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Assessment of aroma release in filled chocolate wafers through electronic nose analysis 通过电子鼻分析评估填充巧克力晶片的香气释放情况
IF 3.3 3区 农林科学 Q1 Agricultural and Biological Sciences Pub Date : 2024-05-19 DOI: 10.1007/s00217-024-04568-y
Pedro Lucas Trombeta Da Silva, Giovana Feltes, Thais Feiden, Sandra Cristina Ballen, Juliana Steffens, Clarice Steffens

The present research sought to evaluate the detection capacity of the electronic nose for the hazelnut aroma in a filled chocolate wafer, measuring its release and physical–chemical, thermal, and microbiological properties during 60 days where the product was stored at 25 °C and 40 °C. It was found that moisture, Aw, pH, thermal resistivity, and diffusivity remained stable during storage at both temperatures, with no significant difference (p > 0.05). While there was variation in color (L*, a*, b*, and ΔE) and in thermal conductivity. The microbiological analyses of mesophilic bacteria, Escherichia coli, Salmonella spp., and coagulase-positive staphylococci were maintained in accordance with the standards established by current legislation. The results obtained with the sensors array showed good sensitivity and a high limit of detection (> 0.001 mg/mL) for hazelnut aroma. The electronic nose was able to discriminate between the release of volatiles from chocolates stored at 25 and 40 °C, with a greater response observed at high temperature (40 °C) at the beginning of storage. Through the application of the Arrhenius model, we successfully determined the activation energy for key color components (L*, a*, b*) and thermal conductivity. Additionally, our findings revealed a good fit of volatile component release to the zero-order model, characterized by a high correlation coefficient (> 0.9). These findings underscore the importance of considering storage temperature when preserving the quality of products such as chocolates. Furthermore, the study validates the use of the electronic nose as a viable technique for analyzing volatiles in food, providing valuable insights for the food industry.

Graphical abstract

本研究旨在评估电子鼻对填充巧克力威化饼中榛子香气的检测能力,测量产品在 25 °C 和 40 °C 下储存 60 天期间的释放、物理化学、热和微生物特性。结果发现,水分、Aw 值、pH 值、热阻率和扩散率在两种温度下储存期间保持稳定,没有显著差异(p > 0.05)。而色泽(L*、a*、b* 和 ΔE)和导热率则存在差异。对中嗜性细菌、大肠杆菌、沙门氏菌和凝固酶阳性葡萄球菌的微生物分析符合现行法律规定的标准。使用传感器阵列获得的结果显示,榛子香气的灵敏度高,检测限(> 0.001 mg/mL)高。电子鼻能够区分巧克力在 25 ℃ 和 40 ℃ 下的挥发物释放情况,在储存初期的高温(40 ℃)条件下,电子鼻的反应更大。通过应用阿伦尼乌斯模型,我们成功确定了主要颜色成分(L*、a*、b*)和热导率的活化能。此外,我们的研究结果表明,挥发性成分的释放与零阶模型非常吻合,相关系数高达 0.9。这些发现强调了在保存巧克力等产品质量时考虑储存温度的重要性。此外,该研究还验证了电子鼻是分析食品挥发性物质的一种可行技术,为食品行业提供了宝贵的见解。
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引用次数: 0
Identifying the sensory profile and fatty acid composition for quality valorization of Marrone chestnut cultivars 确定马龙栗栽培品种的感官特征和脂肪酸组成,提高其质量价值
IF 3.3 3区 农林科学 Q1 Agricultural and Biological Sciences Pub Date : 2024-05-18 DOI: 10.1007/s00217-024-04579-9
Maria Teresa Frangipane, Stefania Garzoli, Daniela de Vita, Riccardo Massantini, Piermaria Corona

Consumers are increasingly interested in chestnuts for their health benefits and also for their organoleptic qualities. It is therefore very important to enhance the chestnut from a sensorial point of view. The sensorial characteristics of commercial chestnuts from three Italian Marrone cultivars (M1 ‘Marrone di Antrodoco’; M2 ‘Marrone dei Monti Cimini’; M3 ‘Marrone del Mugello’ PGI) were investigated with the aim of identifying their sensory profiles. The sensory evaluation was conducted according to (ISO 8589 in Sensory analysis. General guidance for the design of test rooms, 2007; UNI EN ISO 13299 in Sensory analysis. Methodology. General guidance for establishing a sensory profile, 2016). Each descriptor was scored on a range with intervals ranging from 0 (absence of the descriptor) to 10 (maximum intensity of the descriptor). The M1 cultivar is characterized by greater crunchiness (8.0, on a scale from 0 to 10), sweetness (7.5), aromatic intensity (7.9) and caramel aroma (3.3). The M2 cultivar is distinguished by its buttery (3.2) and floral aroma (3.0) with a wood/musk note (1.9) that is missing from the other two cultivars. The M3 cultivar has an almond aroma (5.2) and is distinguished by walnut (3.0) and citrus (2.8) aromas, which are absent in cultivars M1 and M2. The results of this study are important as they experimentally demonstrate that the identification of characteristic sensory profile makes the qualitative differences between cultivars evident. The results showed that linoleic, oleic and palmitic acids were the main components of the lipid fraction of chestnut nuts. In all samples the unsaturated fraction predominated over the saturated one. It is also important to note that there were significant quantitative differences between cultivars. The valorization of Marrone chestnut cultivars contributes to promoting consumer use of these products with their high nutritional value and therefore contributes to the promotion of public health.

消费者对栗子的健康益处和感官品质越来越感兴趣。因此,从感官角度提升栗子的品质非常重要。我们对来自三个意大利马龙栽培品种(M1'Marrone di Antrodoco';M2'Marrone dei Monti Cimini';M3'Marrone del Mugello' PGI)的商品栗子的感官特性进行了调查,目的是确定它们的感官特征。感官评估是根据(ISO 8589 中的感官分析。试验室设计通用指南,2007 年;感官分析中的 UNI EN ISO 13299。方法。建立感官档案的一般指南,2016 年)。每个描述点的评分范围为 0(无描述点)至 10(描述点强度最大)。M1 栽培品种的特点是脆度更高(8.0,从 0 到 10)、甜度更高(7.5)、芳香强度更高(7.9)和焦糖香味更高(3.3)。M2 栽培品种的特点是黄油香味(3.2)和花香(3.0),并带有其他两个栽培品种所没有的木香/麝香味(1.9)。M3 栽培品种具有杏仁香气(5.2),并有核桃(3.0)和柑橘(2.8)香气,而 M1 和 M2 栽培品种则没有这些香气。这项研究的结果非常重要,因为它们通过实验证明,感官特征的识别使栽培品种之间的质量差异显而易见。结果表明,亚油酸、油酸和棕榈酸是栗果脂质部分的主要成分。在所有样本中,不饱和部分比饱和部分占优势。值得注意的是,不同栽培品种在数量上也存在显著差异。马龙栗栽培品种的价值有助于促进消费者使用这些具有高营养价值的产品,从而有助于促进公众健康。
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引用次数: 0
Characterization, components, and chemical structure of a novel natural pigments derived from Streptomyces tauricus 从金牛链霉菌中提取的新型天然色素的特征、成分和化学结构
IF 3.3 3区 农林科学 Q1 Agricultural and Biological Sciences Pub Date : 2024-05-17 DOI: 10.1007/s00217-024-04575-z
Minghui Zhou, Min Han, Jiaxue Qing, Min Yu

Microbial pigments have extensive applications in the food, cosmetic, and biopharmaceutical industries. In this study, a pigment-rich actinomycete identified as Streptomyces tauricus was isolated from soil, and the solubility and stability of its were investigated. The pigment was separated and purified through thin-layer chromatography (TLC), column chromatography, and high performance liquid chromatography (HPLC) to determine its components. The chemical structure of the pigment was characterized through infrared (IR) spectroscopy, gas chromatography-mass spectrometry (GC–MS), tandem mass spectrometry (MS/MS–MS), and nuclear magnetic resonance (NMR). Additionally, the antioxidant properties and safety profile of the pigment were assessed. The S. tauricus pigment was bright, vivid brownish-red, intracellular, and fat-soluble; it exhibited considerable photothermal stability and maintained its color below pH 7. The presence of Cu2+, Fe2+, and Fe3+ ions markedly influenced the pigment’s characteristics. The pigment comprised primarily purple and orange components. The purple component, which is relatively rare in microbial sources, was subjected to detailed study. The core structure of the purple component was identified as methylbenzanthracene dione, which has high antioxidant activity and no toxicity in brine shrimp assays. Due to its resilience to high temperatures and acidic environments, coupled with its bioactivity and lack of toxicity, this pigment may serve as a promising candidate for various industrial and food applications.

微生物色素在食品、化妆品和生物制药行业有着广泛的应用。本研究从土壤中分离出了一种富含色素的放线菌--金牛链霉菌,并对其溶解性和稳定性进行了研究。通过薄层色谱(TLC)、柱层析和高效液相色谱(HPLC)对色素进行分离和纯化,以确定其成分。通过红外光谱(IR)、气相色谱-质谱(GC-MS)、串联质谱(MS/MS-MS)和核磁共振(NMR)分析了色素的化学结构。此外,还对色素的抗氧化性和安全性进行了评估。金牛星色素呈明亮、鲜艳的棕红色,在细胞内溶于脂肪;它具有相当高的光热稳定性,在 pH 值为 7 以下时仍能保持颜色。颜料主要由紫色和橙色成分组成。紫色成分在微生物来源中较为罕见,我们对其进行了详细研究。经鉴定,紫色成分的核心结构为甲基苯并蒽二酮,具有很高的抗氧化活性,在盐水虾试验中无毒性。由于这种色素对高温和酸性环境有很强的适应能力,再加上它的生物活性和无毒性,因此有可能成为各种工业和食品应用的候选物质。
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引用次数: 0
Technological characteristics of whole wheat bread: effects of wheat varieties, sourdough treatments and sourdough levels 全麦面包的工艺特点:小麦品种、酸包处理和酸包水平的影响
IF 3.3 3区 农林科学 Q1 Agricultural and Biological Sciences Pub Date : 2024-05-17 DOI: 10.1007/s00217-024-04560-6
Asiye Seis Subaşı, Recai Ercan
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引用次数: 0
Promising bioactive compounds and biological activities of native Brazilian berries from Myrtaceae and Arecaceae families 巴西本土桃金娘科和山苍子科浆果中具有前景的生物活性化合物和生物活性
IF 3.3 3区 农林科学 Q1 Agricultural and Biological Sciences Pub Date : 2024-05-16 DOI: 10.1007/s00217-024-04571-3
S. Soares, Adriana de Souza Lima, Cynthia Tereza Correa da Silva, Iramaia Angélica Neri Numa, G. M. Pastore
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引用次数: 0
Almond (Prunus dulcis) varieties classification with genetic designed lightweight CNN architecture 利用遗传设计的轻量级 CNN 架构进行杏仁(Prunus dulcis)品种分类
IF 3.3 3区 农林科学 Q1 Agricultural and Biological Sciences Pub Date : 2024-05-16 DOI: 10.1007/s00217-024-04562-4
Mustafa Yurdakul, İrfan Atabaş, Şakir Taşdemir
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引用次数: 0
Gluten migration from biodegradable food contact materials poses a risk to celiac disease patients 可生物降解食品接触材料中的麸质迁移对乳糜泻患者构成风险
IF 3.3 3区 农林科学 Q1 Agricultural and Biological Sciences Pub Date : 2024-05-15 DOI: 10.1007/s00217-024-04570-4
Johanna Mossburger, Katharina Anne Scherf
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引用次数: 0
Mechanical and surface properties of semifinished potato tuber exposed to UV-C radiation at varied operational parameters 在不同操作参数下暴露于紫外线-C 辐射的马铃薯块茎半成品的机械和表面特性
IF 3.3 3区 农林科学 Q1 Agricultural and Biological Sciences Pub Date : 2024-05-15 DOI: 10.1007/s00217-024-04561-5
Addis Lemessa Jembere, Tomasz Jakubowski
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引用次数: 0
Valorization of plant proteins for meat analogues design—a comprehensive review 植物蛋白在肉类类似物设计中的应用--综述
IF 3.3 3区 农林科学 Q1 Agricultural and Biological Sciences Pub Date : 2024-05-15 DOI: 10.1007/s00217-024-04565-1
S. Siddiqui, Ibrahim Khalifa, Tao Yin, Mohamed K. Morsy, Ramy M. Khoder, Molla Salauddin, Wasiya Farzana, Sonu Sharma, Nauman Khalid
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引用次数: 0
Using volatile compounds for the identification of coffee adulterants: marker compounds and non-targeted analysis 利用挥发性化合物鉴定咖啡掺假物:标记化合物和非目标分析
IF 3.3 3区 农林科学 Q1 Agricultural and Biological Sciences Pub Date : 2024-05-14 DOI: 10.1007/s00217-024-04563-3
João Carlos de Souza, Cinthia de Carvalho Couto, A. Mamede, Patrícia Valderrama, A. T. Toci, O. Freitas-Silva
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European Food Research and Technology
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