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Green-Synthesized Sm3+-Doped ZnO Nanoparticles for Multifunctional Applications 用于多功能应用的绿色合成 Sm3+ 掺杂氧化锌纳米粒子
4区 材料科学 Q2 Engineering Pub Date : 2024-02-10 DOI: 10.1155/2024/3618390
Lavanya R., Ramakrishnappa T., Girish K. M., Suresh Kumar K., Basavaraju N., Shilpa B. M.
The present study focuses on the green-mediated synthesis of pristine and Sm3+-doped ZnO nanoparticles using Syzygium cumini fruit extract. The prepared material was characterized by various characterization techniques. Photocatalytic degradation of a fast orange red (FOR) dye under UV light resulted in 88% degradation, with a minimal decrease (87.90%) observed even after five successive runs, indicating the stability and effectiveness of the catalyst. The enhancement in degradation efficiency is attributed to the incorporation of Sm3+ ions into the ZnO lattice. Utilizing the optimized Sm3+ (5 mol%)-doped ZnO nanoparticles, cyclic voltammetry (CV) and electrochemical impedance spectra (EIS) were performed on the prepared electrode, demonstrating the excellent CV properties; this enhancement is attributed to the modification of ZnO’s redox chemistry and the alteration of charge transfer kinetics at the electrode-electrolyte interface due to the addition of Sm3+ into the ZnO structure. The antibacterial activity was performed against two pathogenic strains, i.e., Escherichia coli and Streptococcus aureus. The obtained results suggest that the prepared material holds great promise for catalytic, energy storage, antibacterial, and other multifunctional applications.
本研究的重点是利用茜草果提取物绿色合成原始和 Sm3+ 掺杂的氧化锌纳米粒子。所制备的材料通过各种表征技术进行了表征。在紫外光下光催化降解快速橙红(FOR)染料,降解率达到 88%,即使连续运行五次,降解率也只有极小的下降(87.90%),这表明催化剂的稳定性和有效性。降解效率的提高归功于 Sm3+ 离子融入氧化锌晶格。利用优化的 Sm3+(5 摩尔%)掺杂 ZnO 纳米粒子,对所制备的电极进行了循环伏安法(CV)和电化学阻抗谱(EIS)测试,结果表明电极具有优异的 CV 特性;这种增强归因于在 ZnO 结构中加入 Sm3+ 改变了 ZnO 的氧化还原化学性质,并改变了电极-电解质界面的电荷转移动力学。对两种致病菌,即大肠杆菌和金黄色葡萄球菌,进行了抗菌活性测试。研究结果表明,所制备的材料在催化、储能、抗菌和其他多功能应用方面大有可为。
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引用次数: 0
Crack Propagation Phenomenon in Gangue Concrete Using the Digital Image Correlation (DIC) Method 使用数字图像相关性(DIC)方法分析煤矸石混凝土中的裂缝扩展现象
4区 材料科学 Q2 Engineering Pub Date : 2024-01-30 DOI: 10.1155/2024/7247770
Cheng Pan, Zhiming Zheng, Yu Yang
In order to study the mode I crack propagation mechanism of coal gangue concrete with different contents, the digital image correlation (DIC) method was used to carry out the three-point bending fracture tests on coal gangue concrete with different contents. The results show that the process of the mode I crack propagation of coal gangue concrete with different contents can be divided into three stages as follows: the elastic stage before crack initiation, extended viscoelastic stage, and extended fracture stage. The amount of coal gangue has a significant impact on the crack propagation path. The more the amount of coal gangue, the more the crack penetrates through the coal gangue coarse aggregate, the smaller the bending degree of the failure path, and the faster the crack propagation to the penetration speed. The crack initiation load, ultimate load, external force work, gravity work, and fracture energy all decrease with the increase of the coal gangue content. The data obtained by the DIC method and displacement extensometer are in good agreement, which proves that the DIC method is feasible. Based on the DIC method, before reaching the horizontal displacement on both sides of the crack tip, the horizontal displacement of the horizontal pixel is very small and there is a jump increase after the ultimate load. There are obvious inflection points on the left and right, and the horizontal displacement remains unchanged after the inflection point. After the horizontal displacement field of crack propagation reaches the limit load, there is an obvious limit; the limit gradually extends upward, and the corresponding crack tip strain field is also gradually enhanced. The more the coal gangue is added, the smaller the corresponding horizontal displacement and strain field is at the same limit load moment. The shape of the crack generation area of coal gangue concrete takes the crack tip as the axis of symmetry and is “gourd shaped.” The more the content of the crack, the larger the crack generation area.
为研究不同含量煤矸石混凝土的I型裂缝扩展机理,采用数字图像相关法(DIC)对不同含量煤矸石混凝土进行了三点弯曲断裂试验。结果表明,不同含量煤矸石混凝土的I型裂缝扩展过程可分为以下三个阶段:裂缝萌发前的弹性阶段、扩展粘弹性阶段和扩展断裂阶段。煤矸石的含量对裂缝扩展路径有重要影响。煤矸石量越多,裂缝穿透煤矸石粗集料的程度越大,破坏路径的弯曲度越小,裂缝扩展到穿透速度越快。裂缝起始荷载、极限荷载、外力功、重力功和断裂能均随煤矸石含量的增加而减小。DIC 方法和位移伸长计获得的数据非常吻合,这证明 DIC 方法是可行的。根据 DIC 法,在达到裂缝尖端两侧的水平位移之前,水平像素的水平位移非常小,在达到极限荷载后有一个跳跃式的增长。左右两侧有明显的拐点,拐点后水平位移保持不变。裂纹扩展的水平位移场达到极限荷载后,有一个明显的界限,界限逐渐向上延伸,相应的裂纹尖端应变场也逐渐增强。在相同的极限荷载力矩下,煤矸石加入量越多,相应的水平位移和应变场越小。煤矸石混凝土裂缝产生区的形状以裂缝尖端为对称轴,呈 "葫芦形"。裂缝含量越多,裂缝产生面积越大。
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引用次数: 0
Thermal and Morphological Assessment of the Penta-Layered, Hybrid U-Polyester Composite Reinforced with Glass Fibers and Polypropylene 用玻璃纤维和聚丙烯增强的五层混合 U 型聚酯复合材料的热学和形态学评估
4区 材料科学 Q2 Engineering Pub Date : 2024-01-18 DOI: 10.1155/2024/3911466
Md. Shahin Akanda, Md. Shariful Islam, Md. Ali Akbar, A. M. Sarwaruddin Chowdhury, M. A. Gafur, Md. Sahab Uddin
The interaction between the fibers and matrix in a fiber-reinforced polymer composite material is important in figuring out its properties. The incorporation of fibers with polymers can result in composites with enhanced strength and stiffness. This study aims to investigate the thermal and morphological characteristics of hybrid u-polyester composites reinforced with glass fibers and polypropylene. The fabrication of composite specimens was conducted through a straightforward cold press method. The compositions of the composites were held constant, except for the orientation of the glass fibers and polypropylene. In this study, the TG/DTG technique was used to analyze the thermal characteristics of the composites. In addition, transverse thermal conductivity was measured using the ASTM E1530 method. The test results showed that the composite reinforced with glass fibers exhibited the lowest weight loss and minimal thermal conductivity among all the samples, followed by the hybrid composite. Based on the TGA curves of the samples, the matrix experienced a weight loss of 9.7% at a temperature of 300°C, which reduced to 2.6% and 2.1% for hybrid composites and glass fiber-reinforced composites, respectively. DTG curves for composites demonstrate that the hybrid and fiber-reinforced composites degraded at rates of 0.64 mg/min and 0.36 mg/min, respectively, at 392.3°C and 395.7°C. Moreover, transverse thermal conductivity of the composite which consists of five-glass-fibered layers shows a minimal thermal conductivity of 0.05 W/m·K. The morphological properties were also investigated using scanning electron microscopy (SEM) and Fourier-transform infrared spectroscopy (FTIR). The findings from SEM and FTIR showed that a higher proportion of glass fibers led to a more oriented composite structure, demonstrating enhanced crosslinking between fibers and polyester. Therefore, the insights of this study can be used to improve the performance of glass fibers and polypropylene hybrid-laminated composites intended for high-temperature applications.
纤维增强聚合物复合材料中纤维与基体之间的相互作用对于确定其性能非常重要。纤维与聚合物的结合可提高复合材料的强度和刚度。本研究旨在探讨玻璃纤维和聚丙烯增强的混合 U 型聚酯复合材料的热特性和形态特性。复合材料试样的制作采用直接冷压法。除了玻璃纤维和聚丙烯的取向外,复合材料的成分保持不变。本研究采用 TG/DTG 技术分析复合材料的热特性。此外,还采用 ASTM E1530 方法测量了横向热导率。测试结果表明,在所有样品中,以玻璃纤维增强的复合材料的失重率最低,导热率最小,其次是混合复合材料。根据样品的 TGA 曲线,基体在 300°C 温度下的失重率为 9.7%,而混合复合材料和玻璃纤维增强复合材料的失重率分别降至 2.6% 和 2.1%。复合材料的 DTG 曲线表明,在 392.3°C 和 395.7°C 温度下,混合复合材料和纤维增强复合材料的降解率分别为 0.64 mg/min 和 0.36 mg/min。此外,由五层玻璃纤维组成的复合材料的横向热导率为 0.05 W/m-K。此外,还使用扫描电子显微镜(SEM)和傅立叶变换红外光谱(FTIR)对其形态特性进行了研究。扫描电子显微镜和傅立叶变换红外光谱的研究结果表明,玻璃纤维的比例越高,复合材料结构的取向性就越好,这表明纤维与聚酯之间的交联性增强了。因此,本研究的见解可用于改善高温应用中玻璃纤维和聚丙烯混合层压复合材料的性能。
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引用次数: 0
Dry Sliding Wear Behavior of Copper Matrix Composites Enhanced with TiO2 and MoS2 Hybrids 用二氧化钛和二氧化钼增强的铜基复合材料的干滑动磨损行为
4区 材料科学 Q2 Engineering Pub Date : 2024-01-16 DOI: 10.1155/2024/4384178
V. Subbian, H. Sandeep, K. A. Jayasheel Kumar, R. Suthan, Ananda Mohan Vemula, Chaithanya Kalangi, Perumalla Janaki Ramulu, Dereje H. Georgis Tefera
The paper deals with the properties of copper-based composites. Copper is contributing to the field of automobiles and aerospace industries. The tribological properties of copper are not found to be satisfactory, which may be attributed to the support of producing copper matrix composites with extensive investigations into their properties. Coper-based hybrid composites were fabricated by reinforcing titanium dioxide (TiO2) and molybdenum disulphide (MoS2) to enhance the wear and mechanical properties of copper composites. Three specimens were prepared by powder metallurgy process with the designations of Cu + 5wt.%TiO2, Cu + 5wt.%TiO2 + 2wt.% MoS2, and Cu + 5wt.% TiO2 + 4wt.% MoS2. The metallurgical analysis was done on the specimens using X-ray diffraction (XRD) analysis which confirms the presence and distribution of Cu, TiO2, and MoS2 particles in the specimens. The wear rate was studied on the specimens concerning the sliding velocity, load, and MoS2 content. The statistical analysis and Taguchi analysis highlight the influencing parameters on the wear rate of the material. Linear regression equations were developed to predict the wear rate using DoE. Through this analysis, the sliding velocity of 3 m/s, a load of 30 N, and a 4% addition of MoS2 were identified as the optimum parameters for the minimal wear rate. The wear mechanism was analyzed using scanning electron microscopy techniques to reveal the adhesion, delamination, and oxidation.
本文论述了铜基复合材料的特性。铜为汽车和航空航天工业做出了贡献。铜的摩擦学性能并不令人满意,这可能是由于在生产铜基复合材料的过程中对其性能进行了广泛的研究。通过增强二氧化钛(TiO2)和二硫化钼(MoS2)制备了铜基混合复合材料,以提高铜复合材料的磨损和机械性能。通过粉末冶金工艺制备了三个试样,分别为 Cu + 5wt.% TiO2、Cu + 5wt.% TiO2 + 2wt.% MoS2 和 Cu + 5wt.% TiO2 + 4wt.% MoS2。利用 X 射线衍射 (XRD) 分析法对试样进行了冶金分析,结果证实了试样中铜、二氧化钛和二氧化锰颗粒的存在和分布。试样的磨损率与滑动速度、载荷和 MoS2 含量有关。统计分析和田口分析突出了材料磨损率的影响参数。利用 DoE 建立了线性回归方程来预测磨损率。通过分析,确定了滑动速度为 3 m/s、载荷为 30 N、MoS2 的添加量为 4% 的最佳参数,从而使磨损率最小。使用扫描电子显微镜技术对磨损机制进行了分析,以揭示粘附、分层和氧化现象。
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引用次数: 0
Investigation of Mechanical and Thermal Stabilities of Tamarind Seed- and Peanut Shell Powder-Reinforced Vinyl Ester Composite 罗望子和花生壳粉增强乙烯基酯复合材料的机械稳定性和热稳定性研究
4区 材料科学 Q2 Engineering Pub Date : 2024-01-13 DOI: 10.1155/2024/8818030
Ramakrishnan Kulasekaran Sathish Kumar, Rathinasabapathy Sasikumar, Nagaraj Nagaprasad, Rathinam Ezhilvannan, Ramaswamy Krishnaraj
Efficient exploitation of agricultural waste results in a more sustainable and ecofriendly environment since it lessens the burden of their disposal, which has become increasingly important in recent times. Due to their high mechanical strength and high thermal stability, these biodegradable low-value agrosolid wastes have the potential to successfully replace synthetic fibers and fillers in polymer matrices in the form of reinforcements. This work deals with the addition of low-cost and renewable hybrid natural fillers, tamarind seed filler (TMS), and peanut shell powder (PNS) as particulate reinforcements to the vinyl ester (VE) resin. Traditional compression molding creates TMS/PNS-VE hybrid composites with filler loadings ranging from 5% to 30%. After the composites were fabricated, they were tested for strength properties and heat deflection temperature. A detailed experimental analysis of the mechanical properties was conducted. According to the findings, 20 wt.% hybrid filler loading to the vinyl ester polymer exhibited peak tensile, flexural, and impact strengths of 40.3 MPa, 142 MPa, and 16 kJ/m2, respectively, which is 1.52, 1.69, and 1.29 times the properties of the virgin polymer. However, the peak elongation at break 3.9% was obtained at 30 wt.%. Similarly, the heat deflection temperature (HDT) test of TMS/PNS-VE composites showed a maximum rise of 50.91% at 25 wt.% of filler loading. This is 1.51 times greater than the heat deflection temperature of the pure vinyl ester resin. The findings made it quite clear that adding 20 wt.% biosolid waste hybrid particulate fillers made out of tamarind seed and peanut shell to vinyl ester is the optimum weight, which improves the mechanical and thermal properties of the TMS/PNS-VE composite, making it suitable for making cost-effective materials for lightweight applications. This study also utilizes scanning electron microscopy (SEM) to investigate the microstructural characteristics of the composites, correlating these features with their mechanical performance.
对农业废弃物的有效利用可以减轻处理农业废弃物的负担,从而使环境更具可持续性和生态友好性。由于具有高机械强度和高热稳定性,这些可生物降解的低价值农业固体废弃物有可能以增强材料的形式成功取代聚合物基质中的合成纤维和填料。这项研究涉及在乙烯基酯(VE)树脂中添加低成本、可再生的混合天然填料--罗望子填料(TMS)和花生壳粉末(PNS)作为微粒增强材料。传统的压缩成型工艺可制成 TMS/PNS-VE 混合复合材料,填料含量从 5% 到 30% 不等。复合材料制成后,对其强度性能和热变形温度进行了测试。对机械性能进行了详细的实验分析。实验结果表明,乙烯基酯聚合物中 20 wt.% 混合填料的峰值拉伸强度、弯曲强度和冲击强度分别为 40.3 MPa、142 MPa 和 16 kJ/m2,分别是原始聚合物的 1.52、1.69 和 1.29 倍。然而,在 30 wt.% 时,断裂伸长率达到峰值 3.9%。同样,TMS/PNS-VE 复合材料的热变形温度(HDT)测试表明,在添加 25 wt.% 的填料时,热变形温度最大上升了 50.91%。这比纯乙烯基酯树脂的热变形温度高出 1.51 倍。研究结果清楚地表明,在乙烯基酯中添加 20 重量百分比的罗望子和花生壳制成的生物固体废弃物混合颗粒填料是最佳重量,它能改善 TMS/PNS-VE 复合材料的机械和热性能,使其适用于制造具有成本效益的轻质应用材料。本研究还利用扫描电子显微镜(SEM)研究了复合材料的微观结构特征,并将这些特征与复合材料的机械性能联系起来。
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引用次数: 0
Design Analysis and Optimization of Coil Spring for Three-Wheeler Vehicles Using Composite Materials 使用复合材料的三轮汽车螺旋弹簧的设计分析与优化
4区 材料科学 Q2 Engineering Pub Date : 2024-01-06 DOI: 10.1155/2024/4479427
Solomon Nigusu Abera, Bisrat Yoseph Gebreyesus
The quest for lightweight, efficient, and corrosion-resistant coil springs for vehicle suspension systems has led to the exploration of alternative materials beyond traditional steel. This study delves into the potential of composite materials, particularly carbon/epoxy and carbon/carbon nanotube/epoxy, as replacements for conventional steel coil springs in light vehicles. Through a comprehensive analysis of mechanical properties under static and dynamic loading conditions, the study demonstrates the superior performance of composite springs compared to their steel counterparts. After optimization, the deflection of the carbon/carbon nanotube/epoxy and carbon/epoxy springs decreased to 15.003 mm and 18.703 mm, respectively, and the maximum shear stress decreased by 64.63% and 62.2%, respectively. Likewise, strain energies increased to 2.3644 and 3.5616, respectively. The springs were also studied under dynamic conditions, and the result showed these springs have the ability to perform in dynamic conditions. The carbon/carbon nanotube/epoxy composite emerged as the frontrunner, exhibiting remarkable improvements in shear stress, fatigue life, strain energy, and deformation properties. The study highlights the ability of carbon/carbon nanotube/epoxy composite springs to significantly reduce weight, enhance efficiency, and extend fatigue life, making them a promising alternative for next-generation vehicle suspension systems.
汽车悬挂系统对轻质、高效和耐腐蚀螺旋弹簧的追求促使人们探索传统钢材以外的替代材料。本研究深入探讨了复合材料,尤其是碳/环氧树脂和碳/碳纳米管/环氧树脂,在轻型汽车中替代传统钢制螺旋弹簧的潜力。通过对静态和动态载荷条件下的机械性能进行综合分析,该研究证明复合材料弹簧的性能优于钢制弹簧。经过优化后,碳/碳纳米管/环氧弹簧和碳/环氧弹簧的挠度分别减小到 15.003 毫米和 18.703 毫米,最大剪应力分别减小了 64.63% 和 62.2%。同样,应变能也分别增至 2.3644 和 3.5616。还在动态条件下对弹簧进行了研究,结果表明这些弹簧具有在动态条件下工作的能力。碳/碳纳米管/环氧树脂复合材料表现突出,在剪切应力、疲劳寿命、应变能和变形性能方面都有显著改善。该研究强调了碳/碳纳米管/环氧树脂复合材料弹簧在显著减轻重量、提高效率和延长疲劳寿命方面的能力,使其成为下一代汽车悬挂系统的理想替代品。
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引用次数: 0
A Hybrid Nondominant-Based Genetic Algorithm (NSGA-II) for Multiobjective Optimization to Minimize Vibration Amplitude in the End Milling Process 基于非优势遗传算法(NSGA-II)的混合多目标优化算法,用于最小化端面铣削过程中的振动振幅
4区 材料科学 Q2 Engineering Pub Date : 2024-01-03 DOI: 10.1155/2024/6652973
Mahesh Gopal, Endalkachew Mosisa Gutema, Hirpa G. Lemu, Jaleta Sori
Aluminium is a noncorrosive, lightweight material used to fabricate parts for the aerospace, automobile, and construction industries. Due to the low-temperature resistance, more heat is generated. At the same time, in machining, tremendous efforts are taken to keep friction and chatter to a minimum and to attain better quality and perfect output, and also more attention is required while selecting the machining process parameters. Spindle speed, rate of feed, radial and axial depth of cut, and radial rake angle of the tool are the parameters utilized to machine aluminium 6063 using the HSS tool on CNC milling to estimate spindle and worktable vibration using a prediction model. In this study, the design of the experiment of the response surface methodology approach is used to create a second-order statistical equation for experimentation with the Design-Expert v12 software. The performance characteristics are analyzed using the ANOVA method. The spindle speed achieved the lowest vibration between 2000 and 3000 rpm. Next, axial and radial depths were the most vibration-affecting parameter compared to the rate of feed and radial rake angle of the tool. To find the best feasible response, the nondominant sorting genetic algorithm II (NSGA II) approach was trained and tested using MATLAB software. Using a Pareto-optimal technique, the optimum worktable vibration ranged from 0.00284 to 0.00165 mm/s2, whereas the spindle vibration ranged from 0.02404 to 0.01336 mm/s2. The predicted values were found to be in an excellent argument when Pareto-optimal solutions are used.
铝是一种无腐蚀性的轻质材料,用于制造航空航天、汽车和建筑行业的零部件。由于耐低温,因此会产生更多的热量。同时,在加工过程中,为了将摩擦和颤振控制在最低限度,达到更好的质量和完美的输出,需要付出巨大的努力,同时在选择加工工艺参数时也需要更多的关注。主轴转速、进给速度、径向和轴向切削深度以及刀具的径向前角是使用高速钢刀具在数控铣床上加工铝 6063 时所使用的参数,以便使用预测模型估算主轴和工作台的振动。本研究采用响应面方法进行实验设计,利用 Design-Expert v12 软件建立二阶统计方程进行实验。采用方差分析方法对性能特征进行了分析。主轴转速在 2000 至 3000 rpm 之间的振动最小。其次,与进给速度和刀具径向前角相比,轴向和径向深度是影响振动最大的参数。为了找到最佳可行响应,使用 MATLAB 软件对非主流排序遗传算法 II (NSGA II) 方法进行了训练和测试。使用帕累托最优技术,最佳工作台振动范围为 0.00284 至 0.00165 mm/s2,而主轴振动范围为 0.02404 至 0.01336 mm/s2。在使用帕累托最优解时,发现预测值非常符合实际情况。
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引用次数: 0
Turning SKD 11 Hardened Steel: An Experimental Study of Surface Roughness and Material Removal Rate Using Taguchi Method 车削 SKD 11 淬火钢:使用田口方法对表面粗糙度和材料去除率的实验研究
4区 材料科学 Q2 Engineering Pub Date : 2023-12-20 DOI: 10.1155/2023/6421918
Shah Ashiquzzaman Nipu, Rezaul Karim, Aquib Rahman, Mahjabin Moon, I. A. Choudhury, Junayed Bin Omar, Marsia Sultana Khushbu
Heat-treated steel is widely used in industrial applications due to its high strength and other desirable mechanical qualities. Grinding, which requires a lot of power and is expensive, is typically used to harden machining. In recent times, hard machining has emerged as a viable alternative to grind in select applications. In this investigation, turning operations with a carbide insert (CNMA 120408-KR3215) were carried out on SKD 11 (53 HRC) hardened steel. A total of nine machining tests were completed using the L9 orthogonal array. The response variables considered in this study were surface roughness (Ra) and material removal rate (MRR). The analysis of the signal to noise ratio reveals that the optimal combination of cutting process parameters for achieving a desired surface roughness consists of a cutting speed of 119 m/min, a feed rate of 0.11 mm/rev, and a depth of cut of 0.2 mm. The contribution of each process parameter to the machining performance of the carbide tool-work piece combination is determined through the use of ANOVA. Depth of cut has the greatest impact (57.33%) to MRR, while feed rate has the highest contribution (82.15%) to Ra. Moreover, desirability function analysis (DFA) was conducted to optimize the multiple responses. DFA suggested that, to attain a satisfactory response to the output parameters, higher range of cutting speed, depth of cut, and lower range of feed rate are appreciable; therefore, the analytical findings suggest that a cutting speed of 189 m/min, feed rate of 0.11 mm/rev, and a depth of cut of 0.5 mm can induce a favorable Ra of 0.971 μm and MRR of 10.248 cm3/min. In hard machining, cutting speed has a bigger influence on surface finish than feed rate.
热处理钢因其高强度和其他理想的机械性能而广泛应用于工业领域。磨削需要大量动力,成本高昂,通常用于淬火加工。近来,在某些应用中,硬加工已成为磨削的可行替代方法。在这项研究中,使用硬质合金刀片(CNMA 120408-KR3215)对 SKD 11(53 HRC)淬火钢进行了车削加工。使用 L9 正交阵列共完成了九次加工测试。本研究考虑的响应变量是表面粗糙度 (Ra) 和材料去除率 (MRR)。信噪比分析表明,要达到理想的表面粗糙度,最佳的切削加工参数组合为切削速度 119 m/min、进给量 0.11 mm/rev、切削深度 0.2 mm。通过方差分析确定了各工艺参数对硬质合金刀具-工件组合加工性能的影响。切削深度对 MRR 的影响最大(57.33%),而进给量对 Ra 的影响最大(82.15%)。此外,还进行了可取性函数分析(DFA),以优化多重响应。DFA 表明,要获得令人满意的输出参数响应,较高的切削速度和切削深度范围以及较低的进给量范围是可取的;因此,分析结果表明,切削速度为 189 m/min、进给量为 0.11 mm/rev、切削深度为 0.5 mm 可以获得 0.971 μm 的良好 Ra 值和 10.248 cm3/min 的 MRR 值。在硬加工中,切削速度对表面光洁度的影响大于进给速度。
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引用次数: 0
Numerical Simulation of Acoustic Emission Events in Supporting Roadways under Different Dynamic Loads 不同动态载荷下支承路面声发射事件的数值模拟
4区 材料科学 Q2 Engineering Pub Date : 2023-12-18 DOI: 10.1155/2023/8790995
Wenzheng Shang, Zhigang Liu, Jianbo Yuan, Wuchao You, Shuai Han, Lei Yu, Shihua Zhang
This paper studies the distribution characteristics of acoustic emission (AE) events in supporting roadways under different dynamic load conditions through numerical simulation and theoretical analysis. According to the principle of AE numerical simulation, the roadway model is established by FLAC3D software, and the supporting structure of the bolt cable is established by editing the Fish function. According to the model dynamic load application criterion, the relationship between the peak velocity of the particle, the distance from the source center to the dynamic impact damage point, and the dynamic load intensity is introduced. The velocity-distance-energy relationship is deduced from the relationship to determine the magnitude of the dynamic load energy. The simulation results show that the intensity of the dynamic load source and the distance of the dynamic load source directly impact the AE events. The larger the dynamic load intensity and the closer to the dynamic load source, the more concentrated the AE events. The roadway has a blocking effect on the transmission of the dynamic load stress waves. According to this characteristic, the roadway can be protected by a high-pressure relief roadway. Rock lithology greatly influences the transmission of dynamic load stress waves and the number of AE events. When the dynamic load stress wave passes through the rock strata of different lithologies, the attenuation of the dynamic load energy and the number of AE events are large. However, when the dynamic load stress wave passes through the rock strata of the same lithology, the attenuation of the dynamic load energy and AE events is small. The surrounding rock structure in the bottom corner area of the roadway is susceptible to disturbance from dynamic load sources above the roadway. The results are greatly significant for studying the AE characteristics of support roadways with disturbance-typeimpact failure.
本文通过数值模拟和理论分析,研究了不同动载条件下支护巷道声发射(AE)事件的分布特征。根据 AE 数值模拟原理,利用 FLAC3D 软件建立巷道模型,通过编辑 Fish 函数建立螺栓拉索支护结构。根据模型动荷载应用准则,引入质点峰值速度、源中心到动冲击破坏点的距离与动荷载强度之间的关系。根据速度-距离-能量关系推导出动荷载能量的大小。模拟结果表明,动荷载源的强度和动荷载源的距离直接影响 AE 事件。动荷载强度越大,离动荷载源越近,AE 事件就越集中。巷道对动荷载应力波的传播有阻挡作用。根据这一特性,可采用高压泄压巷道对巷道进行保护。岩石岩性对动荷载应力波的传播和 AE 事件的数量有很大影响。当动荷载应力波穿过不同岩性的岩层时,动荷载能量的衰减和 AE 事件的数量都很大。然而,当动荷载应力波穿过相同岩性的岩层时,动荷载能量和 AE 事件的衰减较小。巷道底角区域的围岩结构容易受到巷道上方动荷载源的扰动。这些结果对于研究具有扰动型冲击破坏的支护巷道的 AE 特性具有重要意义。
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引用次数: 0
In Situ and Real-Time Monitoring of Doping Levels by Reflectance Anisotropy Spectroscopy (RAS) during Molecular Beam Epitaxial (MBE) Growth of III/V Semiconductors 在 III/V 族半导体分子束外延 (MBE) 生长过程中利用反射各向异性光谱 (RAS) 原位和实时监测掺杂水平
4区 材料科学 Q2 Engineering Pub Date : 2023-12-13 DOI: 10.1155/2023/1319081
Henning Fouckhardt, Johannes Richter, Christoph Doering, Johannes Strassner
Reflectance anisotropy/difference spectroscopy (RAS/RDS) had been developed for monitoring epitaxial semiconductor growth, especially for the metal-organic chemical vapor deposition (MOCVD) of III/V semiconductors. But RAS is also well suited for the control of III/V growth with molecular beam epitaxy (MBE). Although the work on RAS has already started at least three decades ago, the potential of this in situ and real-time monitoring technique, especially for doping control, is not well known yet. Experimental results are given here on the identification of doping types and concentration during MBE growth, exemplarily for GaAs and AlGaAs. Especially, the dependence of the majority charge carrier concentration (i.e., the doping concentration) on the RAS signal difference between the nondoping and doping cases is addressed here.
反射各向异性/差分光谱法(RAS/RDS)是为监测半导体外延生长而开发的,尤其适用于 III/V 半导体的金属有机化学气相沉积(MOCVD)。但 RAS 也非常适合控制分子束外延 (MBE) 的 III/V 生长。虽然有关 RAS 的研究工作至少在三十年前就已经开始,但这种原位实时监测技术的潜力,尤其是在掺杂控制方面的潜力,还不为人们所熟知。本文给出了在 MBE 生长过程中识别掺杂类型和浓度的实验结果,以 GaAs 和 AlGaAs 为例。特别是,本文讨论了多数电荷载流子浓度(即掺杂浓度)对未掺杂和掺杂情况下 RAS 信号差异的依赖性。
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引用次数: 0
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Advances in Materials Science and Engineering
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