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Microstructural Information Mapping of a Plastic-deformed α-iron Plate during Tensile Tests using Pulsed Neutron Transmission 用脉冲中子透射法对α-铁板拉伸试验中塑性变形的微结构信息映射
Pub Date : 2017-01-01 DOI: 10.1016/j.phpro.2017.06.006
Takashi Kamiyama , Kenji Iwase , Hirotaka Sato , Stefanus Harjo , Takayoshi Ito , Shin-ichi Takata , Kazuya Aizawa , Yoshiaki Kiyanagi

The spatial-dependent lattice spacing and microstructure of an α-iron plate with two notches was measured during tensile tests using a pulsed neutron transmission method to ascertain changes depending on the load. Changes in microstructural parameters such as macrostrain, microstrain, crystallite size and texture are interesting during the transition from the elastic to plastic deformation region, especially over a relatively wide field of view to see propagation of the change. The method has the capability to show changes in the position-dependence of microstructural information simultaneously over a wide area in the bulk material. Transmission spectra around the Bragg-edge regions of the neutron total cross section of α-iron were obtained, and the microstructural parameters, {110} plane spacing and its distribution, texture coefficient and crystallite size were analyzed. The spatial-dependent distributions (images) of these parameters show sample shape effects including strain concentration around the notches and the effect of dislocations being multiplied during the plastic deformation. The spatial dependence of the microstructural parameters visualized herein provides useful information for evaluating the inhomogeneous progress of deformation of the bulk engineering material.

采用脉冲中子透射法测量了具有两个缺口的α-铁板在拉伸试验中的晶格间距和微观结构随载荷的变化。在从弹性变形区向塑性变形区过渡的过程中,微观结构参数(如大应变、微应变、晶粒尺寸和织构)的变化是有趣的,特别是在相对较宽的视场上观察变化的传播。该方法具有在块状材料的大范围内同时显示微结构信息位置依赖性变化的能力。获得了α-铁中子总截面布拉格边缘区周围的透射光谱,分析了α-铁的显微组织参数、{110}面间距及其分布、织构系数和晶粒尺寸。这些参数的空间相关分布(图像)显示了样品形状的影响,包括缺口周围的应变集中和塑性变形期间的位错倍增效应。本文所显示的微观结构参数的空间依赖性为评价块状工程材料的非均匀变形过程提供了有用的信息。
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引用次数: 4
Neutron Imaging Development at China Academy of Engineering Physics (CAEP) 中国工程物理研究院中子成像研究进展
Pub Date : 2017-01-01 DOI: 10.1016/j.phpro.2017.06.021
Hang Li , Sheng Wang , Chao Cao , Heyong Huo , Bin Tang

Based the China Mianyang Research Reactor (CMRR) and D-T accelerator neutron source, thermal neutron, cold neutron and fast neutron imaging facilities are all installed at China Academy of Engineering Physics (CAEP). Various samples have been imaged by different energy neutrons and shown the neutron imaging application in industry, aerospace and so on. The facilities parameters and recent neutron imaging development will be shown in this paper.

以中国绵阳研究堆(CMRR)和D-T加速器中子源为基础,在中国工程物理研究院(CAEP)安装了热中子、冷中子和快中子成像设备。用不同能量的中子对不同样品进行了成像,展示了中子成像在工业、航天等领域的应用。本文将介绍中子成像的设备参数和最新进展。
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引用次数: 13
Extended Stability of HPGe Spectrometer with Environmental Control at the High Flux Isotope Reactor 高通量同位素反应堆环境控制下HPGe谱仪扩展稳定性研究
Pub Date : 2017-01-01 DOI: 10.1016/j.phpro.2017.09.046
Jordan Heim , Jonathan Nistor , David Koltick

A High Purity Germanium (HPGe) spectrometer has been designed and constructed for making precision measurements over extended time periods at the High Flux Isotope Reactor (HFIR) located at Oak Ridge National Lab (ORNL). Toward the effort of achieving long-term system stability and high spectral resolution, local environment control is utilized as part of the system design. Further, the remote operation of the spectrometer is aided by live-streaming system conditions and automatic out-of-range alert messaging. System performance over the 7-month Phase I period is presented.

为了在橡树岭国家实验室(ORNL)的高通量同位素反应堆(HFIR)上进行长时间的精确测量,设计并建造了一台高纯锗(HPGe)光谱仪。为了实现系统的长期稳定性和高光谱分辨率,局部环境控制被用作系统设计的一部分。此外,光谱仪的远程操作由实时流系统条件和自动超范围警报信息辅助。介绍了第一阶段7个月期间的系统性能。
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引用次数: 1
Investigation of Spectral Lines Broadening in Femtosecond Laser Plasma Generated on the Surface of the Barium Water Solutions 飞秒激光等离子体在钡水溶液表面谱线展宽的研究
Pub Date : 2017-01-01 DOI: 10.1016/j.phpro.2017.01.027
M.Yu. Babiy, S.S. Golik, A.A. Ilyin, Yu.S. Biryukova, T.M. Agapova, V.V. Lisitsa

The spectral lines broadening in femtosecond laser plasma generated by the 45 fs Ti:Sa laser pulses on the surface of the water solutions of Ba is investigated. Under the experimental conditions, determined the temperature of femtosecond laser plasma is 3000K.The contribution of the Doppler broadening for spectral lines width is minimal and amounts 0,0022 nm for Ba. The main mechanism of Ba spectral line broadening in experimental conditions is resonance. The resulting values of resonance broadening constitute a0,0349 nm for Ba I (413,24 nm), 0,0563 nm for Ba I (553,54 nm), 0,0241 nm for Ba II(455,41 nm), 0,0437 nm for Ba II (614,17 nm).

研究了45 fs Ti:Sa激光脉冲在Ba水溶液表面产生的飞秒激光等离子体的谱线展宽。在实验条件下,确定飞秒激光等离子体的温度为3000K。多普勒增宽对谱线宽度的贡献很小,Ba的贡献为0.0022 nm。实验条件下Ba谱线展宽的主要机理是共振。Ba I(413,24 nm)、Ba I(553,54 nm)、Ba II(455,41 nm)、Ba II(614,17 nm)的共振增宽值分别为0,0349 nm、0,0563 nm、0,0241 nm和0,0437 nm。
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引用次数: 1
Structure and Electronic Properties of Nano-complex CCl4…Cr(AcacCl)3 on Evidence Derived from Vibrational Spectroscopy 纳米配合物CCl4…Cr(AcacCl)3的结构和电子性质——基于振动谱的证据
Pub Date : 2017-01-01 DOI: 10.1016/j.phpro.2017.01.012
S.N. Slabzhennikov, L.A. Kuarton, O.B. Ryabchenko

In order to specify influence of intermolecular interaction on IR spectrum of interacting species, an investigation of a process CCl4 + Сr(АcacCl)3 → CCl4…Сr(АcacCl)3 has been performed by means of Hartree–Fock–Roothaan method in MIDI basis set with p- and d- polarization functions. An estimation of intermolecular interaction in geometrical parameters, electron density function both between interacting particles and inside themselves, frequencies and intensities of normal modes has been carried out. Chemical bonds with the most significant shifts of characteristics under formation of nano-complex CCl4…Сr(АcacCl)3 have been noted.

为了明确分子间相互作用对相互作用物质红外光谱的影响,在具有p-和d-极化函数的MIDI基集上,采用Hartree-Fock-Roothaan方法研究了CCl4 + Сr(АcacCl)3→CCl4…Сr(АcacCl)3过程。对分子间相互作用的几何参数、相互作用粒子之间和相互作用粒子内部的电子密度函数、正常模式的频率和强度进行了估计。在纳米配合物CCl4…Сr(АcacCl)3的形成过程中,化学键的特征发生了最显著的变化。
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引用次数: 0
Weldability of Aluminium Alloys for Automotive Applications 汽车用铝合金的可焊性
Pub Date : 2017-01-01 DOI: 10.1016/j.phpro.2017.08.011
D. Löveborn, J.K. Larsson, K.-A. Persson

Restrictions in CO2-emissions have caused increased demands on decreased weight and increased use of lightweight materials in the automotive industry. Aluminium has shown to be of great interest due to its beneficial weight to strength ratio, and are suitable for hang-on parts such as roof, doors etc. However, the use of aluminium requires reliable joining techniques. This project has been focusing on laser welding of aluminium. It have been reported earlier that hot cracks and porosity are common defects while joining aluminium with laser welding. The aim with this project has been to produce crack free laser welds while joining thin aluminium sheets. Two different optics have been used in this project, oscillating- and triple-spot optics. The results from the experiments show that both the oscillating optics and the triple-spot optics can produce crack free welds. The amount of pores is shown to be low for both cases. The results do also show that the amount of pores in the welds increases with the weld length while the flange length is of minor impact. The mechanical properties are similar for the both optics. The oscillation specimens receive a higher tensile strength while the triple-spot specimens receive a larger elongation at break value.

对二氧化碳排放的限制导致汽车行业对减轻重量和增加使用轻质材料的需求增加。由于其有益的重量强度比,铝已显示出极大的兴趣,并且适用于悬挂部件,如屋顶,门等。然而,使用铝需要可靠的连接技术。本项目一直致力于铝的激光焊接。早前有报道称,热裂纹和气孔是铝激光焊接时常见的缺陷。该项目的目标是在连接薄铝板时生产无裂纹激光焊接。在这个项目中使用了两种不同的光学器件,振荡光学和三光斑光学。实验结果表明,振荡光学和三光斑光学都能产生无裂纹焊缝。在这两种情况下,气孔的数量都很低。结果还表明,焊缝气孔数量随焊缝长度的增加而增加,而法兰长度的影响较小。两种光学器件的机械性能相似。振荡试样具有较高的抗拉强度,而三点状试样具有较大的断裂伸长率。
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引用次数: 26
The Structure and Properties of the Samples Produced by Selective Laser Melting of 410L Steel-based Metal Powder 410L钢基金属粉末选择性激光熔化试样的组织和性能
Pub Date : 2017-01-01 DOI: 10.1016/j.phpro.2017.08.013
Artem Deev, Pavel Kuznetsov, Anton Zhukov, Vitaliy Bobyr

Additive technologies, which obtained the wide spreading in the last decade, allow producing items of any shape from metal materials practically without additional mechanical treatment. This approach based on the layer by layer melting of powder material accordingly to the premade 3D-CAD model, provides the geometrical accuracy which mostly depends on the size of the used material. In the present study, as material a 410 L steel powder was chosen, for which the basic dependencies between the selective laser melting (SLM) parameters and the mechanical properties were determined. Trial batches of standard samples for uniaxial tension and impact strength tests (according to the ASTM A370 and ASTM E8 M standards) were produced. It was shown that in the as build (after SLM) the fracture appeared to be brittle with the impact strength 3-5 J/cm2. The carried out heat treatment of quenching-tempering cycle and subsequent tests provide the viscous fracture and evaluation of impact strength up to 20-30 J/cm2. Presumably, this is due to a refinement of the grain structure and the inner stresses reduction of the samples, which also acknowledges the execution EBSD analysis, which points to the presence of quenched and tempered martensite. The presence of high inner stresses can be attributed to two α-γ-α transformations that were revealed by dilatometry investigation. In the range of cooling or heating rates from 1 to 500 °C/s temperatures of phase transformation are shifted.

增材制造技术在过去的十年中得到了广泛的推广,它允许用金属材料生产任何形状的物品,几乎不需要额外的机械处理。这种方法是根据预制的3D-CAD模型逐层熔化粉末材料,提供几何精度,主要取决于所用材料的尺寸。在本研究中,选择了410 L钢粉作为材料,确定了选择性激光熔化(SLM)参数与力学性能之间的基本依赖关系。按ASTM A370和ASTM E8 M标准生产了单轴拉伸和冲击强度试验标准样品。结果表明,在SLM后,断口呈脆性,冲击强度为3 ~ 5 J/cm2。所进行的调质循环热处理和随后的试验提供了高达20-30 J/cm2的粘性断裂和冲击强度评估。据推测,这是由于晶粒结构的细化和样品的内应力降低,这也承认执行EBSD分析,指出存在淬火和回火马氏体。高内应力的存在可归因于两个由膨胀测量法揭示的α-γ-α转变。在从1到500℃/s的冷却或加热速率范围内,相变温度发生了变化。
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引用次数: 6
Electrostatic Field Influence on Luminescence Features of Cadmium Sulphide Quantum Dots in Silica Matrix 静电场对二氧化硅基体中硫化镉量子点发光特性的影响
Pub Date : 2017-01-01 DOI: 10.1016/j.phpro.2017.01.004
S.S. Voznesenskiy , A.A. Sergeev , I.V. Postnova , Y.A. Shchipunov

The effect of electrostatic field on optical properties of silicate nanocomposite with cadmium sulfide quantum dots was investigated. It was found that the electrostatic field causes quantum dot orientation along the field force lines leading to changes in the polarized components of the luminescence spectrum. The influence of field force line direction on photoinduced absorption characteristics arised from λ = 405.9 nm laser radiation exposure to nanocomposite was shown.

研究了静电场对含硫化镉量子点硅酸盐纳米复合材料光学性能的影响。发现静电场使量子点沿场力线取向,导致发光光谱偏振分量的变化。研究了波长为λ = 405.9 nm的激光对纳米复合材料光致吸收特性的影响。
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引用次数: 2
Applications of Neutron Radiography for the Nuclear Power Industry 中子射线照相技术在核动力工业中的应用
Pub Date : 2017-01-01 DOI: 10.1016/j.phpro.2017.06.009
Aaron E. Craft , John P. Barton

The World Conference on Neutron Radiography (WCNR) and International Topical Meeting on Neutron Radiography (ITMNR) series have been running over 35 years. The most recent event, ITMNR-8, focused on industrial applications and was the first time this series was hosted in China. In China, more than twenty new nuclear power plants are under construction and plans have been announced to increase the nuclear capacity by a factor of three within fifteen years. There are additional prospects in many other nations. Neutron tests were vital during previous developments of materials and components for nuclear power applications, as reported in the WCNR and ITMNR conference series. For example a majority of the 140 papers in the Proceedings of the First WCNR are for the benefit of the nuclear power industry. Many of those techniques are being utilized and advanced to the present time. Neutron radiography of irradiated nuclear fuel provides more comprehensive information about the internal condition of irradiated nuclear fuel than any other non-destructive technique to date. Applications include examination of nuclear waste, nuclear fuels, cladding, control elements, and other critical components. In this paper, applications of neutron radiography techniques developed and applied internationally for the nuclear power industry since the earliest years are reviewed, and the question is asked whether neutron test techniques, in general, can be of value in development of the present and future generations of nuclear power plants world-wide.

世界中子放射学会议(WCNR)和国际中子放射学专题会议(ITMNR)系列已经运行了35年。最近的ITMNR-8专注于工业应用,这是该系列首次在中国举办。在中国,有20多座新的核电站正在建设中,并且已经宣布了在15年内将核能力增加3倍的计划。在许多其他国家也有更多的前景。正如WCNR和ITMNR系列会议所报告的那样,中子试验在核电应用材料和组件的先前开发过程中至关重要。例如,《第一届世界核反应堆会议录》(Proceedings of the First WCNR)上的140篇论文中,大多数都是为了核电工业的利益。其中许多技术正在被利用并发展到今天。辐照核燃料的中子射线照相比迄今为止任何其他非破坏性技术都能提供有关辐照核燃料内部状况的更全面的信息。应用包括检查核废料、核燃料、包层、控制元件和其他关键部件。本文回顾了自早期以来国际上开发和应用的中子射线照相技术在核电工业中的应用,并提出了中子试验技术在当今和未来几代世界范围内的核电站的发展中是否有价值的问题。
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引用次数: 23
Accelerated Learning: Undergraduate Research Experiences at the Texas A&M Cyclotron Institute 加速学习:本科生在德州农工大学回旋加速器研究所的研究经历
Pub Date : 2017-01-01 DOI: 10.1016/j.phpro.2017.09.029
S.J. Yennello

The Texas A&M Cyclotron Institute (TAMU CI) has had an NSF funded Research Experiences for Undergraduates program since 2004. Each summer about a dozen students from across the country join us for the 10-week program. They are each imbedded in one of the research groups of the TAMU CI and given their own research project. While the main focus of their effort is their individual research project, we also have other activities to broaden their experience. For instance, one of those activities has been involvement in a dedicated group experiment. Because not every experimental group will run during those 10 weeks and the fact that some of the students are in theory research groups, a group research experience allows everyone to actually be involved in an experiment using the accelerator. In stark contrast to the REU students’ very focused experience during the summer, Texas A&M undergraduates can be involved in research projects at the Cyclotron throughout the year, often for multiple years. This extended exposure enables Texas A&M students to have a learning experience that cannot be duplicated without a local accelerator. The motivation for the REU program was to share this accelerator experience with students who do not have that opportunity at their home institution.

德克萨斯A&M回旋加速器研究所(TAMU CI)自2004年以来一直有一个美国国家科学基金会资助的本科生研究经验项目。每年夏天,大约有十几名来自全国各地的学生参加我们为期10周的项目。他们每个人都加入了TAMU CI的一个研究小组,并有自己的研究项目。虽然他们努力的主要焦点是他们的个人研究项目,但我们也有其他活动来扩大他们的经验。例如,其中一项活动是参与一个专门的小组实验。因为不是每个实验小组都会在这10周内运行,事实上,一些学生在理论研究小组中,一个小组研究经验可以让每个人都实际参与到使用加速器的实验中。与REU学生在夏季非常专注的经历形成鲜明对比的是,德州农工大学的本科生全年都可以参与回旋加速器的研究项目,通常持续数年。这种扩展的接触使德州农工大学的学生获得了一种没有当地加速器无法复制的学习体验。REU项目的动机是与那些在自己的学校没有这种机会的学生分享这种加速器的经验。
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引用次数: 3
期刊
Physics Procedia
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