Pub Date : 2023-11-29eCollection Date: 2023-01-01DOI: 10.1155/2023/9879471
International Journal Of Analytical Chemistry
[This retracts the article DOI: 10.1155/2022/6977424.].
[本文撤消了文章 DOI:10.1155/2022/6977424]。
{"title":"Retracted: Liquid-Phase Synthesis of Nano-Zinc Oxide and Its Photocatalytic Property.","authors":"International Journal Of Analytical Chemistry","doi":"10.1155/2023/9879471","DOIUrl":"https://doi.org/10.1155/2023/9879471","url":null,"abstract":"<p><p>[This retracts the article DOI: 10.1155/2022/6977424.].</p>","PeriodicalId":13888,"journal":{"name":"International Journal of Analytical Chemistry","volume":"2023 ","pages":"9879471"},"PeriodicalIF":1.8,"publicationDate":"2023-11-29","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10701017/pdf/","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"138795724","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2023-11-29eCollection Date: 2023-01-01DOI: 10.1155/2023/9859273
International Journal Of Analytical Chemistry
[This retracts the article DOI: 10.1155/2022/4565260.].
[此文撤稿,DOI: 10.1155/2022/4565260.]。
{"title":"Retracted: Application of Cross-Linked and Non-Cross-Linked Hyaluronic Acid Nano-Needles in Cosmetic Surgery.","authors":"International Journal Of Analytical Chemistry","doi":"10.1155/2023/9859273","DOIUrl":"https://doi.org/10.1155/2023/9859273","url":null,"abstract":"<p><p>[This retracts the article DOI: 10.1155/2022/4565260.].</p>","PeriodicalId":13888,"journal":{"name":"International Journal of Analytical Chemistry","volume":"2023 ","pages":"9859273"},"PeriodicalIF":1.8,"publicationDate":"2023-11-29","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10700974/pdf/","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"138795792","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2023-11-29eCollection Date: 2023-01-01DOI: 10.1155/2023/9854164
International Journal Of Analytical Chemistry
[This retracts the article DOI: 10.1155/2022/7739734.].
[本文撤回了文章 DOI:10.1155/2022/7739734]。
{"title":"Retracted: Application of Nanocomposite Energy Storage Materials in Green Building Design.","authors":"International Journal Of Analytical Chemistry","doi":"10.1155/2023/9854164","DOIUrl":"https://doi.org/10.1155/2023/9854164","url":null,"abstract":"<p><p>[This retracts the article DOI: 10.1155/2022/7739734.].</p>","PeriodicalId":13888,"journal":{"name":"International Journal of Analytical Chemistry","volume":"2023 ","pages":"9854164"},"PeriodicalIF":1.8,"publicationDate":"2023-11-29","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10701072/pdf/","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"138795804","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2023-11-29eCollection Date: 2023-01-01DOI: 10.1155/2023/9807316
International Journal Of Analytical Chemistry
[This retracts the article DOI: 10.1155/2022/3562209.].
[本文撤回了文章 DOI:10.1155/2022/3562209.]。
{"title":"Retracted: Application of Cement-Based Carbon Fiber Material in Construction of Building Durability.","authors":"International Journal Of Analytical Chemistry","doi":"10.1155/2023/9807316","DOIUrl":"https://doi.org/10.1155/2023/9807316","url":null,"abstract":"<p><p>[This retracts the article DOI: 10.1155/2022/3562209.].</p>","PeriodicalId":13888,"journal":{"name":"International Journal of Analytical Chemistry","volume":"2023 ","pages":"9807316"},"PeriodicalIF":1.8,"publicationDate":"2023-11-29","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10701041/pdf/","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"138795785","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2023-11-29eCollection Date: 2023-01-01DOI: 10.1155/2023/9832879
International Journal Of Analytical Chemistry
[This retracts the article DOI: 10.1155/2022/6444367.].
[本文撤消了文章 DOI:10.1155/2022/6444367]。
{"title":"Retracted: Preparation and Sound Insulation Performance of Polystyrene Building Flame Retardant and Thermal Insulation Building Materials.","authors":"International Journal Of Analytical Chemistry","doi":"10.1155/2023/9832879","DOIUrl":"https://doi.org/10.1155/2023/9832879","url":null,"abstract":"<p><p>[This retracts the article DOI: 10.1155/2022/6444367.].</p>","PeriodicalId":13888,"journal":{"name":"International Journal of Analytical Chemistry","volume":"2023 ","pages":"9832879"},"PeriodicalIF":1.8,"publicationDate":"2023-11-29","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10701064/pdf/","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"138795729","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2023-11-29eCollection Date: 2023-01-01DOI: 10.1155/2023/9897809
International Journal Of Analytical Chemistry
[This retracts the article DOI: 10.1155/2022/8339503.].
[本文撤回文章 DOI:10.1155/2022/8339503]。
{"title":"Retracted: Preparation of Porous Ceramic Building Decoration Materials by Foaming Method and Research on Nanomechanical Properties.","authors":"International Journal Of Analytical Chemistry","doi":"10.1155/2023/9897809","DOIUrl":"https://doi.org/10.1155/2023/9897809","url":null,"abstract":"<p><p>[This retracts the article DOI: 10.1155/2022/8339503.].</p>","PeriodicalId":13888,"journal":{"name":"International Journal of Analytical Chemistry","volume":"2023 ","pages":"9897809"},"PeriodicalIF":1.8,"publicationDate":"2023-11-29","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10701010/pdf/","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"138795959","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2023-11-29eCollection Date: 2023-01-01DOI: 10.1155/2023/9783476
International Journal Of Analytical Chemistry
[This retracts the article DOI: 10.1155/2022/6008603.].
[本文撤回了文章 DOI:10.1155/2022/6008603.]。
{"title":"Retracted: Reservoir Physical Properties and Micropore Nanocharacteristics of Cores in the Shihezi Formation, Sudong District, Sulige Gas Field, Ordos Basin.","authors":"International Journal Of Analytical Chemistry","doi":"10.1155/2023/9783476","DOIUrl":"https://doi.org/10.1155/2023/9783476","url":null,"abstract":"<p><p>[This retracts the article DOI: 10.1155/2022/6008603.].</p>","PeriodicalId":13888,"journal":{"name":"International Journal of Analytical Chemistry","volume":"2023 ","pages":"9783476"},"PeriodicalIF":1.8,"publicationDate":"2023-11-29","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10701021/pdf/","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"138796107","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2023-11-24eCollection Date: 2023-01-01DOI: 10.1155/2023/6928167
Sobia Sultana
The main challenges faced by medical researchers while producing novel drugs are time commitment, amplified costs, creating a safety profile for the medications, reduced solubility, and a lack of experimental data. Chemical graph theory makes an important theoretical contribution to drug development and design by investigating the structural properties of molecules. To improve drug research and assess the effectiveness of treatments, topological indices aim to provide a mathematical representation of molecular structures. In this study, the author examined a number of recently used drugs, including tamoxifen, mesterolone, anastrozole, and letrozole which are used to treat infertility. We compute the topological descriptors with the limiting behaviors associated with these pharmaceutical drugs and offer degree-based topological parameters for them. We conducted a QSPR investigation on the prospective degree-based topological descriptors using quadratic, cubic, exponential, and logarithmic regression models.
{"title":"Chemical Application of Topological Indices in Infertility Treatment Drugs and QSPR Analysis.","authors":"Sobia Sultana","doi":"10.1155/2023/6928167","DOIUrl":"10.1155/2023/6928167","url":null,"abstract":"<p><p>The main challenges faced by medical researchers while producing novel drugs are time commitment, amplified costs, creating a safety profile for the medications, reduced solubility, and a lack of experimental data. Chemical graph theory makes an important theoretical contribution to drug development and design by investigating the structural properties of molecules. To improve drug research and assess the effectiveness of treatments, topological indices aim to provide a mathematical representation of molecular structures. In this study, the author examined a number of recently used drugs, including tamoxifen, mesterolone, anastrozole, and letrozole which are used to treat infertility. We compute the topological descriptors with the limiting behaviors associated with these pharmaceutical drugs and offer degree-based topological parameters for them. We conducted a QSPR investigation on the prospective degree-based topological descriptors using quadratic, cubic, exponential, and logarithmic regression models.</p>","PeriodicalId":13888,"journal":{"name":"International Journal of Analytical Chemistry","volume":"2023 ","pages":"6928167"},"PeriodicalIF":1.8,"publicationDate":"2023-11-24","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10691894/pdf/","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"138477541","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Objective. Rubi Fructus (RF) is a dry aggregate fruit of Rubus (Rosaceae). It has shown significant pharmacological effects such as anti-oxidation, hypoglycemic, and anti-inflammatory. A combination of near-infrared (NIR) spectroscopy and partial least squares regression (PLSR) under seven different spectral data preprocessing techniques was used to determine the performance of quantitative analysis correction models which employed moisure, ellagic acid, and total flavonoids as indicators of RF. Methods. Ninety-seven different RF batches were collected for NIR spectra. By using primary analysis techniques such as drying method, high-performance liquid chromatography (HPLC), and ultraviolet visible spectrophotometry (UV-Vis), the contents of moisure, ellagic acid, and total flavonoids were determined. The NIR spectral data and the primary analysis method data were correlated through PLSR. Seven methods were used for pretreating the spectral data, including no spectral pretreatment, first derivative, standard normalized variate, multiple scattering corrections, elimination of constant offset, and minimum maximum normalization. The quantitative analysis correction models adopted PLSR chemometrics for moisture, ellagic acid and total flavonoids were developed, and their effectiveness was evaluated using the correlation coefficient (R), ratio of prediction to deviation (RPD), and root mean square error (RMSE). Results. The first derivative was combined with variable standardization, elimination of constant offset, and multiple scattering corrections, respectively, to pretreat the PLSR models for moisture, ellagic acid, and total flavonoids. The R-values of the PLSR models for moisture, ellagic acid, and total flavonoids were, respectively, 0.9788, 0.9468, and 0.9748, all of which were higher than 0.90, and the RPD values were 4.9, 3.1, and 4.5, respectively, which were all larger than 3.0. The RMSE ratios of the calibration set and the test set were 0.98, 0.94, and 1.0, respectively. Conclusion. The R-values of the NIR-PLSR models for moisture, ellagic acid, and total flavonoids are all greater than 0.90 after suitable pretreatments, indicating that the models are reliable. The RPD values are more than 3.0, which indicate that the models are good and useable for quality control. The RMSE ratios are closed to 1, indicating that the calibration set and test set had same distribution and the models were not overfitting indicating good predictability.
{"title":"Determination of Multicomponents in Rubi Fructus by Near-Infrared Spectroscopy Technique","authors":"Wenjun Du, Chunyan Wu, Hesong Yu, Qingran Kong, Yunjian Xu, Weidong Zhang","doi":"10.1155/2023/5575944","DOIUrl":"https://doi.org/10.1155/2023/5575944","url":null,"abstract":"Objective. Rubi Fructus (RF) is a dry aggregate fruit of Rubus (Rosaceae). It has shown significant pharmacological effects such as anti-oxidation, hypoglycemic, and anti-inflammatory. A combination of near-infrared (NIR) spectroscopy and partial least squares regression (PLSR) under seven different spectral data preprocessing techniques was used to determine the performance of quantitative analysis correction models which employed moisure, ellagic acid, and total flavonoids as indicators of RF. Methods. Ninety-seven different RF batches were collected for NIR spectra. By using primary analysis techniques such as drying method, high-performance liquid chromatography (HPLC), and ultraviolet visible spectrophotometry (UV-Vis), the contents of moisure, ellagic acid, and total flavonoids were determined. The NIR spectral data and the primary analysis method data were correlated through PLSR. Seven methods were used for pretreating the spectral data, including no spectral pretreatment, first derivative, standard normalized variate, multiple scattering corrections, elimination of constant offset, and minimum maximum normalization. The quantitative analysis correction models adopted PLSR chemometrics for moisture, ellagic acid and total flavonoids were developed, and their effectiveness was evaluated using the correlation coefficient (R), ratio of prediction to deviation (RPD), and root mean square error (RMSE). Results. The first derivative was combined with variable standardization, elimination of constant offset, and multiple scattering corrections, respectively, to pretreat the PLSR models for moisture, ellagic acid, and total flavonoids. The R-values of the PLSR models for moisture, ellagic acid, and total flavonoids were, respectively, 0.9788, 0.9468, and 0.9748, all of which were higher than 0.90, and the RPD values were 4.9, 3.1, and 4.5, respectively, which were all larger than 3.0. The RMSE ratios of the calibration set and the test set were 0.98, 0.94, and 1.0, respectively. Conclusion. The R-values of the NIR-PLSR models for moisture, ellagic acid, and total flavonoids are all greater than 0.90 after suitable pretreatments, indicating that the models are reliable. The RPD values are more than 3.0, which indicate that the models are good and useable for quality control. The RMSE ratios are closed to 1, indicating that the calibration set and test set had same distribution and the models were not overfitting indicating good predictability.","PeriodicalId":13888,"journal":{"name":"International Journal of Analytical Chemistry","volume":"15 8","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2023-11-06","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"135679323","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2023-11-04eCollection Date: 2023-01-01DOI: 10.1155/2023/5554877
Li Liu, Nanbiao Long, Juan Zhou, Manxue Liu, Shaobo He, Wuying Chu
This study aimed to investigate a detection method of enrofloxacin and ciprofloxacin to be avail for strictly supervising the quality and safety of aquatic products. The results displayed that the optimal extraction conditions for enrofloxacin and ciprofloxacin were the following five aspects: 15 g dosages of Na2SO4 to dehydrate, 8‰ of acetonitrile and 50% hydrochloric acid to deproteinization, 2 mL dosages of n-hexane to degrease, 10 min of ultrasonic time, and 20 min of extraction (stand) time. Meanwhile, it was also obtained for the optimal detection performance indexes of the recovery, precision, and accuracy from the tests of shrimp, grass carp, and tilapia. In particular, the expanded uncertainties were 2.8601 and 0.8613, and the factors of both the calibration curves (Urel(C)) and the analysis of the experiment (Urel(E)) were the two MU main contributors for enrofloxacin and ciprofloxacin together with the results above 40%. Consequently, the developed novel method was suited for the determination of the enrofloxacin and ciprofloxacin residues in aquatic products and would contribute to reinforce in supervision and inspection of the quality and safety of aquatic products.
{"title":"Method Validation and Measurement Uncertainty (MU) Evaluation on Enrofloxacin and Ciprofloxacin in the Aquatic Products.","authors":"Li Liu, Nanbiao Long, Juan Zhou, Manxue Liu, Shaobo He, Wuying Chu","doi":"10.1155/2023/5554877","DOIUrl":"10.1155/2023/5554877","url":null,"abstract":"<p><p>This study aimed to investigate a detection method of enrofloxacin and ciprofloxacin to be avail for strictly supervising the quality and safety of aquatic products. The results displayed that the optimal extraction conditions for enrofloxacin and ciprofloxacin were the following five aspects: 15 g dosages of Na<sub>2</sub>SO<sub>4</sub> to dehydrate, 8‰ of acetonitrile and 50% hydrochloric acid to deproteinization, 2 mL dosages of n-hexane to degrease, 10 min of ultrasonic time, and 20 min of extraction (stand) time. Meanwhile, it was also obtained for the optimal detection performance indexes of the recovery, precision, and accuracy from the tests of <i>shrimp</i>, <i>grass carp</i>, and <i>tilapia</i>. In particular, the expanded uncertainties were 2.8601 and 0.8613, and the factors of both the calibration curves (<i>U</i><sub>rel(C)</sub>) and the analysis of the experiment (<i>U</i><sub>rel(E)</sub>) were the two MU main contributors for enrofloxacin and ciprofloxacin together with the results above 40%. Consequently, the developed novel method was suited for the determination of the enrofloxacin and ciprofloxacin residues in aquatic products and would contribute to reinforce in supervision and inspection of the quality and safety of aquatic products.</p>","PeriodicalId":13888,"journal":{"name":"International Journal of Analytical Chemistry","volume":"2023 ","pages":"5554877"},"PeriodicalIF":1.8,"publicationDate":"2023-11-04","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10640130/pdf/","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"89718163","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}