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Fast synthesis of Hcy-modified Au nanoclusters under microwave-assisted irradiation and their response to Cu (II) ions 微波辅助下hcy修饰金纳米团簇的快速合成及其对Cu (II)离子的响应
IF 4.6 3区 材料科学 Q2 MATERIALS SCIENCE, COMPOSITES Pub Date : 2023-08-30 DOI: 10.1080/20550324.2023.2251203
Yong-qiang Shen, Xin Wang, Yunfei Xia, Ping Li, Yinan Ding, Tianzhu Luan, Kai Song
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引用次数: 0
Effect of variations in Ni-W molar ratio on the microstructure, mechanical properties and tribology of electrodeposited Ni-W/diamond composite coatings Ni-W摩尔比对电沉积Ni-W/金刚石复合镀层微观结构、力学性能和摩擦学的影响
IF 4.6 3区 材料科学 Q2 MATERIALS SCIENCE, COMPOSITES Pub Date : 2023-06-24 DOI: 10.1080/20550324.2023.2229184
M. K. Das, J. Qin, T. Bovornratanaraks
{"title":"Effect of variations in Ni-W molar ratio on the microstructure, mechanical properties and tribology of electrodeposited Ni-W/diamond composite coatings","authors":"M. K. Das, J. Qin, T. Bovornratanaraks","doi":"10.1080/20550324.2023.2229184","DOIUrl":"https://doi.org/10.1080/20550324.2023.2229184","url":null,"abstract":"","PeriodicalId":18872,"journal":{"name":"Nanocomposites","volume":"14 1","pages":""},"PeriodicalIF":4.6,"publicationDate":"2023-06-24","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"87829948","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Electric fields and local heating in additively manufactured nanocomposite parts 增材制造纳米复合材料零件的电场和局部加热
IF 4.6 3区 材料科学 Q2 MATERIALS SCIENCE, COMPOSITES Pub Date : 2023-06-23 DOI: 10.1080/20550324.2023.2229187
Raymond D. Mee, Ava G. Crowley, M. Mustafa, Micah J. Green
{"title":"Electric fields and local heating in additively manufactured nanocomposite parts","authors":"Raymond D. Mee, Ava G. Crowley, M. Mustafa, Micah J. Green","doi":"10.1080/20550324.2023.2229187","DOIUrl":"https://doi.org/10.1080/20550324.2023.2229187","url":null,"abstract":"","PeriodicalId":18872,"journal":{"name":"Nanocomposites","volume":"139 1","pages":""},"PeriodicalIF":4.6,"publicationDate":"2023-06-23","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"72475282","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Numerical and analytical modelling of effective thermal conductivity of multi-walled carbon nanotubes polymer nanocomposites including the effect of nanotube orientation and interfacial thermal resistance 考虑纳米管取向和界面热阻影响的多壁碳纳米管聚合物纳米复合材料有效导热系数的数值与解析建模
IF 4.6 3区 材料科学 Q2 MATERIALS SCIENCE, COMPOSITES Pub Date : 2023-06-06 DOI: 10.1080/20550324.2023.2218240
Shambhu Kumar, Akhilendra Singh, M. Tiwari
{"title":"Numerical and analytical modelling of effective thermal conductivity of multi-walled carbon nanotubes polymer nanocomposites including the effect of nanotube orientation and interfacial thermal resistance","authors":"Shambhu Kumar, Akhilendra Singh, M. Tiwari","doi":"10.1080/20550324.2023.2218240","DOIUrl":"https://doi.org/10.1080/20550324.2023.2218240","url":null,"abstract":"","PeriodicalId":18872,"journal":{"name":"Nanocomposites","volume":"37 1","pages":""},"PeriodicalIF":4.6,"publicationDate":"2023-06-06","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"72993784","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 1
Crosslinked PAES-based sandwich-structured polymer nanocomposites with covalently strengthened interface towards high-temperature capacitive energy storage 基于共价增强界面交联paes的三明治结构聚合物纳米复合材料的高温电容储能研究
IF 4.6 3区 材料科学 Q2 MATERIALS SCIENCE, COMPOSITES Pub Date : 2023-02-08 DOI: 10.1080/20550324.2023.2173053
Qiannan Cai, Danying Zhao, Hai-Sen Xu, Wenhan Xu, H. Yao, Yunhe Zhang
{"title":"Crosslinked PAES-based sandwich-structured polymer nanocomposites with covalently strengthened interface towards high-temperature capacitive energy storage","authors":"Qiannan Cai, Danying Zhao, Hai-Sen Xu, Wenhan Xu, H. Yao, Yunhe Zhang","doi":"10.1080/20550324.2023.2173053","DOIUrl":"https://doi.org/10.1080/20550324.2023.2173053","url":null,"abstract":"","PeriodicalId":18872,"journal":{"name":"Nanocomposites","volume":"55 1","pages":""},"PeriodicalIF":4.6,"publicationDate":"2023-02-08","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"83786738","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 1
Determination of optimal potential parameters for the self-assembly of various lattice structures 各种晶格结构自组装最优电位参数的确定
IF 4.6 3区 材料科学 Q2 MATERIALS SCIENCE, COMPOSITES Pub Date : 2023-02-08 DOI: 10.1080/20550324.2023.2170028
Jae-Hyun Kim, Seonho Cho
{"title":"Determination of optimal potential parameters for the self-assembly of various lattice structures","authors":"Jae-Hyun Kim, Seonho Cho","doi":"10.1080/20550324.2023.2170028","DOIUrl":"https://doi.org/10.1080/20550324.2023.2170028","url":null,"abstract":"","PeriodicalId":18872,"journal":{"name":"Nanocomposites","volume":"117 1","pages":""},"PeriodicalIF":4.6,"publicationDate":"2023-02-08","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"79834875","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Synthesis, properties and electrocatalytic application of g-C3N4 for oxygen electrodes of fuel cells g-C3N4在燃料电池氧电极上的合成、性能及电催化应用
IF 4.6 3区 材料科学 Q2 MATERIALS SCIENCE, COMPOSITES Pub Date : 2023-02-02 DOI: 10.1080/20550324.2023.2169985
M. Danilov, G. Dovbeshko, I. Rusetskyi, V. Bykov, O. Gnatyuk, S. Fomanyuk, G. Kolbasov
{"title":"Synthesis, properties and electrocatalytic application of g-C3N4 for oxygen electrodes of fuel cells","authors":"M. Danilov, G. Dovbeshko, I. Rusetskyi, V. Bykov, O. Gnatyuk, S. Fomanyuk, G. Kolbasov","doi":"10.1080/20550324.2023.2169985","DOIUrl":"https://doi.org/10.1080/20550324.2023.2169985","url":null,"abstract":"","PeriodicalId":18872,"journal":{"name":"Nanocomposites","volume":"30 3 1","pages":""},"PeriodicalIF":4.6,"publicationDate":"2023-02-02","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"87556488","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 1
In situ synthesis of the Fe3O4@poly(4-vinylpyridine)-block-polystyrene magnetic polymer nanocomposites via dispersion RAFT polymerization 分散RAFT聚合原位合成Fe3O4@poly(4-乙烯基吡啶)嵌段聚苯乙烯磁性聚合物纳米复合材料
IF 4.6 3区 材料科学 Q2 MATERIALS SCIENCE, COMPOSITES Pub Date : 2022-12-31 DOI: 10.1080/20550324.2023.2170003
Lin Wu, T. Pang, Laxia Wu, Yebin Guan, Liwei Yin
Abstract This work presents a facile strategy for the generation of Fe3O4@poly(4-vinylpyridine)-block-polystyrene (Fe3O4@P4VP-b-PS) magnetic polymer nanocomposites. P4VP-b-PS nanoparticles prepared by dispersion RAFT polymerization of styrene in methanol/water in the presence of macro-P4VP chain transfer agent was employed as templates to grow Fe3O4 on polymeric network templates. With the following addition of FeCl3 into the above polymer colloids, pyridyl moieties in P4VP block of nanoparticles could further react with Fe3+ through a coordination reaction to generate Fe3+@P4VP-b-PS nanoparticles. After the subsequent addition of FeCl2 and NH3⋅H2O, the co-precipitation reaction occurred on the surface of the polymeric nanoparticle to form Fe3O4@P4VP-b-PS magnetic polymer nanocomposites. Herein, FT-IR, XRD, TGA, XPS, TEM and VSM were applied to characterize the morphology, structure and magnetism performance of the synthesized magnetic polymeric nanocomposites. Graphical abstract
摘要:本文提出了一种生成Fe3O4@poly(4-乙烯基吡啶)-嵌段聚苯乙烯(Fe3O4@P4VP-b-PS)磁性聚合物纳米复合材料的简便策略。在宏观p4vp链转移剂存在下,将苯乙烯在甲醇/水中分散RAFT聚合制备的P4VP-b-PS纳米粒子作为模板,在聚合物网络模板上生长Fe3O4。在上述聚合物胶体中加入FeCl3后,纳米粒子P4VP嵌段中的吡啶基部分可以进一步与Fe3+发生配位反应,生成Fe3+@P4VP-b-PS纳米粒子。随后加入FeCl2和NH3⋅H2O后,高分子纳米颗粒表面发生共沉淀反应,形成Fe3O4@P4VP-b-PS磁性高分子纳米复合材料。利用FT-IR、XRD、TGA、XPS、TEM和VSM对合成的磁性聚合物纳米复合材料的形貌、结构和磁性进行了表征。图形抽象
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引用次数: 0
Strong and osteoconductive poly(lactic acid) biocomposites by high-shear liquid dispersion of hydroxyapatite nanowhiskers 羟基磷灰石纳米须高剪切液相分散制备的强导骨聚乳酸生物复合材料
IF 4.6 3区 材料科学 Q2 MATERIALS SCIENCE, COMPOSITES Pub Date : 2022-12-31 DOI: 10.1080/20550324.2022.2054212
Dong-mei Zhou, Meng-Han Shen, Lv Ke, Ziwen Zhang, Kaiwen Zhang, Shenghui Zhang, Yanqing Wang, Haoran Yang, Dao-Min Tang, Donghui Huang, Jin-Kui Yang, Huan Xu
Abstract Controlled incorporation of bioactive hydroxyapatite (HA) into poly(lactic acid) (PLA) signifies a promising approach to design and development of biomedical-adaptive materials. Here we unravel a microwave-assisted biomineralization approach to synthesis of HA nanowhiskers (HANWs), which were characterized by well-controlled diameter (∼30 nm) and length (80 − 120 nm), combined with a desirable calcium − phosphorus ratio (Ca/P) of 1.67. A high-shear liquid dispersion (HSLD) method that provided a combination of high pressure (up to 50 kPa) and high shear rate approaching 10000 s −1 was established to fabricate homogeneous PLA/HANWs composites. In particular, upon incorporation of 30 wt % HANWs the tensile strength and elastic modulus of PLA-HA30 (76.7 MPa and 3.3 GPa) were elevated by 48% and 84% compared to those of pure PLA, respectively, as accompanied by a nearly 2-fold increase in the cell viability. This work paves a facile yet effective roadway to strong and osteoconductive PLA composites appealing for bone tissue repairing. Graphical Abstract Synopsis: Biomineralization concepts are abstracted to synthesize well-defined and bioactive HANWs, which could be uniformly dispersed in PLA biofilms by high-shear liquid exfoliation.
生物活性羟基磷灰石(HA)受控掺入聚乳酸(PLA)是设计和开发生物医学适应性材料的一种有前途的方法。在这里,我们揭示了一种微波辅助生物矿化方法来合成HA纳米晶须(HANWs),其特点是直径(~ 30 nm)和长度(80 ~ 120 nm)控制良好,钙磷比(Ca/P)为1.67。建立了一种高剪切液体分散(HSLD)方法,该方法提供了高压(高达50 kPa)和接近10000 s−1的高剪切速率的组合,以制备均质PLA/HANWs复合材料。特别是,在加入30 wt %的HANWs后,PLA- ha30的拉伸强度和弹性模量(76.7 MPa和3.3 GPa)分别比纯PLA提高了48%和84%,同时细胞活力增加了近2倍。本研究为构建具有良好骨导电性的强PLA复合材料用于骨组织修复铺平了一条简单而有效的道路。摘要:生物矿化的概念被抽象为合成定义明确且具有生物活性的HANWs,这些HANWs可以通过高剪切液体剥离均匀地分散在PLA生物膜中。
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引用次数: 5
Flower-like and nanorods ZnO deposited on rGO as efficient photocatalysts for removal of polychlorinated biphenyls (PCBs) 花状和纳米棒状ZnO沉积在氧化石墨烯上作为去除多氯联苯的高效光催化剂
IF 4.6 3区 材料科学 Q2 MATERIALS SCIENCE, COMPOSITES Pub Date : 2022-12-31 DOI: 10.1080/20550324.2023.2168938
A. Merlano, E. Albiter, M. Valenzuela, L. Hoyos, Á. Salazar
Abstract PCBs were used for several decades as coolants, lubricants in transformers, plasticizers, and dielectric fluids, being highly carcinogenic and representing a severe environmental problem in soil and water. Pure and modified TiO2 has been the most studied photocatalyst looking to degrade PCBs into less toxic products. Lately, ZnO-graphene composites have played an essential role in the photocatalytic degradation of various toxic organic compounds. In this work, ZnO nanostructures were coupled with reduced graphene oxide (ZnO-rGO) via a one-pot microwave-assisted hydrothermal route. As a result, the composites exhibited improved photocatalytic performance for PCBs degradation compared to ZnO nanoparticles. Thus, this research provides an in-situ method to grow different morphologies of ZnO on rGO. Graphical Abstract
摘要:几十年来,多氯联苯被用作冷却剂、变压器润滑剂、增塑剂和介质流体,具有高度致癌性,并在土壤和水中构成严重的环境问题。纯的和改性的二氧化钛一直是研究最多的光催化剂,旨在将多氯联苯降解成毒性较低的产品。近年来,zno -石墨烯复合材料在光催化降解各种有毒有机化合物方面发挥了重要作用。在这项工作中,ZnO纳米结构通过一锅微波辅助水热途径与还原氧化石墨烯(ZnO- rgo)偶联。结果表明,与ZnO纳米颗粒相比,复合材料对pcb的光催化性能有所提高。因此,本研究提供了一种在氧化石墨烯上原位生长不同形貌ZnO的方法。图形抽象
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引用次数: 2
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