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A Method for the Direct Determination of Organic Nitrogen by the Kjeldahl Process. 凯氏定氮法直接测定有机氮的方法。
Pub Date : 1906-02-01 DOI: 10.1093/INFDIS/3.SUPPLEMENT_2.S109
A. Kimberly, M. Roberts
One of the most conspicuous recent advances made in sewage analysis in this country may be said to be the development of a direct process for the determination of the nitrogen as ammonia.1 The greater simplicity of the technique, the greater economy of time effected by the elimination of distillation, and the relatively greater accuracy of the process are salient advantages of the direct method which surely cannot fail to be of moment in the routine work of sewage laboratories. To be able to apply a direct process to the determination of the ammonia formed in the determination of total organic nitrogen by the Kjeldahl process seemed the next step toward greater simplicity and rapidity of execution. During a considerable portion of the work at Columbus a direct process was in daily use for the determination of the nitrogen as ammonia, and a more intimate knowledge was gained of local conditions as to the disturbing factor of turbidity, to which, as we all know, has been chiefly due the indifferent success attending earlier attempts at the direct nesslerization of the acid digestate of the Kjeldahl process. Under such circumstances it was thought that a direct method for determinating nitrogen by the Kjeldahl process might be successfully developed. Working along lines by which a direct process for the determination of the nitrogen as free ammonia was successful under such unusually hard water conditions as prevailed at Columbus, a method was finally obtained by which the disturbing turbidity was completely eliminated. It is our purpose to discuss the several factors which have to do with the turbidity occurring in nesslerized tubes, and further to describe a direct method for determination of nitrogen by the Kjeldahl process, found applicable under Columbus condi-
这个国家在污水分析方面最近取得的最显著的进展之一,可以说是开发了一种直接测定氨氮的方法直接法的显著优点是技术更简单,省去蒸馏而节省的时间更少,而且过程相对更准确,这在污水实验室的日常工作中肯定是必不可少的。在凯氏定氮法测定总有机氮的过程中,能够应用一种直接过程来测定氨,似乎是迈向更简单、更快速的下一步。在哥伦布的大部分工作中,每天都使用直接的方法来测定氮和氨,并且对浊度的干扰因素有了更深入的了解,我们都知道,这主要是由于早期在凯氏定氮法中直接消化酸的尝试取得了不成功的成功。在这种情况下,人们认为一种用凯氏定氮法直接测定氮的方法可能会成功地发展起来。沿着直接测定游离氨氮的方法,在哥伦布盛行的异常硬水条件下,成功地获得了一种方法,通过这种方法,可以完全消除令人不安的浑浊。我们的目的是讨论与无氮化管中发生浊度有关的几个因素,并进一步描述在哥伦布条件下适用的凯氏定氮法测定氮的直接方法
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引用次数: 13
The Solubility of Calcium Carbonate and of Magnesium Hydroxide and the Precipitation of these Salts with Lime Water. 碳酸钙和氢氧化镁的溶解度及其在石灰水中的沉淀。
Pub Date : 1906-02-01 DOI: 10.1093/INFDIS/3.SUPPLEMENT_2.S151
G. C. Whipple, A. Mayer
The values given for the solubility of calcium carbonate by the different authorities quoted in Comey's Dictionary of Chemical Solubilities1 vary from 10 to 113 parts per million. About one-half of these authorities give values of more than 50 parts per million, but the high figures represent chiefly the results of early experiments, and are evidently erroneous. The figures which appear to be most reasonable may be divided into two groups, one placing the solubility between 20 and 36 parts per million, the other, between 10 and 16 parts per million. TABLE 1.
《科米化学溶解度词典》中引用的不同权威给出的碳酸钙溶解度值从百万分之10到百万分之113不等。这些权威机构中约有一半给出的数值超过百万分之五十,但较高的数字主要是早期实验的结果,显然是错误的。看来最合理的数字可分为两组,一组把溶解度放在百万分之20到36之间,另一组放在百万分之10到16之间。表1。
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引用次数: 5
Methods of Bacteriological Examination of Milk. 牛奶的细菌学检验方法。
Pub Date : 1906-02-01 DOI: 10.1093/infdis/3.Supplement_2.S214
F. Slack
The bacteriological examination of milk is rapidly becoming one of the essentials in the maintenance of public health. For years milk supplies have been inspected and tested to chemical standards alone, with the result that watered, adulterated, and preserved milks have been practically driven from the markets. These chemical tests are necessary, and only fail in that they do not go far enough, since a milk impure and unwholesome on account of bacterial growth, or a milk from a diseased animal, cannot be detected by them. The bacterial count and the microscopical examination of the milk sediment reveal whether the milk has been properly handled or not, and, to a great extent, the condition of the animal from which it came.
对牛奶进行细菌学检查正迅速成为维护公众健康的一项重要工作。多年来,牛奶供应只按照化学标准进行检查和测试,结果是掺水的、掺假的和腌制的牛奶实际上已经被赶出了市场。这些化学试验是必要的,但它们的失败之处在于它们还不够彻底,因为由于细菌生长而不纯净和不健康的牛奶,或者来自患病动物的牛奶,都不能被它们检测出来。细菌计数和对牛奶沉淀物的显微镜检查显示牛奶是否被妥善处理,并且在很大程度上显示出牛奶来自的动物的状况。
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引用次数: 0
Suggestions for Changes in the Schedules for Making Broth, Gelatin, and Agar, Recommended in the Last Report of the Committee on Standard Methods of Water Analysis. 在水分析标准方法委员会的最后一份报告中推荐的关于制作肉汤、明胶和琼脂的时间表变化的建议。
Pub Date : 1906-02-01 DOI: 10.1093/INFDIS/3.SUPPLEMENT_2.S223
H. Hill
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引用次数: 0
The Way to Stamp out Malarial Fevers. 消灭疟疾热的方法。
Pub Date : 1906-01-01
E Lamicq
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引用次数: 0
Prophylaxis of Paludic Diseases. 预防老年疾病。
Pub Date : 1906-01-01
J Brena
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引用次数: 0
The "Mal del Pinto" from a Hygienic Point of View. 从卫生的角度看“Mal del Pinto”。
Pub Date : 1906-01-01
J G Uruena
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引用次数: 0
Report on the Condition and Prospects of Vital Statistics in the United States. 美国生命统计状况与展望报告。
Pub Date : 1906-01-01
C L Wilbur
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引用次数: 0
Observed Relations between Dissolved Oxygen, Carbonic Acid and Algae Growths in Weequahic Lake, Newark, N. J. 在纽瓦克的维奎希奇湖,溶解氧,碳酸和藻类生长的关系观察。
Pub Date : 1906-01-01
H B Baldwin, G C Whipple
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引用次数: 0
Observations on the Census and Mortality Tables of the City of Mexico. 关于墨西哥城人口普查和死亡率表的意见。
Pub Date : 1906-01-01
J M Ponce
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引用次数: 0
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