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A Quantitative Representation of Damage and Failure Response of 3D Textile SiC/SiC Ceramics Matrix Composites Subjected to Flexural Loading 三维纺织SiC/SiC陶瓷基复合材料在弯曲载荷作用下损伤和失效响应的定量表征
IF 1.2 4区 材料科学 Q3 ENGINEERING, MECHANICAL Pub Date : 2022-12-06 DOI: 10.1115/1.4056414
Zhengmao Yang, Keji Pang, X. Lei, Qing Hu
In the present work, the microstructure deformation and synergetic damage evolution of a three-dimensional textile SiC/SiC ceramic-matrix composites under flexural loading, has been investigated by in situ digital image correlation at ambient temperatures. With the flexural loading increases, matrix cracking occurs on the tensile side initially, and the local stress concentration leads to matrix cracking, interlayer debonding and fiber breakage on the compressive side of materials. Different from traditional 2D braided composite, when matrix fracture occurs, a matrix crack propagates in matrix enrichment regions perpendicular to fiber tows, with local deflection near the fiber/matrix interface surfaces, its propagation is diffused into sinuous fractures, and finally present a H-shaped path feature. This processes dissipate strain energy, resulting in enhancing composites fracture toughness. By using continuum damage mechanics and thermodynamic framework with synergetic effects of microstructure, asymmetric tension and compression load on both sides of the material, the flexural loading-induced damage is characterized by the reduction of the macroscopic effective elastic modulus, and a synergetic damage evolution model is established, which reveals the relationship between energy release rate and elastic modulus degradation, and can be used to predict the flexural stress-strain curves of the 3D textile SiC/SiC composites, further to improve the design and assessment of new textile architecture with specific mechanical properties.
本文采用原位数字图像相关技术,研究了三维纺织SiC/SiC陶瓷基复合材料在室温弯曲载荷作用下的微观结构变形和协同损伤演化。随着弯曲载荷的增大,拉伸侧首先发生基体开裂,局部应力集中导致材料压缩侧基体开裂、层间剥离和纤维断裂。与传统二维编织复合材料不同的是,当基体发生断裂时,基体裂纹在垂直于纤维束的基体富集区扩展,在纤维/基体界面附近发生局部挠曲,其扩展扩散成弯曲裂缝,最终呈现h型路径特征。这一过程耗散了应变能,提高了复合材料的断裂韧性。采用微观结构与材料两侧非对称拉压载荷协同作用的连续损伤力学和热力学框架,分析了材料受弯曲载荷损伤的宏观有效弹性模量降低特征,建立了材料受弯曲载荷损伤的协同演化模型,揭示了能量释放率与弹性模量退化之间的关系。并可用于预测三维纺织SiC/SiC复合材料的弯曲应力应变曲线,进一步改进具有特定力学性能的新型纺织结构的设计和评估。
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引用次数: 0
Research on Strengthening Mechanism of Rare Earth Cemented Carbide Tool Material 稀土硬质合金刀具材料的强化机理研究
IF 1.2 4区 材料科学 Q3 ENGINEERING, MECHANICAL Pub Date : 2022-11-17 DOI: 10.1115/1.4056278
Zhaopeng Hao, Yuan-gen Qiu, Yihang Fan
In this paper, the first principle method based on density functional theory is adopted to establish the interface model of WC/WC-Co through the software Materials Studio (MS). On the basis of this interface structure, rare earth element Y is doped, and then the energy of WC/WC-Co before and after doping is calculated respectively. The electronic structure is analyzed, and the calculation results of the two structures are compared. Finally, the grain growth is simulated by cellular automata of MATLAB to verify our calculation and analysis results. The results show that the interfacial adhesion work increases and the interface structure is more stable after doping Y element. The interface energy decreases and plays a role in grain refinement.
本文采用基于密度泛函理论的第一性原理方法,通过Materials Studio(MS)软件建立了WC/WC-Co的界面模型。在此界面结构的基础上,对稀土元素Y进行掺杂,分别计算了掺杂前后WC/WC-Co的能量。对电子结构进行了分析,并对两种结构的计算结果进行了比较。最后,用MATLAB的元胞自动机模拟了晶粒的生长,验证了我们的计算和分析结果。结果表明,掺杂Y元素后,界面粘附功增加,界面结构更加稳定。界面能降低,在晶粒细化中起作用。
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引用次数: 1
Influence of the Geometric Parameters on the Fiber Stresses in Unidirectional Composites Subject to Transverse Loading 几何参数对单向复合材料横向加载纤维应力的影响
IF 1.2 4区 材料科学 Q3 ENGINEERING, MECHANICAL Pub Date : 2022-11-08 DOI: 10.1115/1.4056179
Challa Geetha Krishna, Yash Anup Vora, Ishan Manoj, Tushar M. Patle, Atul Jain
When a unidirectional (UD) composite is subjected to transverse loading, different fibers are not stressed equally. In this paper, realizations of virtual random representative volume element (RVE) and experimental SEM images are translated into finite element models and the average stresses in each fiber are determined. The average stress in individual fibers is correlated with various geometric parameters like nearest neighbor distance, the angle(s) between the nearest neighbor and local fiber volume fraction. A very loose correlation with significant outliers is observed. For the matrix, the region with the highest fiber content does not necessarily lead to the highest matrix stress. The fibers with highest average stresses and the regions with highest matrix stresses are difficult to determine and cannot be simply correlated with geometric parameters.
当单向(UD)复合材料受到横向载荷时,不同的纤维不会受到同等的应力。本文将虚拟随机代表体积单元(RVE)和实验SEM图像的实现转化为有限元模型,并确定了每条纤维中的平均应力。单个纤维中的平均应力与各种几何参数相关,如最近邻距离、最近邻与局部纤维体积分数之间的角度。观察到与显著异常值之间存在非常松散的相关性。对于基体,具有最高纤维含量的区域不一定导致最高的基体应力。具有最高平均应力的纤维和具有最高基体应力的区域难以确定,并且不能简单地与几何参数相关。
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引用次数: 1
The Effect of Strain Rate on the Hydrogen Embrittlement Susceptibility of Aluminum 7075 应变速率对铝7075氢脆敏感性的影响
IF 1.2 4区 材料科学 Q3 ENGINEERING, MECHANICAL Pub Date : 2022-11-03 DOI: 10.1115/1.4056158
Mehmet Furkan Baltacioglu, B. Çetin, B. Bal
The effects of changing strain rate regime from quasi-static to medium on hydrogen susceptibility of aluminum (Al) 7075 were investigated by means of tensile tests. Strain rates were selected as 10−3 s−1 and 1 s−1 and tensile tests were conducted on both hydrogen uncharged and hydrogen charged specimens at room temperature. Electrochemical hydrogen charging method was utilized and diffusion length of hydrogen inside Al 7075 was modeled. Material characterizations were carried out by X-ray diffraction (XRD) and energy dispersive X-Ray spectroscopy (EDX) and microstructural observations of hydrogen uncharged and hydrogen charged specimens were performed by scanning electron microscope (SEM). As opposed to previous studies hydrogen embrittlement was more pronounced at high strain rate case. Moreover, hydrogen enhanced localized plasticity was the more dominant hydrogen embrittlement mechanism at slower strain rate but coexistence of hydrogen enhanced localized plasticity and hydrogen enhanced decohesion was observed at a medium strain rate. Overall, the current findings shed light on the complicated hydrogen embrittlement behavior of Al 7075 and constitute an efficient guideline for the usage of Al 7075 that can be subject to different strain rate loadings in service.
通过拉伸试验研究了准静态应变速率向介质应变速率变化对铝(Al) 7075氢敏感性的影响。应变速率分别为10−3 s−1和1 s−1,在室温下对未充氢和充氢试样进行拉伸试验。采用电化学充氢方法,建立了氢气在Al 7075内部的扩散长度模型。通过x射线衍射(XRD)和能量色散x射线能谱(EDX)对材料进行了表征,并通过扫描电镜(SEM)对未带电和带电氢样品进行了微观结构观察。与以往的研究相反,在高应变率的情况下,氢脆更为明显。在较慢应变速率下,氢增强的局部塑性是更主要的氢脆机制,而在中等应变速率下,氢增强的局部塑性和氢增强的脱黏同时存在。总的来说,目前的研究结果揭示了Al 7075复杂的氢脆行为,并为Al 7075在不同应变率载荷下的使用提供了有效的指导。
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引用次数: 3
A Unique Method to Determine Ferrite and Martensite Phase Stress Strain Curve for Manufacturing Process 一种确定制造过程中铁素体和马氏体相应力应变曲线的独特方法
IF 1.2 4区 材料科学 Q3 ENGINEERING, MECHANICAL Pub Date : 2022-10-20 DOI: 10.1115/1.4056033
Silvie M Tanu Halim, E. Ng
Finite element (FE) methods have been extensively used to simulate the effects of material's microstructure during the machining processes. However, determination of the individual microstructure phase stress strain curves is experimentally intensive and difficult to measure. Furthermore, these curves were also affected by heat treatment processes, chemical composition, and the percentage of individual microstructure phases. The objective of this paper is to develop and validate the Micromechanical Adaptive Iteration Algorithm to calculate the individual ferrite and martensite plastic behavior for dual phase (DP) steel. This method requires a minimum of three experimental stress-strain curves from the same material with three different martensite volume fractions (Vm). Two of the stress-strain curves with different Vm is required to initialize the iteration algorithm to predict the individual plastic behavior of ferrite and martensite. The third stress strain curve was used to validate the plastic behavior of individual ferrite and martensite for the given DP steel. Following on from here, the proposed algorithm was validated with two different grades of DP steel with 0.088%C and 0.1%C. Validation results shows that the approach has consistent prediction capabilities and the maximum difference observed between predicted and experimental results was 6.5%. The simulated results also shows that the degree of strain partitioning between ferrite and martensite decreases with increasing volumetric fraction of martensite (Vm).
有限元方法已被广泛用于模拟加工过程中材料微观结构的影响。然而,单个微观结构相应力-应变曲线的确定是实验密集的,并且难以测量。此外,这些曲线还受到热处理工艺、化学成分和单个微观结构相的百分比的影响。本文的目的是开发和验证微机械自适应迭代算法,以计算双相钢的单个铁素体和马氏体塑性行为。该方法需要来自具有三个不同马氏体体积分数(Vm)的相同材料的至少三个实验应力-应变曲线。需要两条具有不同Vm的应力-应变曲线来初始化迭代算法,以预测铁素体和马氏体的单独塑性行为。第三条应力-应变曲线用于验证给定DP钢的单个铁素体和马氏体的塑性行为。接下来,用0.088%C和0.1%C两种不同牌号的DP钢对该算法进行了验证。验证结果表明,该方法具有一致的预测能力,预测结果与实验结果的最大差异为6.5%马氏体体积分数(Vm)。
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引用次数: 0
Large Deflections of Functionally Graded Non-Linearly Elastic Cantilever Beams 功能梯度非线性弹性悬臂梁的大挠度
IF 1.2 4区 材料科学 Q3 ENGINEERING, MECHANICAL Pub Date : 2022-10-20 DOI: 10.1115/1.4056034
Ayhan Hacioglu, Adem Candaş, C. Baykara
Uses of functionally graded materials (FGMs) is increasing owing to recent development in manufacturing technologies. Large deflection of beams that made of nonlinearly elastic, Ludwick's type of material and also FGMs has received considerable critical attention during recent years. However, the precise effect of number of laminae on both vertical and horizontal deflection of the beam in the finite element analysis (FEA) are unknown. Here, we examined the large deflections of a cantilever beam that subjected various loading conditions and made of nonlinearly elastic, modified Ludwick's type of material using FEA. The direction dependent material properties in the functionally graded material and non-linearity from modified Ludwick law are combined in the analysis by using Marlow's material model. Our results show that gradient function and number of laminae have significant effect on stress distribution through the thickness and the both vertical and horizontal deflection of the beam.
由于制造技术的最新发展,功能梯度材料的使用正在增加。由非线性弹性、Ludwick类型的材料以及FGM制成的梁的大挠度近年来受到了相当大的关注。然而,在有限元分析(FEA)中,层压板数量对梁的垂直和水平偏转的精确影响是未知的。在这里,我们使用有限元分析研究了悬臂梁的大挠度,该悬臂梁承受各种载荷条件,由非线性弹性、改良的Ludwick型材料制成。利用Marlow材料模型,将功能梯度材料中的方向相关材料特性与修正的Ludwick定律中的非线性相结合进行分析。研究结果表明,梯度函数和层片数量对梁的应力分布以及梁的垂直和水平挠度都有显著影响。
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引用次数: 2
Effect of Vanadium on the Microstructure, Transformation Temperatures and Corrosion Behaviour of NiTi Shape Memory Alloys 钒对NiTi形状记忆合金组织、转变温度和腐蚀行为的影响
IF 1.2 4区 材料科学 Q3 ENGINEERING, MECHANICAL Pub Date : 2022-10-07 DOI: 10.1115/1.4055910
S. Sampath, Sampath Vedamanickam
Ni50Ti50-xVx (x = 0,1,2,3 at. %) shape memory alloys were prepared by vacuum induction melting. They were homogenized and then hot rolled. CHNOS and XRD analyses were carried out on the alloys to find out the oxygen and carbon contents and the phases present in the alloys. Transformation temperatures, determined by differential scanning calorimetry indicate that addition of vanadium reduces the transformation temperatures. Corrosion studies were carried out in Hanks’ solution, while potentiodynamic polarization tests were done to calculate the rate of corrosion of the alloys. Two significant parameters were analyzed from Tafel graph, namely, corrosion rate and corrosion potential. A comparison of these properties of the alloys was also made with commercially pure titanium and binary NiTi alloys. Among the NiTiV alloys, Ni50Ti47V3 (at.%) alloy was found to undergo the least rate of corrosion. With increasing vanadium content, the rate of corrosion was found to decrease. SEM analysis of the corroded surface shows that pitting was the main mechanism of corrosion in these alloys. Results show that addition of V to NiTi has a positive effect on the corrosion properties of the alloys. Elaborate results are discussed in detail in the paper.
Ni50Ti50-xVx (x = 0,1,2,3 at)采用真空感应熔炼法制备了%)形状记忆合金。它们被均质化,然后热轧。对合金进行了CHNOS和XRD分析,确定了合金中的氧、碳含量和物相。差示扫描量热法测定的相变温度表明,钒的加入降低了相变温度。在Hanks溶液中进行腐蚀研究,同时进行动电位极化试验以计算合金的腐蚀速率。从塔菲尔图中分析了腐蚀速率和腐蚀电位两个重要参数。并与工业纯钛和二元NiTi合金进行了这些性能的比较。在NiTiV合金中,Ni50Ti47V3 (at.%)合金的腐蚀速率最小。随着钒含量的增加,腐蚀速率降低。腐蚀表面的SEM分析表明,点蚀是合金腐蚀的主要机理。结果表明,在NiTi中添加V对合金的腐蚀性能有积极的影响。本文对详细的结果进行了讨论。
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引用次数: 7
Effects of Preheating on Microstructural and Mechanical Properties of Friction Stir Welded Thin Low Carbon Steel Joints 预热对低碳钢搅拌摩擦焊接接头组织和力学性能的影响
IF 1.2 4区 材料科学 Q3 ENGINEERING, MECHANICAL Pub Date : 2022-10-07 DOI: 10.1115/1.4055909
Seyed Mehrdad Yamani, S. Raja, Mohammad Ashraf Bin Ariffin, Mohammad Syahid Mohd Isa, M. Muhamad, M. F. Jamaludin, F. Yusof, Muhammad Khairi Faiz Bin Ahmad Hairuddin
Friction stir welding of a low carbon steel plate having thickness 0.5 mm was performed with preheating the base material to increase the joining performance. The rotational speed of the tool was set from 1500 to 2000 rpm with a constant travel speed of 15 mm/min and preheating temperatures of 50 to 150 °C. The tensile strength of 340 MPa was achieved for the preheated specimen compared to 310 MPa for the non-preheating specimen at the welding speed of 15 mm/min. Electron microscope images of the preheated joint revealed plasticised material flow and dynamic recrystallisation, which resulted in the grain refinement that had increased the joining strength. The weld thinning issue was almost eliminated in the preheated welded specimen. However, by increasing the preheat temperature further, the tensile strength decreases due to the formation of defects from excessive heat. The preheated sample fractured at the base metal, revealing a ductile fracture mode.
对厚度为0.5mm的低碳钢板进行搅拌摩擦焊接,同时预热基材以提高接合性能。工具的转速设定为1500至2000 rpm,恒定行进速度为15 mm/min,预热温度为50至150°C。在15毫米/分钟的焊接速度下,预热试样的拉伸强度为340兆帕,而非预热试样的抗拉强度为310兆帕。预热接头的电子显微镜图像显示了塑化材料流动和动态再结晶,这导致晶粒细化,从而提高了接头强度。预热的焊接试样几乎消除了焊缝减薄问题。然而,通过进一步提高预热温度,拉伸强度由于过热而形成缺陷而降低。预热后的样品在基底金属处断裂,显示出韧性断裂模式。
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引用次数: 0
The Mechanism of Slip System Activation with Grain Rotation During Superplastic Forming 超塑性成形过程中晶粒旋转激活滑移体系的机理
IF 1.2 4区 材料科学 Q3 ENGINEERING, MECHANICAL Pub Date : 2022-09-26 DOI: 10.1115/1.4055779
Junzhou Yang, J.J. Wu, Zhiguo Li, H. Xie, Zongcai Zhang, Mengyuan Wang
The activated slip system of Ti-6Al-4V alloy during the superplastic forming (SPF) was investigated by the in-grain misorientation axes analysis (IGMA), and the mechanisms of slip model activation have been discussed. Depending on the distribution of IGMA, one significant discovery from this study is that all the basal, prismatic, and pyramidal slip systems would be activated. Considering the effective slip models, Schmid factors, and the Euler angles together, it is suggested that the dominant slip systems not only desired the largest Schmid factors but strongly demand continuous Schmid factors among the adjacent grains. Meanwhile, the estimated critical resolved shear stress (CRSS) on basal and prismatic at the temperature of 920°C with the strain rate of 10−3/s is given. An original method of roughly estimating dominant slip models with Euler angles has been introduced, which predicts that grain rotation may change the slip model. Furthermore, Crystal Plasticity Finite Element Method (CPFEM) is employed to simulate the evolution of Euler angles, and the grain orientation presents the largest set of significant clusters around the (1 100) after deformation. Besides, the continuity of the Schmid factor assumption for the activated slip model has also been verified by CPFEM. In addition, the eigenvector corresponding to the eigenvalue λ1=1 of Euler angle rotation matrix is calculated to be aligned with the grain rotation axis, which can be applied to describe the grain rotation.
采用晶粒内取向轴差分析方法研究了Ti-6Al-4V合金超塑性成形过程中的激活滑移系统,并对滑移模型激活机制进行了探讨。根据IGMA的分布,本研究的一个重要发现是,所有的基底、棱柱和锥体滑移系统都将被激活。考虑到有效滑移模型、Schmid因子和欧拉角,认为主导滑移系统不仅需要最大的Schmid系数,而且强烈要求相邻晶粒之间的连续Schmid因素。同时,给出了应变速率为10−3/s、温度为920°C时基底和棱柱体上的临界分解剪切应力(CRSS)。介绍了一种利用欧拉角粗略估计主滑移模型的原始方法,该方法预测晶粒旋转可能会改变滑移模型。此外,采用晶体塑性有限元方法(CPFEM)模拟了欧拉角的演变,变形后的晶粒取向在(1100)附近呈现出最大的一组重要团簇。此外,CPFEM还验证了激活滑移模型Schmid因子假设的连续性。此外,计算出欧拉角旋转矩阵的特征值λ1=1对应的特征向量与晶粒旋转轴对齐,可用于描述晶粒旋转。
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引用次数: 0
Thermo-Mechanical Properties of Carbon Nanotube Yarns with High Energy Dissipation Capabilities 高耗能碳纳米管纱的热机械性能
IF 1.2 4区 材料科学 Q3 ENGINEERING, MECHANICAL Pub Date : 2022-09-08 DOI: 10.1115/1.4055540
César Pérez, Raúl Pech, Hugo Carrillo, Gabriela Uribe, Francis Aviles-Cetina
Carbon nanotube yarns (CNTYs) are porous hierarchical fibers which exhibit a strong property-structure relationship. The morphology and structure of dry-spun CNTYs are characterized and correlated with their quasi-static and dynamic mechanical properties. These characterizations include assessment of the CNTY homogeneity by means of Raman spectroscopy mapping, determination of linear density and porosity, atomic force microscopy, and dedicated measurements of the statistical distribution of the yarn's diameter. Tensile testing CNTY yields a specific strength of 0.21–0.34 N/tex, and a specific elastic modulus of 3.59–8.06 N/tex, depending on the gage length. While the strength is weakly sensitive to the gage length, the elastic modulus depends on the gage length. The importance of subtracting the machine compliance for determination of CNTY's elastic modulus is highlighted, since the error can reach up to 28%. Dynamic mechanical analysis shows that the CNTY is a stiff material with an extraordinary high damping ratio, which increases with temperature and reach ~0.6 at 60 °C. In addition, the CNTY presents a frequency-stiffening behavior in the 18–48 Hz range, with storage modulus and loss modulus which increase ~2.5 times and ~7 times, respectively, at 48 Hz.
碳纳米管纱线(CNTY)是一种多孔的分级纤维,表现出很强的性能-结构关系。表征了干纺CNTY的形态和结构,并将其与准静态和动态力学性能联系起来。这些特征包括通过拉曼光谱图谱、线密度和孔隙率的测定、原子力显微镜以及纱线直径统计分布的专门测量来评估CNTY的均匀性。拉伸测试CNTY的比强度为0.21–0.34 N/tex,比弹性模量为3.59–8.06 N/tex,具体取决于标距长度。虽然强度对标距长度敏感较弱,但弹性模量取决于标距长度。强调了减去机器顺应性对于确定CNTY弹性模量的重要性,因为误差可能高达28%。动态力学分析表明,CNTY是一种具有极高阻尼比的刚性材料,阻尼比随着温度的升高而增加,在60°C时达到~0.6。此外,CNTY在18–48 Hz范围内表现出频率硬化行为,在48 Hz时,储能模量和损耗模量分别增加了约2.5倍和约7倍。
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引用次数: 4
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