PURPOSE To evaluate the effects of tribochemical silica coating and different 10-methacryloyloxydecyl dihydrogen phosphate (MDP)-containing primers on the shear bond strength (SBS) of orthodontic metal brackets to yttrium-stabilized tetragonal zirconia polycrystal (Y-TZP) surfaces. MATERIALS AND METHODS One hundred ninety polished Y-TZP specimens were randomly assigned to 19 groups (n = 10): 30 specimens were used for surface analyses after polishing with 600-grit silicon carbide paper, airborneparticle abrasion with 50-μm alumina (A), or tribochemical silica coating (CoJet [C]); 160 specimens were used in SBS testing of orthodontic metal brackets to Y-TZP after alumina airborne-particle abrasion or tribochemical silica coating and application of either ESPE-Sil (S) (ASn, ASa, CSn, CSa), Alloy Primer (AP) (AAPn, AAPa, CAPn, CAPa), Clearfil Ceramic Primer (CP) (ACPn, ACPa, CCPn, CCPa), or Scotchbond Universal (U) (AUn, AUa, CUn, CUa) and either stored in water for 24 h (non-aged, n) or thermocycled 5000 times (aged, a). The surface analyses and SBSs were statistically analyzed with ANOVA and Tukey's tests. RESULTS Both mechanically treated surfaces had significantly greater surface roughness and surface free energy than did the polished surfaces. The type of primer and aging significantly affected the bond strength. Among the thermocycled specimens, the AAPa, AUa, and CCPa groups showed the greatest SBS. CONCLUSION After alumina airborne-particle abrasion, the application of Alloy Primer, Clearfil Ceramic Primer, or Scotchbond Universal provided stable bonding to Y-TZP ceramics. After tribochemical silica coating, however, only Clearfil Ceramic Primer produced a durable bond to Y-TZP ceramics.
{"title":"Bond Strengths of Orthodontic Metal Brackets to Tribochemically Silica-coated Zirconia Surfaces Using Different 10-Methacryloyloxydecyl Dihydrogen Phosphate-containing Primers.","authors":"Na-Hyun Kim, Yoon-Ji Kim, Dong-Yul Lee","doi":"10.3290/j.jad.a37724","DOIUrl":"https://doi.org/10.3290/j.jad.a37724","url":null,"abstract":"PURPOSE To evaluate the effects of tribochemical silica coating and different 10-methacryloyloxydecyl dihydrogen phosphate (MDP)-containing primers on the shear bond strength (SBS) of orthodontic metal brackets to yttrium-stabilized tetragonal zirconia polycrystal (Y-TZP) surfaces. MATERIALS AND METHODS One hundred ninety polished Y-TZP specimens were randomly assigned to 19 groups (n = 10): 30 specimens were used for surface analyses after polishing with 600-grit silicon carbide paper, airborneparticle abrasion with 50-μm alumina (A), or tribochemical silica coating (CoJet [C]); 160 specimens were used in SBS testing of orthodontic metal brackets to Y-TZP after alumina airborne-particle abrasion or tribochemical silica coating and application of either ESPE-Sil (S) (ASn, ASa, CSn, CSa), Alloy Primer (AP) (AAPn, AAPa, CAPn, CAPa), Clearfil Ceramic Primer (CP) (ACPn, ACPa, CCPn, CCPa), or Scotchbond Universal (U) (AUn, AUa, CUn, CUa) and either stored in water for 24 h (non-aged, n) or thermocycled 5000 times (aged, a). The surface analyses and SBSs were statistically analyzed with ANOVA and Tukey's tests. RESULTS Both mechanically treated surfaces had significantly greater surface roughness and surface free energy than did the polished surfaces. The type of primer and aging significantly affected the bond strength. Among the thermocycled specimens, the AAPa, AUa, and CCPa groups showed the greatest SBS. CONCLUSION After alumina airborne-particle abrasion, the application of Alloy Primer, Clearfil Ceramic Primer, or Scotchbond Universal provided stable bonding to Y-TZP ceramics. After tribochemical silica coating, however, only Clearfil Ceramic Primer produced a durable bond to Y-TZP ceramics.","PeriodicalId":94234,"journal":{"name":"The journal of adhesive dentistry","volume":"27 1","pages":"21-29"},"PeriodicalIF":0.0,"publicationDate":"2017-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"74349682","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
A. F. Montagner, N. Opdam, J. de Munck, M. Cenci, B. Van Meerbeek, M. Huysmans
PURPOSE To evaluate the effect of water storage and cyclic loading on the microtensile bond strength (μTBS) and fracture pattern of adhesives to dentin. MATERIALS AND METHODS Midcoronal dentin surfaces (n = 36) were prepared and composite restorations were built up using two adhesives (self-etch and etch-and-rinse). The specimens were randomly divided into 3 groups according to the aging conditions (n = 6): 1. CONTROL storage in water for 24 h (CO); 2. water storage: storage in water for 6 months (WS); 3. mechanical loading: 750,000 mechanical cycles (ML) using the Rub&Roll loading device. Specimens were sections into beams and the μTBS was tested. Fracture patterns were analyzed using stereomicroscopy and fractographic analysis was performed using SEM. μTBS data (n = 53-72 specimens) were subjected to two-way ANOVA and Tukey's post-hoc test. The chi-squared test was used to compare the distribution of failure modes (p < 0.05). RESULTS Aging conditions and adhesives significantly affected μTBS (p < 0.01). The CO group showed no difference between materials and had highest μTBS. After WS, the self-etch adhesive showed higher μTBS than did the etchand- rinse adhesive. ML resulted in lower μTBS for both adhesives. Materials (p < 0.01) and aging (p < 0.01) significantly influenced the distribution of failure modes. SEM analysis showed that specimens submitted to WS or ML showed features of degradation and fatigue at the fractured interface, depending on the adhesive. CONCLUSION Mechanical loading had a negative effect on the bonding efficacy of both adhesives and influenced the fracture pattern, with specimens presenting a different fracture surface from that observed in water-stored specimens.
{"title":"Bonding Efficacy and Fracture Pattern of Adhesives Submitted to Mechanical Aging with the Rub&Roll Device.","authors":"A. F. Montagner, N. Opdam, J. de Munck, M. Cenci, B. Van Meerbeek, M. Huysmans","doi":"10.3290/j.jad.a37721","DOIUrl":"https://doi.org/10.3290/j.jad.a37721","url":null,"abstract":"PURPOSE To evaluate the effect of water storage and cyclic loading on the microtensile bond strength (μTBS) and fracture pattern of adhesives to dentin. MATERIALS AND METHODS Midcoronal dentin surfaces (n = 36) were prepared and composite restorations were built up using two adhesives (self-etch and etch-and-rinse). The specimens were randomly divided into 3 groups according to the aging conditions (n = 6): 1. CONTROL storage in water for 24 h (CO); 2. water storage: storage in water for 6 months (WS); 3. mechanical loading: 750,000 mechanical cycles (ML) using the Rub&Roll loading device. Specimens were sections into beams and the μTBS was tested. Fracture patterns were analyzed using stereomicroscopy and fractographic analysis was performed using SEM. μTBS data (n = 53-72 specimens) were subjected to two-way ANOVA and Tukey's post-hoc test. The chi-squared test was used to compare the distribution of failure modes (p < 0.05). RESULTS Aging conditions and adhesives significantly affected μTBS (p < 0.01). The CO group showed no difference between materials and had highest μTBS. After WS, the self-etch adhesive showed higher μTBS than did the etchand- rinse adhesive. ML resulted in lower μTBS for both adhesives. Materials (p < 0.01) and aging (p < 0.01) significantly influenced the distribution of failure modes. SEM analysis showed that specimens submitted to WS or ML showed features of degradation and fatigue at the fractured interface, depending on the adhesive. CONCLUSION Mechanical loading had a negative effect on the bonding efficacy of both adhesives and influenced the fracture pattern, with specimens presenting a different fracture surface from that observed in water-stored specimens.","PeriodicalId":94234,"journal":{"name":"The journal of adhesive dentistry","volume":"31 1","pages":"59-68"},"PeriodicalIF":0.0,"publicationDate":"2017-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"75278267","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Michael Sawalt, S. Paris, U. Blunck, F. Schwendicke
PURPOSE To assess the fracture resistance (FR) and cusp deflection (CD) of lined or non-lined composite (CO) and glass hybrid (GH) restorations over residual demineralized dentin. MATERIALS AND METHODS In 48 extracted human premolars, artificial residual demineralized dentin was induced on pulpo-axial walls of standardized cavities. Various restorations were placed over this demineralized dentin: an experimental GH, a composite restoration (OptiBond FL+Tetric EvoCeram) without lining, or composite restorations with non-setting (Hypocal) or setting (Dycal) calcium hydroxide lining. After thermomechanical cycling, groups (n = 12) were compared regarding their CD and FR. RESULTS CD did not differ significantly between groups. FR was significantly lower in teeth restored with GH (median: 238 N; 25th/75th percentiles: 191/287 N) than in those restored with lined or non-lined composites (median range: 517-569 N; p < 0.05/Mann-Whitney), which did not differ significantly from each other (p > 0.05). CONCLUSION Within the conditions of this in vitro study, CH lining of pulpo-axial walls had only limited impact on CD and FR. GH showed the lowest FR and might not be optimal for restoring deep or extended cavitated lesions.
{"title":"Fracture Resistance and Cusp Deflection of Lined or Non-lined Composite and Glass Hybrid Restorations Over Residual Demineralized Dentin.","authors":"Michael Sawalt, S. Paris, U. Blunck, F. Schwendicke","doi":"10.3290/j.jad.a37719","DOIUrl":"https://doi.org/10.3290/j.jad.a37719","url":null,"abstract":"PURPOSE To assess the fracture resistance (FR) and cusp deflection (CD) of lined or non-lined composite (CO) and glass hybrid (GH) restorations over residual demineralized dentin. MATERIALS AND METHODS In 48 extracted human premolars, artificial residual demineralized dentin was induced on pulpo-axial walls of standardized cavities. Various restorations were placed over this demineralized dentin: an experimental GH, a composite restoration (OptiBond FL+Tetric EvoCeram) without lining, or composite restorations with non-setting (Hypocal) or setting (Dycal) calcium hydroxide lining. After thermomechanical cycling, groups (n = 12) were compared regarding their CD and FR. RESULTS CD did not differ significantly between groups. FR was significantly lower in teeth restored with GH (median: 238 N; 25th/75th percentiles: 191/287 N) than in those restored with lined or non-lined composites (median range: 517-569 N; p < 0.05/Mann-Whitney), which did not differ significantly from each other (p > 0.05). CONCLUSION Within the conditions of this in vitro study, CH lining of pulpo-axial walls had only limited impact on CD and FR. GH showed the lowest FR and might not be optimal for restoring deep or extended cavitated lesions.","PeriodicalId":94234,"journal":{"name":"The journal of adhesive dentistry","volume":"39 1","pages":"77-82"},"PeriodicalIF":0.0,"publicationDate":"2017-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"80662864","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Ferhan Egilmez, G. Ergun, I. Cekic-Nagas, P. Vallittu, L. Lassila
PURPOSE To evaluate the light transmission characteristics of different types, shades, and thicknesses of novel CAD/CAM materials and their effect on the degree of conversion (DC) of a dual-curing resin cement. MATERIALS AND METHODS Square specimens (12 × 12 mm2) of three CAD/CAM materials - GC Cerasmart, Lava Ultimate, Vita Enamic - of different thicknesses (1.00, 1.50, and 2.00 mm, n = 5 per thickness) were irradiated with an LED unit. The amount of transmitted light was quantified. Thereafter, the DC% of the dual-curing resin cement (RelyX Ultimate) was recorded after 15 min using Fourier transform infrared spectroscopy. Statistical analysis was performed using two-way ANOVA followed by the Tukey's HSD post-hoc test at a significance level of p < 0.05. Regression analysis was performed to investigate the correlation between the DC and radiant energy, and the DC and thickness. RESULTS Although the type and shade of CAD/CAM material significantly affect transmitted light irradiation (p < 0.0001), degrees of conversion are similar when the CAD/CAM material or material shade were taken into consideration (p > 0.05). Conversely, material thickness significantly affected light transmission (p < 0.0001) and DC (p < 0.0001). Multiple effects of material, shade, and thickness did not significantly affect the evaluated parameters (p = 0.638 for light irradiation; p = 0.637 for DC). Linear regression analysis showed a correlation between delivered energy and DC% results of the Vita Enamic (R² = 0.4169, p < 0.0001). CONCLUSION Reduced light transmission in 2-mm-thick specimens of all CAD/CAM materials indicates that proper curing of the cement beneath CAD/CAM materials should be ensured.
{"title":"Light Transmission of Novel CAD/CAM Materials and Their Influence on the Degree of Conversion of a Dual-curing Resin Cement.","authors":"Ferhan Egilmez, G. Ergun, I. Cekic-Nagas, P. Vallittu, L. Lassila","doi":"10.3290/j.jad.a37722","DOIUrl":"https://doi.org/10.3290/j.jad.a37722","url":null,"abstract":"PURPOSE To evaluate the light transmission characteristics of different types, shades, and thicknesses of novel CAD/CAM materials and their effect on the degree of conversion (DC) of a dual-curing resin cement. MATERIALS AND METHODS Square specimens (12 × 12 mm2) of three CAD/CAM materials - GC Cerasmart, Lava Ultimate, Vita Enamic - of different thicknesses (1.00, 1.50, and 2.00 mm, n = 5 per thickness) were irradiated with an LED unit. The amount of transmitted light was quantified. Thereafter, the DC% of the dual-curing resin cement (RelyX Ultimate) was recorded after 15 min using Fourier transform infrared spectroscopy. Statistical analysis was performed using two-way ANOVA followed by the Tukey's HSD post-hoc test at a significance level of p < 0.05. Regression analysis was performed to investigate the correlation between the DC and radiant energy, and the DC and thickness. RESULTS Although the type and shade of CAD/CAM material significantly affect transmitted light irradiation (p < 0.0001), degrees of conversion are similar when the CAD/CAM material or material shade were taken into consideration (p > 0.05). Conversely, material thickness significantly affected light transmission (p < 0.0001) and DC (p < 0.0001). Multiple effects of material, shade, and thickness did not significantly affect the evaluated parameters (p = 0.638 for light irradiation; p = 0.637 for DC). Linear regression analysis showed a correlation between delivered energy and DC% results of the Vita Enamic (R² = 0.4169, p < 0.0001). CONCLUSION Reduced light transmission in 2-mm-thick specimens of all CAD/CAM materials indicates that proper curing of the cement beneath CAD/CAM materials should be ensured.","PeriodicalId":94234,"journal":{"name":"The journal of adhesive dentistry","volume":"44 1","pages":"39-48"},"PeriodicalIF":0.0,"publicationDate":"2017-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"88161676","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Editorial: Editors are Not Publication Police.","authors":"R. Frankenberger, B. Van Meerbeek","doi":"10.3290/j.jad.a35627","DOIUrl":"https://doi.org/10.3290/j.jad.a35627","url":null,"abstract":"","PeriodicalId":94234,"journal":{"name":"The journal of adhesive dentistry","volume":"38 1","pages":"3"},"PeriodicalIF":0.0,"publicationDate":"2016-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"83586046","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
S. Soliman, R. Preidl, Sabine Karl, N. Hofmann, G. Krastl, B. Klaiber
PURPOSE To investigate the influence of three cavity designs on the marginal seal of large Class II cavities restored with low-shrinkage resin composite limited to the enamel. MATERIALS AND METHODS One hundred twenty (120) intact human molars were randomly divided into 12 groups, with three different cavity designs: 1. undermined enamel, 2. box-shaped, and 3. proximal bevel. The teeth were restored with 1. an extra-low shrinkage (ELS) composite free of diluent monomers, 2. microhybrid composite (Herculite XRV), 3. nanohybrid composite (Filtek Supreme XTE), and 4. silorane-based composite (Filtek Silorane). After artificial aging by thermocycling and storage in physiological saline, epoxy resin replicas were prepared. To determine the integrity of the restorations' approximal margins, two methods were sequentially employed: 1. replicas were made of the 120 specimens and examined using SEM, and 2. the same 120 specimens were immersed in AgNO3 solution, and the dye penetration depth was observed with a light microscope. Statistical analysis was performed using the Kruskal-Wallis and the Dunn-Bonferroni tests. RESULTS After bevel preparation, SEM observations showed that restorations did not exhibit a higher percentage of continuous margin (SEM-analysis; p>0.05), but more leakage was found than with the other cavity designs (p<0.05). The lowest percentage of continuous margin was observed in ELS restorations (p<0.05). More fractured margins were observed in the undermined enamel cavity design groups (p<0.05). CONCLUSION Bevel preparation failed to improve margin quality in large Class II composite restorations and is no longer recommended. However, undermined enamel should be removed to prevent enamel fractures.
{"title":"Influence of Cavity Margin Design and Restorative Material on Marginal Quality and Seal of Extended Class II Resin Composite Restorations In Vitro.","authors":"S. Soliman, R. Preidl, Sabine Karl, N. Hofmann, G. Krastl, B. Klaiber","doi":"10.3290/j.jad.a35520","DOIUrl":"https://doi.org/10.3290/j.jad.a35520","url":null,"abstract":"PURPOSE To investigate the influence of three cavity designs on the marginal seal of large Class II cavities restored with low-shrinkage resin composite limited to the enamel. MATERIALS AND METHODS One hundred twenty (120) intact human molars were randomly divided into 12 groups, with three different cavity designs: 1. undermined enamel, 2. box-shaped, and 3. proximal bevel. The teeth were restored with 1. an extra-low shrinkage (ELS) composite free of diluent monomers, 2. microhybrid composite (Herculite XRV), 3. nanohybrid composite (Filtek Supreme XTE), and 4. silorane-based composite (Filtek Silorane). After artificial aging by thermocycling and storage in physiological saline, epoxy resin replicas were prepared. To determine the integrity of the restorations' approximal margins, two methods were sequentially employed: 1. replicas were made of the 120 specimens and examined using SEM, and 2. the same 120 specimens were immersed in AgNO3 solution, and the dye penetration depth was observed with a light microscope. Statistical analysis was performed using the Kruskal-Wallis and the Dunn-Bonferroni tests. RESULTS After bevel preparation, SEM observations showed that restorations did not exhibit a higher percentage of continuous margin (SEM-analysis; p>0.05), but more leakage was found than with the other cavity designs (p<0.05). The lowest percentage of continuous margin was observed in ELS restorations (p<0.05). More fractured margins were observed in the undermined enamel cavity design groups (p<0.05). CONCLUSION Bevel preparation failed to improve margin quality in large Class II composite restorations and is no longer recommended. However, undermined enamel should be removed to prevent enamel fractures.","PeriodicalId":94234,"journal":{"name":"The journal of adhesive dentistry","volume":"1 1","pages":"7-16"},"PeriodicalIF":0.0,"publicationDate":"2016-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"76062133","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
R. Pilo, T. Brosh, Valery Geron, S. Levartovsky, G. Eliades
PURPOSE To investigate the influence of silane reaction time on the repair strength of an aged nanofilled composite and to characterize the bonding mechanism. MATERIALS AND METHODS Nanofilled composite disks (n = 110, Filtek Supreme XT) were aged for 90 days in water. After tribochemical treatment (CoJet-Sand), the specimens were assigned to 5 groups (n = 22), primed with silane (Espe-Sil), and left to react for 1, 2, 3, 4, and 5 min. A thin layer of adhesive (Visio-Bond) was applied and a new composite with the same dimension was placed and cured. Non-aged specimens immediately layered and cured using the incremental technique served as controls. After aging (30 days in water plus 5000 thermal cycles), the interface was subjected to a shearing force until failure. Failure mode was evaluated under a stereomicroscope and scanning electron microscopy (SEM). Additional aged and treated surfaces were evaluated for morphology as well as elemental and molecular composition using SEM/EDX and ATR-FTIR. RESULTS The mean shear bond strength (SBS) of the repaired specimens was 53.9 ± 8.6 MPa, with no significant difference among the various reaction times, but significantly lower compared to the control (88.1 ± 12.5 MPa). Tribochemical treatment created an irregular surface morphology with particles imbedded in the aged surface. Interfacial SEM/EDX analysis showed a 5-μm non-uniform high atomic number zone rich in Al and Si. CONCLUSION Tribochemical treatments for repairing composite using a short silane reaction period (1 min) are equally effective as the prolonged reaction periods (2 to 5 min), yielding interfacial shear strength of ~60% of unrepaired material.
{"title":"Effect of Silane Reaction Time on the Repair of a Nanofilled Composite Using Tribochemical Treatment.","authors":"R. Pilo, T. Brosh, Valery Geron, S. Levartovsky, G. Eliades","doi":"10.3290/j.jad.a35907","DOIUrl":"https://doi.org/10.3290/j.jad.a35907","url":null,"abstract":"PURPOSE To investigate the influence of silane reaction time on the repair strength of an aged nanofilled composite and to characterize the bonding mechanism. MATERIALS AND METHODS Nanofilled composite disks (n = 110, Filtek Supreme XT) were aged for 90 days in water. After tribochemical treatment (CoJet-Sand), the specimens were assigned to 5 groups (n = 22), primed with silane (Espe-Sil), and left to react for 1, 2, 3, 4, and 5 min. A thin layer of adhesive (Visio-Bond) was applied and a new composite with the same dimension was placed and cured. Non-aged specimens immediately layered and cured using the incremental technique served as controls. After aging (30 days in water plus 5000 thermal cycles), the interface was subjected to a shearing force until failure. Failure mode was evaluated under a stereomicroscope and scanning electron microscopy (SEM). Additional aged and treated surfaces were evaluated for morphology as well as elemental and molecular composition using SEM/EDX and ATR-FTIR. RESULTS The mean shear bond strength (SBS) of the repaired specimens was 53.9 ± 8.6 MPa, with no significant difference among the various reaction times, but significantly lower compared to the control (88.1 ± 12.5 MPa). Tribochemical treatment created an irregular surface morphology with particles imbedded in the aged surface. Interfacial SEM/EDX analysis showed a 5-μm non-uniform high atomic number zone rich in Al and Si. CONCLUSION Tribochemical treatments for repairing composite using a short silane reaction period (1 min) are equally effective as the prolonged reaction periods (2 to 5 min), yielding interfacial shear strength of ~60% of unrepaired material.","PeriodicalId":94234,"journal":{"name":"The journal of adhesive dentistry","volume":"81 1","pages":"125-34"},"PeriodicalIF":0.0,"publicationDate":"2016-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"83895870","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
PURPOSE To evaluate the microshear bond strength of tri-calcium silicate-based materials to different restorative materials. MATERIALS AND METHODS Thirty-five disks of TheraCal LC and Biodentine were fabricated using teflon molds according to manufacturers' instructions. Then the specimens were randomly divided into 7 groups according to the materials applied: Fuji IX, Fuji II, Equia Fil, Vertise Flow, Filtek Bulk Fill Posterior Restorative, Filtek Z250 with Prime&Bond NT and with Clearfil SE Bond. All restorative materials were placed onto the disks using tygon tubes. Following a storage period, the specimens underwent microshear bond strength testing in a universal testing machine, and fracture modes were analyzed. Data were analyzed using one-way ANOVA and Tukey's post-hoc test. RESULTS For all restorative materials, TheraCal LC showed significantly higher μSBS values compared to Biodentine. GIC based materials showed the lowest μSBS for TheraCal and Biodentine. For Biodentine, Filtek Z250 applied with Prime&Bond NT and Filtek Bulk Fill Posterior Restorative applied with Scotchbond Universal Adhesive exhibited the highest μSBS, while Filtek Z250 applied with Clearfil SE Bond revealed the highest bond strength to TheraCal LC. CONCLUSION For all restorative materials tested in this study, TheraCal LC showed higher μSBS compared to Biodentine. For both TheraCal LC and Biodentine, the placement of GIC-based materials prior to composite resin restorations might decrease the bond strength. Composite resins applied with self-etching adhesives increased the bond strength of TheraCal LC; however, for Biodentine, application of etch-and-rinse adhesives may improve the adhesion of composite resins.
目的评价硅酸盐三钙基材料与不同修复材料的微剪切结合强度。材料与方法根据生产厂家的说明书，采用特氟龙模具制备了35片TheraCal LC和Biodentine。然后根据所用材料随机分为7组:Fuji IX、Fuji II、Equia Fil、Vertise Flow、Filtek Bulk Fill Posterior Restorative、Filtek Z250 with Prime&Bond NT和Clearfil SE Bond。所有的修复材料都用钛管放置在磁盘上。保存一段时间后，在万能试验机上进行微剪粘结强度测试，并分析断裂模式。数据分析采用单因素方差分析和Tukey事后检验。结果在所有修复材料中，TheraCal LC的μSBS值均显著高于Biodentine。GIC基材料对TheraCal和Biodentine的μSBS最低。对于Biodentine, Filtek Z250与Prime&Bond NT、Filtek Bulk Fill Posterior Restorative与Scotchbond Universal Adhesive的结合μSBS最高，而Filtek Z250与TheraCal LC的结合μSBS最高。结论在所有修复材料中，TheraCal LC的μSBS均高于Biodentine。对于TheraCal LC和Biodentine，在复合树脂修复体之前放置ic基材料可能会降低结合强度。复合树脂与自蚀刻胶粘剂的结合提高了TheraCal LC的结合强度;然而，对于Biodentine，应用蚀刻-漂洗粘合剂可以改善复合树脂的附着力。
{"title":"Microshear Bond Strength of Tri-Calcium Silicate-based Cements to Different Restorative Materials.","authors":"E. Cengiz, N. Ulusoy","doi":"10.3290/j.jad.a35934","DOIUrl":"https://doi.org/10.3290/j.jad.a35934","url":null,"abstract":"PURPOSE To evaluate the microshear bond strength of tri-calcium silicate-based materials to different restorative materials. MATERIALS AND METHODS Thirty-five disks of TheraCal LC and Biodentine were fabricated using teflon molds according to manufacturers' instructions. Then the specimens were randomly divided into 7 groups according to the materials applied: Fuji IX, Fuji II, Equia Fil, Vertise Flow, Filtek Bulk Fill Posterior Restorative, Filtek Z250 with Prime&Bond NT and with Clearfil SE Bond. All restorative materials were placed onto the disks using tygon tubes. Following a storage period, the specimens underwent microshear bond strength testing in a universal testing machine, and fracture modes were analyzed. Data were analyzed using one-way ANOVA and Tukey's post-hoc test. RESULTS For all restorative materials, TheraCal LC showed significantly higher μSBS values compared to Biodentine. GIC based materials showed the lowest μSBS for TheraCal and Biodentine. For Biodentine, Filtek Z250 applied with Prime&Bond NT and Filtek Bulk Fill Posterior Restorative applied with Scotchbond Universal Adhesive exhibited the highest μSBS, while Filtek Z250 applied with Clearfil SE Bond revealed the highest bond strength to TheraCal LC. CONCLUSION For all restorative materials tested in this study, TheraCal LC showed higher μSBS compared to Biodentine. For both TheraCal LC and Biodentine, the placement of GIC-based materials prior to composite resin restorations might decrease the bond strength. Composite resins applied with self-etching adhesives increased the bond strength of TheraCal LC; however, for Biodentine, application of etch-and-rinse adhesives may improve the adhesion of composite resins.","PeriodicalId":94234,"journal":{"name":"The journal of adhesive dentistry","volume":"42 1","pages":"231-7"},"PeriodicalIF":0.0,"publicationDate":"2016-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"88593644","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
京公网安备 11010802042870号
京ICP备2023020795号-1
扫码关注我们
求助内容：
应助结果提醒方式：