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Chemical treatment, fibre length, and fibre loading affecting the mechanical and morphological characteristics of flax fibre/polylactic acid (PLA) green composites developed by injection moulding Einfluss von chemischer Behandlung, Faserlänge und Faserbelastung auf die mechanischen und morphologischen Eigenschaften von im Spritzgiessverfahren hergestellten grünen Verbundwerkstoffen aus Flachsfasern/Polymilchsäure (PLA) 化学处理、纤维长度和纤维负载对注塑成型亚麻纤维/聚乳酸(PLA)绿色复合材料机械和形态特性的影响 化学处理、纤维长度和纤维负载对注塑成型亚麻纤维/聚乳酸(PLA)绿色复合材料机械和形态特性的影响
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-08-06 DOI: 10.1002/mawe.202300316
M. Debnath, P. Chakraborti, G. S. Rao

This paper presents the parametric investigation and optimization of various chemical treatment parameters that affect the mechanical performance of the green composite. The injection moulding method was used to produce the green composites using flax fibre (FF) and polylactic acid (PLA). The chemical parameters chosen to investigate their effects are chemical type (sodium hydroxide, sodium carbonate, and potassium hydroxide), chemical concentrations (1 %, 2 %, and 3 % (w/v)), and duration for fibre treatment (2 h, 4 h, and 6 h). The mechanical performance of the green composites was assessed by evaluating the various properties namely strength, modulus, and elongation under tensile, share, flexural, and compression loading conditions. The morphological study was also performed to examine the failure behavior of the composite after mechanical testing. The effect of fibre length (2 mm, 3 mm, 4 mm, 5 mm, and 6 mm) and fibre loading (10 wt.%, 20 wt.%, and 30 wt.%) on the performance of the flax fibre (FF)/polylactic acid (PLA) composite was also investigated. The fibre dispersion, fibre orientation, and fibre length retention were investigated to assess the characteristics of fibre during injection moulding of the developed flax fibre (FF)/polylactic acid (PLA) composite.

本文对影响绿色复合材料机械性能的各种化学处理参数进行了参数研究和优化。采用注塑成型法生产亚麻纤维(FF)和聚乳酸(PLA)绿色复合材料。为研究其影响而选择的化学参数包括化学类型(氢氧化钠、碳酸钠和氢氧化钾)、化学浓度(1%、2% 和 3%(w/v))以及纤维处理时间(2 小时、4 小时和 6 小时)。通过评估绿色复合材料在拉伸、共用、弯曲和压缩加载条件下的各种性能,即强度、模量和伸长率,对其机械性能进行了评估。此外,还进行了形态学研究,以检查复合材料在机械测试后的失效行为。此外,还研究了纤维长度(2 毫米、3 毫米、4 毫米、5 毫米和 6 毫米)和纤维负载(10 wt.%、20 wt.% 和 30 wt.%)对亚麻纤维(FF)/聚乳酸(PLA)复合材料性能的影响。研究了纤维分散、纤维取向和纤维长度保持,以评估亚麻纤维(FF)/聚乳酸(PLA)复合材料在注塑成型过程中的纤维特性。
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引用次数: 0
Comparative study on periodic immersion+infrared aging corrosion behavior of Q345qNH steel and Q420qNH steel in simulated industrial atmospheric environment medium Korrosionsverhalten der Stähle Q345qNH und Q420qNH bei zyklischer Immersion und Infrarotalterung in einem simulierten industriellen atmosphärischen Medium Q345qNH 钢和 Q420qNH 钢在模拟工业大气环境介质中的周期性浸泡+红外老化腐蚀行为比较研究 Q345qNH 钢和 Q420qNH 钢在模拟工业大气环境介质中的周期性浸泡和红外老化腐蚀行为研究
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-08-02 DOI: 10.1002/mawe.202300248
T. Guo, H. Yang, W. Wu, X. Liu, X. Nan, Y. Hu

The corrosion behavior of Q345qNH steel and Q420qNH steel in simulated industrial atmospheric environment medium was studied by periodic immersion+infrared aging corrosion experiment. The results show that the corrosion type of both samples is uneven comprehensive corrosion, and the rust layer formed in the later stage of corrosion is relatively dense. But average corrosion rate of Q345qNH steel is always lower than that of Q420qNH steel, and the ratio of Iα-FeOOH/Iγ-FeOOH in rust layer is always higher. Compared with Q420qNH steel, Q345qNH steel has fewer surface pits but deeper local pits. The self-corrosion potential of Q345qNH steel increases obviously, the resistance of the rust layer is larger, and protection to the matrix is stronger. This is because the formation of a large number of corrosion microcells induced by fine lamellar sorbite tissue that uneven distributed in Q420qNH steel, which increases the corrosion rate and makes corrosion uneven, while the larger pearlitic group in Q345qNH steel increases the local corrosion rate. However, the higher chromium/carbon ratio in Q345qNH steel promotes the conversion of lepidocrocite to goethite and inhibits the cathode reaction in the infrared drying stage, improving the density and stability of the rust layer.

通过周期性浸泡+红外老化腐蚀实验研究了 Q345qNH 钢和 Q420qNH 钢在模拟工业大气环境介质中的腐蚀行为。结果表明,两种试样的腐蚀类型均为不均匀的全面腐蚀,腐蚀后期形成的锈层相对致密。但 Q345qNH 钢的平均腐蚀速率始终低于 Q420qNH 钢,锈层中 Iα-FeOOH/Iγ-FeOOH 的比值始终较高。与 Q420qNH 钢相比,Q345qNH 钢的表面凹坑较少,但局部凹坑较深。Q345qNH 钢的自腐蚀潜能明显增加,锈层的阻力更大,对基体的保护更强。这是因为 Q420qNH 钢中分布不均匀的细小片状索氏体组织诱导形成了大量的腐蚀微胞,从而增加了腐蚀速率并使腐蚀不均匀,而 Q345qNH 钢中较大的珠光体基团则增加了局部腐蚀速率。然而,Q345qNH 钢中较高的铬/碳比促进了鳞片闪长岩向闪长岩的转化,抑制了红外干燥阶段的阴极反应,提高了锈层的致密性和稳定性。
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引用次数: 0
Materialwiss. Werkstofftech. 7/2024 材料科学材料技术 7/2024
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-07-29 DOI: 10.1002/mawe.202480711
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引用次数: 0
Cover Picture: (Materialwiss. Werkstofftech. 7/2024) 封面图片: (Materialwiss. Werkstofftech. 7/2024)
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-07-29 DOI: 10.1002/mawe.202480701

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引用次数: 0
Impressum: Materialwiss. Werkstofftech. 7/2024 版本说明:Materialwiss.材料技术 7/2024
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-07-29 DOI: 10.1002/mawe.202480721
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引用次数: 0
Effect of aging temperature on the microstructure and properties of alloyed high-manganese steel Einfluss der Alterungstemperatur auf das Gefüge und die Eigenschaften von legiertem hochmanganhaltigem Stahl 时效温度对合金高锰钢微观结构和性能的影响
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-07-25 DOI: 10.1002/mawe.202300074
J. Sun, M. Jiang, L. Dong, Z. Ding, Y. Bao, S. Luo

This paper describes an aging treatment based on alloying the traditional high-carbon high-manganese steel to improve its initial wear resistance (wear resistance after water toughening treatment only). The changes in structure and mechanical properties of alloyed high-manganese steel after aging treatment at different temperatures were investigated using various experimental methods such as metallographic analysis, mechanical property testing, and fracture morphology observation.

The austenite grain boundary began to have the appearance of grain carbide at 550 °C; a large number of pearlites nucleated at the grain boundary and within grain at 600 °C, most phase transitions occur at 650 °C; and the pearlite and carbide began to revert to a soluble state at 700 °C, leaving only a small amount of pearlite in the austenite grain boundary. The hardness and yield strength of alloyed high-manganese steel increase and then decrease with the increasing aging temperature, and the high peaks appear in the range of 600 °C–650 °C; while the tensile strength and plasticity decrease and then slightly increase, with the highest and lowest peaks being approximately 550 °C and 650 °C, respectively.

At the aging temperature of 550 °C, the alloy high manganese steel has good comprehensive mechanical and deformation strengthening properties, with yield strength, tensile strength, elongation, and section shrinkage of 536 MPa, 1058 MPa, 51 % and 35 %, respectively. The changes in the properties of alloyed high-manganese steel are related to the pattern of structural changes that occur during the aging process.

本文介绍了一种基于传统高碳高锰钢合金化的时效处理方法,以提高其初始耐磨性(仅水韧化处理后的耐磨性)。采用金相分析、力学性能测试和断口形貌观察等多种实验方法,研究了合金化高锰钢在不同温度下进行时效处理后的组织和力学性能变化。550 ℃时,奥氏体晶界开始出现晶粒碳化物;600 ℃时,大量珠光体在晶界和晶粒内部成核,大部分相变发生在650 ℃;700 ℃时,珠光体和碳化物开始恢复到可溶状态,奥氏体晶界只剩下少量珠光体。随着时效温度的升高,合金高锰钢的硬度和屈服强度先增大后减小,在600 ℃-650 ℃范围内出现较高的峰值;而抗拉强度和塑性先减小后略有增大,最高和最低峰值分别约为550 ℃和650 ℃。在 550 ℃ 的时效温度下,合金高锰钢具有良好的综合力学性能和变形强化性能,屈服强度、抗拉强度、伸长率和断面收缩率分别为 536 MPa、1058 MPa、51 % 和 35 %。合金高锰钢性能的变化与时效过程中发生的结构变化规律有关。
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引用次数: 0
Features of the structure and properties of stone mastic asphalt Merkmale der Struktur und Eigenschaften von Steinmastixasphalt 石硫合剂沥青的结构和性能特点
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-07-23 DOI: 10.1002/mawe.202300181
A. Bieliatynskyi, S. Yang, V. Pershakov, M. Shao, M. Ta

The purpose of this study is to investigate the features and properties of stone mastic asphalt in the context of its potential for practical application in road repair works, aiming to create a high-quality road surface and replace outdated structural materials with newer alternatives. The leading approach combines a systematic analysis of the issues submitted for consideration and an experimental study of the properties of stone mastic asphalt, which are important in the context of the practical use of this building material to ensure high quality parameters of the roadway and the timeliness of its repair, if necessary. Within the framework of this study, results were obtained that indicate a significant variety of approaches to determining the characteristics and properties of the material under consideration, clearly demonstrating current solutions to the problem of improving the performance of stone mastic asphalt by introducing special admixtures into its composition. The findings and conclusions of this research are valuable for road service employees and developers of modern construction materials, aiding in high-quality road surface repair and creating durable asphalt for safe road use in the future.

本研究的目的是根据石硫合剂沥青在道路维修工程中的实际应用潜力,对其特征和特性进行研究,旨在创造高质量的路面,并用更新的替代材料取代过时的结构材料。主要方法是对提交审议的问题进行系统分析,并对石硫合剂沥青的特性进行实验研究,这些特性在实际使用这种建筑材料时非常重要,可确保路面的高质量参数,并在必要时及时进行修复。在这项研究的框架内获得的结果表明,确定所考虑材料的特征和性能的方法多种多样,清楚地表明了通过在其成分中引入特殊外加剂来改善石硫合剂沥青性能问题的当前解决方案。这项研究的结果和结论对道路服务人员和现代建筑材料开发人员很有价值,有助于高质量的路面修复,并为未来道路的安全使用创造耐用的沥青。
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引用次数: 0
A-prori layer height determination for wire arc additive manufacturing based on weld geometry A-priori-Lagenhöhenbestimmung für drahtbasierte Lichtbogen-Additiv-Schweißverfahren auf Basis der Schweißnahtgeometrie 根据焊缝几何形状确定线弧快速成型制造的 A-prori 层高
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-07-23 DOI: 10.1002/mawe.202300158
K. Mäde, P. J. Kellerwessel, R. Sharma, U. Reisgen

The application of wire arc additive manufacturing (WAAM) for the production of large size components is currently limited, due to strong distortion and unprecise filling behavior. The resulting geometric and metallurgical irregularities pose a challenge to the process. The current approach of a layered structure cannot be adopted without adjustments when using wire arc additive manufacturing. Reasons include incompleteness, material accumulation and deformation. The combination of experimental weld geometry-determination and its numerical estimation is presented here as solution to this challenge. The procedure is based on the measurement of a weld bead cross-section-area. By convolution of a path matrix with a weld-geometry-function, the planned path is filled with the seam geometry. Subsequent summation of multiple matrices results in a height profile showing discontinuities and accumulations. Further validation tests show a good agreement between the method and experimentally determined problem areas. The presented optimisation procedure can be extended with material parameters. A local compensation for deformation can be achieved.

目前,线弧快速成型技术(WAAM)在大尺寸部件生产中的应用受到了限制,原因在于其强烈的变形和不精确的填充行为。由此产生的几何和冶金不规则性对工艺提出了挑战。在使用线弧快速成型技术时,如果不进行调整,就无法采用当前的分层结构方法。原因包括不完整、材料堆积和变形。本文介绍了焊接几何形状的实验确定和数值估算相结合的方法,作为应对这一挑战的解决方案。该程序基于焊缝横截面积的测量。通过路径矩阵与焊缝几何函数的卷积,用焊缝几何填充计划路径。随后对多个矩阵求和,得到一个显示不连续性和堆积的高度剖面图。进一步的验证测试表明,该方法与实验确定的问题区域之间具有良好的一致性。所介绍的优化程序可通过材料参数进行扩展。可以实现变形的局部补偿。
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引用次数: 0
Decreasing the electrostatic discharge generated from friction of polyester and polyamide sing carbon fiber Verringerung der durch Reibung von Polyester und Polyamid erzeugten elektrostatischen Entladung mithilfe von Kohlefasern 减少聚酯和聚酰胺与碳纤维摩擦产生的静电放电
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-07-23 DOI: 10.1002/mawe.202300084
H. Suaad, M. K. Mohamed, W. Y. Ali

The present work discusses the voltage difference as a measure for electrostatic charge generated from the contact-separation and sliding of polymeric textiles on polyamide textile. It is proposed to blend polyester by carbon fiber to decrease the electrostatic charge generated on the contact surfaces. Because polyester acquires a negative charge and polyamide gains a positive one, carbon fiber is proposed to conduct the negative electrostatic charge from polyester to polyamide and conducts the positive one from polyamide to polyester, so that the resultant electrostatic charge decreased. The effect of carbon fiber to decrease the electrostatic charge depends on its area of contact, interaction, and distribution with polyester. Polyester double weaved by carbon fiber showed the lowest voltage. Based on those observations, it can be recommended to use double weaves of carbon fiber with polyester. The reduction in voltage was relatively lower for braided polyester by carbon fiber than that detected for double-weaved polyester by carbon fiber.

本研究讨论了聚合纺织品在聚酰胺纺织品上接触分离和滑动时产生的静电荷的测量电压差。建议用碳纤维混合聚酯,以减少接触面上产生的静电荷。由于聚酯获得负电荷,而聚酰胺获得正电荷,因此建议用碳纤维将负静电荷从聚酯传导到聚酰胺,并将正静电荷从聚酰胺传导到聚酯,从而减少由此产生的静电荷。碳纤维降低静电荷的效果取决于其与聚酯的接触面积、相互作用和分布。碳纤维双层编织的聚酯显示的电压最低。根据上述观察结果,建议使用碳纤维与聚酯双层编织。与碳纤维双织聚酯相比,碳纤维编织聚酯的电压降低幅度相对较低。
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引用次数: 0
Nanosecond laser micromachining of graphene nanoplatelets reinforced ZK60 matrix composites Nanosekunden-Laserstrahl-Mikrobearbeitung von mit Graphen-Nanoplättchen verstärkten ZK60-Matrix-Verbundwerkstoffen 纳秒激光微加工石墨烯纳米片增强 ZK60 矩阵复合材料
IF 1.2 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-07-23 DOI: 10.1002/mawe.202300283
Z. Wu, C. W. Li, Y. Zhang, Y. L. Liu, J. Y. Song, C. M. Yang

In this paper, a nanosecond laser was used to etch the surface of graphene nanoplatelets reinforced ZK60 (GNPs/ZK60) matrix composites, and the effects of different scanning speeds, pulse repetition frequency and laser power on the etched morphology of the machined surface were investigated. The experimental results show that the etched groove width and heat affected zone width of GNPs/ZK60 composites are significantly increased compared with ZK60 material due to the influence of graphene, and the growth rate of the difference in heat affected zone width between GNPs/ZK60 composites and ZK60 materials is most significantly affected by the pulse repetition frequency. In addition, the dross height increases with the increase of laser power, while the scaly dross structure becomes increasingly clear.

本文采用纳秒激光刻蚀石墨烯纳米片增强 ZK60(GNPs/ZK60)基复合材料表面,研究了不同扫描速度、脉冲重复频率和激光功率对加工表面刻蚀形貌的影响。实验结果表明,由于石墨烯的影响,GNPs/ZK60 复合材料的蚀刻沟槽宽度和热影响区宽度与 ZK60 材料相比明显增大,而 GNPs/ZK60 复合材料与 ZK60 材料热影响区宽度差异的增长率受脉冲重复频率的影响最为显著。此外,渣滓高度随激光功率的增加而增加,同时鳞片状渣滓结构变得越来越清晰。
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引用次数: 0
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