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Stilbenes from Stems of Primorsky Grape Variety Alpha and their Antioxidant Activity Primorsky 葡萄品种 Alpha 茎中的芪及其抗氧化活性
IF 0.8 4区 化学 Q4 CHEMISTRY, MEDICINAL Pub Date : 2024-08-06 DOI: 10.1007/s10600-024-04414-3
S. A. Fedoreyev, N. P. Mishchenko, D. V. Tarbeeva, E. A. Vasileva, N. D. Pokhilo, V. P. Grigorchuk, A. N. Emelyanov
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引用次数: 0
New Chalcone Derivative from Persea americana and Its Anti-Tyrosinase Activity 来自 Persea americana 的新查尔酮衍生物及其抗酪氨酸酶活性
IF 0.8 4区 化学 Q4 CHEMISTRY, MEDICINAL Pub Date : 2024-08-06 DOI: 10.1007/s10600-024-04399-z
Parinuch Chumkaew, Saysunee Jumrat, Yutthapong Pianroj

Caneeracone A (1), a new chalcone derivative, together with three known compounds (2–4), was isolated from the seeds of Persea americana Mill. (buccaneer avocado). The structures of these compounds were established by spectroscopic methods including 1D and 2D NMR experiments. Compound 1 exhibited a potent tyrosinase activity with an IC50 of 38.29 μM.

从 Persea americana Mill.的种子中分离出了一种新的查尔酮衍生物 Caneeracone A(1)以及三种已知化合物(2-4)。(牛油果)的种子中分离出来。这些化合物的结构是通过光谱方法(包括一维和二维核磁共振实验)确定的。化合物 1 具有很强的酪氨酸酶活性,其 IC50 值为 38.29 μM。
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引用次数: 0
Antiliver and Colorectal Cancer Activity Metabolites of the Leaves of Michelia crassipes 苁蓉叶中的抗逆转录酶和大肠癌活性代谢物
IF 0.8 4区 化学 Q4 CHEMISTRY, MEDICINAL Pub Date : 2024-08-06 DOI: 10.1007/s10600-024-04428-x
S. J. Wang, Y. Z. Dong, S. T. Huang, W. J. Li, H. T. Li, S. L. Liu, C. H. Chuang, C. Y. Chen
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引用次数: 0
(±)-Mucroniferal D: a Pair of New Phenolic Enantiomers from Corydalis mucronifera (±)-Mucroniferal D:来自堇菜的一对新酚类对映体
IF 0.8 4区 化学 Q4 CHEMISTRY, MEDICINAL Pub Date : 2024-08-06 DOI: 10.1007/s10600-024-04401-8
Xupei Men, Jie Song, Xiaomei Song, Xiangdong Qin, Du-Qiang Luo, Jun Zhang

Chemical investigation of Corydalis mucronifera has resulted in the isolation and identification of a pair of new enantiomeric phenolic constituents (±)-mucroniferal D (1) and five known ones (2–6). Their structures were elucidated based on extensive spectroscopic data analysis of MS, 1D and 2D NMR, and their absolute configurations were confirmed by comparison of the optical rotation data. Compounds 1–6 showed moderate cytotoxic activities against MCF-7, MGC-803, and HeLa cell lines with the IC50 values ranging from 22.61–98.30 μg·mL–1.

对 Corydalis mucronifera 进行化学研究的结果是,分离和鉴定了一对新的对映体酚类成分 (±)-mucroniferal D (1) 和五种已知的对映体酚类成分 (2-6)。根据质谱、一维和二维核磁共振的大量光谱数据分析,阐明了它们的结构,并通过比较旋光数据确认了它们的绝对构型。化合物 1-6 对 MCF-7、MGC-803 和 HeLa 细胞株表现出中等程度的细胞毒性活性,IC50 值范围为 22.61-98.30 μg-mL-1。
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引用次数: 0
Preparation and Physicochemical Properties of Collagen for Wound Dressings 用于伤口敷料的胶原蛋白的制备和理化特性
IF 0.8 4区 化学 Q4 CHEMISTRY, MEDICINAL Pub Date : 2024-08-06 DOI: 10.1007/s10600-024-04412-5
N. E. Tseomashko, A. N. Tretyakova, A. Yu. Vasil′kov

Type I collagen was obtained in gel-like form by enzymatic-acidic extraction from cattle tail tendons and was polymerized at room temperature in ammonia vapor to form a transparent film 60.47–64.9 μm thick with good adhesive properties of 11.6–12.4 kPa and tensile strength 559.5–600.5 kPa. The dependence of the film adhesive properties on its ability to stimulate regenerative processes in tissues was found. The collagen was characterized by X-ray photoelectron spectroscopy. The C 1s spectrum showed peaks for C–C/C–H, C–O–C/C–OH, O=C–N, and O=C–OH groups; the N 1s spectrum for C–NH2, O=C–N, and C–NH3+ groups.

通过酶酸提取法从牛尾肌腱中获得凝胶状的 I 型胶原蛋白,并在室温下在氨蒸气中聚合,形成厚度为 60.47-64.9 μm 的透明薄膜,该薄膜具有良好的粘合性能(11.6-12.4 kPa)和拉伸强度(559.5-600.5 kPa)。研究发现,薄膜的粘合性能取决于其刺激组织再生过程的能力。X 射线光电子能谱对胶原蛋白进行了表征。C 1s 光谱显示了 C-C/C-H、C-O-C/C-OH、O=C-N 和 O=C-OH 基团的峰值;N 1s 光谱显示了 C-NH2、O=C-N 和 C-NH3+ 基团的峰值。
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引用次数: 0
2-Oxomethylcytisine Derivatives with Potential Anti-Coronavirus Activity 具有潜在抗冠状病毒活性的 2-氧甲基胞嘧啶衍生物
IF 0.8 4区 化学 Q4 CHEMISTRY, MEDICINAL Pub Date : 2024-08-06 DOI: 10.1007/s10600-024-04411-6
A. V. Koval′skaya, A. N. Lobov, D. O. Tsypyshev, Ch.V. Lin, I. P. Tsypysheva

Diels−Alder β-endo adducts of 2-oxomethylcytisine and N-substituted maleimides were synthesized. Their ability to interact with the 6LU7 active site of SARS-CoV-2 main protease Mpro was evaluated in silico. The tested compounds included the potential anti-coronavirus agent (3aR,4S,8S,12S,12aS,12bR)-2-(3-methoxyphenyl)-10-methyl-3a,7,8,9,10,12b-hexahydro-1H-4,12a-etheno-8,12-methanopyrrolo[3′,4′:3,4]pyrido[1,2-a][1,5]diazocine-1,3,5,11(2H,4H,12H)-tetrone, which had calculated characteristics exceeding those of the reference ligand tideglusib.

合成了 2-oxomethylcytisine 和 N-取代马来酰亚胺的 Diels-Alder β-endo 加合物。对它们与 SARS-CoV-2 主要蛋白酶 Mpro 的 6LU7 活性位点相互作用的能力进行了硅学评估。测试的化合物包括潜在的抗冠状病毒剂 (3aR,4S,8S,12S,12aS,12bR)-2-(3-甲氧基苯基)-10-甲基-3a,7,8,9,10,12b-六氢-1H-4,12a-乙烯基-8,12-甲烷吡咯并[3′,4′:3,4]吡啶并[1,2-a][1,5]二佐辛-1,3,5,11(2H,4H,12H)-四酮,其计算特性超过了参考配体 tideglusib。
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引用次数: 0
A New Cyclic Peptide from Betel Nut Endophytic Fungus Alternaria sp. RW-AL 来自槟榔内生真菌 Alternaria sp.
IF 0.8 4区 化学 Q4 CHEMISTRY, MEDICINAL Pub Date : 2024-08-06 DOI: 10.1007/s10600-024-04413-4
Wu Ruan, Qing-Yun Ma, Jiao-Cen Guo, Qing-Yi Xie, Li Yang, Hao-Fu Dai, You-Geng Wu, You-Xing Zhao

A new cyclic peptide alternarin A (1), along with seven known compounds, alternariol (2), sulfated derivative of alternariol (3), alternariol methyl ether (4), altenuene (5), 2,5-dimethyl-7-hydroxychromone (6), diaporthein A (7), isopterocarpolone (8), were isolated from the betel nut endophytic fungus Alternaria sp. RW-AL. The structure of 1 was elucidated by 1D and 2D NMR spectra as well as HR-ESI-MS analysis. Compounds 1, 4, and 5 showed definite antibacterial activities against Staphylococcus aureus ATCC 6538 and Bacillus subtilis ATCC 6633.

从槟榔内生真菌 Alternaria sp. RW-AL 中分离出了一种新的环肽交替灵 A(1),以及七种已知化合物:交替醇(2)、交替醇硫酸化衍生物(3)、交替醇甲醚(4)、altenuene(5)、2,5-二甲基-7-羟基色酮(6)、二交替醇 A(7)、异交替醇(8)。通过一维和二维核磁共振光谱以及 HR-ESI-MS 分析,阐明了 1 的结构。化合物 1、4 和 5 对金黄色葡萄球菌 ATCC 6538 和枯草芽孢杆菌 ATCC 6633 具有明确的抗菌活性。
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引用次数: 0
Flavonoids with Leucopoeisis Activity from Extract of Astragalus bungeanus 黄芪提取物中具有白果活性的黄酮类化合物
IF 0.8 4区 化学 Q4 CHEMISTRY, MEDICINAL Pub Date : 2024-08-06 DOI: 10.1007/s10600-024-04425-0
N. Sh. Kavtaradze, M. Z. Getia
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引用次数: 0
Phenylpropanoids with Anti-Inflammatory Effects from the Roots of Platycodon grandiflorus 桔梗根中具有抗炎作用的苯丙酸类化合物
IF 0.8 4区 化学 Q4 CHEMISTRY, MEDICINAL Pub Date : 2024-08-06 DOI: 10.1007/s10600-024-04402-7
Yang Yu, Lan Ding, Ren-Nai Yang, Liang-Ping Zha, Ju-Tao Wang, Shuang-Ying Gui

Two new phenylpropanoids, plagnans (1) and plaganoid (2), along with five known phenylpropanoids, including an enantiomeric mixture (compound 3) were isolated from the roots of Platycodon grandiflorus. Meanwhile, their structures were elucidated by analyzing the spectroscopic data, including NMR, HR-ESI-MS, ECD (ICD), and X-ray analysis. Although all isolates were evaluated for their anti-inflammatory activities, and of them exhibited moderate activities, with IC50 values of around 27.5 μM.

研究人员从桔梗的根中分离出了两种新的苯丙酮类化合物:plagnans (1) 和 plaganoid (2),以及五种已知的苯丙酮类化合物,包括一种对映体混合物(化合物 3)。同时,通过分析光谱数据(包括 NMR、HR-ESI-MS、ECD(ICD)和 X 射线分析)阐明了它们的结构。尽管对所有分离物进行了抗炎活性评估,但它们都表现出中等活性,IC50 值约为 27.5 μM。
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引用次数: 0
Metabolites from Michelia compressa var. lanyuensis with Antioxidant Activity 具有抗氧化活性的扁柏变种代谢物
IF 0.8 4区 化学 Q4 CHEMISTRY, MEDICINAL Pub Date : 2024-08-06 DOI: 10.1007/s10600-024-04418-z
C. T. Chang, W. J. Li, H. T. Li, S. L. Liu, C. Y. Chen
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引用次数: 0
期刊
Chemistry of Natural Compounds
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