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Impact of Carbon Nanotubes Reinforcement on Microstructural and Tribological Characteristics of Air Plasma Sprayed Conventional Alumina-Titania (Al2O3-3wt%TiO2) Coatings 碳纳米管增强对空气等离子喷涂普通氧化铝-二氧化钛(Al2O3-3wt%TiO2)涂层微观结构和摩擦学特性的影响
IF 1 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2020-09-10 DOI: 10.22068/IJMSE.17.3.92
V. Bolleddu
The microstructural characteristics, mechanical properties and wear characterization of air plasma sprayed coatings obtained from Carbon nanotubes (CNTs) reinforced Al2O3-3wt%TiO2 powders were examined at different loading conditions and different percentage proportion of CNTs. The CNTs in the proportion of 2, 4, and 6 wt% were used as nanofillers to modify the properties of coatings. The uniform dispersion of CNTs throughout the powder particles can be observed from the SEM micrographs. The porosity of the microstructure of the coatings was measured by image analysis. Also, the mechanical properties such as microhardness and surface roughness were measured by microhardness tester and profilometer, respectively. The wear tribometer was used to analyze the tribology of the coatings by varying different parameters. The different loading conditions used were low load (0.5 kgf), moderate load (1.0 kgf), and elevated load (1.5 kgf), respectively. The microhardness showed a slight increase with an increase in the percentage of CNTs proportion. Similarly, the surface roughness value showed a decreasing trend, since the CNTs were filled in the pores. From wear tests, it was observed that the coefficient of friction and wear rate were very less at 6wt% CNTs and 1.5 kgf load. This was mainly due to the bridging of CNTs in between the splats. This implies that CNTs were one of the most suitable additives for improving the microstructural and tribological characteristics of the ceramic coatings.
研究了碳纳米管(CNTs)增强Al2O3-3wt%TiO2粉末空气等离子喷涂涂层在不同加载条件和不同CNTs添加比例下的微观组织特征、力学性能和磨损性能。采用比例分别为2、4和6 wt%的CNTs作为纳米填料来修饰涂层的性能。通过SEM显微图可以观察到碳纳米管在粉末颗粒中的均匀分散。用图像分析方法测定了涂层微观组织的孔隙率。用显微硬度计和轮廓仪分别测定了复合材料的显微硬度和表面粗糙度等力学性能。利用磨损摩擦计对不同参数下涂层的摩擦学特性进行了分析。不同的加载条件分别为低负荷(0.5 kgf)、中等负荷(1.0 kgf)和高负荷(1.5 kgf)。随着CNTs添加比例的增加,显微硬度略有升高。同样,由于碳纳米管填充在孔隙中,表面粗糙度值也呈下降趋势。从磨损试验中可以观察到,在6wt% CNTs和1.5 kgf载荷下,摩擦系数和磨损率非常小。这主要是由于在板条之间架桥了CNTs。这表明碳纳米管是改善陶瓷涂层微观组织和摩擦学特性最合适的添加剂之一。
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引用次数: 2
Microstructure-Property Relationships in an Erbium-Modified Al-Si-Mg Alloy 铒改性Al-Si-Mg合金的组织-性能关系
IF 1 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2020-09-10 DOI: 10.22068/IJMSE.17.3.40
R. Niazi, E. Tohidlou, H. Khosravi
The effect of erbium (Er) addition at various weight percentages (0-0.6 wt.% at an interval of 0.2) on the microstructural features, tensile properties and wear behavior of as-cast Al-7.5Si-0.5Mg alloy were evaluated. The microstructure of the specimens was examined by X-ray diffraction (XRD), optical microscopy (OM) and scanning electron microscopy (SEM). The obtained results clearly demonstrated that the incorporation of erbium decreased the α-Al grain size and eutectic Si, and altered the Si morphology from plate to semi-globular. Further addition of erbium (> 0.2 wt.%) did not alter the eutectic morphology and size. Moreover, the Al3Er phase was also observed in the eutectic region after modification. Out of the erbium contents used, 0.2 wt.% erbium showed the best influence on the tensile and wear properties. Compared with those of unmodified specimen, the values of ultimate tensile strength and elongation were enhanced by 31 and 39%, respectively through 0.2 wt. % erbium addition. Additionally, a remarkable enhancement in the wear properties was observed with the addition of 0.2
研究了不同重量百分比(0 ~ 0.6 wt.%,间隔0.2)掺铒对铸态Al-7.5Si-0.5Mg合金组织特征、拉伸性能和磨损性能的影响。采用x射线衍射(XRD)、光学显微镜(OM)和扫描电镜(SEM)对试样的微观结构进行了表征。结果表明,铒的掺入降低了α-Al晶粒尺寸和共晶Si,使Si的形貌由板状变为半球状。进一步添加铒(> 0.2 wt.%)没有改变共晶的形貌和尺寸。此外,改性后的共晶区还出现了Al3Er相。在掺铒量中,掺铒量为0.2 wt.%对拉伸和磨损性能的影响最大。当掺铒量为0.2 wt. %时,试样的极限抗拉强度和伸长率分别提高了31%和39%。此外,当添加0.2时,耐磨性能显著增强
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引用次数: 1
Effect of Heat Treatment on Formation of Calcium Titanate Hollow-Crystals Nanostructures Prepared by Hydrothermal Method 热处理对水热法制备钛酸钙中空晶体纳米结构的影响
IF 1 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2020-06-10 DOI: 10.22068/IJMSE.17.2.51
S. Manafi, S. Joughehdoust
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引用次数: 0
Quantum Dots in Therapeutic, Diagnostic and Drug Delivery Applications “A Brief Review” 量子点在治疗、诊断和药物递送中的应用“简评”
IF 1 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2020-06-10 DOI: 10.22068/IJMSE.17.2.1
A. Nemati
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引用次数: 4
The Effect of Powder Composition on Cyclic Oxidation Behavior of CO-Deposited Al-Si Cating on Nickle-Based Superalloy 粉末组成对镍基高温合金上CO沉积Al-Si Cating循环氧化行为的影响
IF 1 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2020-06-10 DOI: 10.22068/IJMSE.17.2.104
M. Safaei, S. Rastegari, R. Latifi
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引用次数: 1
Effect of ZrSiO4/ZnO Ratio on the Properties of Opaque Glazes Used in -Ceramic Sanitary-ware Industry ZrSiO4/ZnO配比对陶瓷卫浴用不透明釉性能的影响
IF 1 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2020-06-10 DOI: 10.22068/IJMSE.17.2.92
Sa. Benkacem, K. Boudeghdegh, F. Zehani, Y. Belhocine
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引用次数: 1
Chsracterization of Low Temperature Plasma Ion Nitriding (PIN) of Inconel 600 and 601 Alloys Inconel 600和601合金低温等离子体离子氮化(PIN)的特征化
IF 1 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2020-06-10 DOI: 10.22068/IJMSE.17.2.20
R. Kumar, Y. Sharma, V. Sagar, D. Bhardwaj
In this study an effort has been made for the plasma ion nitriding (PIN) of Inconel 600 and 601 alloys at low temperatures. After plasma ion nitriding and microstructural study, growth kinetics of nitrided layer formation and wear properties were investigated by various characterization techniques such as scanning electron microscope (SEM), X-ray diffraction (XRD) analysis, micro-hardness measurement and wear test by pin on disk technique. It was found that surface micro-hardness increases after the PIN process. A mixed peak of epsilon (ε) and fcc (γ) phase was detected for all temperature range (350 to 450 C), while the chromium nitride (CrN) phase was detected at elevated temperature range ~450 C in Inconel 601 alloy. The calculated values of the diffusion coefficient and activation energy for the diffusion of nitrogen are in accordance with the literature. Volume loss and wear rate of the plasma nitrided samples decreases, but it increases as PIN process temperature increases.
本文研究了低温等离子体离子氮化铬镍铁合金(Inconel 600和601)。通过等离子体离子氮化和显微组织研究,采用扫描电镜(SEM)、x射线衍射(XRD)、显微硬度测量和销盘磨损测试等表征技术研究了氮化层形成的生长动力学和磨损性能。结果表明,经过PIN处理后,表面显微硬度有所提高。在350 ~450℃的温度范围内,发现了ε (ε)相和fcc (γ)相的混合峰,而在450℃的高温范围内,发现了氮化铬(CrN)相。氮扩散的扩散系数和活化能计算值与文献一致。等离子体氮化试样的体积损耗和磨损率随PIN工艺温度的升高而减小,但随PIN工艺温度的升高而增大。
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引用次数: 3
A Substantial Red and Blue Shift in the Band Gap of Gamma Alumina Through Controlling the OH/Al and Concentration of Sulfate Precursor 通过控制OH/Al和硫酸盐前体的浓度使γ-氧化铝带隙发生显著的红移和蓝移
IF 1 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2020-06-10 DOI: 10.22068/IJMSE.17.2.85
M. Ghamari, M. Ghasemifard
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引用次数: 0
Investigating the Leaching Behavior of Copper from Chalcopyrite Concentrate in H2SO4/CuCl2 Media 黄铜矿精矿中铜在H2SO4/CuCl2介质中的浸出行为研究
IF 1 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2020-06-10 DOI: 10.22068/IJMSE.17.2.66
R. Katal, Asghar Azizi, M. Gharabaghi
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引用次数: 2
Theoretical Investigation and Optimization of Radiation Thermal Conduction of Thermal-Insulation Polyolefin Foams 聚烯烃泡沫绝热材料辐射导热性能的理论研究与优化
IF 1 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2020-06-10 DOI: 10.22068/IJMSE.17.2.58
R. Hasanzadeh, S. Fathi, T. Azdast, M. Rostami
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引用次数: 3
期刊
Iranian Journal of Materials Science and Engineering
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