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Study on the performance and aging low temperature performance of GO / SBS modified asphalt GO / SBS改性沥青的性能及老化低温性能研究
Pub Date : 2023-09-08 DOI: 10.1590/1517-7076-rmat-2023-0151
Zhenlong Mo
Graphene oxide (GO) has attracted more and more attention in asphalt pavement due to its excellent performance. However, most current research is limited to GO modified base asphalt, and the modification effect is insignificant. In this paper, GO / SBS-modified asphalt was prepared by high-speed shearing. The effects of GO on the physical properties, storage stability, low-temperature performance, and aging resistance of SBS-modified asphalt were studied. A low-temperature beam bending test analyzed the low-temperature performance of GO / SBS composite modified asphalt mixture before and after aging. The results show that adding GO improves SBS-modified asphalt’s high-temperature performance, aging resistance, and storage stability. When the con - tent of GO is 0.75%, the physical properties of modified asphalt are the best. The low-temperature rheological properties of modified asphalt with GO before aging are slightly lower than those of SBS-modified asphalt. However, adding GO improves the low-temperature rheological properties of GO/SBS modified asphalt after aging. GO-modified asphalt slightly improves the low-temperature toughness of the mixture under non-aging and short-term aging. However, it still makes the mixture maintain good low-temperature performance under long-term aging. GO / SBS modified asphalt mixture has excellent low-temperature crack resistance before and after aging, and GO / SBS composite modified asphalt can effectively alleviate the damaging effect of aging on the low-temperature crack resistance of asphalt mixture and prolong the service life of the pavement.
氧化石墨烯(GO)以其优异的性能在沥青路面中受到越来越多的关注。但目前的研究大多局限于GO改性基础沥青,改性效果不显著。本文采用高速剪切法制备GO / sbs改性沥青。研究了氧化石墨烯对sbs改性沥青物理性能、贮存稳定性、低温性能和耐老化性能的影响。通过低温梁弯试验,分析了GO / SBS复合改性沥青混合料老化前后的低温性能。结果表明,氧化石墨烯的加入提高了sbs改性沥青的高温性能、耐老化性能和贮存稳定性。当氧化石墨烯含量为0.75%时,改性沥青的物理性能最好。氧化石墨烯改性沥青老化前的低温流变性能略低于sbs改性沥青。而氧化石墨烯的加入改善了氧化石墨烯/SBS改性沥青老化后的低温流变性能。氧化石墨烯改性沥青在非老化和短期老化条件下,能略微提高混合料的低温韧性。但在长期时效下仍能使混合料保持良好的低温性能。GO / SBS改性沥青混合料在老化前后均具有优异的低温抗裂性能,GO / SBS复合改性沥青可有效缓解老化对沥青混合料低温抗裂性能的破坏作用,延长路面使用寿命。
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引用次数: 1
Rheological properties and engineering application of low-grade asphalt mixture 低标号沥青混合料的流变特性及工程应用
Pub Date : 2023-09-08 DOI: 10.1590/1517-7076-rmat-2023-0208
Lianguo Song, Pengcheng Tu, Xiao-lu Xie, Jingjing Fan, Lulu Hou, Jie Gao
This study investigates the feasibility of low-grade hard asphalt in high-temperature regions. We conducted an analysis of the high-temperature rheological properties of asphalt before and after short-term and long-term aging using the dynamic shear rheological (DSR) test and multi-stress creep recovery (MSCR) test. Additionally, the road performance of the asphalt mixture was studied by rutting test and low temperature beam bending test. The results indicate that the 30# asphalt demonstrates superior anti-rutting performance compared to the 50# asphalt. Furthermore, the rutting factor and fatigue factor of the 30# asphalt during aging are significantly higher than those of the 50# asphalt. With increasing temperature, stress level, and stress action time, the strain of the asphalt gradually increases. The unrecoverable creep compliance of the 50# asphalt exceeds that of the 30#. Although the high-temperature performance of the 30# asphalt mixture outperforms that of the 50# asphalt mixture, it exhibits lower flexural tensile strength and deformation ability at low temperatures compared to the 50# asphalt mixture. Overall, low-grade asphalt demonstrates relatively stable stress variations and exhibits good high-temperature stability.
本研究探讨了高温地区低标号硬沥青的可行性。采用动态剪切流变学(DSR)试验和多应力蠕变恢复(MSCR)试验对沥青在短期和长期老化前后的高温流变特性进行了分析。另外,通过车辙试验和低温梁弯试验对沥青混合料的路用性能进行了研究。结果表明:30#沥青的抗车辙性能优于50#沥青;此外,30#沥青在老化过程中的车辙系数和疲劳系数显著高于50#沥青。随着温度、应力水平和应力作用时间的增加,沥青的应变逐渐增大。50#沥青的不可恢复蠕变柔度大于30#沥青。虽然30#沥青混合料的高温性能优于50#沥青混合料,但与50#沥青混合料相比,30#沥青混合料的低温弯曲抗拉强度和变形能力较低。总体而言,低等级沥青表现出相对稳定的应力变化,并表现出良好的高温稳定性。
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引用次数: 0
Statistical optimization of fibre reinforced polymer concrete made with recycled plastic aggregates by central composite design 基于中心复合设计的再生塑料骨料纤维增强聚合物混凝土的统计优化
Pub Date : 2023-09-04 DOI: 10.1590/1517-7076-rmat-2023-0182
Ravisankar Venugopal, N. Muthusamy, Balasundaram Natarajan, Venkatesan Govindan
To meet the present needs of concrete consumption, it is the need of the hour to discover different alterna - tives and unique techniques. By Incorporating the latest trends, Polymer Concrete (PC) and Fibre-Reinforced Concrete (FRC) are being used to improve the strength of concrete. It is proposed to produce M30 grade Fibre Reinforced Polymer Concrete (FRPC) with the help of Polyester Resins (PR), Polypropylene Fibres (PF) and Recycled Waste Plastics (RWPA). FRPC is a combination of three different variables of different replacement percentages, which requires extensive and detailed experimentation to optimize each variable used in this investigation. In this study (research), optimization was done by keeping the two variables constant. To reduce the number of experiments, optimization of ingredients was done by statistical modelling technique of Central Composite Design (CCD). In conclusion, the optimal input parameters for achieving a 28-day CS are determined to be 12.05% PR, 2.19% PF, and 30% RWPA. These findings are based on the analysis of experimental results, statistical modelling, and the CCD approach, demonstrating the successful optimization and correlation between the input parameters and the desired CS output.
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引用次数: 0
A study on the refractive index of sol-gel Ba1-xGdxTiO3 thin films using spectroscopic ellipsometry 溶胶-凝胶Ba1-xGdxTiO3薄膜折射率的椭偏光谱研究
Pub Date : 2023-09-04 DOI: 10.1590/1517-7076-rmat-2023-0176
Ala’eddin A. Saif, Yen Chin Teh, Prabakaran Poopalan
Ba 1-x Gd x TiO 3 thin films have been fabricated at different Gd 3+ ionic concentrations, film thicknesses, and anneal - ing temperatures using the sol-gel method. The refractive index of the Ba 1-x Gd x TiO 3 films on a silicon substrate is characterized using Spectroscopic Ellipsometry (SE), where the ellipsometry angles Ψ and Δ are fitted very well with the Cauchy dispersion model. The results show that the refractive index at 632.8 nm decreases from 2.18 to 1.892 with the increase of the Gd 3+ ratio, while it increases with film thickness and annealing tempera - ture. This trend for refractive index variation is explained based on interatomic spacing and density densification of the films. Using Wemple–Di Domenico (WDD) model shows that the dispersion energy increases with film thickness and annealing temperature and decreases with Gd 3+ doping. The relatively high refractive index of the samples supports the possibility of using Ba 1-x Gd x TiO 3 thin films as AR coating for solar cells.
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引用次数: 0
Influence of presaturated coconut fibre ash pellets in concrete 预饱和椰子纤维灰粒对混凝土性能的影响
Pub Date : 2023-09-04 DOI: 10.1590/1517-7076-rmat-2023-0190
Gopi Rajamanickam, Saravanakumar Ramasamy, Elango Krishnan Soundararajan, Kathiresan Karuppanan, Chandrasekar Arumugam
River sand is becoming increasingly scarce. As a result, an alternative material is required to replace river sand in order to save river sand. In the construction of quality concrete, artificial aggregate is now frequently employed as a substitute for river sand. Coconut fibre ash (CFA) aggregate obtained from Coconut fibre is prev - alent in India. Partially replacing river sand (fine aggregate) with presaturated CFA aggregate for self curing purpose is presented in the paper. Fine aggregates were replaced by CFA aggregate by 5%, 10%, 15%, 20% and 25% by volume. The workability and strength characteristics of the concrete are studied. Internal curing is the solution to today's water scarcity's insufficient curing. During compared to other mixtures, test results show that the concrete mix with 20% CFA aggregate produced better results when self curing.
河沙越来越少了。因此,为了节约河砂,需要一种替代材料来代替河砂。在高质量混凝土的施工中,人工骨料现在经常被用作河砂的替代品。从椰子纤维中提取的椰子纤维灰分(CFA)骨料在印度很普遍。本文提出用预饱和CFA骨料部分替代河砂(细骨料)自养护。细骨料用CFA骨料代替,体积比分别为5%、10%、15%、20%和25%。研究了混凝土的和易性和强度特性。内部养护是当今水资源短缺的解决方案,养护不足。试验结果表明,掺加20% CFA骨料的混凝土自养护效果较好。
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引用次数: 0
Effects of Nb and V microalloying on the thermoplasticity of new martensitic low-density steels Nb和V微合金化对新型马氏体低密度钢热塑性的影响
Pub Date : 2023-09-04 DOI: 10.1590/1517-7076-rmat-2023-0214
Ce Sun, Xiaoqing Li, Fanghui Guo, Junru Li, Lianjun Cheng, P. Zhang
By performing tensile tests in the temperature range of 800°C to 1200°C, the thermoplastic behavior of microal-loyed and unmicroalloyed new martensitic low-density steels were investigated, and the mechanism of the effect of Nb and V microalloying on the thermoplasticity was revealed. The results showed that both microalloyed and unmicroalloyed steels have good thermoplasticity and the plasticity increased with increasing deformation temperature. The microalloyed steels above 1000°C could have their high-temperature plasticity significantly enhanced by Nb, V microalloying, while the microalloyed steels at or below 1000°C could have their plasticity reduced. When the deformation temperature exceeds 1000°C, complete recrystallization occurs in both microal-loyed and unmicroalloyed steels. The Nb, V microalloys were able to refine the recrystallized grains, which could obtain a stronger resistance to crack expansion and give the microalloyed steels better high-temperature plasticity. When the deformation temperature at or below 1000°C, the unmicroalloyed steel exhibited significant recrystallization. The presence of numerous small-sized NbC precipitation phases, abundant in the microal-loyed steel, hindered the recrystallization. This made dynamic recrystallization of microalloyed steels almost non-existent when deformation occurred at lower temperatures, which lead to lower plasticity compared to the unmicroalloyed steel.
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引用次数: 0
Análise estatística da influência dos parâmetros de processamento na planicidade de placas de zircônia estabilizada com 8%mol de ítrio obtidas por colagem de fita 统计分析了工艺参数对8%mol钇稳定氧化锆板平整度的影响
Pub Date : 2023-09-01 DOI: 10.1590/1517-7076-rmat-2023-0106
Augusto Prata Sigeiro, R. Marcomini
RESUMO No presente estudo, lotes de placas de zircônia estabilizada com 8% mol de ítrio (TZ8Y) foram fabricados pela técnica de colagem de fita, variando entre eles a composição da suspensão, como o volume de sólidos e os teores de ligantes, de plastificante do tipo I e de plastificante do tipo II com o intuito de verificar a influência destes parâmetros e do comportamento tixotrópico da suspensão sobre o empenamento do produto final. Após sinterizadas, a topografia das placas foi mapeada por meio de um relógio comparador, tomando medidas sobre a superficia das placas em um sistema de coordenadas, e, a partir desse sistema, foi definido um índice numérico que quantifica a planicidade das amostras. A influência foi investigada através de uma análise estatística bivariada, relacionando o índice de planicidade com cada um dos parâmetros alvo. A análise apresentou uma correlação negativa forte e significativa pelo teste de Spearman (⍴ ≅ 0,95 e valor-p < 10–3) entre o teor de plastificante do tipo I e a planicidade das placas produzidas, porém para os outros parâmetros analisados a correlação não pôde ser considerada estatisticamente significativa. Além disso, os resultados mostraram também que a utilização de um pós processamento nas fitas à verde, como uma laminação, melhorou substancialmente a planicidade das placas após a sinterização.
总结在这项研究中,大量的医疗8%摩尔钇稳定氧化锆(TZ8Y)技术制造了粘贴胶带,从他们的成分悬浮固体的体积和配体的水平,增塑剂的I型和II型增塑剂,以验证这些参数的影响和触变行为停职empenamento的最终产品。烧结后,通过比较时钟绘制板的地形,在坐标系上测量板的表面,并从这个坐标系中定义了量化样品平整度的数值指标。通过双变量统计分析,将平面度指数与每个目标参数联系起来,研究其影响。作为一个强大的负相关关系,分析有意义的斯皮尔曼(测试⍴≅95和- p值< 10—3)I型增塑剂的含量与planicidade板的生产,但其他人分析相关参数不能被认为是统计学意义。此外,结果还表明,在绿带中使用后处理,如轧制,大大提高了烧结后板的平整度。
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引用次数: 0
Avaliação da aplicabilidade do ensaio de compressão de anel à quente para determinar o coeficiente de atrito no ensaio de torneamento do aço ABNT 1045 por meio de análise estatística 通过统计分析评价热环压缩试验在确定ABNT 1045钢车削试验摩擦系数方面的适用性
Pub Date : 2023-09-01 DOI: 10.1590/1517-7076-rmat-2023-0085
Thaís Ramos Capai Jardim, M. Câmara, F. C. Magalhães, Anderson Júnior dos Santos
RESUMO O atrito nas interfaces ferramenta/cavaco e ferramenta/peça é complexo dificultando a determinação do coeficiente de atrito nos processos de usinagem. Assim, vários ensaios tribológicos foram desenvolvidos para simular as condições de corte e determinar o coeficiente de atrito. Este trabalho apresentou análise comparativa do coeficiente de atrito entre o aço ABNT 1045 e WC-10Co revestido com AlCrN por meio de dois métodos: ensaio de torneamento e ensaio de compressão de anel à quente. O ensaio de torneamento foi realizado com corte oblíquo nas velocidades de corte 150 e 220 m/min. A aquisição dos sinais das componentes de força da usinagem por meio de um dinamômetro. O ensaio de compressão de anel foi realizado nas temperaturas de 200 e 400 °C. Os coeficientes de atrito foram obtidos por meio de modelos matemáticos. A análise estatística do coeficiente de atrito apontou equivalência do coeficiente de atrito no ensaio de torneamento na velocidade de corte 150 m/min com o ensaio de compressão de anel à quente 200 °C. Assim como no ensaio de torneamento na velocidade de corte 220 m/min com o ensaio de compressão de anel à quente 400 °C. A análise macrográfica do anel após a deformação no ensaio de compressão de anel observou a influência da temperatura de ensaio no deslocamento do raio neutro. A análise superficial dos anéis e das matrizes do ensaio de compressão foi realizada por meio de microscopia óptica (MO) e rugosidade Ra, onde observou-se o aumento da rugosidade após o ensaio e a presença de desgaste abrasivo.
刀具/切屑和刀具/工件界面的摩擦复杂,难以确定加工过程中的摩擦系数。因此,进行了各种摩擦学试验来模拟切削条件并确定摩擦系数。摘要采用车削试验和热环压缩试验两种方法,对ABNT 1045钢与WC-10Co涂AlCrN钢的摩擦系数进行了比较分析。车削试验在150和220 m/min的切削速度下进行斜切。用测力计采集加工力部件的信号。环压试验在200℃和400℃的温度下进行。通过数学模型得到了摩擦系数。摩擦系数的统计分析表明,在切削速度为150 m/min的车削试验中,摩擦系数与热环压缩试验200℃时的摩擦系数相等。以及在切割速度220 m/min下的车削试验和400°C热环压缩试验。对环压缩试验变形后的环进行宏观分析,观察了试验温度对中性半径位移的影响。通过光学显微镜(om)和粗糙度Ra对环和压缩试验基体进行表面分析,观察到测试后粗糙度的增加和磨料磨损的存在。
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引用次数: 0
Study on time-effect to the strength deterioration of carbonaceous mudstone under water-rock interaction 水岩相互作用下碳质泥岩强度劣化的时间效应研究
Pub Date : 2023-08-28 DOI: 10.1590/1517-7076-rmat-2023-0166
Peng Mo, Qiongzhen Tang, Junhui Luo, Haifeng Huang, Qingping Yang, Yu Chen
While excavation activities in mountain terrain regions, the exposure of carbonaceous mudstone could deteriorate the strength under the water-rock interaction, which impacts slope stability and affects the safety of the engineering project. The present study conducted the Point Loading Test (PLT), Acoustic Emission (AE)
在山地地形区开挖时,碳质泥岩的暴露会使其在水岩相互作用下的强度变差,从而影响边坡的稳定性,影响工程的安全。本研究进行了点加载试验(PLT)、声发射试验(AE)。
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引用次数: 0
Caracterização física e mecânica de painéis LVL de paricá (Schizolobium parahyba var. amazonicum (Huber x Ducke)) colados com ureia-formaldeído 尿素甲醛胶合parica (Schizolobium parahyba变种amazonicum (Huber x Ducke)) LVL面板的物理和机械特性
Pub Date : 2023-08-28 DOI: 10.1590/1517-7076-rmat-2023-0178
Vinícius de Sousa Lima, Sandriel Lima Nascimento, Maria Luiza Rodrigues Gurgel da Silva, Marco Antonio Siviero, S. César, J. Molina, João Miguel Santos Dias
RESUMO O trabalho teve como objetivo determinar as propriedades físicas e mecânicas de painéis LVL de paricá (Schizolobium parahyba var. amazonicum (Huber x Ducke)) colados com resina ureia-formaldeído. Foram produzidos 6 painéis LVL com 17 lâminas de 2,5 mm de espessura, sendo 14 lâminas de paricá e 3 lâminas de marupá (Simarouba amara Aubl.). Para a condição de umidade padrão de 12%, foram realizados ensaios de teor de umidade, densidades aparente e básica (caracterização física), resistências à compressão paralela e perpendicular às fibras, tração paralela às fibras, cisalhamento na linha de cola e flexão estática flatwise e edgewise (caracterização mecânica). Na condição de saturação total da madeira, foram realizados ensaios de compressão paralela às fibras e cisalhamento na linha de cola do LVL. Os resultados mostraram que os painéis LVL se enquadram na classe de resistência D30, caracterizado com média densidade. Foi observado o modo de ruptura do tipo frágil em todos os ensaios mecânicos, exceto nos ensaios de compressão paralela e perpendicular às fibras. O aumento do teor de umidade, decorrente da saturação total da madeira, influenciou de forma negativa nas resistências à compressão paralela às fibras e ao cisalhamento na linha de cola. O LVL apresentou desempenho mecânico compatível com as solicitações estruturais.
摘要本研究旨在测定尿素甲醛树脂胶合parica (Schizolobium parahyba var. amazonicum (Huber x Ducke)) LVL板的物理力学性能。生产了6个LVL面板,17个2.5 mm厚的刀片,14个parica刀片和3个marupa刀片(Simarouba amara Aubl.)。在12%的标准湿度条件下,进行了含水率、表观密度和基本密度(物理特性)、平行和垂直于纤维的抗压强度、平行于纤维的拉伸强度、胶线剪切强度、平面和边缘静态弯曲强度(力学特性)等试验。在木材完全饱和条件下,进行了与纤维平行的压缩试验和LVL胶线的剪切试验。结果表明,LVL板的电阻等级为D30,密度为中等。除平行和垂直于纤维的压缩试验外,所有力学试验均观察到脆性断裂模式。由于木材的总饱和,水分含量的增加对纤维平行抗压强度和胶线剪切强度有负面影响。LVL的力学性能与结构要求一致。
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引用次数: 0
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