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Comparative Analysis of the Effect of Fibre Architecture on the Tensile Properties of Sisal Fibre Reinforced Polyethylene Polymer Composite 纤维结构对剑麻纤维增强聚乙烯聚合物复合材料拉伸性能影响的对比分析
Pub Date : 2022-01-01 DOI: 10.11648/j.ijmsa.20221102.12
Mohammed Umar Faruk, Ladan Ibrahim Fakai
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引用次数: 0
Contribution to the Study of the Thermal, Rheological and Morphological Properties of Biocomposites Based on Typha/PP 基于Typha/PP的生物复合材料的热、流变和形态学研究
Pub Date : 2022-01-01 DOI: 10.11648/j.ijmsa.20221101.15
B. Niang, Abdou Karim Farota, Abdoul Karim Mbodji, Nicola Schiavone, H. Askanian, V. Verney, Diène Ndiaye, Abdoulaye Bouya Diop, B. Diop
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引用次数: 1
Suitable Na2O-SiO2, BaO-SiO2 Based Coatings for Stainless Steels 适用于不锈钢的na20 - sio2, BaO-SiO2基涂料
Pub Date : 2021-11-15 DOI: 10.32732/jma.2021.10.2.90
A. Faeghinia, E. Jabbari
Two frites with 40 wt.%SiO2-20 wt.%B2O3-17 wt.%Na2O (G1) and 42wt.%SiO2-24wt.%BaO-18 wt.%CoO (G2) compositions were prepared and applied on stainless steel by the slurry method. The samples were heated at 950ºC (G2) and 860ºC (G1). The XRD results revealed the sodium silicate and barium silicate phases as well as almost 770 HV, 543 HV microhardness in G1 and G2 coats respectively. The thermal expansion coefficients were α=10.9×10-6/K(G1) and α=13.31×10-6/K (G2) respectively. According to EDS results the alkaline earth ions (and CoO) migration into the glass- steel interface was occurred in both coats. The dry sliding friction and wear behavior were investigated using a 4mm diameter AISI52100 steel pin on disk geometry under 5,10 and 18 N loads. The average wear rate were w.r: 32 ×10-14(m3/N.m) and w.r:5×10-14(m3/N.m) in G1 and G2 coats. Then two frites were mixed and heat treated at 800ºC with high heating and cooling rate. The resulted composite (G1-G2) shows almost the average wear rate 4×10-14(m3/N.m), while the coefficient friction of G1-G2 composite was not improved significantly.
两份含有40 wt.%SiO2-20 wt.%B2O3-17 wt.%Na2O (G1)和42wt.%SiO2-24wt的薯条。采用浆料法制备了% bao - 18wt .%CoO (G2)组合物,并将其应用于不锈钢上。样品分别在950℃(G2)和860℃(G1)下加热。XRD结果表明,G1和G2涂层存在硅酸钠和硅酸钡相,显微硬度分别接近770 HV和543 HV。热膨胀系数分别为α=10.9×10-6/K(G1)和α=13.31×10-6/K (G2)。能谱分析结果表明,两种涂层均发生了碱土离子(和CoO)向玻璃钢界面的迁移。采用直径4mm的AISI52100钢销,在5、10和18 N载荷作用下研究了干滑动摩擦磨损行为。G1和G2的平均磨损率w.r: 32 ×10-14(m3/N.m)和w.r:5×10-14(m3/N.m)。然后将两种薯条混合,在800℃下进行高加热和高冷却速率的热处理。所得复合材料(G1-G2)的磨损率几乎为平均4×10-14(m3/N.m),而G1-G2复合材料的摩擦系数没有明显提高。
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引用次数: 0
Irradiation Hardening and Microstructure Characterization of Zr -1% Nb During Low Dose Neutron Irradiation Zr -1% Nb在低剂量中子辐照下的辐照硬化及微观结构表征
Pub Date : 2021-11-15 DOI: 10.32732/jma.2021.10.2.63
C. Vazquez, E. Zelaya, A. Fortis, P. Bozzano
Due to low neutron absorption cross section, high mechanical strength, high thermal conductivity and good corrosion resistance in water and steam, Zirconium alloys are widely used as fuel cladding material in nuclear reactors. During life-time of a reactor the microstructure of this alloy is affected due to, among other factors, radiation damage and hydrogen damage. In this work mechanical properties changes on neutron irradiated Zr-1wt.% Nb at low temperatures (< 100 °C) and low dose (3.5 ´ 1023 n m-2 (E > 1 MeV)) were correlated with hydrides and crystal defects evolution during irradiation. To achieve this propose, tensile tests of: 1) Non-hydrided and non-irradiated material, 2) Hydrided and non-irradiated material and 3) Hydrided and irradiated material were performed at 25 ºC and 300 ºC. Different phases, hydrides and second phase precipitates were characterized by transmission electron microscopy (TEM) techniques. For the hydrided and irradiated material, the ductility decreased sharply with respect to the hydrided and non-irradiated material, among other factors, due to the change in the microstructure produced mainly by neutron irradiation. Even if the presence of the hydride ζ (zeta) was observed, both in the irradiated and non-irradiated material, tensile tests showed that ζ-hydrides did not affect ductility, since hydrided samples are more ductile than non-hydrided samples.
锆合金具有中子吸收截面小、机械强度高、导热系数高、在水和蒸汽中的耐腐蚀性好等优点,被广泛用作核反应堆的燃料包壳材料。在反应堆的使用寿命期间,这种合金的微观结构会受到辐射损伤和氢损伤等因素的影响。本文研究了中子辐照Zr-1wt后力学性能的变化。低温(< 100°C)和低剂量(3.5´1023 n m-2 (E > 1 MeV))下的% Nb与辐照过程中的氢化物和晶体缺陷演化相关。为了实现这一建议,在25ºC和300ºC下进行了1)非氢化和未辐照材料,2)氢化和未辐照材料以及3)氢化和辐照材料的拉伸试验。采用透射电镜(TEM)对不同相、氢化物和第二相析出物进行了表征。对于氢化和辐照的材料,由于主要由中子辐照引起的微观结构的变化,其延展性相对于氢化和未辐照的材料急剧下降。即使在辐照和未辐照材料中观察到氢化物ζ (zeta)的存在,拉伸试验表明,ζ-氢化物不影响延展性,因为氢化样品比非氢化样品更具延展性。
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引用次数: 0
Development and Research Status of ZA27 Zinc Alloy ZA27锌合金的发展与研究现状
Pub Date : 2021-10-21 DOI: 10.11648/J.IJMSA.20211005.15
Wang Heng, M. Yiming
In recent years, due to the rapid development of industry, the manufacturing processing quality was required to be higher and higher day by day, which made a major breakthrough in the research of metal materials. A series of new technologies and processes have been developed. The application and promotion of these technologies and processes have greatly improved the technical level of the non-ferrous metal industry, especially in the field of zinc alloy. ZA27 zinc alloy received extensive attention during this period. ZA27 zinc alloy is widely used in automobiles, construction, household appliances, ships, light industry, machinery, batteries and other industries due to its excellent wear resistance, friction reduction and mechanical properties. For these reasons, ZA27 zinc alloy has become a good substitutive material for copper alloy. In this paper, according to the research history and current situation of ZA27 zinc alloy around the world, the effects of different adding elements and the characteristics of different processes were comparatively analyzed, and summarized the progress at home and abroad. At the same time, this paper pointed out the problems existing in the development and production of ZA27 zinc alloy, which provided the basis for the development of ZA27 zinc alloy in the future.
近年来,由于工业的快速发展,对制造加工质量的要求日益提高,这使得金属材料的研究取得了重大突破。开发了一系列新技术和新工艺。这些技术和工艺的应用和推广,极大地提高了有色金属工业特别是锌合金领域的技术水平。ZA27锌合金在这一时期受到了广泛的关注。ZA27锌合金因其优异的耐磨性、减摩性和力学性能,广泛应用于汽车、建筑、家电、船舶、轻工、机械、电池等行业。因此,ZA27锌合金已成为铜合金的良好替代材料。本文根据国内外对ZA27锌合金的研究历史和现状,对比分析了不同添加元素的效果和不同工艺的特点,总结了国内外的研究进展。同时指出了ZA27锌合金在开发生产中存在的问题,为今后ZA27锌合金的发展提供了依据。
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引用次数: 0
Evaluation of the Mechanical Behavior of Clay Bricks Stabilized at 4% Cement and Mixed with Limba Wood Waste 掺林巴木废料的4%水泥稳定粘土砖力学性能评价
Pub Date : 2021-10-16 DOI: 10.11648/J.IJMSA.20211005.14
H. Elenga, Ferland Ngoro-Elenga, M. Tchoumou, Jude Novelgi Ngakosso Ngolo, Ottard Mwa Ngo Ossiby, T. Nsongo
In this study, the authors evaluated the mechanical behavior of bricks made of clay material stabilized with 4% cement and mixed with different contents (0; 2; 4; 6 and 8%) of limba wood waste (sawdust and chips). The clayey raw material ANMK was characterized by the method of X-ray diffraction (XRD) on oriented sheets (normal, glycol and heated to 490°C), by scanning electron microscopy (SEM) and energy dispersive spectroscopy (EDS). The chemical and mineralogical compositions of cement used were determined by inductively coupled plasma – optical emission spectrometry (ICP-OES) and by X-ray diffraction. This clay material consists of 96% kaolinite and 4% of the chlorite / montmorillonite interstratified. The morphology of the material observed by scanning electron microscopy showed an irregularity of clusters. The elementary analysis by energy dispersive spectroscopy shows that this material is essentially aluminosilicate. The chemical analysis of the cement showed a predominance of CaO (67%) and SiO2 (21%), however the mineralogical analysis showed the presence of calcite, alite, hatrurite and brownmillerite. This clay material has a mass shrinkage on drying of 26.6% and the linear shrinkage is 6.4%. The formulation with sawdust appears to give greater flexural and compressive strengths than those obtained with chips.
在这项研究中,作者评估了粘土材料在4%水泥稳定下,不同掺量(0;2;4;林巴木材废料(锯末和木片)的6%和8%。采用x射线衍射(XRD)、扫描电子显微镜(SEM)和能谱仪(EDS)对粘土原料ANMK进行了表征。采用电感耦合等离子体发射光谱法(ICP-OES)和x射线衍射法测定了水泥的化学和矿物组成。该粘土材料由96%的高岭石和4%的绿泥石/蒙脱石组成。通过扫描电子显微镜观察到材料的形貌显示出不规则的团簇。能量色散光谱的元素分析表明,该材料本质上是硅酸铝。化学分析结果表明,水泥主要以CaO(67%)和SiO2(21%)为主,而矿物学分析结果显示,水泥中存在方解石、阿利石、红褐石和褐粒石。该粘土材料的干燥质量收缩率为26.6%,线收缩率为6.4%。用木屑制成的配方似乎比用木屑制成的配方具有更大的抗折和抗压强度。
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引用次数: 0
Heat Transfer and Solidification Methodology Involved in the Simulation of Steelmaking 炼钢过程模拟中涉及的传热和凝固方法
Pub Date : 2021-10-15 DOI: 10.11648/J.IJMSA.20211005.13
Nitin Amratav, K. K. Kumar, M. Pillai
The research work done in the last three decades has made continuous casting an advanced and sophisticated technology. The continuous casting process comprises many complicated phenomena in terms of fluid flow, heat transfer and structural deformation. The important numerical modeling method of the continuous casting process has been discussed in reference in this work. The present work describes molten steel flow, heat transfer, solidification, formation of the shell by solidification and coupling, etc. Continuous casting process is presently a well-established manufacturing process for steel production. The continuous casting process comprises many complicated phenomena in terms of fluid flow, heat transfer, and structural deformation. To achieve efficient and effective production, the manufacturers of steel keep on searching for new methods which increase productivity. One such kind of method has become more popular to use optimizing using numerical modeling. It describes molten steel flow, formation of the shell by solidification. With the recent advancement in metallurgical methods, the continuous casting process now becomes the main method for steel production. To achieve efficient and effective production, the manufacturers of steel keep on searching for new methods which increase productivity. In this work, we have studied and reviewed the literature to provide current information on the numerical modeling of continuous casting processes.
近三十年来的研究工作使连铸成为一项先进而精密的技术。连铸过程包含了流体流动、传热和组织变形等诸多复杂现象。本文对连铸过程的重要数值模拟方法进行了探讨。本文介绍了钢水的流动、传热、凝固、凝固耦合成壳等过程。连铸工艺是目前一种行之有效的钢铁生产工艺。连铸过程包含了流体流动、传热和组织变形等多种复杂现象。为了实现高效率的生产,钢铁制造商不断寻求提高生产率的新方法。其中一种比较流行的方法是利用数值模拟进行优化。它描述了钢水的流动,凝固形成的外壳。随着冶金技术的进步,连铸法已成为炼钢的主要方法。为了实现高效率的生产,钢铁制造商不断寻求提高生产率的新方法。在这项工作中,我们研究和回顾了文献,以提供有关连铸过程数值模拟的最新信息。
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引用次数: 0
Toward Low-Energy Spark-Plasma Sintering of Hot-Deformed Nd-Fe-B Magnets 热变形Nd-Fe-B磁体低能火花等离子烧结研究
Pub Date : 2021-09-29 DOI: 10.11648/J.IJMSA.20211005.12
M. Korent, M. Soderznik, Urška Ročnik, S. Drev, K. Rožman, S. Šturm, S. Kobe, K. Ž. Soderžnik
High-coercivity Nd-Fe-B permanent magnets are key materials for producing electrical components on the macro- and nanoscale. We present a newly developed, economically efficient method for processing Nd-Fe-B magnets based on spark-plasma sintering (SPS) that makes it possible to retain the technologically essential properties of the magnet, but by consuming about 30% less energy compared to the conventional SPS process. A magnet with an anisotropic microstructure was fabricated from MQU-F commercial ribbons with a low energy consumption (0.37 MJ) during the deformation process and compared to a conventionally prepared hot-deformed magnet that consumed three-times more energy (1.2 MJ). Both magnets were post-annealed at 650°C for 120 min in a vacuum. After the post-annealing process, the low-energy processing (LEP) hot-deformed magnet exhibited a coercivity of 1327 kAm-1, and a remanent magnetization of 1.27 T. In comparison, the high-energy processing (HEP) hot-deformed magnet had a coercivity of 1337 kAm-1 and a remanent magnetization of 1.31 T. A complete microstructural characterization and detailed statistical analyses revealed a better texture orientation for the HEP hot-deformed magnet processed with the larger energy consumption. This texture is the main reason for the difference in the remanent magnetization between the two hot-deformed magnets. The results show that although the LEP hot-deformed magnet was processed with three-times less energy than in a typical hot-deformation process, the maximum energy product is only 8% lower than that of a HEP hot-deformed magnet.
高矫顽力钕铁硼永磁体是制造宏观和纳米级电子元件的关键材料。我们提出了一种基于火花等离子烧结(SPS)的新开发的经济高效的Nd-Fe-B磁体加工方法,该方法可以保留磁体的技术基本特性,但与传统的SPS工艺相比,消耗的能量减少了约30%。利用MQU-F商用带制备了具有各向异性微结构的磁体,在变形过程中能耗低(0.37 MJ),与传统制备的热变形磁体相比,其能耗高3倍(1.2 MJ)。两个磁体在650°C真空中退火120分钟。经过退火处理后,低能量加工(LEP)热变形磁体的矫顽力为1327 μ m-1,剩余磁化强度为1.27 μ m,而高能加工(HEP)热变形磁体的矫顽力为1337 μ m-1,剩余磁化强度为1.31 μ m。完整的显微组织表征和详细的统计分析表明,能量消耗较大的HEP热变形磁体具有更好的织构取向。这种织构是造成两种热变形磁体剩余磁化强度差异的主要原因。结果表明,虽然LEP热变形磁体的加工能量比典型热变形磁体低3倍,但其最大能量积仅比HEP热变形磁体低8%。
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引用次数: 0
Spintronics: Overview on Spin Based Electronics and Its Potential Applications 自旋电子学:自旋电子学综述及其潜在应用
Pub Date : 2021-09-11 DOI: 10.11648/J.IJMSA.20211005.11
Bushra Irfan
Spintronics is a branch of electronics that utilizes the spin of an electron to carry information. Spin is a quantum phenomenon and attracted researchers because it is an ideal way for representing logic “0" and “1" (used in electronics) with spin pointing “up" or “down" with respect to a magnetic field. Therefore, spin imparts itself into a new kind of binary logic of "one" and "zero". These characteristics open a new possibility of spintronics application in various fields such as magnetic storage technology and quantum computers. Spintronics is an emerging field for next-generation nanoelectronic devices to minimize their power consumption (which is the major issue in future microelectronics technology) and increase memory capabilities. This article briefly introduces the fundamentals of spintronics, progress in spintronics and its applications; it also features the current trend and challenging goal in this area.
自旋电子学是电子学的一个分支,它利用电子的自旋来携带信息。自旋是一种量子现象,吸引了研究人员,因为它是表示逻辑“0”和“1”(在电子学中使用)的理想方式,自旋相对于磁场指向“上”或“下”。因此,自旋赋予自己一种新的“1”和“0”的二元逻辑。这些特性为自旋电子学在磁存储技术、量子计算机等领域的应用开辟了新的可能性。自旋电子学是下一代纳米电子器件的新兴领域,旨在最大限度地降低其功耗(这是未来微电子技术的主要问题)并增加存储能力。本文简要介绍了自旋电子学的基本原理、研究进展及其应用;分析了该领域的发展趋势和挑战目标。
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引用次数: 0
Genotoxicity Induced by Cellular Uptake of Chitosan Nanoparticles in Human Dental Pulp Cells 壳聚糖纳米颗粒对人牙髓细胞的遗传毒性研究
Pub Date : 2021-07-15 DOI: 10.11648/J.IJMSA.20211004.11
Rami Alhomrany, Chang Zhang, L. Chou
Objective: Recent in vitro studies have shown that chitosan nanoparticles in several root canal sealers, intracanal medicament, and irrigation solutions could enhance the antimicrobial activity. However, the nanotoxicity of chitosan has not been fully studied. The aim of this study was to evaluate cellular uptake and genotoxicity of various sizes and concentrations of chitosan nanoparticles cultured with human dental pulp cells. Methods: Human dental pulp cells were derived from human dental pulp tissues and cultured for 24 hours with 50 nm and 318 nm FITC-tagged chitosan nanoparticles in concentrations: 0.1 mg/mL, 0.5 mg/mL, and 2 mg/mL as study groups, and 0 mg/mL as a control. The fluorescence intensity of the FITC tagged chitosan nanoparticles was measured using a spectrophotometer to determine the cellular uptake. Genotoxicity was assessed by the Cytokinesis-block micronucleus method and by measuring the fluorescent intensity of the phosphorylated H2AX nuclear foci. Statistical analysis was performed using One-Way ANOVA, post-hoc Tukey, and Chi-square tests. Results: Chitosan nanoparticles were able to internalize the human dental pulp cells and significantly induced micronuclei, nuclear buds, and pH2AX foci at concentrations of 0.5 mg/mL and 2 mg/mL as compared to 0.1 mg/mL (P < 0.01) and control group (P < 0.01). At both concentrations, 0.5 mg/mL and 2 mg/mL, 50 nm chitosan significantly induced higher proportions of micronuclei (P=0.001), nuclear buds (P=0.009), and pH2AX nuclear foci (P=0.00004) as compared to 318 nm chitosan. Conclusion: 50 nm and 318 nm chitosan nanoparticles at concentrations 0.5 mg/mL and 2 mg/mL penetrated human dental pulp cells and induced genotoxicity in dose-dependent and size-associated manners.
目的:最近的体外研究表明,壳聚糖纳米颗粒在几种根管密封剂、根管内药物和根管灌洗液中可以增强根管的抗菌活性。然而,壳聚糖的纳米毒性尚未得到充分的研究。本研究的目的是评估不同大小和浓度的壳聚糖纳米颗粒与人牙髓细胞的细胞摄取和遗传毒性。方法:从人牙髓组织中提取人牙髓细胞,以50 nm和318 nm的fitc标记的壳聚糖纳米颗粒(浓度分别为0.1 mg/mL、0.5 mg/mL和2 mg/mL)作为研究组,0 mg/mL为对照组,培养24 h。用分光光度计测量FITC标记的壳聚糖纳米颗粒的荧光强度,以确定细胞摄取。通过细胞分裂阻断微核法和磷酸化H2AX核灶的荧光强度评估遗传毒性。统计分析采用单因素方差分析、事后检验和卡方检验。结果:0.5 mg/mL和2 mg/mL浓度的壳聚糖纳米颗粒能使人牙髓细胞内化,与0.1 mg/mL浓度组(P < 0.01)和对照组(P < 0.01)相比,能显著诱导微核、核芽和pH2AX灶。在0.5 mg/mL和2 mg/mL两种浓度下,50 nm壳聚糖诱导的微核(P=0.001)、核芽(P=0.009)和pH2AX核灶(P=0.00004)的比例均显著高于318 nm壳聚糖。结论:50 nm和318 nm浓度为0.5 mg/mL和2 mg/mL的壳聚糖纳米颗粒可穿透人牙髓细胞,并具有剂量依赖性和大小相关性。
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引用次数: 2
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International Journal of Materials Science and Applications
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