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Time-Resolved Detection of Vaporization during Laser Metal Processing with Laser-induced Fluorescence 激光诱导荧光在激光金属加工过程中汽化的时间分辨检测
Pub Date : 2018-09-03 DOI: 10.1002/HTTPS://DX.DOI.ORG/10.1016/J.PROCIR.2018.08.072
B. Simonds, P. Williams, J. Lehman
Abstract Element loss during high-power laser processing of metals can lead to deleterious chemical and mechanical effects that negatively impact the processed material’s quality. Currently, there is no suitable way to measure time-resolved element loss in situ during laser processing. In this work, we show that laser-induced fluorescence (LIF) can be used to temporally resolve individual element vaporization during a laser spot welding of 316L stainless steel. As a proof-of-concept, we measured iron loss during a 500 µs laser spot weld with a time resolution of 5 microseconds. We found that keyhole formation could clearly be identified by a dramatic increase in iron emission from the weld pool. This conclusion was validated by independent, time-resolved measurements of laser absorptance during laser spot welding from our previous work.
高功率激光金属加工过程中的元素损耗会导致有害的化学和机械效应,从而对加工材料的质量产生负面影响。目前,还没有合适的方法来测量激光加工过程中时间分辨元素的原位损耗。在这项工作中,我们证明了激光诱导荧光(LIF)可以暂时解决316L不锈钢激光点焊过程中单个元素的汽化。作为概念验证,我们测量了500µs激光点焊期间的铁损失,时间分辨率为5微秒。我们发现,通过焊缝池中铁排放量的急剧增加,可以清楚地识别出锁孔的形成。这一结论得到了我们之前工作中对激光点焊过程中激光吸收的独立、时间分辨测量结果的验证。
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引用次数: 5
Dynamic and absolute measurements of laser coupling efficiency during laser spot welds 激光点焊过程中激光耦合效率的动态和绝对测量
Pub Date : 2018-09-03 DOI: 10.1002/HTTPS://DX.DOI.ORG/10.1016/J.PROCIR.2018.08.065
B. Simonds, J. Sowards, J. Hadler, E. Pfeif, B. Wilthan, Jack R. Tanner, C. Harris, P. Williams
Abstract Laser absorptance (coupling efficiency) changes rapidly during laser metal processing due to temperature and multiple phase changes. We find that there is limited literature data available, but that this property is vital for accurate process simulations, as well as the fundamental understanding of the dynamics of high-power laser-matter interaction. We measure the dynamic, absolute absorbed power with sub-microsecond resolution during a 10 ms laser spot weld in 316L stainless steel from conduction to keyhole welding conditions using an integrating sphere. Our data show several important features including the points of melting and keyhole formation. Conclusions from the optical data are supported by weld cross-section analysis.
激光金属加工过程中,由于温度和多相变化,激光吸收(耦合效率)变化很快。我们发现可用的文献数据有限,但这一特性对于精确的过程模拟以及对高功率激光-物质相互作用动力学的基本理解至关重要。在316L不锈钢激光点焊过程中,采用积分球测量了从传导到锁孔焊接过程中10 ms激光点焊的动态绝对吸收功率,其分辨率为亚微秒级。我们的数据显示了几个重要的特征,包括熔点和钥匙孔的形成。从光学数据得出的结论得到了焊缝截面分析的支持。
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引用次数: 7
Performance of Self-developing Radiography Films in LVR-15's Neutron Beams 自显影胶片在LVR-15中子束中的性能
Pub Date : 2017-01-01 DOI: 10.1016/j.phpro.2017.06.033
Jaroslav Soltes , Ladislav Viererbl , Vit Klupak , Miroslav Vins , Bozena Michalcova

In the search for a suitable detector for demonstration neutron radiography measurements on the zero-power VR-1 training reactor at the Czech Technical University in Prague, some options were considered. Due to the reactor's low power and spatial limitations, an easy and practical solution had to be found. Self-developing films represent a flexible detection tool in x-ray imaging. Therefore, the goal of this study was to evaluate their potential for neutron detection. For this purpose, bare and converter covered films were studied in the thermal and epithermal neutron beams at the LVR-15 research reactor in Rez, Czech Republic.

在为布拉格捷克技术大学的零功率VR-1训练反应堆的示范中子射线照相测量寻找合适的探测器时,考虑了一些备选办法。由于反应堆的低功率和空间限制,必须找到一个简单实用的解决方案。自显影胶片是一种灵活的x射线成像检测工具。因此,本研究的目的是评估它们在中子探测方面的潜力。为此,在捷克共和国Rez的LVR-15研究堆上,对热中子束和超热中子束中的裸膜和转炉覆盖膜进行了研究。
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引用次数: 0
Features of Optical Breakdown of Liquid under the Action of Ultrasound 超声作用下液体光击穿特性研究
Pub Date : 2017-01-01 DOI: 10.1016/j.phpro.2017.01.005
A.V. Bulanov , I.G. Nagorny , A.V. Storozhenko

The experimental results show the sharply strengthened effects of acoustic emission from a breakdown zone by the joint influence of laser and ultrasonic irradiation. Various breakdown thresholds and character of acoustic emission in fresh and sea water are observed. The experimental result established that acoustic emission from optical breakdown of sea water in the presence and absence of ultrasound exceeds acoustic emission for the same experimental conditions in fresh water.

实验结果表明,在激光和超声的共同作用下,击穿区的声发射效应急剧增强。观察了淡水和海水声发射的各种击穿阈值和特征。实验结果表明,在超声波存在和不存在的情况下,海水光击穿的声发射超过淡水中相同实验条件下的声发射。
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引用次数: 0
A Comparative Study of the Crystallite Size and the Dislocation Density of Bent Steel Plates using Bragg-edge Transmission Imaging, TOF Neutron Diffraction and EBSD 利用bragg边缘透射成像、TOF中子衍射和EBSD对弯曲钢板晶粒尺寸和位错密度的比较研究
Pub Date : 2017-01-01 DOI: 10.1016/j.phpro.2017.06.004
K. Oikawa , Y.H. Su , Y. Tomota , T. Kawasaki , T. Shinohara , T. Kai , K. Hiroi , S.Y. Zhang , J.D. Parker , H. Sato , Y. Kiyanagi

Line broadening analysis was performed on the time-of-flight neutron diffraction data for the plastically bent plates of a ferritic steel and a duplex stainless steel. A Rietveld analysis program, Z-Rietveld ver. 1.0 was used to fit the anisotropically broadened patterns where the increase in Lorentzian full width at half maximum (FWHM) and the Gaussian FWHM involves information of the crystallite size and the dislocation density, respectively. The derived results were compared with those obtained by using Bragg-edge transmission spectrum analysis and electron backscatter diffraction (EBSD) observations.

对铁素体钢和双相不锈钢塑性弯曲板的飞行时间中子衍射数据进行了线展宽分析。一个Rietveld分析程序,Z-Rietveld ver。采用1.0拟合各向异性加宽图,其中洛伦兹半最大全宽(FWHM)和高斯半最大宽分别涉及晶体尺寸和位错密度的信息。将所得结果与Bragg-edge透射谱分析和电子背散射衍射(EBSD)观测结果进行了比较。
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引用次数: 5
Terbium Radionuclides for Theranostics Applications: A Focus On MEDICIS-PROMED 铽放射性核素在治疗学上的应用:以医学为重点
Pub Date : 2017-01-01 DOI: 10.1016/j.phpro.2017.09.053
R. Formento Cavaier , F. Haddad , T. Sounalet , T. Stora , I. Zahi

A new facility, named CERN-MEDICIS, is under construction at CERN to produce radionuclides for medical applications. In parallel, the MEDICIS-PROMED, a Marie Sklodowska-Curie innovative training network of the Horizon 2020 European Commission‘s program, is being coordinated by CERN to train young scientists on the production and use of innovative radionuclides and develop a network of experts within Europe. One program within MEDICIS-PROMED is to determine the feasibility of producing innovative radioisotopes for theranostics using a commercial middle-sized high-current cyclotron and the mass separation technology developed at CERN-MEDICIS. This will allow the production of high specific activity radioisotopes not achievable with the common post-processing by chemical separation. Radioisotopes of scandium, copper, arsenic and terbium have been identified. Preliminary studies of activation yield and irradiation parameters optimization for the production of Tb-149 will be described.

一个名为CERN- medicis的新设施正在CERN建造,以生产用于医疗用途的放射性核素。与此同时,欧洲核子研究中心正在协调欧洲委员会地平线2020计划的玛丽·斯克洛多夫斯卡-居里创新培训网络MEDICIS-PROMED,以培训年轻科学家生产和使用创新放射性核素,并在欧洲建立一个专家网络。MEDICIS-PROMED的一个项目是确定使用商用中型大电流回旋加速器和CERN-MEDICIS开发的质量分离技术为治疗学生产创新放射性同位素的可行性。这将允许生产高比活度放射性同位素,这是通过化学分离的普通后处理无法实现的。已鉴定出钪、铜、砷和铽的放射性同位素。本文将对生产Tb-149的活化产率和辐照参数优化进行初步研究。
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引用次数: 33
Recent Progress of Radiography and Tomography at the Energy-resolved Neutron Imaging System RADEN 能量分辨中子成像系统RADEN的放射学和层析成像研究进展
Pub Date : 2017-01-01 DOI: 10.1016/j.phpro.2017.06.022
Y. Matsumoto , M. Segawa , T. Kai , T. Shinohara , T. Nakatani , K. Oikawa , K. Hiroi , Y.H. Su , H. Hayashida , J.D. Parker , S.Y. Zhang , Y. Kiyanagi

We have performed neutron radiography and tomography using a CCD camera-type detector for some test samples at RADEN. The current spatial resolution for neutron radiography is estimated to about 350 μm in the largest field-of-view of 300 × 300 mm2 and 100 μm in the field-of-view of 60 × 60 mm2. It is thought that the latter spatial resolution is strongly affected by the image blur in the scintillator screen. In the case of neutron tomography, the current spatial resolution is estimated to be better than 0.5 mm using an iron and aluminum test sample. Furthermore, we have performed neutron tomography for a cast aluminum product. As a result, small blowholes are found in the center of the product. This demonstrates the importance of non-destructive testing by neutron radiography and tomography for industrial products.

我们使用CCD相机型探测器对RADEN的一些测试样品进行了中子射线照相和断层扫描。目前中子射线照相的空间分辨率估计在300 × 300 mm2的最大视场中约为350 μm,在60 × 60 mm2的视场中约为100 μm。认为闪烁屏中图像模糊对后一种空间分辨率的影响很大。在中子层析成像的情况下,使用铁和铝测试样品估计当前的空间分辨率优于0.5 mm。此外,我们还对铸铝产品进行了中子层析成像。结果,在产品的中心发现了小的气孔。这证明了中子射线照相和层析成像对工业产品无损检测的重要性。
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引用次数: 8
Inline Repair of Blowouts During Laser Welding 激光焊接时爆孔的在线修复
Pub Date : 2017-01-01 DOI: 10.1016/j.phpro.2017.08.022
K.S. Hansen , F.O. Olsen , M. Kristiansen , O. Madsen

In a current laser welding production process of components of stainless steel, a butt joint configuration may lead to failures in the form of blowouts, causing an unacceptable welding quality. A study to improve the laser welding process was performed with the aim of solving the problem by designing a suitable pattern of multiple small laser spots rather than a single spot in the process zone.

The blowouts in the process are provoked by introducing small amounts of zinc powder in the butt joint. When the laser heats up the zinc, this rapidly evaporates and expands, leaving the melt pool to be blown away locally. Multiple spot pattern designs are tested. Spot patterns are produced by applying diffractive optics to a beam from a single mode fiber laser.

Results from welding while applying spot patterns both with and without trailing spots are presented. Data showing the power ratio between a trailing spot and two main spots as a function of spot distance is also presented.

The results of the study show that applying multiple spots in the welding process may improve the process stability when welding materials with small impurities in the form of zinc particles.

在目前不锈钢构件的激光焊接生产过程中,对接接头的配置可能会导致爆裂形式的失效,从而导致不可接受的焊接质量。为了改善激光焊接工艺,在加工区域设计合适的多个小激光光斑而不是单个光斑,进行了一项研究。在对接接头中加入少量锌粉会引起井喷。当激光加热锌时,锌迅速蒸发和膨胀,留下熔池被局部吹走。测试了多个点图案设计。光斑图案是通过对单模光纤激光器的光束施加衍射光学而产生的。给出了采用带尾点和不带尾点的点焊图案进行焊接的结果。数据显示了尾随光斑和两个主光斑之间的功率比作为光斑距离的函数。研究结果表明,在焊接过程中采用多点焊可以提高锌颗粒形式杂质较少的材料的焊接稳定性。
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引用次数: 2
Calibration and Correction Method of the Deflection Angle of Rotation Axis Projection on Neutron Tomography 中子层析成像旋转轴投影偏转角的标定与校正方法
Pub Date : 2017-01-01 DOI: 10.1016/j.phpro.2017.06.041
Zhilong Ji, Qiang Lin, Xu Han, Jiawei Liu, Wen Zhang, Min Yang

For neutron tomography, reconstruction accuracy greatly relies on exact registration of the projection and the back-projection coordinate system. Since the manufacturing and installing errors of mechanical components make the rotation axis projected in CCD camera deflect a certain angle, a mismatch between the projection coordinate and the detector coordinate will be caused consequently, resulting in obvious artifacts on the reconstructed images. In this paper, a calibration and correction method of the deflection angle of rotation axis projection is proposed to eliminate artifacts on neutron tomography images. First, all the projections among 360° rotation range are superposed together to create an averaged image with a unique symmetry axis. Then by segmentation and principal component analysis on the averaged image, the deflection angle is figured out. The calibrated angle is introduced to the reconstruction algorithm as an extra correction parameter, and artifacts-free images are finally obtained.

对于中子层析成像,重建精度很大程度上依赖于投影和反投影坐标系的精确配准。由于机械部件的制造和安装误差,会使CCD相机中投影的旋转轴发生一定角度的偏转,从而导致投影坐标与探测器坐标不匹配,从而导致重建图像上出现明显的伪影。为了消除中子层析成像图像上的伪影,提出了一种旋转轴投影偏转角的标定和校正方法。首先,将360°旋转范围内的所有投影叠加在一起,形成具有唯一对称轴的平均图像。然后对平均图像进行分割和主成分分析,求出偏转角度。将校正后的角度作为一个额外的校正参数引入到重建算法中,最终得到无伪影的图像。
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引用次数: 4
Theoretical Model of Controllable Waveguide Channels System Holographic Formation in Photopolymer-liquid Crystalline Composition 光聚合物-液晶组成中可控波导通道系统全息形成的理论模型
Pub Date : 2017-01-01 DOI: 10.1016/j.phpro.2017.01.020
A.O. Semkin, S.N. Sharangovich

In this work the theoretical model of holographic formation of controllable waveguide channels system in photopolymer-liquid crystalline composition is developed. The ability to control the light propagation conditions in waveguides by external electric field impact is demonstrated.

本文建立了光聚合物-液晶组合物中可控波导通道系统全息形成的理论模型。论证了利用外电场冲击控制光在波导中的传播条件的能力。
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引用次数: 2
期刊
Physics Procedia
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