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Thermal heat-balance mode flow-to-frequency converter 热平衡式流量-频率转换器
Pub Date : 2016-11-10 DOI: 10.1117/12.2243598
E. Pawłowski
This paper presents new type of thermal flow converter with the pulse frequency output. The integrating properties of the temperature sensor have been used, which allowed for realization of pulse frequency modulator with thermal feedback loop, stabilizing temperature of sensor placed in the flowing medium. The system assures balancing of heat amount supplied in impulses to the sensor and heat given up by the sensor in a continuous way to the flowing medium. Therefore the frequency of output impulses is proportional to the heat transfer coefficient from sensor to environment. According to the King’s law, the frequency of those impulses is a function of medium flow velocity around the sensor. The special feature of presented solution is total integration of thermal sensor with the measurement signal conditioning system. Sensor and conditioning system are not the separate elements of the measurement circuit, but constitute a whole in form of thermal heat-balance mode flow-to-frequency converter. The advantage of such system is easiness of converting the frequency signal to the digital form, without using any additional analogue-to-digital converters. The frequency signal from the converter may be directly connected to the microprocessor input, which with use of standard built-in counters may convert the frequency into numerical value of high precision. Moreover, the frequency signal has higher resistance to interference than the voltage signal and may be transmitted to remote locations without the information loss.
介绍了一种新型脉冲频率输出的热流变换器。利用温度传感器的积分特性,实现了带热反馈回路的脉冲调频器,稳定了传感器在流动介质中的温度。该系统保证了以脉冲形式提供给传感器的热量和传感器以连续方式向流动介质释放的热量的平衡。因此,输出脉冲的频率与从传感器到环境的传热系数成正比。根据金定律,这些脉冲的频率是传感器周围介质流速的函数。该方案的特点是将热传感器与测量信号调理系统完全集成。传感器和调节系统不是测量电路中单独的元件,而是以热平衡模式的流量-频率转换器的形式构成一个整体。这种系统的优点是易于将频率信号转换为数字形式,而不需要使用任何额外的模数转换器。变频器的频率信号可直接连接到微处理器输入端,微处理器使用标准内置计数器将频率转换成高精度的数值。此外,频率信号比电压信号具有更高的抗干扰性,并且可以在不丢失信息的情况下传输到远程位置。
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引用次数: 3
Zirconia-based mixed potential sensor with Pt electrode prepared by spin-coating of polymeric precursor 聚合前驱体自旋涂覆制备氧化锆基Pt电极混合电位传感器
Pub Date : 2016-11-10 DOI: 10.1117/12.2247539
A. Chrzan, Ł. Woźniak, D. Szymczewska, P. Jasiński
Many types of yttria-stabilized zirconia (YSZ) based gas sensors have been explored extensively in recent years. Great attention have been directed to mixed-potential-type gas sensors. It is due to growing concerns with environmental issues. Not without a significance is the fact of very attractive performance of this type of sensor allowing to detect low concentration of pollutant gases. In this paper two types of YSZ based mixed-potential planar sensors were investigated, with platinum electrode painted using commercial paste and with spin coated platinum layer. Both types had second electrode in the form of porous gold. Measurements were performed at 400 °C in synthetic air and different concentrations of SO2. Gas flow was set to 100 cm3min-1 and the concentration of 50 ppm SO2 was tested. During this measurements the sensor was sintered in-situ at increasing temperatures. Sensor with 100 nm spin-coated platinum layer sintered at 700 °C was shown to exhibit two times smaller response than sensor with 5 μm porous electrode, while consisting of over 20 times smaller amount of Pt. The influence of sintering temperature on electrical conductivity of platinum films was also examined. Moreover, the platinum microstructure was investigated using SEM microscopy.
近年来,许多类型的氧化钇稳定氧化锆(YSZ)气体传感器得到了广泛的研究。混合电位型气体传感器受到了极大的关注。这是由于人们越来越关注环境问题。并非没有意义的事实是非常有吸引力的性能,这种类型的传感器允许检测低浓度的污染气体。本文研究了两种基于YSZ的混合电位平面传感器,一种是用商业浆料涂覆铂电极,另一种是用自旋涂覆铂层。两种类型都有多孔金形式的第二电极。测量在400°C的合成空气和不同浓度的SO2中进行。气体流量设置为100 cm3min-1,测试SO2浓度为50 ppm。在测量过程中,传感器在不断升高的温度下就地烧结。结果表明,在700℃下烧结的100 nm自旋涂覆铂层传感器的响应比5 μm多孔电极传感器的响应小2倍,而铂的含量却少20倍以上。同时,研究了烧结温度对铂膜电导率的影响。利用扫描电镜对铂的微观结构进行了研究。
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引用次数: 0
Comparison of the measurement techniques employed for evaluation of ambient air odor quality 环境空气气味质量评价测量技术的比较
Pub Date : 2016-11-10 DOI: 10.1117/12.2244678
Wojciech Wojnowski, T. Majchrzak, J. Gębicki, T. Dymerski, J. Namieśnik
The paper presents the results of investigation on ambient air odor quality in a vicinity of the industrial sewage treatment plant being a part of the crude oil processing plant. The investigation was performed during spring-winter season using a prototype of electronic nose and the Nasal Ranger field olfactometers. The prototype was equipped with a set of six semiconductor sensors by FIGARO Co. and one PID-type sensor. The field olfactometers were used to determine mean concentration of odorants, which amounted from 2.2 to 20.2 ou/m3 depending on the place of measurement. In case of the investigation with the electronic nose prototype a classification of the ambient air samples with respect to the place of sampling was performed utilizing the kNN (where k=3) algorithm supported with a cross-validation method. Correct classification of the ambient air samples was at the level of 47.9%. Performed investigation revealed that evaluation of the ambient air samples with respect to odor was possible using the electronic nose instrument.
本文介绍了某原油加工厂所属工业污水处理厂附近环境空气气味质量的调查结果。调查在春冬季节使用电子鼻原型和鼻游骑兵现场嗅觉计进行。原型机配备了一套由费加罗公司生产的6个半导体传感器和一个pid型传感器。使用现场嗅觉仪确定气味剂的平均浓度,根据测量地点的不同,平均浓度为2.2至20.2 ou/m3。在使用电子鼻原型进行调查的情况下,利用交叉验证方法支持的kNN(其中k=3)算法对采样地点的环境空气样本进行分类。环境空气样本分类正确率为47.9%。进行的调查显示,使用电子鼻仪器对环境空气样本的气味进行评估是可能的。
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引用次数: 1
Sol-gel layers for ceramic microsystems application 用于陶瓷微系统的溶胶-凝胶层
Pub Date : 2016-11-10 DOI: 10.1117/12.2245785
Mateusz Czok, L. Golonka
This paper describes research on sol-gel solutions preparation process. Utilize of a sol-gel layers in the LTCC technology for reduction of surface roughness and influence on the ceramics properties is examined and described. The influence of sol-gel layer on possible sedimentation of dyes or biological substances in channels, mixers or chambers of ceramic microfluidic structures was investigated. Moreover, properties of sol-gel coated surfaces have been precisely examined and described. Finally, positive results of conducted experiments made it possible to design and manufacture a simple microfluidic ceramic structure, with embedded protective layer of sol-gel, for fluorescence measurements.
本文对溶胶-凝胶溶液的制备工艺进行了研究。在LTCC技术中利用溶胶-凝胶层来降低表面粗糙度和对陶瓷性能的影响进行了研究和描述。研究了溶胶-凝胶层对染料或生物物质在陶瓷微流控结构的通道、混合器或腔室中可能沉降的影响。此外,溶胶-凝胶涂层表面的性质已经被精确地检查和描述。最后,实验的积极结果使设计和制造一种简单的微流控陶瓷结构成为可能,该结构具有嵌入的溶胶-凝胶保护层,用于荧光测量。
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引用次数: 1
Properties of PZT thick film made on LTCC substrates with dielectric intermediate layers 具有介电中间层的LTCC衬底PZT厚膜的性能
Pub Date : 2016-11-10 DOI: 10.1117/12.2244195
A. Dąbrowski, L. Golonka
Results of experiments on application of various interlayers between LTCC (Low Temperature Cofired Ceramics) substrate and thick-film PZT (Lead Zirconate - Titanate) are described in this work. Thick-film intermediate layers were based on several dielectric materials: TiN, Al2O3, SiC, TiO2, SiC, YSZ, BN. Seven screen printable pastes were prepared on the base of powders of mentioned materials with addition of glass and organic vehicle. The substrates were made of 951 (DuPont), CeramTapeGC (CeramTec) and HL2000 (Heraeus) LTCC tapes. Sandwich type transducers, consisting of barrier layer, gold bottom electrode, PZT layer and silver top electrode were prepared and characterized. Basic piezoelectric parameters – permittivity, effective charge constant (d33(eff)) and remanent polarization were determined. The best properties were obtained for substrates made of 951. In general, interlayers based on TiO2, SiC and Al2O3 improved permittivity and charge constant comparing to bare substrates. For example, for 951 substrate the PZT layer exhibited d33(eff) equal to 160, 215, 250 and 230 pC/N for bare substrate, TiO2 interlayer, SiC interlayer and Al2O3 interlayer, respectively. In case of CeramTape GC substrates determined permittivity was equal to 215, 245, 235 and 275 for bare substrate, TiO2 interlayer, SiC interlayer and Al2O3 interlayer, respectively. In case of TiN and BN materials the parameters were considerably deteriorated.
本文介绍了低温共烧陶瓷(LTCC)衬底与厚膜PZT(锆酸铅-钛酸铅)衬底之间不同中间层的应用实验结果。厚膜中间层是基于几种介电材料:TiN, Al2O3, SiC, TiO2, SiC, YSZ, BN。在上述材料粉末的基础上,添加玻璃和有机载体制备了7种可丝网印刷的浆料。衬底由951(杜邦)、CeramTapeGC (CeramTec)和HL2000(贺利氏)LTCC胶带制成。制备了由阻挡层、金底电极、PZT层和银顶电极组成的夹层型换能器,并对其进行了表征。测定了压电基本参数介电常数、有效电荷常数d33(eff)和剩余极化。951基板的性能最好。总的来说,与裸衬底相比,基于TiO2、SiC和Al2O3的中间层提高了介电常数和电荷常数。例如,对于951衬底,裸衬底、TiO2夹层、SiC夹层和Al2O3夹层的PZT层的d33(eff)分别为160、215、250和230 pC/N。陶瓷带GC衬底的介电常数分别为215、245、235和275,分别为裸衬底、TiO2夹层、SiC夹层和Al2O3夹层。在TiN和BN材料的情况下,参数明显恶化。
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引用次数: 1
Electronic system for floor surface type detection in robotics applications 机器人应用中地板表面类型检测的电子系统
Pub Date : 2016-11-10 DOI: 10.1117/12.2249331
G. Tarapata, D. Paczesny, Łukasz Tarasiuk
The paper reports a recognizing method base on ultrasonic transducers utilized for the surface types detection. Ultra-sonic signal is transmitted toward the examined substrate, then reflected and scattered signal goes back to another ultra-sonic receiver. Thee measuring signal is generated by a piezo-electric transducer located at specified distance from the tested substrate. The detector is a second piezo-electric transducer located next to the transmitter. Depending on thee type of substrate which is exposed by an ultrasonic wave, the signal is partially absorbed inn the material, diffused and reflected towards the receiver. To measure the level of received signal, the dedicated electronic circuit was design and implemented in the presented systems. Such system was designed too recognize two types of floor surface: solid (like concrete, ceramic stiles, wood) and soft (carpets, floor coverings). The method will be applied in electronic detection system dedicated to autonomous cleaning robots due to selection of appropriate cleaning method. This work presents the concept of ultrasonic signals utilization, the design of both the measurement system and the measuring stand and as well number of wide tests results which validates correctness of applied ultrasonic method.
本文报道了一种基于超声换能器的表面类型识别方法。超声波信号向被检测的衬底发射,然后反射和散射信号返回到另一个超声波接收器。三个测量信号由一个压电换能器产生,该换能器位于距离被测基板指定的距离处。探测器是位于发射器旁边的第二个压电换能器。根据超声波所暴露的三种类型的衬底,信号部分被材料吸收,扩散并向接收器反射。为了测量接收信号的电平,设计并实现了专用的电子电路。这样的系统被设计为识别两种类型的地板表面:固体(如混凝土,陶瓷台阶,木材)和柔软(地毯,地板覆盖物)。由于选择了合适的清洁方法,该方法将应用于自主清洁机器人专用的电子检测系统中。本文介绍了超声信号利用的概念、测量系统和测量台的设计以及大量的试验结果,验证了应用超声方法的正确性。
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引用次数: 4
Monitoring of odor nuisance in the tri-city agglomeration 三城市群气味滋扰监测
Pub Date : 2016-11-10 DOI: 10.1117/12.2244679
J. Gębicki, T. Dymerski, J. Namieśnik
The paper describes a principle of operation of odor nuisance monitoring network, which is being designed in the tri-city agglomeration. Moreover, it presents the preliminary results of an investigation on ambient air quality with respect to odour nuisance in a vicinity of the municipal landfill. The investigation was performed during spring-winter season using a prototype of electronic nose and the Nasal Ranger field olfactometers. The prototype was equipped with a set of six semiconductor sensors by FIGARO Co. and one PID-type sensor. The field olfactometers were used to determine mean concentration of odorants, which amounted from 2.2 to 30.2 ou/m3 depending on the place of measurement. In case of the investigation with the electronic nose prototype a classification of the ambient air samples with respect to the place of sampling was performed utilizing kNN algorithm supported with a cross-validation method. Correct classification of the ambient air samples was at the level of 66.7%. Performed investigation revealed that discrimination of the ambient air samples differing in concentration of odorants and place of origin was possible.
本文介绍了正在设计的三城市群恶臭危害监测网络的工作原理。此外,它还介绍了对城市垃圾填埋场附近环境空气质量有关气味滋扰的初步调查结果。调查在春冬季节使用电子鼻原型和鼻游骑兵现场嗅觉计进行。原型机配备了一套由费加罗公司生产的6个半导体传感器和一个pid型传感器。使用现场嗅觉计测定气味剂的平均浓度,根据测量地点的不同,平均浓度为2.2至30.2 ou/m3。在使用电子鼻原型进行调查的情况下,利用交叉验证方法支持的kNN算法对采样地点的环境空气样本进行分类。环境空气样本分类正确率为66.7%。进行的调查显示,环境空气样品的不同浓度的气味剂和原产地的区别是可能的。
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引用次数: 0
Extraction and evaluation of gas-flow-dependent features from dynamic measurements of gas sensors array 从气体传感器阵列动态测量数据中提取与评价气体流量相关特征
Pub Date : 2016-11-10 DOI: 10.1117/12.2247541
P. Kalinowski, Ł. Woźniak, G. Jasinski, P. Jasiński
Gas analyzers based on gas sensors are the devices which enable recognition of various kinds of volatile compounds. They have continuously been developed and investigated for over three decades, however there are still limitations which slow down the implementation of those devices in many applications. For example, the main drawbacks are the lack of selectivity, sensitivity and long term stability of those devices caused by the drift of utilized sensors. This implies the necessity of investigations not only in the field of development of gas sensors construction, but also the development of measurement procedures or methods of analysis of sensor responses which compensate the limitations of sensors devices. One of the fields of investigations covers the dynamic measurements of sensors or sensor-arrays response with the utilization of flow modulation techniques. Different gas delivery patterns enable the possibility of extraction of unique features which improves the stability and selectivity of gas detecting systems. In this article three utilized flow modulation techniques are presented, together with the proposition of the evaluation method of their usefulness and robustness in environmental pollutants detecting systems. The results of dynamic measurements of an commercially available TGS sensor array in the presence of nitrogen dioxide and ammonia are shown.
基于气体传感器的气体分析仪是一种能够识别各种挥发性化合物的设备。它们已经持续开发和研究了三十多年,但是仍然存在限制,这些限制减慢了这些设备在许多应用中的实现。例如,主要的缺点是由于所用传感器的漂移导致这些设备缺乏选择性、灵敏度和长期稳定性。这意味着不仅需要在气体传感器结构的发展领域进行研究,而且还需要开发测量程序或传感器响应分析方法,以弥补传感器设备的局限性。其中一个研究领域包括利用流量调制技术动态测量传感器或传感器阵列的响应。不同的气体输送模式使得提取独特特征成为可能,从而提高了气体检测系统的稳定性和选择性。本文介绍了三种常用的流量调制技术,并提出了它们在环境污染物检测系统中的实用性和鲁棒性的评价方法。在二氧化氮和氨的存在下,显示了市售TGS传感器阵列的动态测量结果。
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引用次数: 1
Chlorine sensing properties of zinc oxide resistive gas sensor doped with platinum 掺杂铂氧化锌电阻式气体传感器的氯感特性
Pub Date : 2016-11-10 DOI: 10.1117/12.2246775
M. Fiedot, P. Suchorska-Woźniak, O. Rac, W. Nawrot, H. Teterycz
In presented studies resistive chlorine gas sensor with gas sensitive layer in the form of zinc oxide microrods doped with platinum was developed. The growth of active layer was carried out in water solution containing zinc nitrate (V), hexamethylenetetramine and chloroplatinic acid using the chemical bath deposition method. The structure and morphology of obtained sensors was characterized by scanning electron microscope (SEM) and energy-dispersive X-ray spectroscopy (EDX). To determine the chlorine gas sensing properties Temperature-Stimulated Conductance method (TSC) was used. During the measurements sensor was tested in a reference atmosphere and an atmosphere with 2, 5 or 8 ppm of chlorine. Obtained results have shown that zinc oxide microrods doped with platinum were obtained. TSC measurements showed that developed sensor allows to detect chlorine with very good sensitivity.
本文研究了一种以掺杂铂的氧化锌微棒为气敏层的电阻式氯气传感器。采用化学浴沉积法在硝酸锌(V)、六亚甲基四胺和氯铂酸的水溶液中生长活性层。利用扫描电子显微镜(SEM)和能量色散x射线能谱(EDX)对所得传感器的结构和形貌进行了表征。采用温度激发电导法(TSC)测定氯气传感性能。在测量期间,传感器在参考大气和含氯2、5或8 ppm的大气中进行了测试。结果表明,得到了掺杂铂的氧化锌微棒。TSC测量结果表明,所研制的传感器能够以非常好的灵敏度检测氯。
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引用次数: 2
Response of a fiber-optic Fabry-Pérot interferometer to refractive index and absorption changes: modeling and experiments 光纤法布里-普氏干涉仪对折射率和吸收变化的响应:建模和实验
Pub Date : 2016-11-10 DOI: 10.1117/12.2247510
J. Plucinski, K. Karpienko
This paper describes how the refractive index and the absorption of investigated substances change the spectrum of the optical radiation at the output of the fiber-optic Fabry-Pérot interferometer. The modeling of the operation of the interferometer takes into account not only the spectra of the refractive index and the absorption of the medium that is inside the cavity, but also spectra of the refractive indices of the core and the cladding of the optical fiber connected to the interferometer cavity and the parameters of the mirrors forming the cavity. The physical phenomena related to the beam diffraction inside the cavity (i.e. the beam divergence, the curvature of the wavefront, and the phase shift caused by the Gouy effect) are taken into account, too. The spectra obtained from simulations were compared to the spectra registered during measurements. The preliminary results indicate that the fiber-optic Fabry-Pérot interferometer can measure both the refractive index and the absorption of investigated substances with high accuracy.
本文描述了所研究物质的折射率和吸收如何改变光纤法布里-帕氏干涉仪输出的光辐射光谱。干涉仪工作的建模不仅考虑了干涉腔内介质的折射率光谱和吸收光谱,还考虑了连接到干涉仪腔内的光纤芯和包层的折射率光谱以及形成腔的反射镜参数。与腔内光束衍射有关的物理现象(即光束发散、波前曲率和由盖伊效应引起的相移)也被考虑在内。将模拟所得的光谱与实测所得的光谱进行了比较。初步结果表明,光纤法布里-帕姆罗干涉仪可以高精度地测量所研究物质的折射率和吸收率。
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引用次数: 3
期刊
Scientific Conference on Optical and Electronic Sensors
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