Ferhan Egilmez, G. Ergun, I. Cekic-Nagas, P. Vallittu, L. Lassila
PURPOSE To evaluate the light transmission characteristics of different types, shades, and thicknesses of novel CAD/CAM materials and their effect on the degree of conversion (DC) of a dual-curing resin cement. MATERIALS AND METHODS Square specimens (12 × 12 mm2) of three CAD/CAM materials - GC Cerasmart, Lava Ultimate, Vita Enamic - of different thicknesses (1.00, 1.50, and 2.00 mm, n = 5 per thickness) were irradiated with an LED unit. The amount of transmitted light was quantified. Thereafter, the DC% of the dual-curing resin cement (RelyX Ultimate) was recorded after 15 min using Fourier transform infrared spectroscopy. Statistical analysis was performed using two-way ANOVA followed by the Tukey's HSD post-hoc test at a significance level of p < 0.05. Regression analysis was performed to investigate the correlation between the DC and radiant energy, and the DC and thickness. RESULTS Although the type and shade of CAD/CAM material significantly affect transmitted light irradiation (p < 0.0001), degrees of conversion are similar when the CAD/CAM material or material shade were taken into consideration (p > 0.05). Conversely, material thickness significantly affected light transmission (p < 0.0001) and DC (p < 0.0001). Multiple effects of material, shade, and thickness did not significantly affect the evaluated parameters (p = 0.638 for light irradiation; p = 0.637 for DC). Linear regression analysis showed a correlation between delivered energy and DC% results of the Vita Enamic (R² = 0.4169, p < 0.0001). CONCLUSION Reduced light transmission in 2-mm-thick specimens of all CAD/CAM materials indicates that proper curing of the cement beneath CAD/CAM materials should be ensured.
{"title":"Light Transmission of Novel CAD/CAM Materials and Their Influence on the Degree of Conversion of a Dual-curing Resin Cement.","authors":"Ferhan Egilmez, G. Ergun, I. Cekic-Nagas, P. Vallittu, L. Lassila","doi":"10.3290/j.jad.a37722","DOIUrl":"https://doi.org/10.3290/j.jad.a37722","url":null,"abstract":"PURPOSE To evaluate the light transmission characteristics of different types, shades, and thicknesses of novel CAD/CAM materials and their effect on the degree of conversion (DC) of a dual-curing resin cement. MATERIALS AND METHODS Square specimens (12 × 12 mm2) of three CAD/CAM materials - GC Cerasmart, Lava Ultimate, Vita Enamic - of different thicknesses (1.00, 1.50, and 2.00 mm, n = 5 per thickness) were irradiated with an LED unit. The amount of transmitted light was quantified. Thereafter, the DC% of the dual-curing resin cement (RelyX Ultimate) was recorded after 15 min using Fourier transform infrared spectroscopy. Statistical analysis was performed using two-way ANOVA followed by the Tukey's HSD post-hoc test at a significance level of p < 0.05. Regression analysis was performed to investigate the correlation between the DC and radiant energy, and the DC and thickness. RESULTS Although the type and shade of CAD/CAM material significantly affect transmitted light irradiation (p < 0.0001), degrees of conversion are similar when the CAD/CAM material or material shade were taken into consideration (p > 0.05). Conversely, material thickness significantly affected light transmission (p < 0.0001) and DC (p < 0.0001). Multiple effects of material, shade, and thickness did not significantly affect the evaluated parameters (p = 0.638 for light irradiation; p = 0.637 for DC). Linear regression analysis showed a correlation between delivered energy and DC% results of the Vita Enamic (R² = 0.4169, p < 0.0001). CONCLUSION Reduced light transmission in 2-mm-thick specimens of all CAD/CAM materials indicates that proper curing of the cement beneath CAD/CAM materials should be ensured.","PeriodicalId":94234,"journal":{"name":"The journal of adhesive dentistry","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2017-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"88161676","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Editorial: Editors are Not Publication Police.","authors":"R. Frankenberger, B. Van Meerbeek","doi":"10.3290/j.jad.a35627","DOIUrl":"https://doi.org/10.3290/j.jad.a35627","url":null,"abstract":"","PeriodicalId":94234,"journal":{"name":"The journal of adhesive dentistry","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2016-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"83586046","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
S. Soliman, R. Preidl, Sabine Karl, N. Hofmann, G. Krastl, B. Klaiber
PURPOSE To investigate the influence of three cavity designs on the marginal seal of large Class II cavities restored with low-shrinkage resin composite limited to the enamel. MATERIALS AND METHODS One hundred twenty (120) intact human molars were randomly divided into 12 groups, with three different cavity designs: 1. undermined enamel, 2. box-shaped, and 3. proximal bevel. The teeth were restored with 1. an extra-low shrinkage (ELS) composite free of diluent monomers, 2. microhybrid composite (Herculite XRV), 3. nanohybrid composite (Filtek Supreme XTE), and 4. silorane-based composite (Filtek Silorane). After artificial aging by thermocycling and storage in physiological saline, epoxy resin replicas were prepared. To determine the integrity of the restorations' approximal margins, two methods were sequentially employed: 1. replicas were made of the 120 specimens and examined using SEM, and 2. the same 120 specimens were immersed in AgNO3 solution, and the dye penetration depth was observed with a light microscope. Statistical analysis was performed using the Kruskal-Wallis and the Dunn-Bonferroni tests. RESULTS After bevel preparation, SEM observations showed that restorations did not exhibit a higher percentage of continuous margin (SEM-analysis; p>0.05), but more leakage was found than with the other cavity designs (p<0.05). The lowest percentage of continuous margin was observed in ELS restorations (p<0.05). More fractured margins were observed in the undermined enamel cavity design groups (p<0.05). CONCLUSION Bevel preparation failed to improve margin quality in large Class II composite restorations and is no longer recommended. However, undermined enamel should be removed to prevent enamel fractures.
{"title":"Influence of Cavity Margin Design and Restorative Material on Marginal Quality and Seal of Extended Class II Resin Composite Restorations In Vitro.","authors":"S. Soliman, R. Preidl, Sabine Karl, N. Hofmann, G. Krastl, B. Klaiber","doi":"10.3290/j.jad.a35520","DOIUrl":"https://doi.org/10.3290/j.jad.a35520","url":null,"abstract":"PURPOSE To investigate the influence of three cavity designs on the marginal seal of large Class II cavities restored with low-shrinkage resin composite limited to the enamel. MATERIALS AND METHODS One hundred twenty (120) intact human molars were randomly divided into 12 groups, with three different cavity designs: 1. undermined enamel, 2. box-shaped, and 3. proximal bevel. The teeth were restored with 1. an extra-low shrinkage (ELS) composite free of diluent monomers, 2. microhybrid composite (Herculite XRV), 3. nanohybrid composite (Filtek Supreme XTE), and 4. silorane-based composite (Filtek Silorane). After artificial aging by thermocycling and storage in physiological saline, epoxy resin replicas were prepared. To determine the integrity of the restorations' approximal margins, two methods were sequentially employed: 1. replicas were made of the 120 specimens and examined using SEM, and 2. the same 120 specimens were immersed in AgNO3 solution, and the dye penetration depth was observed with a light microscope. Statistical analysis was performed using the Kruskal-Wallis and the Dunn-Bonferroni tests. RESULTS After bevel preparation, SEM observations showed that restorations did not exhibit a higher percentage of continuous margin (SEM-analysis; p>0.05), but more leakage was found than with the other cavity designs (p<0.05). The lowest percentage of continuous margin was observed in ELS restorations (p<0.05). More fractured margins were observed in the undermined enamel cavity design groups (p<0.05). CONCLUSION Bevel preparation failed to improve margin quality in large Class II composite restorations and is no longer recommended. However, undermined enamel should be removed to prevent enamel fractures.","PeriodicalId":94234,"journal":{"name":"The journal of adhesive dentistry","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2016-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"76062133","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
R. Pilo, T. Brosh, Valery Geron, S. Levartovsky, G. Eliades
PURPOSE To investigate the influence of silane reaction time on the repair strength of an aged nanofilled composite and to characterize the bonding mechanism. MATERIALS AND METHODS Nanofilled composite disks (n = 110, Filtek Supreme XT) were aged for 90 days in water. After tribochemical treatment (CoJet-Sand), the specimens were assigned to 5 groups (n = 22), primed with silane (Espe-Sil), and left to react for 1, 2, 3, 4, and 5 min. A thin layer of adhesive (Visio-Bond) was applied and a new composite with the same dimension was placed and cured. Non-aged specimens immediately layered and cured using the incremental technique served as controls. After aging (30 days in water plus 5000 thermal cycles), the interface was subjected to a shearing force until failure. Failure mode was evaluated under a stereomicroscope and scanning electron microscopy (SEM). Additional aged and treated surfaces were evaluated for morphology as well as elemental and molecular composition using SEM/EDX and ATR-FTIR. RESULTS The mean shear bond strength (SBS) of the repaired specimens was 53.9 ± 8.6 MPa, with no significant difference among the various reaction times, but significantly lower compared to the control (88.1 ± 12.5 MPa). Tribochemical treatment created an irregular surface morphology with particles imbedded in the aged surface. Interfacial SEM/EDX analysis showed a 5-μm non-uniform high atomic number zone rich in Al and Si. CONCLUSION Tribochemical treatments for repairing composite using a short silane reaction period (1 min) are equally effective as the prolonged reaction periods (2 to 5 min), yielding interfacial shear strength of ~60% of unrepaired material.
{"title":"Effect of Silane Reaction Time on the Repair of a Nanofilled Composite Using Tribochemical Treatment.","authors":"R. Pilo, T. Brosh, Valery Geron, S. Levartovsky, G. Eliades","doi":"10.3290/j.jad.a35907","DOIUrl":"https://doi.org/10.3290/j.jad.a35907","url":null,"abstract":"PURPOSE To investigate the influence of silane reaction time on the repair strength of an aged nanofilled composite and to characterize the bonding mechanism. MATERIALS AND METHODS Nanofilled composite disks (n = 110, Filtek Supreme XT) were aged for 90 days in water. After tribochemical treatment (CoJet-Sand), the specimens were assigned to 5 groups (n = 22), primed with silane (Espe-Sil), and left to react for 1, 2, 3, 4, and 5 min. A thin layer of adhesive (Visio-Bond) was applied and a new composite with the same dimension was placed and cured. Non-aged specimens immediately layered and cured using the incremental technique served as controls. After aging (30 days in water plus 5000 thermal cycles), the interface was subjected to a shearing force until failure. Failure mode was evaluated under a stereomicroscope and scanning electron microscopy (SEM). Additional aged and treated surfaces were evaluated for morphology as well as elemental and molecular composition using SEM/EDX and ATR-FTIR. RESULTS The mean shear bond strength (SBS) of the repaired specimens was 53.9 ± 8.6 MPa, with no significant difference among the various reaction times, but significantly lower compared to the control (88.1 ± 12.5 MPa). Tribochemical treatment created an irregular surface morphology with particles imbedded in the aged surface. Interfacial SEM/EDX analysis showed a 5-μm non-uniform high atomic number zone rich in Al and Si. CONCLUSION Tribochemical treatments for repairing composite using a short silane reaction period (1 min) are equally effective as the prolonged reaction periods (2 to 5 min), yielding interfacial shear strength of ~60% of unrepaired material.","PeriodicalId":94234,"journal":{"name":"The journal of adhesive dentistry","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2016-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"83895870","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
PURPOSE To evaluate the microshear bond strength of tri-calcium silicate-based materials to different restorative materials. MATERIALS AND METHODS Thirty-five disks of TheraCal LC and Biodentine were fabricated using teflon molds according to manufacturers' instructions. Then the specimens were randomly divided into 7 groups according to the materials applied: Fuji IX, Fuji II, Equia Fil, Vertise Flow, Filtek Bulk Fill Posterior Restorative, Filtek Z250 with Prime&Bond NT and with Clearfil SE Bond. All restorative materials were placed onto the disks using tygon tubes. Following a storage period, the specimens underwent microshear bond strength testing in a universal testing machine, and fracture modes were analyzed. Data were analyzed using one-way ANOVA and Tukey's post-hoc test. RESULTS For all restorative materials, TheraCal LC showed significantly higher μSBS values compared to Biodentine. GIC based materials showed the lowest μSBS for TheraCal and Biodentine. For Biodentine, Filtek Z250 applied with Prime&Bond NT and Filtek Bulk Fill Posterior Restorative applied with Scotchbond Universal Adhesive exhibited the highest μSBS, while Filtek Z250 applied with Clearfil SE Bond revealed the highest bond strength to TheraCal LC. CONCLUSION For all restorative materials tested in this study, TheraCal LC showed higher μSBS compared to Biodentine. For both TheraCal LC and Biodentine, the placement of GIC-based materials prior to composite resin restorations might decrease the bond strength. Composite resins applied with self-etching adhesives increased the bond strength of TheraCal LC; however, for Biodentine, application of etch-and-rinse adhesives may improve the adhesion of composite resins.
目的评价硅酸盐三钙基材料与不同修复材料的微剪切结合强度。材料与方法根据生产厂家的说明书，采用特氟龙模具制备了35片TheraCal LC和Biodentine。然后根据所用材料随机分为7组:Fuji IX、Fuji II、Equia Fil、Vertise Flow、Filtek Bulk Fill Posterior Restorative、Filtek Z250 with Prime&Bond NT和Clearfil SE Bond。所有的修复材料都用钛管放置在磁盘上。保存一段时间后，在万能试验机上进行微剪粘结强度测试，并分析断裂模式。数据分析采用单因素方差分析和Tukey事后检验。结果在所有修复材料中，TheraCal LC的μSBS值均显著高于Biodentine。GIC基材料对TheraCal和Biodentine的μSBS最低。对于Biodentine, Filtek Z250与Prime&Bond NT、Filtek Bulk Fill Posterior Restorative与Scotchbond Universal Adhesive的结合μSBS最高，而Filtek Z250与TheraCal LC的结合μSBS最高。结论在所有修复材料中，TheraCal LC的μSBS均高于Biodentine。对于TheraCal LC和Biodentine，在复合树脂修复体之前放置ic基材料可能会降低结合强度。复合树脂与自蚀刻胶粘剂的结合提高了TheraCal LC的结合强度;然而，对于Biodentine，应用蚀刻-漂洗粘合剂可以改善复合树脂的附着力。
{"title":"Microshear Bond Strength of Tri-Calcium Silicate-based Cements to Different Restorative Materials.","authors":"E. Cengiz, N. Ulusoy","doi":"10.3290/j.jad.a35934","DOIUrl":"https://doi.org/10.3290/j.jad.a35934","url":null,"abstract":"PURPOSE To evaluate the microshear bond strength of tri-calcium silicate-based materials to different restorative materials. MATERIALS AND METHODS Thirty-five disks of TheraCal LC and Biodentine were fabricated using teflon molds according to manufacturers' instructions. Then the specimens were randomly divided into 7 groups according to the materials applied: Fuji IX, Fuji II, Equia Fil, Vertise Flow, Filtek Bulk Fill Posterior Restorative, Filtek Z250 with Prime&Bond NT and with Clearfil SE Bond. All restorative materials were placed onto the disks using tygon tubes. Following a storage period, the specimens underwent microshear bond strength testing in a universal testing machine, and fracture modes were analyzed. Data were analyzed using one-way ANOVA and Tukey's post-hoc test. RESULTS For all restorative materials, TheraCal LC showed significantly higher μSBS values compared to Biodentine. GIC based materials showed the lowest μSBS for TheraCal and Biodentine. For Biodentine, Filtek Z250 applied with Prime&Bond NT and Filtek Bulk Fill Posterior Restorative applied with Scotchbond Universal Adhesive exhibited the highest μSBS, while Filtek Z250 applied with Clearfil SE Bond revealed the highest bond strength to TheraCal LC. CONCLUSION For all restorative materials tested in this study, TheraCal LC showed higher μSBS compared to Biodentine. For both TheraCal LC and Biodentine, the placement of GIC-based materials prior to composite resin restorations might decrease the bond strength. Composite resins applied with self-etching adhesives increased the bond strength of TheraCal LC; however, for Biodentine, application of etch-and-rinse adhesives may improve the adhesion of composite resins.","PeriodicalId":94234,"journal":{"name":"The journal of adhesive dentistry","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2016-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"88593644","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
PURPOSE The aim of this finite-element stress analysis (FEA) was to determine the effect of degradation due to water storage on stress distributions in root-filled premolar models restored with composite using either a self-etch (SE) or an etch-and-rinse (E&R) adhesive. MATERIALS AND METHODS Four premolar FEA models including root filling, MOD cavity, and composite restorations were created. The cavities were assumed to be treated by SE or E&R adhesives and stored in water for 18 months. The elastic properties of the adhesive-dentin interface after 24-h and 18-month water storage were obtained from the literature and applied to the FEA models. A 300-N load was applied on the functional cusps of the models. The SolidWorks/Cosmosworks structural analysis program was used and the results were presented considering the von Mises stresses. RESULTS Stresses in the cervical region increased over time on the load-application side of the main tooth models (SE: 84.11 MPa to 87.51 MPa; E&R: 100.24 MPa to 120.8 MPa). When the adhesive interfaces (hybrid layer, adhesive layer) and dentin were evaluated separately, the stresses near the root canal orifices increased over time in both models; however, this change was more noticeable in the E&R models. Stresses at the cavity corners decreased in the E&R model (within the adhesive layer), while SE models showed the opposite (within the hybrid layer). CONCLUSION Change in the elastic modulus of the adhesive layer, hybrid layer, and dentin due to water storage has an effect on stresses in root-filled premolar models. The location and the level of the stresses differed depending on the adhesive used.
{"title":"Can Degradation of Adhesive Interfaces Due to Water Storage Affect Stress Distributions? A Finite-Element Stress Analysis Study.","authors":"S. Belli, O. Eraslan, G. Eskitaşçıoğlu","doi":"10.3290/j.jad.a37142","DOIUrl":"https://doi.org/10.3290/j.jad.a37142","url":null,"abstract":"PURPOSE The aim of this finite-element stress analysis (FEA) was to determine the effect of degradation due to water storage on stress distributions in root-filled premolar models restored with composite using either a self-etch (SE) or an etch-and-rinse (E&R) adhesive. MATERIALS AND METHODS Four premolar FEA models including root filling, MOD cavity, and composite restorations were created. The cavities were assumed to be treated by SE or E&R adhesives and stored in water for 18 months. The elastic properties of the adhesive-dentin interface after 24-h and 18-month water storage were obtained from the literature and applied to the FEA models. A 300-N load was applied on the functional cusps of the models. The SolidWorks/Cosmosworks structural analysis program was used and the results were presented considering the von Mises stresses. RESULTS Stresses in the cervical region increased over time on the load-application side of the main tooth models (SE: 84.11 MPa to 87.51 MPa; E&R: 100.24 MPa to 120.8 MPa). When the adhesive interfaces (hybrid layer, adhesive layer) and dentin were evaluated separately, the stresses near the root canal orifices increased over time in both models; however, this change was more noticeable in the E&R models. Stresses at the cavity corners decreased in the E&R model (within the adhesive layer), while SE models showed the opposite (within the hybrid layer). CONCLUSION Change in the elastic modulus of the adhesive layer, hybrid layer, and dentin due to water storage has an effect on stresses in root-filled premolar models. The location and the level of the stresses differed depending on the adhesive used.","PeriodicalId":94234,"journal":{"name":"The journal of adhesive dentistry","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2016-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"91136600","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
PURPOSE To test the effect of surface conditioning protocols on the reparability of CAD/CAM zirconia-reinforced lithium silicate ceramic compared to lithium-disilicate glass ceramic. MATERIALS AND METHODS Zirconia-reinforced lithium silicate ceramic (Vita Suprinity) and lithium disilicate glass-ceramic blocks (IPS e.max CAD) were categorized into four groups based on the surface conditioning protocol used. Group C: no treatment (control); group HF: 5% hydrofluoric acid etching for 60 s, silane (Monobond-S) application for 60 s, air drying; group HF-H: 5% HF acid etching for 60 s, application of silane for 60 s, air drying, application of Heliobond, light curing for 20 s; group CO: sandblasting with CoJet sand followed by silanization. Composite resin (Tetric EvoCeram) was built up into 4 x 6 x 3 mm blocks using teflon molds. All specimens were subjected to thermocycling (5000x, 5°C to 55°C). The microtensile bond strength test was employed at a crosshead speed of 1 mm/min. SEM was employed for evaluation of all the debonded microbars, the failure type was categorized as either adhesive (failure at adhesive layer), cohesive (failure at ceramic or composite resin), or mixed (failure between adhesive layer and substrate). Two-way ANOVA and the Tukey's HSD post-hoc test were applied to test for significant differences in bond strength values in relation to different materials and surface pretreatment (p < 0.05). RESULTS The highest microtensile repair bond strength for Vita Suprinity was reported in group CO (33.1 ± 2.4 MPa) and the lowest in group HF (27.4 ± 4.4 MPa). Regarding IPS e.max CAD, group CO showed the highest (30.5 ± 4.9 MPa) and HF the lowest microtensile bond strength (22.4 ± 5.7 MPa). Groups HF, HF-H, and CO showed statistically significant differences in terms of all ceramic types used (p < 0.05). The control group showed exclusively adhesive failures, while in HF, HF-H, and CO groups, mixed failures were predominant. CONCLUSIONS Repair bond strength to zirconia-reinforced lithium silicate ceramics and lithium-disilicate glass ceramic could be improved when ceramic surfaces are sandblasted with CoJet sand followed by silanization.
{"title":"Influence of Surface Conditioning Protocols on Reparability of CAD/CAM Zirconia-reinforced Lithium Silicate Ceramic.","authors":"Rana Al-Thagafi, W. Al-Zordk, Samah Saker","doi":"10.3290/j.jad.a35909","DOIUrl":"https://doi.org/10.3290/j.jad.a35909","url":null,"abstract":"PURPOSE To test the effect of surface conditioning protocols on the reparability of CAD/CAM zirconia-reinforced lithium silicate ceramic compared to lithium-disilicate glass ceramic. MATERIALS AND METHODS Zirconia-reinforced lithium silicate ceramic (Vita Suprinity) and lithium disilicate glass-ceramic blocks (IPS e.max CAD) were categorized into four groups based on the surface conditioning protocol used. Group C: no treatment (control); group HF: 5% hydrofluoric acid etching for 60 s, silane (Monobond-S) application for 60 s, air drying; group HF-H: 5% HF acid etching for 60 s, application of silane for 60 s, air drying, application of Heliobond, light curing for 20 s; group CO: sandblasting with CoJet sand followed by silanization. Composite resin (Tetric EvoCeram) was built up into 4 x 6 x 3 mm blocks using teflon molds. All specimens were subjected to thermocycling (5000x, 5°C to 55°C). The microtensile bond strength test was employed at a crosshead speed of 1 mm/min. SEM was employed for evaluation of all the debonded microbars, the failure type was categorized as either adhesive (failure at adhesive layer), cohesive (failure at ceramic or composite resin), or mixed (failure between adhesive layer and substrate). Two-way ANOVA and the Tukey's HSD post-hoc test were applied to test for significant differences in bond strength values in relation to different materials and surface pretreatment (p < 0.05). RESULTS The highest microtensile repair bond strength for Vita Suprinity was reported in group CO (33.1 ± 2.4 MPa) and the lowest in group HF (27.4 ± 4.4 MPa). Regarding IPS e.max CAD, group CO showed the highest (30.5 ± 4.9 MPa) and HF the lowest microtensile bond strength (22.4 ± 5.7 MPa). Groups HF, HF-H, and CO showed statistically significant differences in terms of all ceramic types used (p < 0.05). The control group showed exclusively adhesive failures, while in HF, HF-H, and CO groups, mixed failures were predominant. CONCLUSIONS Repair bond strength to zirconia-reinforced lithium silicate ceramics and lithium-disilicate glass ceramic could be improved when ceramic surfaces are sandblasted with CoJet sand followed by silanization.","PeriodicalId":94234,"journal":{"name":"The journal of adhesive dentistry","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2016-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"79632633","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"International Academy for Adhesive Dentistry (IAAD).","authors":"M. Blatz","doi":"10.3290/j.jad.a35978","DOIUrl":"https://doi.org/10.3290/j.jad.a35978","url":null,"abstract":"","PeriodicalId":94234,"journal":{"name":"The journal of adhesive dentistry","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2016-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"83382151","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Sandra Ribeiro Barros da Cunha, Pedro Augusto Mendes Ramos, C. Haddad, J. L. D. da Silva, E. Fregnani, A. Aranha
PURPOSE To evaluate the effects of three different radiation doses on the bond strengths of two different adhesive systems to enamel and dentin. MATERIALS AND METHODS Eighty human third molars were randomly divided into four groups (n = 20) according to the radiation dose (control/no radiation, 20 Gy, 40 Gy, and 70 Gy). The teeth were sagittally sectioned into three slices: one mesial and one distal section containing enamel and one middle section containing dentin. The sections were then placed in the enamel and dentin groups, which were further divided into two subgroups (n = 10) according to the adhesive used. Three restorations were performed in each tooth (one per section) using Adper Single Bond 2 (3M ESPE) or Universal Single Bond (3M ESPE) adhesive system and Filtek Z350 XT (3M ESPE) resin composite and subjected to the microshear bond test. Data were analyzed using a two-way ANOVA followed by Tukey's test. Failure modes were examined under a stereoscopic loupe. RESULTS Radiotherapy did not affect the bond strengths of the adhesives to either enamel or dentin. In dentin, the Universal Single Bond adhesive system showed higher bond strength values when compared with the Adper Single Bond adhesive system. More adhesive failures were observed in the enamel for all radiation doses and adhesives. CONCLUSION Radiotherapy did not influence the bond strength to enamel or dentin, irrespective of the adhesive or radiation dose used.
目的评价三种不同辐射剂量对两种不同粘接系统对牙本质和牙釉质粘接强度的影响。材料与方法将80颗人第三磨牙按辐照剂量(对照/无辐照、20 Gy、40 Gy、70 Gy)随机分为4组(n = 20)。牙矢状切面分为三片:含牙釉质的近端和远端切片，含牙本质的中间切片。然后将切片分为牙本质组和牙釉质组，根据使用的粘接剂再分为两个亚组(n = 10)。使用Adper Single Bond 2 (3M ESPE)或Universal Single Bond (3M ESPE)胶粘剂系统和Filtek Z350 XT (3M ESPE)树脂复合材料对每颗牙齿进行3次修复(每节1次)，并进行微剪切粘接测试。数据分析采用双因素方差分析和Tukey检验。在立体镜下检测了失效模式。结果放疗对牙本质和牙釉质黏合剂的结合强度均无影响。在牙本质中，Universal Single Bond系统比Adper Single Bond系统具有更高的粘接强度值。在所有辐射剂量和黏合剂的情况下，牙釉质中黏合剂失效的情况较多。结论放疗不影响牙本质与牙釉质的结合强度，与使用的黏合剂或放射剂量无关。
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A. Tsujimoto, W. Barkmeier, T. Takamizawa, M. Latta, M. Miyazaki
PURPOSE To examine the influence of the oxygen inhibited layer (OIL) on shear bond strength (SBS) to dentin and surface free energy (SFE) characteristics of different adhesive systems. MATERIALS AND METHODS Three adhesive systems were used: Scotchbond Multipurpose (SM), Clearfil SE Bond (CS), and Scotchbond Universal (SU). Resin composite was bonded to dentin surfaces to determine SBS with and without OIL of adhesives. The SFE, dispersion force (γSd), polarity force (γSp), and hydrogen bonding force (γSh) of cured adhesives with and without an OIL were measured. Two-way ANOVA and Tukey's honestly significant difference (HSD) test were used for analysis of SBS data, and one-way ANOVA and Tukey's HSD test were used for the SFE and contact angle data. RESULTS The SBS of SM and CS showed no significant differences between specimens with and without the OIL. However, the SBS of SU with the OIL was significantly higher than without the OIL. The SFE, γSp, and γSh of cured adhesives with an OIL were significantly higher than those of cured adhesives without an OIL. The SFE, γSp, and γSh of SM and CS with an OIL were significantly higher than those of SU with an OIL. CONCLUSION The results of this study indicate that the presence of an OIL with a single-step self-etching adhesive promotes higher SBS to dentin, unlike in the other types of adhesive systems. The SFE characteristics of the OIL of dental adhesives differed depending on the type of adhesive system.
目的探讨抑氧层(OIL)对不同粘接体系牙本质剪切粘接强度(SBS)和表面自由能(SFE)特性的影响。材料与方法采用三种胶粘剂体系:Scotchbond Multipurpose (SM)、Clearfil SE Bond (CS)和Scotchbond Universal (SU)。将树脂复合材料粘接在牙本质表面，测定了粘接剂有油和无油情况下的SBS。测定了添加和不添加OIL固化胶粘剂的SFE、分散力(γSd)、极性力(γSp)和氢键力(γSh)。SBS数据采用双因素方差分析和Tukey’s honest significant difference (HSD)检验，SFE和接触角数据采用单因素方差分析和Tukey’s HSD检验。结果SM和CS的SBS在加油和不加油的标本间无显著差异。然而，添加了OIL的SU的SBS显著高于未添加OIL的SU。添加了OIL的胶粘剂的SFE、γSp和γSh均显著高于未添加OIL的胶粘剂。SM和CS组的SFE、γSp和γSh均显著高于SU组。结论与其他类型的粘接系统不同，单步自蚀刻粘接油的存在可以提高牙本质的SBS。齿科胶粘剂油的SFE特性随胶粘剂体系的不同而不同。
{"title":"Influence of the Oxygen-inhibited Layer on Bonding Performance of Dental Adhesive Systems: Surface Free Energy Perspectives.","authors":"A. Tsujimoto, W. Barkmeier, T. Takamizawa, M. Latta, M. Miyazaki","doi":"10.3290/j.jad.a35515","DOIUrl":"https://doi.org/10.3290/j.jad.a35515","url":null,"abstract":"PURPOSE To examine the influence of the oxygen inhibited layer (OIL) on shear bond strength (SBS) to dentin and surface free energy (SFE) characteristics of different adhesive systems. MATERIALS AND METHODS Three adhesive systems were used: Scotchbond Multipurpose (SM), Clearfil SE Bond (CS), and Scotchbond Universal (SU). Resin composite was bonded to dentin surfaces to determine SBS with and without OIL of adhesives. The SFE, dispersion force (γSd), polarity force (γSp), and hydrogen bonding force (γSh) of cured adhesives with and without an OIL were measured. Two-way ANOVA and Tukey's honestly significant difference (HSD) test were used for analysis of SBS data, and one-way ANOVA and Tukey's HSD test were used for the SFE and contact angle data. RESULTS The SBS of SM and CS showed no significant differences between specimens with and without the OIL. However, the SBS of SU with the OIL was significantly higher than without the OIL. The SFE, γSp, and γSh of cured adhesives with an OIL were significantly higher than those of cured adhesives without an OIL. The SFE, γSp, and γSh of SM and CS with an OIL were significantly higher than those of SU with an OIL. CONCLUSION The results of this study indicate that the presence of an OIL with a single-step self-etching adhesive promotes higher SBS to dentin, unlike in the other types of adhesive systems. The SFE characteristics of the OIL of dental adhesives differed depending on the type of adhesive system.","PeriodicalId":94234,"journal":{"name":"The journal of adhesive dentistry","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2016-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"83900029","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
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