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Composite waste-based aramid aerogel separators 基于废弃物的复合芳纶气凝胶分离器
IF 3.2 4区 工程技术 Q1 MATERIALS SCIENCE, TEXTILES Pub Date : 2024-08-28 DOI: 10.1177/15280837241279985
Hale Bulbul, Meltem Yanilmaz, Juran Kim
Lithium ion batteries are one of the most promising electrochemical energy storage systems. They generally consist of four components: anode, cathode, electrolyte, and separator. The separators are crucial for batteries since they prevent physical contact of electrodes and thus short circuit. In this study, reutilization of aramid fabric was highlighted by transforming it into a high value product: battery separator. A waste aramid fabric was used to synthesize aramid aerogels by deprotonation, sol-gel, and freeze-drying processes and then investigated as lithium ion battery separators. Aramid fabric was collected from a scrap plant of an industrial automotive company. Nanoclay or TiO2 nanoparticles were added into this waste-based aramid aerogel matrix in the sol-gel stage to further enhance the performance of the separators. The samples were characterized by scanning electron microscope (SEM), linear sweep voltammetry, electrochemical impedance spectroscopy (EIS) and galvanostatic charge/discharge tests. A uniform and bead-free morphology was observed for all samples with over 60% porosity. Electrolyte uptake and ionic conductivity test results showed that addition of TiO2 nanoparticles increased electrolyte uptake and ionic conductivity up to 365% and 2.2 mS/cm, respectively. The cells prepared by using nanocomposite aramid aerogels with TiO2 exhibited excellent cycling performance with a capacity of around 160 mAh/g in 200 cycles.
锂离子电池是最有前途的电化学储能系统之一。它们通常由四个部分组成:阳极、阴极、电解质和隔膜。隔膜对电池至关重要,因为它能防止电极物理接触,从而防止短路。本研究通过将芳纶织物转化为高价值产品:电池隔膜,强调了芳纶织物的再利用。研究人员利用废弃芳纶织物,通过去质子化、溶胶-凝胶和冷冻干燥工艺合成了芳纶气凝胶,然后将其作为锂离子电池隔膜进行了研究。芳纶织物是从一家工业汽车公司的废料厂收集的。在溶胶-凝胶阶段,将纳米粘土或二氧化钛纳米颗粒添加到这种基于废料的芳纶气凝胶基质中,以进一步提高分离器的性能。样品通过扫描电子显微镜(SEM)、线性扫描伏安法、电化学阻抗谱(EIS)和电静态充放电测试进行了表征。所有样品都呈现出均匀无珠的形态,孔隙率超过 60%。电解质吸收和离子传导测试结果表明,加入 TiO2 纳米粒子后,电解质吸收和离子传导率分别提高了 365% 和 2.2 mS/cm。使用添加了 TiO2 的纳米复合芳纶气凝胶制备的电池具有优异的循环性能,在 200 次循环中的容量约为 160 mAh/g。
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引用次数: 0
Easily scalable and highly flexible machine knitted resistive pressure sensor for smart textile applications 用于智能纺织品应用的易于扩展且高度灵活的机织电阻式压力传感器
IF 3.2 4区 工程技术 Q1 MATERIALS SCIENCE, TEXTILES Pub Date : 2024-08-28 DOI: 10.1177/15280837241279454
Md. Mohaddesh Hosen, Ahmadul Ferdous, Safi Ahmed
This study presents textile based resistive pressure sensor that incorporates off-the-shelf PES/stainless steel conductive yarn and nonconductive acrylic yarn. The fabrication process involves integrating the resistive pressure sensors directly into the base fabric during one knitting operation through computerized machine knitting technology with little human involvement. This work also explores opportunities for manufacturing of soft, highly flexible, and easily controllable double-layered out-of-plane sensors in an easily scalable way. A custom resistance measuring circuit was built to characterize the sensors and the resulting equivalent resistance under various loads, i.e., (0 g–900 g). Reproducibility was confirmed by developing and testing several sensors with the same structural characteristics. The results obtained from the experiments showed that the conductive yarn types and the design parameters significantly affect the sensing properties of knitted sensors. It has been found that sensor types 2, 5, and 6 show better stability, repeatability, high response and recovery time, dynamic ranges, and sensitivity when subjected to various loadings, compared to other developed sensors in this work. As a proof of concept, this sensor demonstrates various smart textile applications, including interactive sleeves for wearable user interface, soft controllable switch, and human movement detection.
本研究介绍了基于纺织品的电阻式压力传感器,它采用了现成的聚醚砜/不锈钢导电纱线和不导电的丙烯酸纱线。制造过程包括通过计算机化机器编织技术,在一次编织操作中将电阻式压力传感器直接集成到基布中,几乎不需要人工参与。这项工作还探索了以易于扩展的方式制造柔软、高度灵活和易于控制的双层平面外传感器的机会。我们建立了一个定制电阻测量电路,以确定传感器的特性以及在各种负载(0 克-900 克)下产生的等效电阻。通过开发和测试具有相同结构特征的多个传感器,确认了可重复性。实验结果表明,导电纱线类型和设计参数对针织传感器的传感性能有很大影响。研究发现,与本研究中开发的其他传感器相比,2、5 和 6 型传感器在承受各种负载时具有更好的稳定性、可重复性、高响应和恢复时间、动态范围和灵敏度。作为概念验证,该传感器展示了各种智能纺织品应用,包括用于可穿戴用户界面的交互式袖套、软可控开关和人体运动检测。
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引用次数: 0
Development of flexible packaging sheet from aluminium foil laminated jute web 利用铝箔复合黄麻网开发柔性包装板材
IF 3.2 4区 工程技术 Q1 MATERIALS SCIENCE, TEXTILES Pub Date : 2024-08-28 DOI: 10.1177/15280837231214741
Surajit Sengupta, Nilimesh Mirdha, Papai Ghosh, Izhar Mustafa
This study develops an impermeable and flexible sheet for food packaging using aluminium foil and jute web. A hot melt sheet is used for laminating foil with a jute web. A simple manufacturing process has been suggested. The effect of different process parameters has been studied and optimized. The optimized calendaring temperature (top/bottom), pressure, and speed are 150/120°C, 15 kPa, and 1 m/min, respectively. Preheating and three consecutive runs show higher tenacity. This hybrid sheet uses around 88% or 78% jute (by weight) in one and both side laminated sheets, respectively. The failure mechanism shows the role of fibre-to-foil bonding. The developed fabric is lighter and more cost-effective than jute woven laminated fabric. The packet from hybrid fabric is sufficiently strong and pliable with excellent barrier properties to use as a hygienic sheet for food packaging.
这项研究利用铝箔和黄麻网开发了一种用于食品包装的防渗柔性薄片。在铝箔与黄麻网的复合过程中使用了热熔片。研究提出了一种简单的制造工艺。对不同工艺参数的影响进行了研究和优化。优化后的压延温度(顶部/底部)、压力和速度分别为 150/120°C、15 千帕和 1 米/分钟。预热和连续三次运行显示出更高的韧性。这种混合板在单面和双面层压板中分别使用了约 88% 或 78% 的黄麻(按重量计)。失效机理显示了纤维与箔之间的粘合作用。与黄麻编织层压织物相比,所开发的织物更轻、更具成本效益。混合织物制成的包装具有足够的强度和柔韧性,并具有出色的阻隔性能,可用作食品包装的卫生片材。
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引用次数: 0
Optimization and experimental validation of reinforcing fibers winding pattern for carbon/carbon composite crucible preform 碳/碳复合材料坩埚瓶坯增强纤维缠绕模式的优化与实验验证
IF 3.2 4区 工程技术 Q1 MATERIALS SCIENCE, TEXTILES Pub Date : 2024-08-28 DOI: 10.1177/15280837241277748
Jiuzhi Dong, Jiafei Zhao, Rui Li, Xiuming Jiang
In order to address the problem of transition slip between the cylindrical segment and the ellipsoidal head segment of the carbon/carbon composite crucible preform with asymmetrical structure during the winding process, a winding pattern combining geodesic and non-geodesic is presented innovatively. Firstly, the formulae for the winding angle and the winding central rotation angle of the crucible cylindrical segment and the ellipsoidal head segment are established, and the fourth-order Runge-Kutta numerical method is employed for parametrical design. The two-tangent point winding path is determined by analyzing the effect of the cylindrical segment’s winding pitch, different ellipsoidal head segment heights, and slip coefficient on the winding angle. Secondly, the needle disk winding method is proposed to address the slight winding angle at the open end of the cylinder, making it easier to hang the yarn. Finally, the experiment on dry yarn winding of 3k carbon fiber (linear density: 198 g/km) is carried out. The results indicate that the relative error rate between the actual winding angle and the theoretical design angle differs by no more than 1.66%, demonstrating that carbon fibers can be stably and uniformly wound onto the surface of the carbon/carbon composite crucible preform. Compared to the traditional manual winding method, the winding pattern enhances winding efficiency, ensures carbon fibers’ uniformity and structural stability, and provides a new technological approach to producing high-performance composite materials.
针对非对称结构碳/碳复合材料坩埚预型件在缠绕过程中圆柱段和椭圆头段之间的过渡滑移问题,创新性地提出了一种大地线与非大地线相结合的缠绕模式。首先,建立了坩埚圆柱段和椭圆头段的缠绕角和缠绕中心旋转角公式,并采用四阶 Runge-Kutta 数值方法进行参数设计。通过分析圆柱段缠绕节距、不同椭圆头段高度和滑移系数对缠绕角的影响,确定了两切点缠绕路径。其次,针对筒子开口端卷绕角度较小的问题,提出了针盘卷绕法,便于挂纱。最后,对 3k 碳纤维(线密度:198 g/km)进行了干纱卷绕实验。结果表明,实际卷绕角度与理论设计角度之间的相对误差率不超过 1.66%,表明碳纤维可以稳定、均匀地卷绕到碳/碳复合材料坩埚预型件的表面。与传统的手工缠绕方法相比,该缠绕模式提高了缠绕效率,确保了碳纤维的均匀性和结构稳定性,为生产高性能复合材料提供了新的技术途径。
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引用次数: 0
Mechanical and fatigue behavior of the three-section artificial ligament 三节人工韧带的机械和疲劳行为
IF 3.2 4区 工程技术 Q1 MATERIALS SCIENCE, TEXTILES Pub Date : 2024-08-23 DOI: 10.1177/15280837241280402
Jiaqi Huang, Mengru Wu, Qinwen Huang, Tong Yang, Gang Zhao, Pibo Ma
Artificial ligaments transplanted into the human body are subject to ligament rupture and ligament fatigue injury during exercise. The three-section structure of artificial ligaments has a tight structure which can improve the breaking strength at the two ends, and a looser structure which can keep the flexibility in the middle. At present, scholars have studied braided artificial ligaments with high elasticity and creep resistance, and three-section artificial ligaments have other advantages on this basis. In this study, the three-section artificial ligaments were braided with UHMWPE, and a core-shell structure was used at both ends of the ligament as a way to strengthen the tightness and strength, facilitate the fixation of the ligament, and improve the fatigue resistance of artificial ligaments. In addition, the mechanical properties of artificial ligaments were investigated with different numbers of cores. This study proved that the three-section artificial ligament, which is made of UHMWPE has high strength, excellent elastic recovery rate, and fatigue resistance, which can provide mechanical support for the daily activities of the knee joint and help maintain the stability of the knee joint.
移植到人体的人工韧带在运动过程中会出现韧带断裂和韧带疲劳损伤。人工韧带的三段式结构两端紧密,可提高断裂强度,中间松散,可保持弹性。目前,学者们研究的编织人工韧带具有高弹性和抗蠕变性,三节人工韧带在此基础上还具有其他优点。本研究采用超高分子量聚乙烯编织三节人工韧带,并在韧带两端采用核壳结构,以此增强韧带的紧密性和强度,便于韧带的固定,提高人工韧带的抗疲劳性。此外,还研究了不同芯数人工韧带的力学性能。该研究证明,由超高分子量聚乙烯制成的三节人工韧带具有较高的强度、出色的弹性恢复率和抗疲劳性,可为膝关节的日常活动提供机械支撑,并有助于保持膝关节的稳定性。
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引用次数: 0
Preparation and properties of thermal insulation felts for firefighting protective clothing 消防防护服隔热毡的制备和特性
IF 3.2 4区 工程技术 Q1 MATERIALS SCIENCE, TEXTILES Pub Date : 2024-08-23 DOI: 10.1177/15280837241276917
Zhenrong Zheng, Lingli Ren, Hongyang Wang
In this paper, preoxidized fibers, flame-retardant acrylic fibers and polyphenylene sulfide (PPS) fibers were chosen to prepare thermal insulation felts by the spunlaced process. The preparation of thermal insulation felts by single-component fibers, bicomponent fibers and multi-component fibers was studied. The breaking strength of the single fibers, flame retardancy, thermal conductivity, air permeability, thermal stability, shrinkage rate after washing, and the breaking strength of the thermal insulation felts were characterized. The results show that, for the single-component felts, preoxidized fiber felt had a longitudinal char length of only 35 mm, which was less than that of flame-retardant acrylic fiber felts and PPS felts. However, its longitudinal breaking strength was only 39.8 N. The bicomponent thermal insulation felt, blended with flame-retardant acrylic fibers and preoxidized fibers, had a higher breaking strength than the single-component felt, but it had char lengths greater than 100 mm after the vertical burning test. When the ratio of the multi-component insulation felts (preoxidized fibers, PPS fibers and flame-retardant acrylic fibers) was 35:60:5, the felt’s longitudinal char length measured 23 mm, which was less than that of the aramid felt 72 mm. This felt’s thermal conductivity was 0.0515 W/mK. It had an air permeability of 1995 mm/s, and the longitudinal dimensional shrinkage rate following the thermal stability test was only 1.1%. Multi-component thermal insulation felts are very important for the development of high-performance firefighting protective clothing.
本文选择了预氧化纤维、阻燃腈纶纤维和聚苯硫醚(PPS)纤维,通过纺粘法制备隔热毡。研究了单组分纤维、双组分纤维和多组分纤维制备隔热毡的情况。对单组分纤维的断裂强度、阻燃性、导热性、透气性、热稳定性、洗涤后收缩率以及隔热毡的断裂强度进行了表征。结果表明,就单组分毡而言,预氧化纤维毡的纵向炭化长度仅为 35 毫米,小于阻燃丙烯酸纤维毡和聚苯硫醚毡。由阻燃腈纶纤维和预氧化纤维混合而成的双组分隔热毡的断裂强度高于单组分隔热毡,但在垂直燃烧试验后,其纵向炭化长度大于 100 毫米。当多组分绝缘毡(预氧化纤维、PPS 纤维和阻燃腈纶纤维)的比例为 35:60:5 时,毡的纵向炭化长度为 23 毫米,小于芳纶毡的 72 毫米。这种毡的导热系数为 0.0515 W/mK。它的透气性为 1995 毫米/秒,热稳定性测试后的纵向尺寸收缩率仅为 1.1%。多组分隔热毡对于开发高性能消防防护服非常重要。
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引用次数: 0
Optimization of tire-ground performance through meshed belt layer structure 通过网格带层结构优化轮胎-地面性能
IF 3.2 4区 工程技术 Q1 MATERIALS SCIENCE, TEXTILES Pub Date : 2024-08-14 DOI: 10.1177/15280837241275137
Rui Mao, Pengfei Sun, Shuiting Zhou, Luwen Chen, Junling Meng, Wenqi Yang, Chenyi Yang, Kejie Luo
Using Abaqus finite element software, this study investigates the impact of different carcass belt layer structures on the grounding characteristics of tires. Focusing on the 215/55R17 radial tire, the research proposes a structural optimization scheme and establish a finite element model. The standard tire belt layer structure is replaced with a mesh belt layer structure to achieve optimized performance. Through static loading tests on the tire, the accuracy of the finite element model was validated. By altering the density, number of layers of the mesh belt structure, and radial load of the tire, a simulation analysis is conducted to study the impact on tire deformation and stress on the carcass material. The optimized tire features increased radial stiffness and reduced tread wear. The density of the mesh belt layer in the contact area affects tire deformation as well as the stress on the belt layer and ply layer. The results indicate that the mesh belt layer can effectively absorb the radial load of the tire, optimizing tire deformation by 20% to 30%. Under different loads, the tire with a 70-density mesh belt layer can reduce surface stress by approximately 40%, or around 230J. The mesh belt layer tire can reduce the sensitivity of the tire center to high load stresses, optimizing 25% of the concentrated stress at the shoulder position of the ply layer. When a double-layer belt is used, the strength at the shoulder increases with the number of belt layers, reducing stress by approximately 2-4N. The structural form of the belt layer has little impact on the trend of stored strain energy changes, but the number of belt layers significantly affects the amount of change in the tire’s strain energy. On average, about 10% of the stored strain energy is reduced due to changes in the belt layer structure.
本研究使用 Abaqus 有限元软件研究了不同胎体带束层结构对轮胎接地特性的影响。研究以 215/55R17 子午线轮胎为重点,提出了结构优化方案并建立了有限元模型。用网状带层结构取代标准轮胎带层结构,实现性能优化。通过对轮胎进行静态加载试验,验证了有限元模型的准确性。通过改变网格带结构的密度、层数和轮胎的径向载荷,进行了模拟分析,以研究轮胎变形和胎体材料应力的影响。优化后的轮胎增加了径向刚度,减少了胎面磨损。接触区网状带束层的密度会影响轮胎变形以及带束层和帘布层的应力。结果表明,网状带束层可以有效吸收轮胎的径向载荷,使轮胎变形优化 20% 至 30%。在不同载荷下,采用 70 密度网状带束层的轮胎可减少约 40% 的表面应力,约为 230J。网状带束层轮胎可降低轮胎中心对高负荷应力的敏感性,优化帘布层肩部位置 25% 的集中应力。当使用双层带束层时,肩部的强度会随着带束层数的增加而增加,可减少约 2-4N 的应力。带束层的结构形式对储存应变能的变化趋势影响不大,但带束层的数量对轮胎应变能的变化量影响很大。由于带束层结构的变化,平均约有 10% 的存储应变能被降低。
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引用次数: 0
Studying the influence of micro-particles on the mechanical performance and damage failures of composite laminates 研究微颗粒对复合材料层压板机械性能和损坏失效的影响
IF 3.2 4区 工程技术 Q1 MATERIALS SCIENCE, TEXTILES Pub Date : 2024-08-09 DOI: 10.1177/15280837241275018
Hussein Kommur Dalfi, Amer Alomarah, Anwer Al-Obaidi
Composite materials are increasingly used in a broad range of applications due to their recognizable mechanical properties and the high strength-to-weight ratio. The aim of the current study is to improve the mechanical properties and fracture toughness of composite laminates. Several types of fabrics, such as glass, carbon, and Kevlar, and micro-particles are adopted to create composite laminates via the vacuum infusion method. The mechanical performances of the proposed laminates were evaluated via tensile and flexural strength tests. Moreover, the impact strength tests were conducted to examine their dynamic performances. Results showed that woven laminates such as glass woven, carbon woven, and Kevlar woven composites with micro-particles revealed better tensile properties compared with those without micro-particles. For instance, enhancement in the Young’s modulus with around 5%, 6%, and 13% were resulted from the glass, carbon, and Kevlar fabrics with fillers, respectively. Furthermore, higher impact strength and fracture toughness were obtained from the laminates of glass, carbon and Kevlar with inclusion of thermoplastic particles. For example, the glass, carbon and Kevlar fabrics composites with fillers samples showed improvement in the fracture toughness with around 24%, 17% and 14%, respectively. In addition, numerical simulation findings of flexural failure load and damage failure modes were in accordance with experimental results both qualitatively and quantitatively.
由于复合材料具有公认的机械性能和高强度重量比,因此其应用越来越广泛。本研究旨在提高复合材料层压板的机械性能和断裂韧性。研究采用了多种类型的织物,如玻璃纤维、碳纤维、凯夫拉纤维和微颗粒,通过真空灌注法制造复合材料层压板。通过拉伸和弯曲强度测试,对所提出的层压板的机械性能进行了评估。此外,还进行了冲击强度测试,以检验其动态性能。结果表明,与不含微颗粒的复合材料相比,含有微颗粒的编织层压材料(如玻璃编织、碳编织和凯夫拉编织复合材料)具有更好的拉伸性能。例如,含有填料的玻璃、碳和凯夫拉纤维织物的杨氏模量分别提高了约 5%、6% 和 13%。此外,加入热塑性颗粒的玻璃、碳和凯夫拉纤维层压板也获得了更高的冲击强度和断裂韧性。例如,含有填料的玻璃、碳和凯夫拉纤维复合材料样品的断裂韧性分别提高了约 24%、17% 和 14%。此外,挠曲破坏载荷和破坏失效模式的数值模拟结果在定性和定量方面都与实验结果一致。
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引用次数: 0
Compression behavior of warp-knitted spacer fabric based on simplified finite element method 基于简化有限元法的经编间隔织物压缩行为
IF 3.2 4区 工程技术 Q1 MATERIALS SCIENCE, TEXTILES Pub Date : 2024-08-02 DOI: 10.1177/15280837241267775
Wenxiang Song, Xiaotao Ma, Pibo Ma
Warp-knitted spacer fabrics (WKSF), with their unique structure and excellent energy absorption properties, are widely utilized in the automotive industry, medical field, and aerospace sectors. However, during practical applications, WKSF undergo repeated compression, which can lead to compressive fatigue of the spacer yarns and consequently cause the WKSF to undergo irreversible deformation, which subsequently affects its performance and appearance. Therefore, to enhance the compressive properties of WKSF and investigate the mechanisms of plastic failure, this study used a warp knitting double needle bar raschel machine to fabricate a WKSF with a thickness of 20 mm. Through fabric structure analysis, we developed a unit cell model consisting of 32 fibers and a more comprehensive analysis model with 320 fibers to quantitatively assess the geometric changes of the WKSF during the compression process. Furthermore, we experimentally studied the performance changes of the WKSF under different compression speeds, various compression strains, and 1000 cycles of loading. By integrating experimental test with the finite element method, we have conducted an in-depth study of the compression process of WKSF, simulating the displacement U, Von Mises stress distribution, and plastic compression failure behavior during compression. By comparing data on Von Mises stress, equivalent plastic strain (PEEQ), and energy density distribution (SENER), we can clearly observe the performance of spacer yarns under compression conditions, providing significant insights into the underlying plastic failure mechanisms of WKSF’s. This study not only enriches the theoretical framework for WKSF compression but also lays a solid foundation for improving its performance and extending its applications.
经编间隔织物(WKSF)具有独特的结构和优异的能量吸收性能,被广泛应用于汽车工业、医疗领域和航空航天领域。然而,在实际应用过程中,WKSF 会受到反复压缩,这可能会导致间隔纱产生压缩疲劳,进而导致 WKSF 发生不可逆变形,进而影响其性能和外观。因此,为了提高 WKSF 的抗压性能并研究塑性破坏的机理,本研究使用经编双针棒拉舍尔机制造了厚度为 20 毫米的 WKSF。通过织物结构分析,我们建立了一个由 32 根纤维组成的单元格模型和一个由 320 根纤维组成的更全面的分析模型,以定量评估 WKSF 在压缩过程中的几何变化。此外,我们还通过实验研究了 WKSF 在不同压缩速度、不同压缩应变和 1000 次循环加载下的性能变化。通过将实验测试与有限元方法相结合,我们对 WKSF 的压缩过程进行了深入研究,模拟了压缩过程中的位移 U、Von Mises 应力分布和塑性压缩破坏行为。通过比较 Von Mises 应力、等效塑性应变 (PEEQ) 和能量密度分布 (SENER) 等数据,我们可以清楚地观察到间隔纱在压缩条件下的性能,从而对 WKSF 的塑性破坏机制提供了重要的启示。这项研究不仅丰富了 WKSF 压缩的理论框架,还为改善其性能和扩大其应用范围奠定了坚实的基础。
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引用次数: 0
Enhancement of mechanical and thermal properties of carbon fiber phenolic resin composites using silicon carbide filler for thermal protection system applications 使用碳化硅填料提高热保护系统应用中碳纤维酚醛树脂复合材料的机械和热性能
IF 3.2 4区 工程技术 Q1 MATERIALS SCIENCE, TEXTILES Pub Date : 2024-08-02 DOI: 10.1177/15280837241263312
Praveen Kumar Basingala, Venkata Swamy Naidu Neigapula
Thermal protection systems (TPS) are vital for re-entry vehicles for their safe passage into the atmosphere from space. Hence, researchers took a keen interest in improving the thermal and ablative properties of composites to be used in making thermal protection systems. Therefore, an attempt was made to improve the thermal and ablative properties of composites made of carbon fibers (Cf) and resorcinol formaldehyde phenolic (Ph) resin with the incorporation of silicon carbide (SiC) particles. The filler was added in various percentages (0 wt% - blank, 1 wt%, 3 wt%, and 5 wt%), and the composites were tested for ablative, thermal and mechanical properties. The results demonstrate that the SiC-modified PAN-based carbon fiber reinforced phenolic (SiC-PANCf-Ph) composite with 3 wt% SiC enhancement exhibited ideal properties. The post-ablation phase composition and microstructure were examined through X-ray diffraction (XRD), Scanning electron microscopy (SEM), and energy-dispersive X-ray spectroscopy (EDS). The surface morphology evidences the formation of a silicon dioxide (SiO2) layer on the composites. The SiC-PANCf-Ph composites demonstrated the lowest ablation rate, enhancing their potentiality for effective TPS applications.
热保护系统(TPS)对于重返大气层飞行器从太空安全进入大气层至关重要。因此,研究人员对改善用于制造热保护系统的复合材料的热性能和烧蚀性能产生了浓厚的兴趣。因此,研究人员尝试在碳纤维(Cf)和间苯二酚甲醛酚醛树脂(Ph)制成的复合材料中加入碳化硅(SiC)颗粒,以改善复合材料的热性能和烧蚀性能。填料的添加比例各不相同(0 wt% - 空白、1 wt%、3 wt% 和 5 wt%),并对复合材料进行了烧蚀、热和机械性能测试。结果表明,SiC 增强 3 wt% 的 SiC 改性 PAN 基碳纤维增强酚醛(SiC-PANCf-Ph)复合材料具有理想的性能。通过 X 射线衍射(XRD)、扫描电子显微镜(SEM)和能量色散 X 射线光谱(EDS)检测了烧结后的相组成和微观结构。表面形貌证明复合材料上形成了二氧化硅(SiO2)层。SiC-PANCf-Ph 复合材料的烧蚀率最低,增强了其有效应用于 TPS 的潜力。
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引用次数: 0
期刊
Journal of Industrial Textiles
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