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Sealing ability of various endodontic sealers with or without ethylenediaminetetraacetic acid (EDTA) treatment on bovine root canal. 经过或未经乙二胺四乙酸 (EDTA) 处理的各种牙髓封闭剂对牛根管的封闭能力。
IF 2.5 4区 医学 Q2 Dentistry Pub Date : 2024-04-19 DOI: 10.4012/dmj.2023-305
Yusuke Aigami, T. Sawada, Shunsuke Shimizu, Akiko Asano, Mamoru Noda, Shinji Takemoto
This study investigated the wettability and consistency of various endodontic sealers, both inorganic and organic, and evaluated their sealing ability of root canals using the single-cone obturation technique, with and without ethylenediaminetetraacetic acid (EDTA) treatment. Bovine root canals were endodontically prepared and filled in preparation for the dye penetration test with toluidine blue solution. All sealers exhibited contact angles similar to or lower than dentin and displayed superior consistency. Among the sealers, organic sealers used without EDTA treatment showed reduced dye penetration compared to inorganic sealers. However, some inorganic and organic sealers showed dye penetration in the sealer and dentin of root canals subjected to EDTA treatment. In conclusion, the single-cone obturation technique, combined with these endodontic sealers, achieved close contact with root canal dentin due to their wettability and consistency. However, the sealing ability of certain sealers was influenced by EDTA treatment.
本研究调查了各种无机和有机牙髓封闭剂的润湿性和稠度,并评估了它们使用单锥体封闭技术、经乙二胺四乙酸(EDTA)处理和未经乙二胺四乙酸(EDTA)处理时对根管的封闭能力。对牛根管进行根管预备和填充,准备用甲苯胺蓝溶液进行染料渗透测试。所有封闭剂的接触角都与牙本质相近或更低,并显示出卓越的一致性。在封闭剂中,与无机封闭剂相比,未经 EDTA 处理的有机封闭剂显示出较低的染料渗透性。不过,一些无机和有机封闭剂在经过 EDTA 处理的根管封闭剂和牙本质中显示出染料渗透。总之,单锥封闭技术与这些根管封闭剂相结合,由于其润湿性和一致性,可以实现与根管牙本质的紧密接触。不过,某些封闭剂的封闭能力受到 EDTA 处理的影响。
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引用次数: 0
Influence of resin-coating techniques on the marginal adaptation and the bond strengths of CAD/CAM-fabricated hybrid ceramic inlays. 树脂涂层技术对 CAD/CAM 制作的混合陶瓷嵌体的边缘适应性和粘接强度的影响。
IF 2.5 4区 医学 Q2 Dentistry Pub Date : 2024-04-19 DOI: 10.4012/dmj.2023-182
Y. Kanamori, R. Takahashi, T. Nikaido, Hiroshi Nitta, Y. Shimada, J. Tagami, K. Kunzelmann
This study aimed to evaluate the effects of different resin-coating technique strategies and dual-cure resin luting materials on proximal marginal adaptation and the microtensile bond strengths (μTBSs) of CAD/CAM hybrid ceramic inlays. Extracted human molars were classified into four groups, depending on the coating technique: No coating (None), single coating (1-coating), double coating (2-coating), and flowable resin-coating (Combination). The inlays were bonded with one of the three materials: Panavia V5 (V5), Rely X Ultimate (RXU), and Calibra Ceram (CC). The differences with regard to adaptation were not significant. In the case of μTBS data for V5, no significant differences were observed, whereas for RXU, μTBS values for Combination statistically exceeded those for None and 1-coating. For CC, μTBS values for Combination statistically exceeded those for None, 1-coating, and 2-coating. The coating techniques did not influence the adaptation but influenced the bond strength, and Combination performed the best.
本研究旨在评估不同树脂涂层技术策略和双固化树脂衬垫材料对 CAD/CAM 混合陶瓷嵌体近端边缘适应性和微拉伸结合强度(μTBS)的影响。根据涂层技术的不同,拔出的人类臼齿被分为四组:无涂层(None)、单涂层(1-coating)、双涂层(2-coating)和可流动树脂涂层(Combination)。嵌体使用三种材料中的一种进行粘合:分别是 Panavia V5(V5)、Rely X Ultimate(RXU)和 Calibra Ceram(CC)。适应性方面的差异并不明显。就 V5 的 μTBS 数据而言,没有观察到明显的差异,而就 RXU 而言,组合的 μTBS 值在统计上超过了无涂层和单涂层的值。对于 CC,组合的 μTBS 值在统计学上超过了无涂层、1 涂层和 2 涂层。涂层技术对适应性没有影响,但对粘接强度有影响,而组合涂层的性能最好。
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引用次数: 0
Detection of senescent cells in the mucosal healing process on type 2 diabetic rats after tooth extraction for biomaterial development. 检测 2 型糖尿病大鼠拔牙后粘膜愈合过程中的衰老细胞,以开发生物材料。
IF 2.5 4区 医学 Q2 Dentistry Pub Date : 2024-04-19 DOI: 10.4012/dmj.2023-262
Chuyi Luo, Masato Nakagawa, Yoichi Sumi, Yasuhiko Matsushima, Mamoru Uemura, Yoshitomo Honda, Naoyuki Matsumoto
The delayed mucosal healing of tooth extraction sockets in diabetes has few known effective treatment strategies, and its underlying mechanism remains unknown. Senescent cells may play a pivotal role in this delay, given the well-established association between diabetes, senescent cells, and wound healing. Here, we demonstrated an increase in p21- or p16-positive senescent cells in the epithelial and connective tissues of extraction sockets in type 2 diabetic rats compared to those in control rats. Between 7 and 14 days after tooth extraction, a decrease in senescent cells and improvement in re-epithelialization failure were observed in the epithelium, while an increase in senescent cells and persistence of inflammation were observed in the connective tissue. These results suggest that cellular senescence may have been induced by diabetes and contributed to delayed mucosal healing by suppressing re-epithelization and persistent inflammation. These findings provide new targets for treatment using biomaterials, cells, and drugs.
糖尿病患者拔牙窝粘膜愈合延迟,目前已知的有效治疗策略很少,其根本机制仍不清楚。鉴于糖尿病、衰老细胞和伤口愈合之间的关联已得到证实,衰老细胞可能在这种延迟中扮演了关键角色。在这里,我们证实,与对照组大鼠相比,2 型糖尿病大鼠拔牙窝上皮和结缔组织中 p21 或 p16 阳性的衰老细胞有所增加。拔牙后 7 至 14 天,观察到上皮细胞中衰老细胞减少,再上皮化失败情况有所改善,而结缔组织中衰老细胞增加,炎症持续存在。这些结果表明,细胞衰老可能是由糖尿病诱发的,并通过抑制再上皮化和持续炎症而导致粘膜愈合延迟。这些发现为使用生物材料、细胞和药物进行治疗提供了新的目标。
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引用次数: 0
Sex estimation from maxillofacial radiographs using a deep learning approach. 利用深度学习方法从颌面部 X 光片估测性别。
IF 2.5 4区 医学 Q2 Dentistry Pub Date : 2024-04-11 DOI: 10.4012/dmj.2023-253
Hiroki Hase, Y. Mine, S. Okazaki, Yuki Yoshimi, S. Ito, Tzu-Yu Peng, Mizuho Sano, Yuma Koizumi, Naoya Kakimoto, Kotaro Tanimoto, Takeshi Murayama
The purpose of this study was to construct deep learning models for more efficient and reliable sex estimation. Two deep learning models, VGG16 and DenseNet-121, were used in this retrospective study. In total, 600 lateral cephalograms were analyzed. A saliency map was generated by gradient-weighted class activation mapping for each output. The two deep learning models achieved high values in each performance metric according to accuracy, sensitivity (recall), precision, F1 score, and areas under the receiver operating characteristic curve. Both models showed substantial differences in the positions indicated in saliency maps for male and female images. The positions in saliency maps also differed between VGG16 and DenseNet-121, regardless of sex. This analysis of our proposed system suggested that sex estimation from lateral cephalograms can be achieved with high accuracy using deep learning.
本研究的目的是构建深度学习模型,以实现更高效、更可靠的性别估计。这项回顾性研究使用了两个深度学习模型,即 VGG16 和 DenseNet-121。总共分析了 600 张侧头颅图像。通过梯度加权类激活映射为每个输出生成了一个突出图。两个深度学习模型在准确度、灵敏度(召回率)、精确度、F1得分和接收者工作特征曲线下面积等各项性能指标上都达到了较高的数值。这两个模型在男性和女性图像的显著性图谱中显示的位置存在很大差异。无论性别如何,VGG16 和 DenseNet-121 在突出图中的位置也存在差异。对我们提出的系统的分析表明,利用深度学习可以从侧头颅图像中高精度地估计性别。
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引用次数: 0
Exploring prosthetic screw rupture in titanium and zirconia superstructures under various conditions. 探索各种条件下钛和氧化锆上部结构中修复螺钉的断裂情况。
IF 2.5 4区 医学 Q2 Dentistry Pub Date : 2024-04-11 DOI: 10.4012/dmj.2023-285
Myu Hayashi, Yu Kataoka, Yuji Sato, Tokiko Osawa, Kohei Yamashita, Junichi Furuya
The fastening mechanics of prosthetic screws under various conditions is crucial to the maintenance of dental implants. This study comprehensively explores the prosthetic screw rupture in titanium (Ti) and zirconia (ZrO2) superstructures under wet and dry conditions. Superstructures were fabricated using digital technology and subjected to tightening torque trials. Experimental results suggested that the implications of the conventionally recommended torque of 15 N•cm differ significantly between dry and wet environments. Both Ti and ZrO2 exhibited preloads of >30 N•cm under dry conditions; however, differences emerged under wet conditions. In addition, screw rupture posed a prominent clinical challenge -particularly during long-term cyclic loading. Notably, the ZrO2 superstructures exhibited a greater resistance to breaking torque than that of Ti. This study underscores the importance of reevaluating torque recommendations with consideration to the distinct characteristics of Ti and ZrO2 in diverse environments.
修复螺钉在各种条件下的紧固力学对牙科植入物的维护至关重要。本研究全面探讨了钛 (Ti) 和氧化锆 (ZrO2) 上部结构在潮湿和干燥条件下的修复螺钉断裂情况。使用数字技术制作了上部结构,并对其进行了拧紧扭矩试验。实验结果表明,传统推荐的 15 N-cm 扭矩在干燥和潮湿环境下的影响差别很大。在干燥条件下,钛和氧化锆的预紧力均大于 30 牛米;但在潮湿条件下,两者的预紧力出现了差异。此外,螺钉断裂也是一个突出的临床难题--尤其是在长期循环加载时。值得注意的是,与钛相比,ZrO2 上部结构表现出更强的抗断裂扭矩能力。这项研究强调了根据钛和氧化锆在不同环境中的不同特性重新评估扭矩建议的重要性。
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引用次数: 0
Shock absorption and dispersion capability of a novel five-layer mouthguard sheet material. 新型五层护齿片材料的减震和分散能力
IF 2.5 4区 医学 Q2 Dentistry Pub Date : 2024-04-05 DOI: 10.4012/dmj.2023-179
Miho Motoyoshi, Hiroshi Suzuki, H. Churei, Toshiyuki Nakayama, Tatsuo Yagi, Shiori Sanjo, Takashi Asano, Yasuhiro Tanimoto, Osamu Komiyama
There is a growing need for a mouthguard sheet material with higher shock absorption and dispersion capacity than those obtained by conventional materials. A five-layer mouthguard sheet material was previously developed using laminated ethylene vinyl acetate and polyolefin copolymer resin. In this study, the shock absorption capacity and dispersion capability of the new sheet material were investigated and compared with those of other materials. Impact testing for the new sheet material showed that the force required to displace the sheet by 1 mm was significantly higher at all thicknesses (p<0.001), whereas the puncture energy and displacement were significantly lower than those for ethylene vinyl acetate (p<0.05). The five-layer mouthguard sheet material successfully absorbed and resisted shock. Therefore, the sheet material potentially increases resistance to applied deformation in teeth and alveolar bone and maintains structure. The five-layer sheet material could expand the range of mouthguard products and help prevent oral trauma.
与传统材料相比,人们越来越需要一种具有更强减震和分散能力的护齿片材料。以前曾使用层压乙烯-醋酸乙烯和聚烯烃共聚物树脂开发出一种五层护齿片材料。在这项研究中,对新型片材的冲击吸收能力和分散能力进行了调查,并与其他材料进行了比较。对新型片材的冲击测试表明,使片材位移 1 毫米所需的力在所有厚度上都明显较高(p<0.001),而穿刺能量和位移量则明显低于醋酸乙烯酯(p<0.05)。五层护齿片材料成功地吸收和抵抗了冲击。因此,护齿片材料有可能增加牙齿和牙槽骨的抗外力变形能力,并保持结构。五层护齿片材料可以扩大护齿产品的范围,有助于预防口腔创伤。
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引用次数: 0
Influence of etching mode on bonding performance of self-adhesive flowable resin composites to bovine teeth. 蚀刻模式对牛齿自粘流动树脂复合材料粘接性能的影响
IF 2.5 4区 医学 Q2 Dentistry Pub Date : 2024-04-05 DOI: 10.4012/dmj.2023-226
Kana Hayashi, R. Ishii, T. Takamizawa, R. Aoki, Rei Muto, S. Suda, Atsushi Kamimoto, M. Miyazaki
This study aimed to evaluate the bonding performance of self-adhesive flowable resin composites (SARs) to bovine teeth. Three SARs, one experimental, and two commercially available products, were used. The study parameters were shear bond strength (SBS), microleakage, and scanning electron microscopy (SEM) evaluation of bonding interfaces. The SBS of the materials was 14.1-15.1 MPa to enamel, 22.2-23.2 MPa to etched enamel, and 7.4-10.7 MPa to dentin. Specimens with pre-etching showed lower microleakage scores than those without pre-etching. SEM images of the interfaces of the materials showed excellent adaptation regardless of the substrate or etching mode. The study results indicate that enamel pre-etching can improve the bonding performance of SARs.
本研究旨在评估自粘性可流动树脂复合材料(SAR)与牛牙的粘接性能。研究使用了三种 SAR,一种是实验产品,另两种是市售产品。研究参数包括剪切粘接强度(SBS)、微渗漏和粘接界面的扫描电子显微镜(SEM)评估。这些材料对珐琅质的 SBS 为 14.1-15.1 兆帕,对蚀刻珐琅质的 SBS 为 22.2-23.2 兆帕,对牙本质的 SBS 为 7.4-10.7 兆帕。与未预蚀刻的试样相比,预蚀刻试样的微渗漏分数较低。材料界面的扫描电子显微镜图像显示,无论基底或蚀刻模式如何,都能很好地适应。研究结果表明,釉质预蚀刻可以提高 SAR 的粘结性能。
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引用次数: 0
Novel pit and fissure sealant with nano-CaF2 and antibacterial monomer: Fluoride recharge, microleakage, sealing ability and cytotoxicity. 含有纳米 CaF2 和抗菌单体的新型坑隙封闭剂:氟补给、微渗漏、密封能力和细胞毒性。
IF 2.5 4区 医学 Q2 Dentistry Pub Date : 2024-04-05 DOI: 10.4012/dmj.2023-166
Xiuzhi Fei, Yuncong Li, Qian Zhang, Chunli Tian, Yue Li, Qiannan Dong, M. Weir, Negar Homayounfar, Thomas W. Oates, Satoshi Imazato, Quan Dai, H. Xu, J. Ruan
Conventional resin-based sealants release minimal fluoride ions (F) and lack antibacterial activity. The objectives of this study were to: (1) develop a novel bioactive sealant containing calcium fluoride nanoparticles (nCaF2) and antibacterial dimethylaminohexadecyl methacrylate (DMAHDM), and (2) investigate mechanical performance, F recharge and re-release, microleakage, sealing ability and cytotoxicity. Helioseal F served as commercial control. The initial F release from sealant containing 20% nCaF2 was 25-fold that of Helioseal F. After ion exhaustion and recharge, the F re-release from bioactive sealant did not decrease with increasing number of recharge and re-release cycles. Elastic modulus of new bioactive sealant was 44% higher than Helioseal F. The new sealant had excellent sealing, minimal microleakage, and good cytocompatibility. Hence, the nanostructured sealant had substantial and sustained F release and antibacterial activity, good sealing ability and biocompatibility. The novel bioactive nCaF2 sealant is promising to provide long-term F ions for caries prevention.
传统的树脂密封剂只能释放极少量的氟离子(F),而且缺乏抗菌活性。本研究的目的是(1) 开发一种新型生物活性封闭剂,其中含有纳米氟化钙颗粒(nCaF2)和抗菌甲基丙烯酸二甲基氨基十六烷基酯(DMAHDM);(2) 研究机械性能、氟离子补给和再释放、微渗漏、封闭能力和细胞毒性。Helioseal F 用作商业对照。含有 20% nCaF2 的密封剂的初始钙离子释放量是 Helioseal F 的 25 倍,在离子耗尽和再充电后,生物活性密封剂的钙离子再释放量并没有随着充电和再释放循环次数的增加而减少。新型生物活性密封剂的弹性模量比 Helioseal F 高 44%。新型密封剂具有出色的密封性、最小的微渗漏和良好的细胞相容性。因此,纳米结构密封剂具有大量和持续的 F 释放和抗菌活性、良好的密封能力和生物相容性。这种新型生物活性 nCaF2 密封剂有望为预防龋齿提供长期的 F 离子。
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引用次数: 0
Influence of attaching mechanical retentive devices onto frameworks on fracture resistance of implant-supported zirconia crowns. 在骨架上安装机械固位装置对种植体支撑的氧化锆冠抗折性的影响。
IF 2.5 4区 医学 Q2 Dentistry Pub Date : 2024-04-05 DOI: 10.4012/dmj.2023-188
Tatsuro Kobayashi, Junichi Honda, Kei Kubochi, Taro Iwasaki, Yusuke Watanabe, Futoshi Komine
This study investigated the fracture load of implant-supported zirconia crowns (IZCs), in which indirect composite resin or feldspathic porcelain was layered onto zirconia frameworks with mechanical retentive devices. Three different zirconia frameworks were assessed: attaching mechanical retentive devices on glaze and opaque porcelain materials (GL and OP groups, respectively), and no attaching mechanical retentive devices (ND group). The frameworks were layered using feldspathic porcelain (FP veneer) and indirect composite resin (IC veneer). Fracture load of the specimens was measured. In FP veneer, the GL group recorded the highest fracture load. In the IC veneer, the GL and OP groups had significantly higher fracture load than the ND group. The fracture resistance of IZCs can be enhanced by applying glaze material before attaching mechanical retentive devices for porcelain layering. The mechanical retentive devices effectively yielded mechanical interlocking between the zirconia frameworks and the IC veneer in GL and OP groups.
这项研究调查了种植体支持的氧化锆冠(IZC)的断裂负荷,在这种冠中,间接复合树脂或长石瓷被层叠在带有机械固位装置的氧化锆框架上。对三种不同的氧化锆框架进行了评估:在釉质和不透明瓷材料上安装机械固位装置(分别为 GL 组和 OP 组),以及不安装机械固位装置(ND 组)。牙架使用长石瓷(FP贴面)和间接复合树脂(IC贴面)进行分层。对试样的断裂负荷进行了测量。在 FP 贴面中,GL 组的断裂载荷最高。在 IC 贴面中,GL 组和 OP 组的断裂载荷明显高于 ND 组。在粘贴瓷层的机械固定装置之前涂抹釉料,可以增强 IZC 的抗断裂性。在 GL 组和 OP 组中,机械固位装置能有效地使氧化锆框架和 IC 贴面之间产生机械联锁。
{"title":"Influence of attaching mechanical retentive devices onto frameworks on fracture resistance of implant-supported zirconia crowns.","authors":"Tatsuro Kobayashi, Junichi Honda, Kei Kubochi, Taro Iwasaki, Yusuke Watanabe, Futoshi Komine","doi":"10.4012/dmj.2023-188","DOIUrl":"https://doi.org/10.4012/dmj.2023-188","url":null,"abstract":"This study investigated the fracture load of implant-supported zirconia crowns (IZCs), in which indirect composite resin or feldspathic porcelain was layered onto zirconia frameworks with mechanical retentive devices. Three different zirconia frameworks were assessed: attaching mechanical retentive devices on glaze and opaque porcelain materials (GL and OP groups, respectively), and no attaching mechanical retentive devices (ND group). The frameworks were layered using feldspathic porcelain (FP veneer) and indirect composite resin (IC veneer). Fracture load of the specimens was measured. In FP veneer, the GL group recorded the highest fracture load. In the IC veneer, the GL and OP groups had significantly higher fracture load than the ND group. The fracture resistance of IZCs can be enhanced by applying glaze material before attaching mechanical retentive devices for porcelain layering. The mechanical retentive devices effectively yielded mechanical interlocking between the zirconia frameworks and the IC veneer in GL and OP groups.","PeriodicalId":11065,"journal":{"name":"Dental materials journal","volume":null,"pages":null},"PeriodicalIF":2.5,"publicationDate":"2024-04-05","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140739715","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"医学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Effect of the difference water amounts and hydrolysis times of silane coupling agent on the shear bond strength between lithium disilicate glass ceramic and composite resin. 硅烷偶联剂的不同水量和水解时间对二硅酸锂玻璃陶瓷和复合树脂剪切粘接强度的影响
IF 2.5 4区 医学 Q2 Dentistry Pub Date : 2024-04-05 DOI: 10.4012/dmj.2023-190
Pimchanok Osotprasit, Sasipin Lauvahutanon, Yosnarong Sirimethawong, Patcharanun Chaiamornsup, P. Jiangkongkho
This study was to evaluate the effect of different water amounts and hydrolysis times of silane coupling agent on shear bond strength between lithium disilicate glass ceramic (LDS) and composite resin. Fourteen groups (n=7) of different water amounts (90, 50 and 10%v/v) and hydrolysis times (5, 19, 75 and 300 s) of experimental silane coupling agent that were prepared for silanization, non-silanization and commercial silane coupling agent (CSC) groups. Two-way analysis of variance (ANOVA) revealed no interaction between water amounts and hydrolysis times of ESC on shear bond strength between LDS and composite resin. One-way ANOVA exhibited the highest shear bond strength and the highest mean percentage in mixed failure mode in the 50%v/v group. Molecular analysis of 13C and 29Si indicated that nuclear magnetic resonance spectra of M2 and M3 hydrolysis species were found in 50%v/v group. The presenting of M2 and M3 which was predominant factor contributing to the highest shear bond strength.
本研究旨在评估不同水量和水解时间的硅烷偶联剂对二硅酸锂玻璃陶瓷(LDS)与复合树脂之间剪切粘接强度的影响。制备了 14 组(n=7)不同水量(90、50 和 10%v/v )和水解时间(5、19、75 和 300 秒)的实验硅烷偶联剂,分别用于硅烷化组、非硅烷化组和商用硅烷偶联剂(CSC)组。双向方差分析(ANOVA)显示,ESC 的水量和水解时间对 LDS 和复合树脂之间的剪切粘接强度没有交互作用。单因素方差分析显示,50%v/v 组的剪切粘接强度最高,混合失效模式的平均百分比最高。13C 和 29Si 分子分析表明,在 50%v/v 组中发现了 M2 和 M3 水解物种的核磁共振谱。M2 和 M3 的出现是导致剪切粘接强度最高的主要因素。
{"title":"Effect of the difference water amounts and hydrolysis times of silane coupling agent on the shear bond strength between lithium disilicate glass ceramic and composite resin.","authors":"Pimchanok Osotprasit, Sasipin Lauvahutanon, Yosnarong Sirimethawong, Patcharanun Chaiamornsup, P. Jiangkongkho","doi":"10.4012/dmj.2023-190","DOIUrl":"https://doi.org/10.4012/dmj.2023-190","url":null,"abstract":"This study was to evaluate the effect of different water amounts and hydrolysis times of silane coupling agent on shear bond strength between lithium disilicate glass ceramic (LDS) and composite resin. Fourteen groups (n=7) of different water amounts (90, 50 and 10%v/v) and hydrolysis times (5, 19, 75 and 300 s) of experimental silane coupling agent that were prepared for silanization, non-silanization and commercial silane coupling agent (CSC) groups. Two-way analysis of variance (ANOVA) revealed no interaction between water amounts and hydrolysis times of ESC on shear bond strength between LDS and composite resin. One-way ANOVA exhibited the highest shear bond strength and the highest mean percentage in mixed failure mode in the 50%v/v group. Molecular analysis of 13C and 29Si indicated that nuclear magnetic resonance spectra of M2 and M3 hydrolysis species were found in 50%v/v group. The presenting of M2 and M3 which was predominant factor contributing to the highest shear bond strength.","PeriodicalId":11065,"journal":{"name":"Dental materials journal","volume":null,"pages":null},"PeriodicalIF":2.5,"publicationDate":"2024-04-05","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140737181","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"医学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
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Dental materials journal
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