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Studies on the Effect of Substrate Preheating, Interlayer Dwell, and Heat Treatment on Microstructure, Residual Stress, and Mechanical Properties of IN625 Superalloy built by Direct Metal Deposition 基体预热、层间停留和热处理对金属直接沉积IN625高温合金组织、残余应力和力学性能影响的研究
IF 1.2 4区 材料科学 Q3 ENGINEERING, MECHANICAL Pub Date : 2023-05-05 DOI: 10.1115/1.4062503
Mohsin Khan K, T. B. Rao, R. Mohammed, Manjunath B N, K. Abhinav, Vinod A R
In this investigation, IN625 alloy samples were processed by directed energy deposition (DED) under various metal deposition strategies such as substrate preheating, inter-layer dwell, and with combined substrate preheating, inter-layer dwell as well as post-heat treatment. The processed sample's microstructural characteristics, residual stress, microhardness, and tensile properties are assessed in comparison to the manufacturing strategies. Rapid heat dissipation caused finer microstructure near the substrate. There is a growth of columnar grain structure epitaxially in the build direction. The progressive microstructure change seen in the build direction across the cross-section was due to the gradual rise of heat accumulation between subsequent layers. The inter-dendritic zones contained Laves phases. Laves phases have a high Nb, Mo as well as Si content, according to the EDS spectrum. The FESEM microstructural morphology of the deposited samples after their post-heat treatment has shown a new microstructure with the combination of equiaxed (recrystallized) and columnar dendritic structure with the reconstruction of columnar dendritic solidification microstructure into equiaxed grains. Heat treatment caused the Laves phases to dissolve in the matrix of IN625 alloy, which led to the precipitation of nanometric γ″ phases. The deposition strategies with substrate preheating significantly decreased the residual stress with moderately improved mechanical properties. The combination of substrate preheating, inter-layer dwell, and post-heat treatment has shown an outstanding reduction of residual stress along with a remarkable improvement in tensile strength with the retainment of an equivalent ductility compared with the other strategies.
在本研究中,IN625合金样品在各种金属沉积策略下通过定向能量沉积(DED)进行处理,如基底预热、层间停留、以及组合基底预热、层层间停留和后热处理。与制造策略相比,对加工样品的微观结构特征、残余应力、显微硬度和拉伸性能进行了评估。快速散热导致衬底附近的微观结构更加精细。在构建方向上外延生长柱状晶粒结构。在整个横截面的构建方向上看到的渐进微观结构变化是由于后续层之间的热量积累逐渐增加。枝晶间带含有Laves相。根据EDS光谱,Laves相具有高Nb、Mo以及Si含量。沉积样品经过后热处理后的FESEM微观结构形态显示出一种新的微观结构,其具有等轴(再结晶)和柱状树枝状结构的组合,并将柱状树枝晶凝固微观结构重建为等轴晶粒。热处理使Laves相溶解在IN625合金基体中,导致纳米γ〃相的析出。衬底预热的沉积策略显著降低了残余应力,并适度改善了机械性能。与其他策略相比,基材预热、层间停留和后热处理的组合显示出残余应力的显著降低,以及拉伸强度的显著提高,同时保持了等效的延展性。
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引用次数: 1
Fatigue Damage Study of Steel-aluminum Friction Stir Welding Joints Based on Equivalent Damage Model 基于等效损伤模型的钢铝搅拌摩擦焊接头疲劳损伤研究
IF 1.2 4区 材料科学 Q3 ENGINEERING, MECHANICAL Pub Date : 2023-04-27 DOI: 10.1115/1.4062444
Haifeng Wu, Shan Xu, Hao Chen, Yali Yang, K. Gao, Yongfang Li
An equivalent damage model was established to study the fatigue damage behavior of steel-aluminum friction stir welding (FSW) joints. Internal defects of friction stir welding joint under various cyclic loading stages were observed by X-ray microcomputed tomography (X-CT). For the characteristics of defects of the steel-aluminum FSW joints, a simplified method of defects considering key parameters is proposed and then the defect model is established. The FSW joint model was established based on the steel-aluminum boundary contour identified by using image processing techniques. Based on the defect model and the FSW joint model, the equivalent damage model was developed. The equivalent damage model was subjected to finite element analysis and compared with the test using the strain amplitude as the damage variable. The equivalent damage model can be used to assess fatigue damage in steel-aluminum FSW joints, which provides some theoretical basis for fatigue life prediction.
建立了钢铝搅拌摩擦焊(FSW)接头的等效损伤模型,研究了FSW接头的疲劳损伤行为。利用X射线微计算机断层扫描(X-CT)对搅拌摩擦焊接接头在不同循环加载阶段的内部缺陷进行了观察。针对钢铝FSW节点缺陷的特点,提出了一种考虑关键参数的缺陷简化方法,并建立了缺陷模型。基于图像处理技术识别出的钢铝边界轮廓,建立了FSW接头模型。在缺陷模型和FSW节点模型的基础上,建立了等效损伤模型。对等效损伤模型进行了有限元分析,并与以应变幅度为损伤变量的试验进行了比较。等效损伤模型可用于评估钢铝FSW接头的疲劳损伤,为疲劳寿命预测提供了一定的理论依据。
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引用次数: 0
Influence of Diffusion Bonding Pressure on Microstructural Features and Strength Performance of Dissimilar Ti6Al4V Alloy and AISI 304 Steel Joints using Copper Interlayer 扩散接合压力对异种Ti6Al4V合金和AISI 304钢铜中间层接头组织特征和强度性能的影响
IF 1.2 4区 材料科学 Q3 ENGINEERING, MECHANICAL Pub Date : 2023-04-27 DOI: 10.1115/1.4062443
A. A, Rajakumar Selvarajan, Tushar Sonar, M. Ivanov
The joining of Ti6Al4V (Ti64) alloy and AISI 304 austenitic stainless steel (ASS 304) carries significant importance in aero-engines for turbine blade applications. However, it is difficult to join using fusion welding. The fusion welding of Ti64 alloy and ASS 304 steel promotes the evolution of various Fe-Cr-Ti and Fe-Ti intermetallics in weld zone owing to limited solid solubility of Fe, Cr, Ti, and Ni with each other. The evolution of these intermetallics deteriorates the strength properties of joints. Hence for joining Ti6Al4 alloy and ASS 304 steel, vacuum diffusion bonding (VBD) method is employed with thin Copper (Cu) foil as an interlayer. DB pressure extends a significant influence on microstructural evolution and strength of joints. So, for the feasibility of joining Ti alloy and ASS, the effect of DB pressure on microstructure and strength of joints is investigated. Results showed that the dissimilar joints of Ti64 alloy and ASS 304 steel developed using the DB pressure of 14 MPa exhibited greater lap shear strength (LSS) and bonding strength (BS) of 180 MPa and 268 MPa respectively. It is mostly related to improved joining interface coalescence and the development of the ideal bonding width with the least amount of embrittlement consequences. An increase in DB pressure increases the width of diffusion region which favors the development of detrimental intermetallics of Ti-Fe and curtails the strength of dissimilar joints.
Ti6Al4V (Ti64)合金与AISI 304奥氏体不锈钢(ASS 304)的结合在航空发动机涡轮叶片应用中具有重要意义。然而,用熔焊连接是困难的。Ti64合金与as304钢的熔焊,由于Fe、Cr、Ti和Ni之间的固溶性有限,促进了焊缝区各种Fe-Cr-Ti和Fe-Ti金属间化合物的析出。这些金属间化合物的演化使接头的强度性能恶化。因此,采用真空扩散焊(VBD)的方法将Ti6Al4合金与as304钢连接,并采用薄铜箔作为中间层。DB压力对接头的组织演化和强度有显著影响。因此,为了验证钛合金与ASS连接的可行性,研究了DB压力对接头组织和强度的影响。结果表明:DB压力为14 MPa时,Ti64合金与as304钢异种接头的搭接剪切强度(LSS)和结合强度(BS)分别达到180 MPa和268 MPa;这主要与改善连接界面的聚结和发展理想的结合宽度和最小的脆化后果有关。DB压力的增加增加了扩散区的宽度,有利于有害的Ti-Fe金属间化合物的发展,降低了异种接头的强度。
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引用次数: 1
Fabrication and Characterization of Magnesium-Based WE43/TiC Nanocomposite Material Developed via Friction Stir Processing and Study of Significant Parameters 搅拌摩擦法制备镁基WE43/TiC纳米复合材料及其重要参数研究
IF 1.2 4区 材料科学 Q3 ENGINEERING, MECHANICAL Pub Date : 2023-04-12 DOI: 10.1115/1.4062321
Magnesium Metal Matrix Composites (MMMCs) have exceptional mechanical and metallurgical characteristics, which has drawn the interest of researchers across the world. In the present research study, an attempt has been made to fabricate WE43 magnesium (Mg) based nanocomposites using Friction stir processing (FSP) after incorporating nano-Titanium carbide(TiC) as a reinforcement. Further, the impact of different FSP variables such as transverse speeds (40 mm/min and 80 mm/min), and tool rotation speeds (900 rpm and 1800rpm) over the metallurgical, wear, and mechanical performance has been studied. The large thermal energy generated by the rotating FSP tool gives rise to the mechanism of dynamic recrystallization and plastic deformation. This contributes to refining the microstructure and improvement in microhardness as per Hall–Patch relation- contributing to prominent grain size refinement and Orowan mechanism strengthening, due to the dispersion of reinforcement particulates. The outcome of the results depicts that the nanocomposite fabricated at a tool rotation speed of 1800 rpm and 80 mm/min transverse shows better mechanical and tribological characteristics than other developed composites and the base alloy. More specifically, the grain size was reduced nearly 12 times, microhardness was 2.58 times higher, and ultimate tensile strength (UTS) was 2.08 times higher when contrasted to the base alloy. Moreover, the un-processed base material was characterized by an adhesive wear mechanism whereas the presence of scratches depicts the abrasive wear mechanism was dominant for WE43/TiC nanocomposite.
镁金属基复合材料(MMMC)具有优异的力学和冶金特性,引起了世界各地研究人员的兴趣。在本研究中,在掺入纳米碳化钛(TiC)作为增强材料后,尝试使用摩擦搅拌处理(FSP)制备WE43镁基纳米复合材料。此外,还研究了不同FSP变量,如横向速度(40mm/min和80mm/min)和刀具转速(900rpm和1800rpm)对冶金、磨损和机械性能的影响。旋转FSP刀具产生的巨大热能产生了动态再结晶和塑性变形的机制。根据霍尔-帕奇关系,这有助于细化微观结构和提高显微硬度——由于增强颗粒的分散,有助于显著的晶粒细化和奥罗万机制强化。结果表明,在1800rpm和80mm/min横向工具转速下制备的纳米复合材料比其他开发的复合材料和基础合金显示出更好的机械和摩擦学特性。更具体地说,与基体合金相比,晶粒尺寸减小了近12倍,显微硬度提高了2.58倍,极限抗拉强度(UTS)提高了2.08倍。此外,未加工的基体材料的特征是粘附磨损机制,而划痕的存在表明WE43/TiC纳米复合材料的磨损机制占主导地位。
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引用次数: 0
Study on the Corrosion Behavior and Numerical Simulation of TC18 Titanium Alloy under Tensile Stress TC18钛合金拉伸应力腐蚀行为及数值模拟研究
IF 1.2 4区 材料科学 Q3 ENGINEERING, MECHANICAL Pub Date : 2023-04-11 DOI: 10.1115/1.4062289
Both understanding and simulation of the process of corrosion damage are crucial for the prediction of remaining service life of engineering structures, sound reliability analysis, and design for the purpose of enhancing overall resistance of the material to corrosion damage. A coupled mechano-electrochemical PD corrosion model was established by using the peridynamic (PD) corrosion theory and the mechano-chemical effect theory.The model is capable of simulating the occurrence of degradation caused by the conjoint and mutually interactive influences of mechano-electrochemical phenomena. Corrosion behavior of TC18 titanium alloy in EXCO solution under stress loads of 31% σ0.2, 47% σ0.2 and 62% σ0.2 was studied. The effect of tensile loads on the corrosion behavior of TC18 titanium alloy was examined by combining the micromorphology and electrochemical parameters to verify the dependence of reaction rate occurring at the anode on tensile stress. Results of this study shed light as the stress level increases, the corrosion potential of TC18 titanium alloy shifts negatively, the corrosion current density increases and the corrosion intensifies. When the phase transition mechanism is satisfied, boundary movement occurs spontaneously.This model can safely be employed to complex geometric shapes and as a basis for studying crack propagation in environments that are favorable or conducive for inducing corrosion.
对腐蚀损伤过程的理解和模拟对于预测工程结构的剩余使用寿命、进行可靠的可靠性分析和设计以提高材料对腐蚀损伤的整体抵抗力至关重要。利用周动力学腐蚀理论和机械化学效应理论,建立了机械-电化学耦合的PD腐蚀模型。该模型能够模拟由机械-电化学现象的共同和相互作用影响引起的降解的发生。研究了TC18钛合金在EXCO溶液中在31%σ0.2、47%σ0.2和62%σ0.2应力载荷下的腐蚀行为。结合微观形貌和电化学参数,研究了拉伸载荷对TC18钛合金腐蚀行为的影响,以验证阳极反应速率对拉伸应力的依赖性。研究结果表明,随着应力水平的增加,TC18钛合金的腐蚀电位负移,腐蚀电流密度增加,腐蚀加剧。当满足相变机制时,边界运动自发发生。该模型可以安全地用于复杂的几何形状,并作为研究有利于或有利于诱发腐蚀的环境中裂纹扩展的基础。
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引用次数: 0
Comparison of Fatigue Life of AA2050-T852 and AA7050-T7452 Alloy Forgings at Different Orientations AA2050-T852和AA7050-T7452合金锻件不同方位疲劳寿命的比较
IF 1.2 4区 材料科学 Q3 ENGINEERING, MECHANICAL Pub Date : 2023-04-03 DOI: 10.1115/1.4062257
Ngoc Fuhr, S. Zhou, Keren Shen, Aseel Rajab, Salim Es-Said, Thaung Shonnu, Skyler Tan, Ryan Riebe, Nathan Santos, Ye Thura Hein, R. Toal, Yong Jun Li, M. Timko, O. Es-Said
This study compares the fatigue performance between the AA2050-T852 alloy and AA7050-T7452 alloy traditionally used in aircraft structures. Rotating beam fatigue tests were performed on AA2050-T852 and AA7050-T7452 specimens cut from forged plates with different orientations and at different thickness levels. The samples were tested at 345 MPa (50 ksi), 276 MPa (40 ksi), 207 MPa (30 ksi) and 172 MPa (25 ksi). Scanning Electron Microscope (SEM) images showed mixed mode in all samples. However, the equiaxed dimples were more abundant and finer in the AA2050-T852 alloy. The results indicated that AA2050-T852 alloy demonstrated better fatigue life performance compared to AA7050-T7452 alloy at almost all stresses. No significant difference in fatigue anisotropy was found in one alloy versus the other.
本研究比较了飞机结构中常用的AA2050-T852合金和AA7050-T7452合金的疲劳性能。对不同取向、不同厚度的锻造板上切割的AA2050-T852和AA7050-T7452试样进行了旋转梁疲劳试验。样品分别在345 MPa (50 ksi)、276 MPa (40 ksi)、207 MPa (30 ksi)和172 MPa (25 ksi)下进行了测试。所有样品的扫描电镜(SEM)图像均为混合模式。而AA2050-T852合金的等轴韧窝更丰富、更细小。结果表明:在几乎所有应力下,AA2050-T852合金的疲劳寿命性能均优于AA7050-T7452合金。两种合金的疲劳各向异性无显著差异。
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引用次数: 0
Analytical Modeling of Electronic and Photonic Materials Reliability: Perspective and Extension 电子和光子材料可靠性的分析建模:透视与扩展
IF 1.2 4区 材料科学 Q3 ENGINEERING, MECHANICAL Pub Date : 2023-03-08 DOI: 10.1115/1.4062085
E. Suhir
The objective of this review is double-folded: to show materials scientists, mechanical engineers and reliability physicists not involved in electronics, photonics, micro-electronic-mechanical-systems (MEMS) or MOEMS (optical MEMS) engineering what kind of value they could bring to this important “high-tech” area, as well as to demonstrate to “high-tech” engineers how they could benefit from the application of what has been developed, for many years, in the general field of physical design for reliability of materials and structures employed in various fields of engineering and applied science and what could be effectively applied to their body of knowledge. Accordingly, in the perspective part of the review some critical and even paradoxical, i.e., a-priori non-obvious, problems encountered in microelectronics and photonics materials science, reliability physics and structural analysis are addressed using what could be called analytical (“mathematical”) modeling. The extension part has to do with some specific, mostly aerospace, recent applications of the probabilistic design for reliability concept and analytical modeling effort.
本次审查的目的是双重的:向材料科学家、机械工程师和不涉及电子、光子学、微电子机械系统(MEMS)或MOEMS(光学MEMS)工程的可靠性物理学家展示他们可以为这一重要的“高科技”领域带来什么样的价值,以及向“高科技”工程师展示他们如何从多年来开发的应用中受益。在物理设计的一般领域中,用于各种工程和应用科学领域的材料和结构的可靠性,以及什么可以有效地应用于他们的知识体系。因此,在回顾的观点部分,一些关键的,甚至是矛盾的,即先验的非明显的,在微电子和光子材料科学,可靠性物理和结构分析中遇到的问题,使用所谓的分析(“数学”)建模来解决。扩展部分与一些具体的,主要是航空航天,可靠性概念的概率设计的最新应用和分析建模工作有关。
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引用次数: 0
Multiphysics Simulations of Microwave Induced Damage Applied to Rock Samples of Varying Strength and Absorptivity 不同强度和吸收率岩石样品微波损伤的多物理模拟
IF 1.2 4区 材料科学 Q3 ENGINEERING, MECHANICAL Pub Date : 2023-02-24 DOI: 10.1115/1.4056996
J. Allen, Reena Patel, Oliver W. Taylor
In this work, we show the development of a numerical model to investigate the 3D interactions between microwave radiation and basalt, granite, and sandstone rock samples. In particular, we assign sample heterogeneity based on the Weibull statistical distribution, and invoke a damage model for elemental tensile and compressive stresses based on the maximum tensile stress and the Mohr-Coulomb theories, respectively. Model implementation is facilitated by the use of COMSOL for use in coupling the electromagnetic, thermal, and solid displacement relations. Various parametric studies are conducted related to variable input power and waveguide port alignment, with model validation conducted with respect to damage resulting from a uniaxial compression test. The results indicate that relatively high induced temperatures will promote damage potential, but its impact must be placed within the context of the sample strength to quantify the true potential damage evolution of a given rock mass. As observed herein, a mechanically weaker rock may be prone to mechanical damage; however, it may also possess a relatively large relative permittivity, enabling it to absorb the least amount of microwave radiation thus yielding comparatively low overall damage profiles compared to a more mechanically competent rock mass.
在这项工作中,我们展示了一个数值模型的发展,以研究微波辐射与玄武岩,花岗岩和砂岩岩石样品之间的三维相互作用。特别地,我们基于Weibull统计分布分配了样品的非均匀性,并分别基于最大拉应力和Mohr-Coulomb理论调用了元素拉伸和压缩应力的损伤模型。通过使用COMSOL来耦合电磁、热和固体位移关系,促进了模型的实现。我们进行了与可变输入功率和波导端口对准相关的各种参数研究,并对单轴压缩试验造成的损伤进行了模型验证。结果表明,相对较高的诱导温度会促进潜在的损伤,但其影响必须放在样品强度的背景下,才能量化给定岩体的真实潜在损伤演变。由此可见,力学性质较弱的岩石更容易发生力学损伤;然而,它也可能具有相对较大的相对介电常数,使其能够吸收最少的微波辐射,因此与机械性能更好的岩体相比,产生相对较低的总体损伤剖面。
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引用次数: 0
XFEM Analysis of Strain Rate Dependent Mechanical Properties of Additively Manufactured 17-4 PH Stainless Steel 添加17-4PH不锈钢应变速率相关力学性能的XFEM分析
IF 1.2 4区 材料科学 Q3 ENGINEERING, MECHANICAL Pub Date : 2023-01-23 DOI: 10.1115/1.4056729
B. Kalita, J. R.
Additively manufactured (AM) specimens of 17-4PH stainless steel corresponding to the three-point bend test, compact tension test and single edge cracks were analysed using Extended Finite Element Method (XFEM) approach. A two-dimensional and three-dimensional elastic-plastic simulation were conducted using “Abaqus 6.14” software based on the experimental results and validated with the simulation results. In XFEM, the partition of unity (PU) was used to model a crack in the standard finite element mesh. Based on simulation results, the present study compares the mechanical properties of AM 17-4 PH stainless steel samples with those of wrought 17-4 PH samples. Stress intensity factor and J integral were used to measure fracture toughness of the specimens. The change in fracture toughness with strain rate was evaluated by simulating two-dimensional compact tension specimens. The presence of defects such as pores resulting from entrapped gas, un-melted regions, and powder particles resulting from lack of fusion were the main reasons for lower elongation to failure of LPBF produced 17-4PH SS reported in the literature.
采用扩展有限元法(XFEM)分析了与三点弯曲试验、紧凑拉伸试验和单边裂纹相对应的17-4PH不锈钢增材(AM)试样。基于实验结果,使用“Abaqus 6.14”软件进行了二维和三维弹塑性模拟,并与模拟结果进行了验证。在XFEM中,使用单位划分(PU)对标准有限元网格中的裂纹进行建模。基于模拟结果,本研究将AM 17-4PH不锈钢样品与锻造17-4PH样品的力学性能进行了比较。采用应力强度因子和J积分测量了试样的断裂韧性。通过模拟二维致密拉伸试样,评估了断裂韧性随应变速率的变化。文献中报道的LPBF生产的17-4PH SS的断裂伸长率较低的主要原因是存在缺陷,如由截留气体引起的孔隙、未熔化区域和由未熔合引起的粉末颗粒。
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引用次数: 0
A Finite Volume Framework for the Simulation of Additive Friction Stir Deposition 加性搅拌摩擦沉积模拟的有限体积框架
IF 1.2 4区 材料科学 Q3 ENGINEERING, MECHANICAL Pub Date : 2023-01-10 DOI: 10.1115/1.4056642
Kellis Kincaid, David W. MacPhee, G. Stubblefield, J. Jordon, T. Rushing, P. Allison
In this study, a finite volume simulation framework was developed, validated, and employed for the first time in a new solid-state additive manufacturing and repair process, Additive Friction Stir Deposition (AFSD). The open-source computational fluid dynamics (CFD) code OpenFOAM was used to simulate the deposition of a single layer of Aluminum Alloy 6061 feedstock onto a substrate, using a viscoplastic model to predict the flow behavior of the material. Conjugate heat transfer was considered between the build layer, the surrounding atmosphere, and the substrate, and the resulting temperatures were validated against experimental data recorded for three processing cases. Excellent agreement between simulated and measured temperature data was obtained, as well as a good qualitative prediction of overall build layer morphology. Further analysis of the temperature field was conducted to reveal the variation of temperature in the build direction, an analysis not possible with previous experimental or numerical methods, as well as a global heat transfer analysis to determine the relative importance of various modes of heat input and cooling. Tool heating was found to be the primary heat input to the system, representing 73% of energy input, while conduction to the substrate was the main mode of part cooling, representing 73% of heat loss from the build layer.
在这项研究中,开发、验证了一个有限体积模拟框架,并首次将其用于一种新的固态增材制造和修复工艺,即增材摩擦搅拌沉积(AFSD)。开源计算流体力学(CFD)代码OpenFOAM用于模拟单层铝合金6061原料在基底上的沉积,使用粘塑性模型来预测材料的流动行为。考虑了构建层、周围大气和基底之间的共轭传热,并根据三种加工情况下记录的实验数据验证了所得温度。模拟温度数据和测量温度数据之间取得了良好的一致性,并对整个构建层形态进行了良好的定性预测。对温度场进行了进一步的分析,以揭示温度在构建方向上的变化,这是以前的实验或数值方法无法进行的分析,以及全局传热分析,以确定各种热输入和冷却模式的相对重要性。工具加热被发现是系统的主要热输入,占能量输入的73%,而传导到基底是零件冷却的主要模式,占构建层热损失的73%。
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引用次数: 2
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