Quaternary Geochronology最新文献

The Shandong Peninsula along the coastal Bohai Sea in China is a vast alluvial plain formed by the Yellow River. It is an ideal place for investigating the evolution of landform in a river–sea interaction area where chronology is key. However, detailed optically stimulated luminescence (OSL) chronology studies of cores are still limited and have mainly concentrated on the Yellow River Delta, while they are scarce on the south coast of the Bohai Sea. In this study 16 OSL samples were collected from the upper 32 m of core DZK01 (192 m in depth) to establish a chronological framework using quartz OSL. Results indicated that the quartz OSL ages ranged from 217 ± 19 ka to 1.63 ± 0.14 ka, and we believe they were the minimum ages when D_e > ca. 200 Gy owing to OSL signal saturation. Our dating results reveal two sedimentary hiatuses with age gaps of 71–37 ka and 37–9.5 ka. Holocene sediments are located above a depth of 11.8 m with an onset age of approximately 9.5 ± 0.6 ka. Based on the sedimentary facies and dating results, no transgression sediment has been observed during marine isotopic stage (MIS) 3. This sedimentary sequence pattern is consistent with global sea-level change. We also summarized the extents of three transgressions around the Bohai Sea, and found very different patterns for different part of the coasts, e.g., in the north, the west, and the south. This requires further investigation.

We present new K–Ar ages extending the volcanic history of Mauritius Island towards the Holocene. Mauritius volcanism is associated with the activity of the Réunion hotspot, the magmatism of which produced the Deccan Traps across the Cretaceous-Tertiary (KT) boundary and continues up to present on Réunion Island. After shield building from before 8.9 Ma to 4.7 Ma, Mauritius Island underwent an unusual volcanic evolution involving two rejuvenation stages (3.5–1.9 Ma and <0.7 Ma) separated by a 1.2 Myr hiatus. The lower bound of the second rejuvenation stage being poorly constrained, it is not clear whether volcanism in this island has come to a rest. Given the occurrence of uneroded, and yet undated strombolian cones in Mauritius, it is important to better constrain the latest activity of this island in order to assess its volcanic hazard. The importance of dating the end of this stage is also enhanced by the fact that most of the surface of Mauritius is covered by the lavas of the rejuvenation stages, hence indicating a recent volcanic activity that needs to be better characterized for risk assessment.

We focus here on the last 150 ka interval which lacked precise age controls with only a few whole-rock and groundmass ⁴⁰Ar/³⁹Ar plateau ages available (Moore et al., 2011), ranging from 138 ± 29 to 40 ± 48 ka (uncertainties are 1 $\sigma$). Our six new Cassignol-Gillot unspiked K–Ar ages obtained on plagioclase or groundmass range from 113 ± 7 to 14 ± 3 ka, with much lower uncertainties than previous ages available. Our major and trace element analyses of the dated samples highlight the compositional homogeneity of the lavas erupted in the last rejuvenation stage, showing no geochemical evolution.

Our results, with ages as young as 14 ± 3 ka, demonstrate that near-Holocene volcanism is present in Mauritius Island, with no evidence of fading magmatism in the last 150 ka. Our second youngest age at 44 ± 5 ka implies that the latest activity occurred after a ∼30 kyr repose interval, with the consequence that Mauritius volcanism may resume at any time.

The Rodderberg Volcanic Complex (RVC) is well-known for the long climate record archived in its crater basin, which lasts for several glacial-interglacial cycles. However, a detailed chronological framework is still lacking. Here, we perform high-resolution luminescence dating on a 72.8 m-long sediment core with the optically stimulated luminescence (OSL) signal from fine-grained (4–11 μm) quartz and three kinds of post-infrared infrared (pIRIR) stimulated luminescence signals from fine-grained polymineral fractions. Together with magnetic susceptibility, grain size and quartz OSL sensitivity measurements, a numerical age framework is built for the upper half of the sediment core. Quartz OSL ages align well with pIRIR ages for the last 45 ka, but they underestimate in relation to pIRIR ages for ages beyond 45 ka. The three pIRIR signals, including the pIRIR signal at 225 °C (pIRIR₂₂₅), the pulsed pIRIR signal at 150 °C (pulsed pIRIR₁₅₀) and the multi-elevated-temperature pIRIR at 250 °C (MET-pIRIR₂₅₀), yield consistent ages up to ca. 250 ka at a sediment depth of 37.5 m. Below that depth, dating limits of the protocols are reached. Nevertheless, our results indicate that sediments below 37.5 m predate Marine Isotope Stage (MIS) 7. Altogether, obtained ages reveal continuous dust accumulation during MIS 7 and MIS 6. One erosional event happened at the end of the Eemian (MIS 5e), which eroded the Eemian soil. The sedimentation rate during the Weichselian glacial period is tenfold lower compared to the sedimentation rate observed during MIS 7–6. This low sedimentation rate likely arises from the cessation of slope wash effects and the occurrence of various wind erosional events alternating with dust deposition as the basin is filled by dust. A notably high sedimentation rate is observed at the transition from MIS 6 to the Eemian, marked by the deposition of a 7 m-thick loess layer between 135 and 129 (±5) ka. This high sedimentation rate could be attributed to intensified slope wash and solifluction processes resulting from the thawing of permafrost at the time of deglaciation. Alternatively, it might be a signature of Heinrich event 11, during which strong winds brought large amounts of dust into the basin within a short time.

Optically stimulated luminescence (OSL) dating of quartz using the single-aliquot regenerative-dose (SAR) procedure requires construction of dose-response curves (DRCs). The shapes of DRCs and their characteristic saturation doses (D₀ values) are well-known to be highly variable between samples and among individual grains from the same sample, but the factors that control DRC characteristics are imperfectly understood. Here we report correlations between OSL DRC shapes and thermoluminescence (TL) glow curve characteristics for a sample of quartz from northern Australia. Individual grains were measured using the SAR procedure and one of two preheat temperatures (160 °C and 260 °C), and grouped according to similarities in their DRC shapes. Grains from each DRC group were then physically transferred onto a separate disc for TL measurement as a multi-grain aliquot. A strong correlation was observed between DRC group and laboratory-irradiated TL glow curve shapes, along with some differences between the two preheats. Irrespective of the selected preheat, earlier saturating DRC groups are associated with the most intense 110 °C TL signal, and the least intense 325 °C TL signal, which corresponds to the main OSL trap. Later saturating DRC groups generally show the opposite trend. There are also trends within other regions of the glow curve and DRC group, such as prominent TL responses at 140–160 °C, 220–240 °C and 390–410 °C. We assessed the effect on the accuracy of equivalent dose (D_e) estimation using an associated radiocarbon age as an independent cross-check of the OSL ages for the DRC groups. D_e over- and under-estimates were obtained for some DRC groups. Most notably, grains preheated to 160 °C displayed a pattern of D_e values which decreased with an increase in D₀. We relate this to variable concentrations of charge at the ∼230 °C TL trap prior to regenerative dose OSL measurements. OSL ages for most DRC groups preheated to 260 °C are close to the radiocarbon age, as are those of later saturating DRC groups preheated to 160 °C; the latter DRC groups have the smallest TL signals at ∼230 °C relative to the TL peak at 325 °C. The results of this study suggest that correlations between single-grain D_e and D₀ values can occur due to underlying differences in the TL characteristics of grains with different DRC shapes. In the absence of independent age control and prior to measuring multi-grain aliquots of quartz, we recommend that OSL dating practitioners screen their samples for any single-grain patterns of D_e as a function of DRC shape, to determine the optimal SAR measurement conditions and data-analysis procedures for D_e estimation.

Nebkhas, a unique type of biogeomorphological aeolian landforms formed by sand accumulation around plants, are widely distributed in arid and semi-arid regions globally. Previous studies have highlighted the potential of nebkha sediments as valuable archives for understanding past climate and environmental changes. However, establishing a reliable chronological framework for nebkha sediments has posed challenges due to the lack of suitable dating methods. In this study, we applied both the quartz OSL and K-feldspar pIRIR₁₅₀ protocols to date nebkha sediments from three different sites within the Mu Us dune field in north-central China. Internal checks indicate that the quartz OSL protocol is suitable for equivalent dose measurements, though age determinations for some quartz samples with weak luminescence signals may be subject to uncertainties. K-feldspar exhibits brighter signal intensity and a higher signal-to-noise ratio, making K-feldspar pIRIR₁₅₀ ages reliable, particularly when residual doses are low, luminescence signals are stable, and dose recovery ratios are satisfactory. The results indicate that the luminescence ages derived from both the quartz OSL and K-feldspar pIRIR₁₅₀ protocols are comparable, and these ages align with stratigraphic sequences and independent ¹³⁷Cs dating results. Based on the established chronologies, our findings suggest that some large nebkhas in the southwestern Mu Us dune field likely originated 100–200 years ago, possibly in response to either climate-driven or human-induced aridification in this region.

Accurately dating of eruptive events is crucial for understanding the eruptive history of a volcano. The optically stimulated luminescence (OSL) dating technique has been widely used in the geochronological studies of volcanic eruption events. However, its application is challenging due to the complex components of OSL signals in which the unstable medium component often results in age underestimation for quartz related to volcanic activity. In this study, we investigated the quartz OSL properties from a lava-baked sediment layer from the Tengchong volcanic field, southwest China. The results indicated that the initial OSL signal of the lava-baked quartz was primarily dominated by the medium component, which exhibited small Fast Ratio values (<10). The equivalent dose (D_e) values showed a negative correlation with recuperation, and the D_e-t plot concurrently showed a decreasing trend. Pulse-annealing tests confirmed the medium component in the initial OSL signal to be thermally unstable, hence resulting in age underestimation. Consequently, the early background subtraction method and another two correction strategies were employed to derive D_e values from the more stable fast component: Ⅰ) fitting the D_e-t plot, and Ⅱ) fitting the D_e-recuperation plot. The study found that D_e values could only be partially corrected using the early background subtraction method. In contrast, the latter two methods allowed for successful correction. The corrected quartz OSL ages agree well with independent MET-pIRIR ages of potassium feldspar and ¹⁴C ages. The reliable chronological results suggest that the Dayingshan volcano erupted approximately 41–45 thousand years ago.

In radioisotope dating, statistical fluctuations of atom counts or decay counts can sometimes lead to unphysical results, such as negative counts after subtracting the background or negative apparent ages near the boundaries of the dating range. How to treat these boundary cases with a unified approach and give proper estimates on age limits and confidence intervals is an important issue in radioisotope dating. In this work, we combine the Feldman-Cousins likelihood-ratio ordering method for interval estimation, a Frequentist approach to make consistent transitions from the choice of one-sided limits to two-sided confidence intervals, and a Bayesian method to treat the background uncertainties. This data treatment method naturally eliminates the unphysical results. We use ⁸¹Kr dating and Atom Trap Trace Analysis as an example to illustrate the advantages. This method can be generalized to other radioisotopes and ultra-sensitive analysis techniques.

Given its high accumulation rate in sediments, the endorheic basin in arid regions plays a crucial role in reconstructing paleo-environment. However, it would not provide high-resolution climatic records if significant wind-eroded depositional hiatuses were inevitable within a severe wind environment. Unconformable contacts have been found during field survey in the top part of the stratigraphy in the Qaidam Basin, a prototypical endorheic basin in central Asia. To elucidate whether the sediment is continuous, we employed luminescence dating methods of feldspar pIR₂₀₀IR₂₅₀ and quartz OSL to date sediments, including lacustrine sediments and salt crusts, from the Qarhan Playa that is the Quaternary depositional center of the Qaidam Basin. Various experiment tests, including preheat plateau, dose recovery, and residual dose, were conducted. The dating results show that the feldspar pIR₂₀₀IR₂₅₀ can provide dependable ages with negligible residual doses. The pIR₂₀₀IR₂₅₀ dating ages within the last glacial cycle reveal several environmental shifts. A Qarhan paleolake in Marine Isotope Stage (MIS) 5 was demonstrated by the cluster ages of ∼140–80 ka of lacustrine sediments. The salt crust ages of 136 ± 10 ka and 97 ± 6 ka indicate that, before completely disappeared, the paleolake with shallow dish-shape depression had been dried up more than once, illustrating “shallow——dry——shallow” cycles. The playa in the eastern Qaidam Basin evolved mainly in warm periods, such as MIS 5 and MIS 1, supported by the salt crust ages of MIS 5 (136 ± 10 ka and 97 ± 6 ka) and MIS 1 (10 ± 1 ka and 0.6 ± 0.1 ka). Depositional hiatus in the last glacial cycle were identified by unconformable contacts in three sections between the lacustrine strata and their overlying playa strata, with corresponding age gaps of 158 ± 20–97 ± 6 ka, 131 ± 10–10 ± 1 ka, and 84 ± 7–0.6 ± 0.1 ka, respectively. In all the three sections the sediments for the whole of the last glacial period is missing, eroded by wind. This process should have occurred periodically during the glacial-interglacial cycles of the orbital global climatic changes. The results also show that hiatuses are common for endorheic basins on the Earth with age gaps of up to ∼100 ka, suggesting that robust chronology should be established before any climatic correlation due to severe wind erosion leading to episodic sediment accumulation.

Unrevealing the stratigraphy of volcanic systems is fundamental to understanding their eruptive history and requires a multiproxy approach for the accurate correlation and interpretation of deposits. We present new volcanological, ⁴⁰Ar/³⁹Ar ages and paleomagnetic data from the volcanic rocks of Trindade Island, located at ∼1.260 km from the Brazilian coast in the South Atlantic Ocean. The reconstruction of the volcanic history of Trindade Island is important because it is the youngest volcanic terrain in Brazil and part of a submarine chain that represents the most recent plume-induced alkaline manifestation beneath the South American plate. Our results suggest Trindade Island underwent two main phases of volcanism. The first phase (3.9–1.5 Ma) formed the Trindade Complex and Desejado Formation, with eruptive styles ranging from phreatomagmatic/Surtseyan to Vulcanian and of dominant phonolitic composition. The second phase (1.0–0.06 Ma) formed the nephelinitic monogenetic centers Morro Vermelho, Valado and Paredão Volcano Formations through dominant Hawaiian and Strombolian styles. The new ages imply a revised stratigraphy for the youngest units of Trindade Island, with partial overlap between them. The revised chronology integrated to the paleomagnetic directional data evidence that Trindade Complex formed during Gauss normal chron (D = 355.4°; I = −49.6°), Valado and Paredão Volcano during Brunhes normal chron (D = 14°; I = −42.3° and D = 9.2°; I = −35.2°, respectively), while Morro Vermelho records the late Matuyama-early Brunhes chron (D = 36.5°; I = −19.8°), with site-level mean paleodirections of normal and transitional polarity within the reverse Matuyama interval.