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Time-Resolved Detection of Vaporization during Laser Metal Processing with Laser-induced Fluorescence 激光诱导荧光在激光金属加工过程中汽化的时间分辨检测
Pub Date : 2018-09-03 DOI: 10.1002/HTTPS://DX.DOI.ORG/10.1016/J.PROCIR.2018.08.072
B. Simonds, P. Williams, J. Lehman
Abstract Element loss during high-power laser processing of metals can lead to deleterious chemical and mechanical effects that negatively impact the processed material’s quality. Currently, there is no suitable way to measure time-resolved element loss in situ during laser processing. In this work, we show that laser-induced fluorescence (LIF) can be used to temporally resolve individual element vaporization during a laser spot welding of 316L stainless steel. As a proof-of-concept, we measured iron loss during a 500 µs laser spot weld with a time resolution of 5 microseconds. We found that keyhole formation could clearly be identified by a dramatic increase in iron emission from the weld pool. This conclusion was validated by independent, time-resolved measurements of laser absorptance during laser spot welding from our previous work.
高功率激光金属加工过程中的元素损耗会导致有害的化学和机械效应,从而对加工材料的质量产生负面影响。目前,还没有合适的方法来测量激光加工过程中时间分辨元素的原位损耗。在这项工作中,我们证明了激光诱导荧光(LIF)可以暂时解决316L不锈钢激光点焊过程中单个元素的汽化。作为概念验证,我们测量了500µs激光点焊期间的铁损失,时间分辨率为5微秒。我们发现,通过焊缝池中铁排放量的急剧增加,可以清楚地识别出锁孔的形成。这一结论得到了我们之前工作中对激光点焊过程中激光吸收的独立、时间分辨测量结果的验证。
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引用次数: 5
Dynamic and absolute measurements of laser coupling efficiency during laser spot welds 激光点焊过程中激光耦合效率的动态和绝对测量
Pub Date : 2018-09-03 DOI: 10.1002/HTTPS://DX.DOI.ORG/10.1016/J.PROCIR.2018.08.065
B. Simonds, J. Sowards, J. Hadler, E. Pfeif, B. Wilthan, Jack R. Tanner, C. Harris, P. Williams
Abstract Laser absorptance (coupling efficiency) changes rapidly during laser metal processing due to temperature and multiple phase changes. We find that there is limited literature data available, but that this property is vital for accurate process simulations, as well as the fundamental understanding of the dynamics of high-power laser-matter interaction. We measure the dynamic, absolute absorbed power with sub-microsecond resolution during a 10 ms laser spot weld in 316L stainless steel from conduction to keyhole welding conditions using an integrating sphere. Our data show several important features including the points of melting and keyhole formation. Conclusions from the optical data are supported by weld cross-section analysis.
激光金属加工过程中,由于温度和多相变化,激光吸收(耦合效率)变化很快。我们发现可用的文献数据有限,但这一特性对于精确的过程模拟以及对高功率激光-物质相互作用动力学的基本理解至关重要。在316L不锈钢激光点焊过程中,采用积分球测量了从传导到锁孔焊接过程中10 ms激光点焊的动态绝对吸收功率,其分辨率为亚微秒级。我们的数据显示了几个重要的特征,包括熔点和钥匙孔的形成。从光学数据得出的结论得到了焊缝截面分析的支持。
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引用次数: 7
Calibration and Correction Method of the Deflection Angle of Rotation Axis Projection on Neutron Tomography 中子层析成像旋转轴投影偏转角的标定与校正方法
Pub Date : 2017-01-01 Epub Date: 2017-06-24 DOI: 10.1016/j.phpro.2017.06.041
Zhilong Ji, Qiang Lin, Xu Han, Jiawei Liu, Wen Zhang, Min Yang

For neutron tomography, reconstruction accuracy greatly relies on exact registration of the projection and the back-projection coordinate system. Since the manufacturing and installing errors of mechanical components make the rotation axis projected in CCD camera deflect a certain angle, a mismatch between the projection coordinate and the detector coordinate will be caused consequently, resulting in obvious artifacts on the reconstructed images. In this paper, a calibration and correction method of the deflection angle of rotation axis projection is proposed to eliminate artifacts on neutron tomography images. First, all the projections among 360° rotation range are superposed together to create an averaged image with a unique symmetry axis. Then by segmentation and principal component analysis on the averaged image, the deflection angle is figured out. The calibrated angle is introduced to the reconstruction algorithm as an extra correction parameter, and artifacts-free images are finally obtained.

对于中子层析成像,重建精度很大程度上依赖于投影和反投影坐标系的精确配准。由于机械部件的制造和安装误差,会使CCD相机中投影的旋转轴发生一定角度的偏转,从而导致投影坐标与探测器坐标不匹配,从而导致重建图像上出现明显的伪影。为了消除中子层析成像图像上的伪影,提出了一种旋转轴投影偏转角的标定和校正方法。首先,将360°旋转范围内的所有投影叠加在一起,形成具有唯一对称轴的平均图像。然后对平均图像进行分割和主成分分析,求出偏转角度。将校正后的角度作为一个额外的校正参数引入到重建算法中,最终得到无伪影的图像。
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引用次数: 4
Recent Progress of Radiography and Tomography at the Energy-resolved Neutron Imaging System RADEN 能量分辨中子成像系统RADEN的放射学和层析成像研究进展
Pub Date : 2017-01-01 Epub Date: 2017-06-24 DOI: 10.1016/j.phpro.2017.06.022
Y. Matsumoto , M. Segawa , T. Kai , T. Shinohara , T. Nakatani , K. Oikawa , K. Hiroi , Y.H. Su , H. Hayashida , J.D. Parker , S.Y. Zhang , Y. Kiyanagi

We have performed neutron radiography and tomography using a CCD camera-type detector for some test samples at RADEN. The current spatial resolution for neutron radiography is estimated to about 350 μm in the largest field-of-view of 300 × 300 mm2 and 100 μm in the field-of-view of 60 × 60 mm2. It is thought that the latter spatial resolution is strongly affected by the image blur in the scintillator screen. In the case of neutron tomography, the current spatial resolution is estimated to be better than 0.5 mm using an iron and aluminum test sample. Furthermore, we have performed neutron tomography for a cast aluminum product. As a result, small blowholes are found in the center of the product. This demonstrates the importance of non-destructive testing by neutron radiography and tomography for industrial products.

我们使用CCD相机型探测器对RADEN的一些测试样品进行了中子射线照相和断层扫描。目前中子射线照相的空间分辨率估计在300 × 300 mm2的最大视场中约为350 μm,在60 × 60 mm2的视场中约为100 μm。认为闪烁屏中图像模糊对后一种空间分辨率的影响很大。在中子层析成像的情况下,使用铁和铝测试样品估计当前的空间分辨率优于0.5 mm。此外,我们还对铸铝产品进行了中子层析成像。结果,在产品的中心发现了小的气孔。这证明了中子射线照相和层析成像对工业产品无损检测的重要性。
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引用次数: 8
Historic binnacle of 14C/12C concentration in Mexico City 墨西哥城14C/12C浓度的历史坐标
Pub Date : 2017-01-01 Epub Date: 2017-10-26 DOI: 10.1016/j.phpro.2017.09.007
J.A. Flores , C. Solís , A. Huerta , M.E. Ortiz , M.G. Rodríguez-Ceja , J. Villanueva , E. Chávez

The radiocarbon concentration is reduced in urban areas, generally due to high CO2 emissions derived from fossil fuels. In this paper, new Δ14C measurements in cellulose extracted from the growth rings of two trees over a 43-year period are presented. The first is in a zone with clean air (El Nayar, Durango, Mexico) and the second is from the Greater Mexico City area (Chapultepec). Data from El Nayar is consistent with that reported for Zone 2 of the Northern Hemisphere while that from the urban area shows a significant decrease in Δ14C. Our results are compared with data from other cities (Nagoya, Japan and Valladolid, Spain).

城市地区的放射性碳浓度降低,通常是由于化石燃料产生的大量二氧化碳排放。在本文中,新的Δ14C测量从两棵树的生长年轮中提取的纤维素在43年期间提出。第一个是在空气清新的地区(墨西哥杜兰戈的El Nayar),第二个是在大墨西哥城地区(查普尔特佩克)。来自El Nayar的数据与北半球第2区报告的数据一致,而来自城市地区的数据显示Δ14C显著减少。我们的结果与其他城市(日本名古屋和西班牙巴利亚多利德)的数据进行了比较。
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引用次数: 6
Performance of Self-developing Radiography Films in LVR-15's Neutron Beams 自显影胶片在LVR-15中子束中的性能
Pub Date : 2017-01-01 Epub Date: 2017-06-24 DOI: 10.1016/j.phpro.2017.06.033
Jaroslav Soltes , Ladislav Viererbl , Vit Klupak , Miroslav Vins , Bozena Michalcova

In the search for a suitable detector for demonstration neutron radiography measurements on the zero-power VR-1 training reactor at the Czech Technical University in Prague, some options were considered. Due to the reactor's low power and spatial limitations, an easy and practical solution had to be found. Self-developing films represent a flexible detection tool in x-ray imaging. Therefore, the goal of this study was to evaluate their potential for neutron detection. For this purpose, bare and converter covered films were studied in the thermal and epithermal neutron beams at the LVR-15 research reactor in Rez, Czech Republic.

在为布拉格捷克技术大学的零功率VR-1训练反应堆的示范中子射线照相测量寻找合适的探测器时,考虑了一些备选办法。由于反应堆的低功率和空间限制,必须找到一个简单实用的解决方案。自显影胶片是一种灵活的x射线成像检测工具。因此,本研究的目的是评估它们在中子探测方面的潜力。为此,在捷克共和国Rez的LVR-15研究堆上,对热中子束和超热中子束中的裸膜和转炉覆盖膜进行了研究。
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引用次数: 0
Terbium Radionuclides for Theranostics Applications: A Focus On MEDICIS-PROMED 铽放射性核素在治疗学上的应用:以医学为重点
Pub Date : 2017-01-01 Epub Date: 2017-10-26 DOI: 10.1016/j.phpro.2017.09.053
R. Formento Cavaier , F. Haddad , T. Sounalet , T. Stora , I. Zahi

A new facility, named CERN-MEDICIS, is under construction at CERN to produce radionuclides for medical applications. In parallel, the MEDICIS-PROMED, a Marie Sklodowska-Curie innovative training network of the Horizon 2020 European Commission‘s program, is being coordinated by CERN to train young scientists on the production and use of innovative radionuclides and develop a network of experts within Europe. One program within MEDICIS-PROMED is to determine the feasibility of producing innovative radioisotopes for theranostics using a commercial middle-sized high-current cyclotron and the mass separation technology developed at CERN-MEDICIS. This will allow the production of high specific activity radioisotopes not achievable with the common post-processing by chemical separation. Radioisotopes of scandium, copper, arsenic and terbium have been identified. Preliminary studies of activation yield and irradiation parameters optimization for the production of Tb-149 will be described.

一个名为CERN- medicis的新设施正在CERN建造,以生产用于医疗用途的放射性核素。与此同时,欧洲核子研究中心正在协调欧洲委员会地平线2020计划的玛丽·斯克洛多夫斯卡-居里创新培训网络MEDICIS-PROMED,以培训年轻科学家生产和使用创新放射性核素,并在欧洲建立一个专家网络。MEDICIS-PROMED的一个项目是确定使用商用中型大电流回旋加速器和CERN-MEDICIS开发的质量分离技术为治疗学生产创新放射性同位素的可行性。这将允许生产高比活度放射性同位素,这是通过化学分离的普通后处理无法实现的。已鉴定出钪、铜、砷和铽的放射性同位素。本文将对生产Tb-149的活化产率和辐照参数优化进行初步研究。
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引用次数: 33
Experimental Evaluation of Neutron Absorption Grating Fabricated by Oblique Evaporation of Gadolinium for Phase Imaging 钆斜蒸发中子吸收光栅相位成像的实验评价
Pub Date : 2017-01-01 Epub Date: 2017-06-24 DOI: 10.1016/j.phpro.2017.06.030
Yoshichika Seki , Takenao Shinohara , Wakana Ueno , Joseph D. Parker , Tetsuo Samoto , Wataru Yashiro , Atsushi Momose

For the neutron phase imaging with a Talbot-Lau interferometer, we have fabricated neutron absorption gratings with a pitch of 9 μm by oblique evaporation of gadolinium. The performances of these gratings for the phase measurement were experimentally evaluated at RADEN in J-PARC, by observing the neutron transmission and the visibility of moiré fringe in the interferometer. A new analysis method using the wavelength-resolved neutron transmission was also attempted to estimate the characteristics of gratings.

为了在塔尔伯特-劳干涉仪上进行中子相位成像,我们采用钆斜蒸发法制备了9 μm的中子吸收光栅。在J-PARC的RADEN上,通过观察中子透射率和干涉条纹的可见性,对这些光栅的相位测量性能进行了实验评价。本文还尝试了一种利用波长分辨中子透射率分析光栅特性的新方法。
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引用次数: 14
Computational Analysis Supporting the Design of a New Beamline for the Mines Neutron Radiography Facility 支持矿山中子射线照相设备新型光束线设计的计算分析
Pub Date : 2017-01-01 Epub Date: 2017-06-24 DOI: 10.1016/j.phpro.2017.06.045
C. Wilson, J. King

The Colorado School of Mines installed a neutron radiography system at the United States Geological Survey TRIGA reactor in 2012. An upgraded beamline could dramatically improve the imaging capabilities of this system. This project performed computational analyses to support the design of a new beamline, with the major goals of minimizing beam divergence and maximizing beam intensity. The new beamline will consist of a square aluminum tube with an 11.43 cm (4.5 in) inner side length and 0.635 cm (0.25 in) thick walls. It is the same length as the original beam tube (8.53 m) and is composed of 1.22 m (4 ft) and 1.52 m (5 ft) flanged sections which bolt together. The bottom 1.22 m of the beamline is a cylindrical aluminum pre-collimator which is 0.635 cm (0.25 in) thick, with an inner diameter of 5.08 cm (2 in). Based on Monte Carlo model results, when a pre-collimator is present, the use of a neutron absorbing liner on the inside surface of the beam tube has almost no effect on the angular distribution of the neutron current at the collimator exit. The use of a pre-collimator may result in a non-uniform flux profile at the image plane; however, as long as the collimator is at least three times longer than the pre-collimator, the flux distortion is acceptably low.

2012年,科罗拉多矿业学院在美国地质调查局(United States Geological Survey)的TRIGA反应堆上安装了中子射线照相系统。升级后的光束线可以显著提高该系统的成像能力。该项目进行了计算分析,以支持新光束线的设计,其主要目标是最小化光束发散和最大化光束强度。新的光束线将由一个方形铝管组成,内径为11.43厘米(4.5英寸),壁厚为0.635厘米(0.25英寸)。它与原来的梁管(8.53米)长度相同,由1.22米(4英尺)和1.52米(5英尺)的法兰部分螺栓连接在一起。光束线的底部1.22米是一个圆柱形的铝预准直器,厚度为0.635厘米(0.25英寸),内径为5.08厘米(2英寸)。基于蒙特卡罗模型的结果表明,当存在预准直器时,在束流管内表面使用中子吸收衬垫对准直器出口处中子电流的角分布几乎没有影响。预准直器的使用可能导致像面上的通量分布不均匀;然而,只要准直器至少比预准直器长三倍,磁通畸变是可接受的低。
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引用次数: 0
Structural Change of Carbon Anode in a Lithium-ion Battery Product Associated with Charging Process Observed by Neutron Transmission Bragg-edge Imaging 锂离子电池产品碳负极结构随充电过程的变化
Pub Date : 2017-01-01 Epub Date: 2017-06-24 DOI: 10.1016/j.phpro.2017.06.003
Takashi Kamiyama , Yuki Narita , Hirotaka Sato , Masato Ohnuma , Yoshiaki Kiyanagi

Spectroscopic neutron Bragg-edge imaging was performed to study a lithium-ion battery (LIB) product. This non-destructive neutron imaging method is suitable for the evaluation of industrial products, but presents some difficulties for application to multicomponent products. The LIB includes a strong neutron scatterer and an absorber, and is thus a suitable test case for the use of neutron imaging in actual product measurement. In this study, we analyzed the variation of the graphite anode structure with changes in the battery charge level. The experiments were carried out using the compact neutron source at the Hokkaido University neutron source facility (HUNS). To eliminate the effect of scattered neutron contamination, we first determined the distance between the sample and detector required to reduce this effect to under 1%. Using this separation, the charge level dependence of the anode structure was measured. The graphite {002} Bragg-edge could be recognized on the neutron transmission spectra. The Bragg-edge was shifted and broadened with increasing battery charge. The edge was consistent with the existence of multiple graphite structural stages. The layer spacing distribution images for different charge levels showed the inhomogeneous fluctuation on the LIB lattice plane. Based on the images the fraction of the graphite structural stages were analyzed. The ratio of each stage varied with the charge level, and the ideal intercalation structure, in which the graphite layers are stuffed with Li-ions, was found to be minor in the final charging state.

利用中子布拉格边缘成像技术对锂离子电池产品进行了研究。这种无损中子成像方法适用于工业产品的评价,但应用于多组分产品存在一定的困难。LIB包括一个强中子散射体和一个吸收体,因此是在实际产品测量中使用中子成像的合适测试案例。在本研究中,我们分析了石墨阳极结构随电池充电水平变化的变化。实验是在北海道大学中子源设施(HUNS)使用紧凑型中子源进行的。为了消除散射中子污染的影响,我们首先确定了将这种影响降低到1%以下所需的样品和探测器之间的距离。利用这种分离,测量了阳极结构对电荷水平的依赖性。在中子透射谱上可以识别出石墨{002}布拉格边缘。随着电池电量的增加,布拉格边发生了位移和变宽。边缘与多个石墨结构阶段的存在相一致。不同电荷水平的层间距分布图像显示了LIB晶格平面上的不均匀波动。在此基础上,分析了石墨结构阶段的比例。各阶段的比例随充电水平而变化,在最终充电状态下,石墨层填充锂离子的理想嵌入结构较少。
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引用次数: 15
期刊
Physics Procedia
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