomplete illumination for pixels on the border of the phosphor features, and phosphor emission evolution as a function of applied substrate strain. This work demonstrates the combination of phosphor thermography and DIC and lays the foundation for further development of TP + DIC for testing in combined thermo‐mechancial environments.
热成像磷光体(TP)与立体数字图像相关(DIC)结合在一种新的诊断方法TP+DIC中,以同时测量全场表面应变和温度。提出了TP+DIC方法,包括对非线性CMOS相机检测器的校正,以及生成像素校准曲线,以将已知温度与两个不同波段之间的像素强度比联系起来。此外,DIC不仅用于应变测量,还用于磷酸热成像的双色比方法的两台相机之间的精确图像配准。TP+DIC用于表征304L不锈钢狗骨在不同应变速率下拉伸试验过程中的热机械响应。通过荫罩的气溶胶沉积,用Mg3F2GeO4:Mn(MFG)对狗骨头进行DIC图案化。温度高达425°K(150°C),应变高达1.0 mm/mm是在局部颈缩区域测量的,保守噪声水平为10°K和0.01 mm/mm或更小。最后,将TP+DIC与更成熟的将红外(IR)热成像与DIC(IR+DIC)相结合的方法进行了比较,结果一致。确定了三个持续研究的主题,包括气溶胶沉积的磷光体DIC特征的破裂、磷光体特征边界上像素的不完全照明,以及作为施加的衬底应变的函数的磷光体发射演化。这项工作展示了磷光体热成像和DIC的结合,并为进一步开发TP+DIC在热-机械复合环境中的测试奠定了基础。
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引用次数: 3
Microscale deformation mechanisms in paperboard during continuous tensile loading and 4D synchrotron X‐ray tomography 纸板在连续拉伸加载过程中的微观变形机制和4D同步加速器X射线断层扫描
IF 2.1 3区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2022-04-13 DOI: 10.1111/str.12414
S. Johansson, J. Engqvist, J. Tryding, S. A. Hall
A better physical understanding of mesoscale and microscale mechanisms behind deformation and failure of paperboard material is important to optimize industrial packaging converting processes and decrease waste. In this study, these mechanisms were investigated using synchrotron X‐ray tomography during in situ continuous uniaxial tensile loading. High spatial and temporal data resolution enabled quantification of rapid changes in the material occurring before, during and after material failure. The evolution of 3D strain fields, fibre orientations and sample thickness showed that deformation and failure mechanisms differ significantly between samples tested in machine direction (MD), cross direction (CD) and 45° from the loading direction. In 45° and CD, gradual failure processes could be followed across several load steps. Immediately after failure, the in‐plane fracture region was significantly larger in both 45° and CD compared to MD. Both fracture characteristics and strain field distributions differed between the three material directions. Significant fibre reorientation was an active deformation mechanism in 45° already from the beginning of the loading, also present in CD after peak load but absent in MD. The MD‐dependent mechanisms interpreted and quantified at the scale of the fibre network in this study can help guide model development and likely have wider applicability to other paper‐based materials.
更好地了解纸板材料变形和失效背后的中尺度和微观机制,对于优化工业包装转化过程和减少浪费非常重要。在本研究中,使用同步加速器X射线断层扫描在原位连续单轴拉伸加载过程中研究了这些机制。高的空间和时间数据分辨率能够量化材料失效之前、期间和之后发生的材料快速变化。三维应变场、纤维取向和样品厚度的演变表明,在机器方向(MD)、横向(CD)和与加载方向成45°测试的样品之间,变形和失效机制存在显著差异。在45°和CD中,可以在几个加载步骤中遵循逐渐失效过程。失效后,与MD相比,45°和CD的平面内断裂区域明显更大。三个材料方向之间的断裂特征和应变场分布都不同。从加载开始,显著的纤维重新定向就已经是45°的一种主动变形机制,在峰值加载后的CD中也存在,但在MD中不存在。本研究中在纤维网络规模上解释和量化的MD相关机制有助于指导模型开发,并可能对其他纸基材料具有更广泛的适用性。
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引用次数: 5
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Strain
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