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Influence of sequential pyrolisis methods on the properties of the carbon nanostructure (CNS) from sugarcane leaf biomass 顺序热解方法对甘蔗叶片生物质碳纳米结构性质的影响
Q3 Engineering Pub Date : 2022-08-31 DOI: 10.22201/icat.24486736e.2022.20.4.1324
T. Setianingsih, B. Susilo, Siti Mutrofin, B. Ismuyanto, Andreas Novan Endaryana, Yoandra Nadya Yoniansyah
Plant biomass is a potential lignocellulose material  for synthesis of carbon nano structure. Its characteristics as adsorbent and its size particle  make it good additive for liquid fertilizer. In this research, we study influence of sequential different  pressure pyrolysis methods (hydrothermal–microwave method and reflux–microwave method) toward characteristics of carbon nanostructure from sugarcane leaf biomass. Each reflux and hydrothermal method was adjusted at 200oC, then followed by microwave at 800W. Characterization showed that the hydrothermal - microwave method using X-ray diffraction indicates diffractogram patterns of both carbon nanostructure and cellulose. SEM micrographs show sphere and block shapes. FTIR spectra indicates different concentration of oxy surface functional groups. UV spectra of the dispersed product in water indicates  existence of aromatics C=C groups. The hydrothermal - microwave method resulted the product inwhich lower crystalinity index of cellulose, smaller particles, lower concentration of oxy surface groups than the reflux - microwave one. Correlation of chemical properties (aromaticity and fraction of polar groups) was more linier than of physical - chemical properties  (indexe of cellulose crystalinity and fraction of polar groups). The stability of colloid was indicated by dispersing technique in order of sonication < blending < blending - sonication.
植物生物量是合成碳纳米结构的潜在木质纤维素材料。它的吸附剂特性和颗粒大小使其成为液体肥料的良好添加剂。在本研究中,我们研究了顺序不同压力热解方法(水热-微波法和回流-微波法)对甘蔗叶片生物质碳纳米结构特性的影响。每次回流和水热法在200oC下调节,然后在800W下微波。表征结果表明,水热微波法x射线衍射显示了碳纳米结构和纤维素的衍射图。扫描电镜显微图显示球形和块状。FTIR光谱显示不同浓度的氧表面官能团。分散产物在水中的紫外光谱表明存在芳烃C=C基团。与回流微波法相比,水热微波法制备的产物纤维素的结晶度指数更低,颗粒更小,表面氧基浓度更低。化学性质(芳香性和极性基团分数)的相关性比理化性质(纤维素结晶度指数和极性基团分数)的相关性更小。用分散法对胶体的稳定性进行了表征,其顺序为超声<共混<共混-超声。
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引用次数: 0
Information System Evaluation for Cervical Cancer Detection Program in Mexican Women 墨西哥妇女子宫颈癌检测项目的信息系统评价
Q3 Engineering Pub Date : 2022-08-31 DOI: 10.22201/icat.24486736e.2022.20.4.1384
Edgar Leonel Gonzalez Gonzalez, Ismael Ruíz Fraga, Lina Sofía Palacio, Mildred Yazmin Chávez Cárdenas, Diana Molina Vélez, Concepción García Morales, Rosa Ivonne Hernández Montes, Vesta L. Richardson López Collada
The aim of this study was to evaluate the design and implementation of the Information System for Cervical Cancer Detection Program in Women in the Institute for Social Security and Services for State Workers. We performed a retrospective study applying the framework and tools for Performance Routine Information System Management (PRISM). A sample of 38 subjects was interviewed in 13 health facilities. The information system’s evaluation showed an overall performance of 73.7% at the beginning of 2017. The improvement between versions was mainly observed in the quality of the data (64.6% vs 72.5%), while the use of the information was very similar (78.6% vs 78.9%). We concluded that this information system provides good information to follow-up and control of its beneficiary population. However, there is an opportunity to improve health staff training, also new indicators for health outcomes are required.
本研究的目的是评估社会保障和国家工作人员服务研究所妇女宫颈癌检测方案信息系统的设计和实施情况。我们应用绩效常规信息系统管理(PRISM)的框架和工具进行了回顾性研究。在13个卫生机构对38名受试者进行了访谈。2017年初,信息系统评价总体绩效为73.7%。版本之间的改进主要体现在数据质量上(64.6% vs 72.5%),而信息的使用非常相似(78.6% vs 78.9%)。我们的结论是,该信息系统为跟踪和控制其受益人口提供了良好的信息。但是,有机会改进对保健工作人员的培训,而且需要制定新的保健结果指标。
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引用次数: 0
A homemade freezing unit for ice-templating 自制的冰模板冷冻装置
Q3 Engineering Pub Date : 2022-08-31 DOI: 10.22201/icat.24486736e.2022.20.4.1328
L. S. Aguilera, Eustáquio de Souza Baêta Júnior, R. Marçal, L. Brandão, M. H. P. da Silva, Ronaldo Sergio De Baisi, A. B. S. Figueiredo
A novel freezing unit was developed for use in ceramic processing by the freeze casting technique. This step is crucial, since the macrostructure promoted by this technique is formed during freezing. Several authors present basic information about the apparatus used in the freezing step, but there are no studies that describe a complete unit as we do in this work and there is no commercial equipment for this purpose. The components of the freezing unit were selected according to function, suitability to project, cost and market availability. Advanced ceramic samples of ZnFe2O4, MnFe2O4, CoFe2O4, NiFe2O4, SiO2, Al2O3 and metallic Cu were produced using the freezing unit and the results of typical macrostructure and porosity analysis validated the chosen setup.
采用冷冻铸造技术,研制了一种用于陶瓷加工的新型冷冻装置。这一步骤至关重要,因为该技术促进的宏观结构是在冷冻过程中形成的。几位作者介绍了冷冻步骤中使用的设备的基本信息,但没有像我们在这项工作中所做的那样描述完整单元的研究,也没有用于此目的的商业设备。冷冻装置的部件是根据功能、项目适用性、成本和市场可用性进行选择的。使用冷冻装置制备了ZnFe2O4、MnFe2O4和CoFe2O4的高级陶瓷样品,NiFe2O4,SiO2,Al2O3和金属Cu,典型的宏观结构和孔隙率分析结果验证了所选择的装置。
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引用次数: 0
Doping lanthanum manganites particles with strontium-calcium for application in hyperthermia 锶钙掺杂锰酸镧粒子在热疗中的应用
Q3 Engineering Pub Date : 2022-08-31 DOI: 10.22201/icat.24486736e.2022.20.3.1405
L. Rivera-Rios, I. Perez-Lopez, J. T. Elizalde-Galindo, J. R. Farias-Mancilla, P. Mani-Gonzalez
The use of materials capable of controlling the threshold temperature required in hyperthermia, as well as meeting desired requirements in biomedical applications is still a challenge. In the present study, strontium doped calcium lanthanum manganites La0.7Ca0.3-xSrxMnO3 (x=0, 0.1, 0.15 and 0.2) were synthesized by co-precipitation method. Vibrating sample magnetometry (VSM) was used to study the effect of change Ca-Sr ratio on magnetic properties. The Curie temperature (Tc) increases from 272 to 315 K as the concentration increases from x=0 to x=0.2 respectively. Hence the strontium amount plays an important role in achieving the desired Tc . X-ray diffraction (XRD) was used to identify rhombohedral structure and scanning electronic microscopy (SEM) was used to characterize the cubic morphology and around 800 nm as particles size.
使用能够控制热疗所需阈值温度以及满足生物医学应用所需要求的材料仍然是一个挑战。本研究采用共沉淀法合成了锶掺杂的钙镧锰酸盐La0.7Ca0.3-xSrxMnO3(x=0,0.1,0.15和0.2)。采用振动样品磁强计(VSM)研究了Ca-Sr比值变化对磁性能的影响。居里温度(Tc)随着浓度从x=0增加到x=0.2而分别从272增加到315K。因此,锶的量在实现期望的Tc方面起着重要作用。X射线衍射(XRD)用于鉴定菱面体结构,扫描电子显微镜(SEM)用于表征立方形态和约800nm的颗粒尺寸。
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引用次数: 0
Transshipment and Routing Model for Multi-Product Planning and Distribution at a Refreshment Company in Bogota, Colombia 哥伦比亚波哥大一家点心公司多产品计划和分销的转运和路线模型
Q3 Engineering Pub Date : 2022-08-31 DOI: 10.22201/icat.24486736e.2022.20.4.1330
Oscar Javier Herrera Ochoa, Nicolas Arrieta Camacho, Vianey Lizeth Jerez Amador, Geraldine Camacho Perez, Ivan Dario Romero
In this article, a model is established for the planning of the weekly distribution of refreshments in a company that produces 6 types of beverages in 3 Production Centers, with the potential use of 3 Distribution Centers and supplying 22 Consumer Centers located in Bogota. Due to the impact of transportation costs on the company profits, it is necessary to determine the optimal planning of the allocation of sources to destinations in the nodal network of the system and its subsequent routing with two types of vehicles. Therefore, a two-phase model is proposed. In the first, the initial optimal assignments are established by comparing two techniques; one based on the Open Transshipment Problem (OTP) and the other on the Capacitated Transshipment Problem (CTP), which determine the trips to be made from production centers to consumer centers using distribution centers as intermediaries. This comparison allowed to analyze its efficiency to choose the model with the lowest cost and number of trips. In the second phase, routing was performed on routes that do not use the full capacity of the vehicles. The routes were established through the Travelling Salesman Problem (TSP). As a result, a comprehensive model was obtained to carry out the planning of the product distribution, obtaining in Phase II the use of the OTM model, which presented 14% less distance; 2.6% less time and 0.28% less than the total cost compared to the CTP model. In Phase II  5 routes were obtained, of which Distribution Center 2 covers 59% of customers.
在本文中,建立了一个模型,用于规划一家在3个生产中心生产6种饮料的公司的每周点心配送,该公司有可能使用位于波哥大的3个配送中心并供应22个消费者中心。由于运输成本对公司利润的影响,有必要确定系统节点网络中资源到目的地的最优规划,以及随后使用两种类型车辆的路线。因此,提出了一个两相模型。首先,通过比较两种技术建立了初始最优分配;一个基于开放转运问题(OTP),另一个基于容量转运问题(CTP),其确定使用配送中心作为中介从生产中心到消费者中心的行程。这种比较可以分析其效率,以选择成本和出行次数最低的模型。在第二阶段,在没有使用全部车辆容量的路线上进行了选路。这些路线是通过旅行推销员问题(TSP)确定的。因此,获得了一个全面的模型来进行产品分销的规划,在第二阶段获得了OTM模型的使用,该模型的距离减少了14%;与CTP模型相比,时间减少2.6%,总成本减少0.28%。在第二阶段获得了5条路线,其中配送中心2覆盖了59%的客户。
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引用次数: 0
Analysis of the Influence of Contaminants on Microhardness Sintered Boron Carbide Samples 污染物对烧结碳化硼试样显微硬度的影响分析
Q3 Engineering Pub Date : 2022-08-31 DOI: 10.22201/icat.24486736e.2022.20.4.1327
L. S. Aguilera, Manoel Antônio Da Fonseca Costa Filho, Celio Albano Costa Neto, J. D. de Campos
This work presents ANOVA and Tukey’s statistic tests that were carried out in Knoop microhardness results of boron carbide sintered samples. Three samples, A, B and C, of different processing conditions were tested and statistical analysis showed that microhardness results are strongly influenced by porosity and chemical composition, mainly due to presence of C(2H) and WB2.5 contaminant phases. Those phases promoted higher densification in A and B samples and it was found that A ≈ B > C is the relation between the microhardness results of the samples, while A ≈ B < C is the porosity ratio of the samples. Furthermore, this work aims to apply a statistical tool to evaluate the microhardness results performed on advanced ceramics and, using these results, to control parameters in the sintering process, showing that a deeper statistical analysis is necessary for the interpretation and validation of the results merit.
本文介绍了对碳化硼烧结样品的Knoop显微硬度结果进行的方差分析和Tukey统计检验。对不同加工条件下的A、B、C三种样品进行了测试,统计分析表明,孔隙度和化学成分对显微硬度结果的影响很大,主要是由于C(2H)和WB2.5污染物相的存在。结果表明:A≈B > C为试样显微硬度结果之间的关系,A≈B < C为试样的孔隙率比。此外,本工作旨在应用统计工具来评估高级陶瓷的显微硬度结果,并使用这些结果来控制烧结过程中的参数,这表明需要更深入的统计分析来解释和验证结果的价值。
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引用次数: 0
Current-controlled grounded memristor emulator circuit based on analog multiplier 基于模拟乘法器的电流控制接地忆阻仿真电路
Q3 Engineering Pub Date : 2022-07-01 DOI: 10.22201/icat.24486736e.2022.20.3.932
M. A. Carrasco-Aguilar, C. Sánchez-López, F. E. Morales-Lopez
This paper proposes a current-controlled grounded memristor emulator circuit based on single four-quadrant analog multiplier, a resistor and a capacitor. The behavioral model of the proposed emulator circuit is analyzed, highlighting its characteristics. Experimental results are given to investigate its ability for different operating frequencies and they are in accordance with theoretical analysis and simulation results. By using a divider circuit, the memristance variation in the time domain is obtained. It is observed that the pinched hysteresis loop at high frequency loses symmetry due in part to the shift that introduces a multiplication of sinusoidal signals.
本文提出了一种基于单四象限模拟乘法器、电阻和电容的电流控制接地忆阻器仿真电路。分析了仿真电路的行为模型,突出了仿真电路的特点。实验结果与理论分析和仿真结果相吻合。利用分频电路,得到了时域内的忆阻变化。可以观察到,在高频处,由于引入正弦信号倍增的移位,压缩的迟滞环失去了对称性。
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引用次数: 0
Repetitive corrugation and straightening effect on the microstructure, crystallographic texture and electrochemical behavior for the Al-7075 alloy 重复波纹和矫直对Al-7075合金组织、织构和电化学行为的影响
Q3 Engineering Pub Date : 2022-07-01 DOI: 10.22201/icat.24486736e.2022.20.3.1789
L. Romero-Resendiz, M. Hernández, J. Cabrera, S. Elizalde, V. Amigó-Borrás, I. A. Figueroa, A. Covelo, G. Gonzalez
Anti-corrosion susceptibility is one of the top criteria for selecting metallic materials for several industrial applications. This work studies the corrosion performance on an Al-7075 alloy obtained by Repetitive Corrugation and Straightening (RCS). This processing method generated a microstructure formed by randomly distributed micro-, submicro-, and nano- metric grain sizes. The samples exhibited a drop in corrosion resistance for a longer duration in the electrolyte and higher deformation. However, the samples processed by RCS showed better electrochemical stability in comparison with the non-deformed condition. The improvement of electrochemical stability could be associated with the particular microstructure generated during the RCS process.
抗腐蚀敏感性是选择用于多种工业应用的金属材料的首要标准之一。本工作研究了通过重复波纹和矫直(RCS)获得的Al-7075合金的腐蚀性能。这种加工方法产生了由随机分布的微米、亚微米和纳米晶粒尺寸形成的微观结构。样品在电解质中的耐腐蚀性在更长的时间内下降,变形更大。然而,与非变形条件相比,RCS处理的样品显示出更好的电化学稳定性。电化学稳定性的提高可能与RCS过程中产生的特定微观结构有关。
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引用次数: 0
Electromagnetic fields as a non-invasive alternative therapy for the treatment of musculoskeletal diseases 电磁场作为治疗肌肉骨骼疾病的非侵入性替代疗法
Q3 Engineering Pub Date : 2022-07-01 DOI: 10.22201/icat.24486736e.2022.20.3.1790
J. J. Vaca-González, Juliana I. P. Cantillo Bermúdez, Liliana Andrea Rodríguez Sarmiento, Aldemar Fonseca Velásquez
This review article elucidates the application and viability of electromagnetic fields as therapy and rehabilitation method for the treatment of musculoskeletal pathologies. All studies were found in different databases such as Science Direct, Scielo, IEEE, ProQuest, Pubmed, among others, where the search for information contemplated a period of 5 years (2016-2020). Results evidenced that electromagnetic fields used to treat musculoskeletal conditions showed positive results and improvements in reducing chronic and acute pain in different musculoskeletal pathologies such as osteoarthritis, osteoporosis, nonunions, fractures, fibromyalgia, muscular system injuries, among others. It was possible to evidence that one of the most used magnetic treatments were pulsed electromagnetic fields, which have been implemented to treat joint, muscle and nervous diseases. Additionally, several devices to generate the magnetic stimulation have been designed with a therapeutic and rehabilitation approach, which elucidate the progress in the implementation and acceptance of this type of therapeutic alternatives to treat musculoskeletal conditions. Finally, magnetic stimulation has been also implemented to enhance biomaterials function, evidencing that scaffolds stimulated with electromagnetic fields improve musculoskeletal tissue regeneration.
本文综述了电磁场作为一种治疗和康复方法在肌肉骨骼疾病治疗中的应用和可行性。所有的研究都是在不同的数据库中发现的,如Science Direct、Scielo、IEEE、ProQuest、Pubmed等,其中的信息搜索预计为期5年(2016-2020)。结果证明,用于治疗肌肉骨骼疾病的电磁场在减少不同肌肉骨骼疾病(如骨关节炎、骨质疏松症、骨不连、骨折、纤维肌痛、肌肉系统损伤等)的慢性和急性疼痛方面显示出积极的效果和改善。有可能有证据表明,最常用的磁疗之一是脉冲电磁场,它已被用于治疗关节、肌肉和神经疾病。此外,一些产生磁刺激的设备已经被设计成具有治疗和康复方法,这阐明了在实施和接受这种类型的治疗替代方案来治疗肌肉骨骼疾病方面的进展。最后,磁刺激也被用于增强生物材料的功能,证明电磁场刺激的支架可以改善肌肉骨骼组织的再生。
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引用次数: 3
First Principles Calculations of Co2MSi (M=Cr, Mn, Fe) Heusler Alloys Co2MSi(M=Cr,Mn,Fe)Heusler合金的第一性原理计算
Q3 Engineering Pub Date : 2022-07-01 DOI: 10.22201/icat.24486736e.2022.20.3.780
Ashish Pathak, R. Sankarasubramanian
The present work describes the electronic structure, magnetic and elastic properties of ordered Co2MSi (M = Cr, Mn, Fe) Heusler alloys in L21 structure calculated using density functional theory within generalized gradient approximation. The calculated band structures, density of states and magnetic moments have been discussed. The magnetic moment values obtained in present study follow the Slater-Pauling rule. A small band gap in the minority band structure at the Fermi level suggests half-metallicity. Hundred percentage spin polarization in this ordered structure implies that these materials possess ferromagnetism. All the three materials satisfy stability criteria in terms of elastic constants and are predicted to have ductile behaviour based on the ratio of shear to bulk modulus.
本文描述了用密度泛函理论在广义梯度近似下计算L21结构中有序Co2MSi (M = Cr, Mn, Fe) Heusler合金的电子结构、磁性和弹性。讨论了计算得到的能带结构、态密度和磁矩。本研究得到的磁矩值符合Slater-Pauling规则。在费米能级的少数能带结构中,一个小的带隙表明了半金属性。在这个有序结构中,100%的自旋极化意味着这些材料具有铁磁性。这三种材料都满足弹性常数方面的稳定准则,并根据剪切与体积模量的比值预测具有延性。
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引用次数: 0
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Journal of Applied Research and Technology
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