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Microwave-assisted fabrication of high-strength natural fiber hybrid composites for sustainable applications: An experimental and computational study 用于可持续应用的高强度天然纤维混合复合材料的微波辅助制造:实验与计算研究
IF 2.4 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-08-06 DOI: 10.1177/14644207241269567
Ravi Vijaykumar Sevak, Ramesh Gupta Burela, Gaurav Arora, Ankit Gupta
The present study deals with the fabrication of hybrid composites using biodegradable and ecologically friendly natural fibers and a recyclable thermoplastic matrix. Pure and hybrid natural fiber composites of high-density polyethylene (HDPE) with Kenaf and Ramie fiber, 20 wt%, were fabricated using microwave-assisted compression molding. The composite's mechanical characterization was performed using tensile, flexural, impact, and hardness tests. X-ray diffraction was done to investigate the crystallinity percentage, and scanning electron microscopy of fractured surfaces was performed to determine failure mechanisms. The hybrid composite of HDPE/Ramie and Kenaf exhibited the highest ultimate tensile strength (UTS) at 29.3 ± 1.2 MPa, surpassing HDPE/Kenaf (21.6 ± 1.1 MPa) and HDPE/Ramie (24.3 ± 1.4 MPa) composites. In terms of flexural strength, HDPE/Ramie demonstrated the highest at 19.9 ± 1.5 MPa, while HDPE/Kenaf had the lowest at 18 ± 1.1 MPa. The hybrid composite's flexural strength was intermediate at 19 ± 1.3 MPa. Impact strength followed a similar trend, with the hybrid composite leading at 40.2 KJ/m2, followed by HDPE/Ramie (26.9 KJ/m2) and HDPE/Kenaf (12.3 KJ/m2). Hardness tests revealed the highest hardness in the hybrid composite and the lowest in HDPE/Kenaf. A computational study has been performed to develop a model for predicting the hybrid composites. A strong agreement between both studies has been observed. The developed composite is deemed suitable for various light-duty applications, such as roofing, car interior panels, and mobile covers, offering potential benefits in reducing carbon footprint.
本研究涉及使用可生物降解的生态友好型天然纤维和可回收的热塑性基体制造混合复合材料。研究人员利用微波辅助压缩成型技术制造了纯天然纤维和混合天然纤维复合材料,高密度聚乙烯(HDPE)中含有 20 wt% 的 Kenaf 和苎麻纤维。使用拉伸、弯曲、冲击和硬度测试对复合材料进行了力学表征。通过 X 射线衍射研究了结晶度百分比,并对断裂表面进行了扫描电子显微镜观察,以确定失效机理。HDPE/Ramie 和 Kenaf 混合复合材料的极限拉伸强度(UTS)最高,为 29.3 ± 1.2 兆帕,超过了 HDPE/Kenaf(21.6 ± 1.1 兆帕)和 HDPE/Ramie(24.3 ± 1.4 兆帕)复合材料。在抗弯强度方面,高密度聚乙烯/拉米复合材料的抗弯强度最高,为 19.9 ± 1.5 兆帕,而高密度聚乙烯/槿麻的抗弯强度最低,为 18 ± 1.1 兆帕。混合复合材料的抗弯强度介于 19 ± 1.3 兆帕之间。冲击强度也呈类似趋势,混合复合材料的冲击强度最高,为 40.2 KJ/m2,其次是 HDPE/Ramie(26.9 KJ/m2)和 HDPE/Kenaf(12.3 KJ/m2)。硬度测试表明,混合复合材料的硬度最高,而 HDPE/Kenaf 的硬度最低。为了建立预测混合复合材料的模型,还进行了计算研究。结果表明,这两项研究结果非常吻合。所开发的复合材料被认为适用于各种轻型应用,如屋顶、汽车内饰板和手机套,在减少碳足迹方面具有潜在优势。
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引用次数: 0
A comparative study on mechanical properties between linear and zigzag pattern holes reinforced with tialite particles during FSW of AA6082 alloy 在 AA6082 合金的 FSW 过程中,对用泰利特颗粒加固的线形孔和人字形孔的机械性能进行比较研究
IF 2.4 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-08-06 DOI: 10.1177/14644207241269598
GN Shiva Kumar, G Raja murugan
In this study, a comparison between linear and zigzag patterned holes is carried out where the holes in the pattern are incorporated with tialite/aluminium titanate (Al2TiO5) particles at the weldment region during friction stir welding of AA6082-T6 aluminium alloy. Different values of tool rotational speed (TRS: 1000, 1200 and 1400 rpm) and welding speed (WS: 35, 40 and 45 mm/min) are considered for the fabrication of joints by both patterns. Visually, no defects are found in all the welded samples. Microstructural analysis has proven that the uniform distribution of particles along the weld region can be obtained by using a zigzag pattern. Maximum hardness is found in the stir zone (SZ), whereas minimum hardness is found in the heat-affected zone (HAZ) for all the samples. The maximum ultimate tensile strength (UTS: 268 MPa), maximum yield strength (YS: 200 MPa) and relatively higher elongation (EL: 7.89%) are exhibited by the Z5 sample, whereas minimum UTS (206 MPa) and minimum YS (142 MPa) was exhibited by L3 and Z7 samples, respectively.
在本研究中,对线形和人字形图案孔进行了比较,在 AA6082-T6 铝合金的搅拌摩擦焊接过程中,在图案孔中的焊接区域加入了钛酸铝(Al2TiO5)颗粒。在使用这两种图案焊接时,考虑了不同的工具转速(TRS:1000、1200 和 1400 rpm)和焊接速度(WS:35、40 和 45 mm/min)。从外观上看,所有焊接样品均未发现缺陷。微观结构分析表明,采用人字形模式可以获得沿焊接区域均匀分布的颗粒。所有样品的最大硬度都出现在搅拌区(SZ),而最小硬度则出现在热影响区(HAZ)。Z5 样品显示出最大极限拉伸强度(UTS:268 兆帕)、最大屈服强度(YS:200 兆帕)和相对较高的伸长率(EL:7.89%),而 L3 和 Z7 样品分别显示出最小极限拉伸强度(206 兆帕)和最小屈服强度(142 兆帕)。
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引用次数: 0
Investigation of open air and under water laser surface texturing on surface roughness and wettability of Al-Mg alloy 露天和水下激光表面纹理加工对铝镁合金表面粗糙度和润湿性的影响研究
IF 2.4 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-08-06 DOI: 10.1177/14644207241269652
Prashant Kaushik, Shashi Prakash
Aluminum-Magnesium (Al-Mg) alloy is widely used in aerospace and marine related applications due to its high corrosion resistance, tensile strength and ductility properties. However, due to hydrophilic nature, its applications are restricted in areas where water absorption may cause problems like corrosion. In this research work, high speed laser texturing was carried out on Al-Mg alloy (AA5754) to improve hydrophobic properties of the material surface. Four different types of pattern, namely lines, grids, concentric circles and concentric rectangles were created on the material surface using a nanosecond fiber laser. Scanning speed was varied at two levels i.e., 500 mm/s and 1000 mm/s. Line density of texture designs was also varied at two levels of 10 lines per mm and 15 lines per mm. The texturing process was carried out in two different processing environment namely open air and in underwater condition. Distilled water with 1 mm thickness above the surface was used during underwater texturing condition. Surface morphology, surface roughness and wettability of all the surfaces were studied for all the experimental conditions. It was observed that lower scanning speed of 500 mm/s resulted in higher values of surface roughness and contact angles. Also, larger texture density leads to lower surface roughness and contact angles for all the pattern designs. Among all the studied texture patterns, grid structures, textured at 500 mm/s of scanning speed resulted in largest surface roughness and surface hydrophobicity.
铝镁合金(Al-Mg)具有高耐腐蚀性、抗拉强度和延展性,因此被广泛应用于航空航天和海洋相关领域。然而,由于其亲水性,在吸水可能导致腐蚀等问题的领域,铝镁合金的应用受到了限制。在这项研究工作中,对铝镁合金(AA5754)进行了高速激光纹理加工,以改善材料表面的疏水性。使用纳秒光纤激光器在材料表面制作了四种不同类型的图案,即线条、网格、同心圆和同心矩形。扫描速度分为两个等级,即 500 毫米/秒和 1000 毫米/秒。纹理设计的线条密度也在每毫米 10 条和每毫米 15 条两个水平上变化。纹理加工在两种不同的加工环境中进行,即露天和水下条件。在水下纹理加工条件下,使用的是比表面厚 1 毫米的蒸馏水。在所有实验条件下,对所有表面的表面形态、表面粗糙度和润湿性进行了研究。结果表明,扫描速度越低(500 毫米/秒),表面粗糙度和接触角值越高。此外,纹理密度越大,所有图案设计的表面粗糙度和接触角越低。在所有研究的纹理图案中,以 500 毫米/秒的扫描速度纹理的网格结构的表面粗糙度和表面疏水性最大。
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引用次数: 0
Assessment of biodegradability and biocompatibility: An experimental and comparative analysis of magnesium and magnesium-(zinc-tin)/hydroxyapatite composites 生物降解性和生物相容性评估:镁和镁-(锌-锡)/羟基磷灰石复合材料的实验和比较分析
IF 2.4 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-08-05 DOI: 10.1177/14644207241270799
Chandrahasa Chowdeswarihalli Narayanappa, Beemkumar Nagappan, P Vignesh, Arunkumar Thirugnanasambandam
This study presents the fabrication and comparative assessment of biodegradation and biocompatibility behaviors of pure Mg, Mg/HA (Hydroxyapatite), Mg-Zn/HA, and Mg-Sn/HA composites with fixed 5 wt% HA and 1 wt% each of Zn and Sn, using novel ultrasonic-assisted rheo casting technology. Characterization techniques, including X-ray diffractometry and scanning electron microscopy integrated with energy dispersive spectroscopy, were employed to analyze phase formation, surface morphology, and elemental composition. Microhardness tests were conducted to assess indentation resistance, while in vitro corrosion performance was evaluated in simulated bodily fluid to compare degradation behavior. Results indicate a uniform distribution of reinforced particles within the matrix with minimal casting defects. Intermetallic phases MgZn and Mg2Sn precipitated along grain boundaries in Mg-Zn/HA and Mg-Sn/HA composites. The Mg-Sn/HA composite exhibited peak microhardness (94.8 HV) due to precipitation strengthening. In contrast, Mg-Zn/HA samples showed a low degradation rate (0.19 mm/yr) and H2 gas evolution rate (0.035 ml/mm2), attributed to uniform distribution of secondary phases and fine grains that mitigate galvanic cell formation and control degradation. Cell viability assay results demonstrated that Mg-Zn/HA composite outperformed all other samples, showing a 94% relative cell growth rate of osteosarcoma MG-63 cells after 2 h of incubation, attributed to strong apatite formation (rich in Ca and P) on the surface post-immersion, promoting cell proliferation.
本研究采用新型超声波辅助流变铸造技术,制备了纯镁、镁/HA(羟基磷灰石)、镁-锌/HA 和镁-锌/HA 复合材料,并对其生物降解和生物相容性行为进行了比较评估。表征技术包括 X 射线衍射仪、扫描电子显微镜和能量色散光谱仪,用于分析相的形成、表面形态和元素组成。此外,还进行了微硬度测试以评估抗压痕性能,并在模拟体液中对体外腐蚀性能进行了评估,以比较降解行为。结果表明,强化颗粒在基体中分布均匀,铸造缺陷极少。在 Mg-Zn/HA 和 Mg-Sn/HA 复合材料中,金属间相 MgZn 和 Mg2Sn 沿晶界析出。由于析出强化作用,Mg-Sn/HA 复合材料显示出峰值显微硬度(94.8 HV)。相比之下,Mg-Zn/HA 样品的降解率(0.19 mm/yr)和 H2 气体进化率(0.035 ml/mm2)较低,这归因于均匀分布的次生相和细小晶粒缓解了电化细胞的形成并控制了降解。细胞活力检测结果表明,Mg-Zn/HA 复合材料的性能优于所有其他样品,在培养 2 小时后,骨肉瘤 MG-63 细胞的相对细胞生长率达到 94%,这归因于浸泡后表面形成了大量磷灰石(富含 Ca 和 P),促进了细胞增殖。
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引用次数: 0
Induction heating simulation for aircraft RTM toolings 飞机 RTM 模具感应加热模拟
IF 2.4 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-08-05 DOI: 10.1177/14644207241270761
L Brieskorn, M Rahman
Aircraft CFRP parts as sharklets are produced in resin transfer molding (RTM) tooling. The parts need to be heated up homogenously over the whole area with a constant temperature. The complex shape and accessibility of the tooling make it hard to introduce a common heating system. In addition, the heat must be transferred through the Invar metal tooling structure onto the CFRP. Infrared lamp, air fan and microwave heating are concepts in development. Electrical heating layer mats and cages are laborious in applying. Induction has the advantage of contact-less, efficient, and fast heating. Induction heating was tested for the structural bonding of CFRP frames and stringers showing high bonding strengths. To apply this technology for the RTM tooling, the placement and distance of the induction coils is important. Simulation can help to find the right adjustments and power needed for induction heating. With the program COMSOL the surface and the coils are modeled, and the numerically structured net is divided in small tetrahedron and quadratic sub elements. Since there is no magnetic streamline in the middle of the coil-section, a symmetric halving of the structure is applied as a boundary condition. The temperature-time development and the distance of the coils are simulated in 2D and 3D. Due to the material properties of the magnetic flux concentrator (MFC), higher flux concentration of the magnetic field occurred only in 2D. The results are validated by experiments and are in good agreement.
飞机 CFRP 部件(如鲨鱼小翼)是用树脂传递模塑(RTM)模具生产的。部件需要在整个区域以恒定的温度均匀加热。由于模具形状复杂且易于接近,因此很难采用通用的加热系统。此外,热量必须通过因瓦金属模具结构传递到 CFRP 上。红外线灯、风扇和微波加热是正在开发的概念。电加热层垫和电加热笼的应用非常费力。感应加热具有无接触、高效和快速的优点。对 CFRP 框架和弦杆的结构粘接进行了感应加热测试,结果显示粘接强度很高。要将这项技术应用于 RTM 工具,感应线圈的位置和距离非常重要。模拟可以帮助找到感应加热所需的正确调整和功率。利用 COMSOL 程序对表面和线圈进行建模,并将数值结构网划分为小四面体和二次子元素。由于线圈截面中间没有磁流线,因此采用对称减半结构作为边界条件。温度-时间发展和线圈距离分别以二维和三维方式进行模拟。由于磁通量集中器(MFC)的材料特性,只有在二维情况下才会出现较高的磁通量集中。实验对结果进行了验证,结果非常吻合。
{"title":"Induction heating simulation for aircraft RTM toolings","authors":"L Brieskorn, M Rahman","doi":"10.1177/14644207241270761","DOIUrl":"https://doi.org/10.1177/14644207241270761","url":null,"abstract":"Aircraft CFRP parts as sharklets are produced in resin transfer molding (RTM) tooling. The parts need to be heated up homogenously over the whole area with a constant temperature. The complex shape and accessibility of the tooling make it hard to introduce a common heating system. In addition, the heat must be transferred through the Invar metal tooling structure onto the CFRP. Infrared lamp, air fan and microwave heating are concepts in development. Electrical heating layer mats and cages are laborious in applying. Induction has the advantage of contact-less, efficient, and fast heating. Induction heating was tested for the structural bonding of CFRP frames and stringers showing high bonding strengths. To apply this technology for the RTM tooling, the placement and distance of the induction coils is important. Simulation can help to find the right adjustments and power needed for induction heating. With the program COMSOL the surface and the coils are modeled, and the numerically structured net is divided in small tetrahedron and quadratic sub elements. Since there is no magnetic streamline in the middle of the coil-section, a symmetric halving of the structure is applied as a boundary condition. The temperature-time development and the distance of the coils are simulated in 2D and 3D. Due to the material properties of the magnetic flux concentrator (MFC), higher flux concentration of the magnetic field occurred only in 2D. The results are validated by experiments and are in good agreement.","PeriodicalId":20630,"journal":{"name":"Proceedings of the Institution of Mechanical Engineers, Part L: Journal of Materials: Design and Applications","volume":"46 1","pages":""},"PeriodicalIF":2.4,"publicationDate":"2024-08-05","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"141929913","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Characterization and erosion wear behavior of Ni-13%WC8Co microwave clad on AISI-316 steel 微波包覆 AISI-316 钢的 Ni-13%WC8Co 表征和侵蚀磨损行为
IF 2.4 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-08-02 DOI: 10.1177/14644207241266661
Manavendra Mishra, SB Mishra, DK Shukla
A microwave hybrid heating technique was used to develop a protective composite cladding of Ni-13%WC8Co over AISI-316 stainless steel. The metallurgical and mechanical characterizations were done using XRD, SEM, EDS, and Vickers microhardness testers. The erosion wear was assessed at impact angles of 30°, 45°, 60°, and 90° and a velocity of 40 m/s. The dilution of clad material with steel resulted in good metallurgical bonding between the two. The SEM images have shown the hard cemented carbides within the soft nickel matrix. The diffraction pattern indicated the formation of WC, NiW, FeNi3, Co2C, and Co3W3C2 phases. Ni-13%WC8Co clad has a microhardness value of 1000.8 HV and a four times lower erosion rate than AISI-316 stainless steel. The craters, scratches and plowing marks are observed on the eroded clad surface. The erosion wear mechanism of Ni-WC-Co clad was mixed ductile-brittle, with an overall lower erosion rate.
采用微波混合加热技术,在 AISI-316 不锈钢上形成了镍-13%WC8Co 的保护性复合包层。采用 XRD、SEM、EDS 和维氏硬度测试仪进行了冶金和机械表征。在冲击角为 30°、45°、60° 和 90°、速度为 40 米/秒的条件下对侵蚀磨损进行了评估。将包覆材料与钢稀释后,两者之间形成了良好的冶金结合。扫描电子显微镜图像显示了软镍基体中的硬质合成碳化物。衍射图样显示形成了 WC、NiW、FeNi3、Co2C 和 Co3W3C2 相。Ni-13%WC8Co 复合材料的显微硬度值为 1000.8 HV,侵蚀率比 AISI-316 不锈钢低四倍。在被侵蚀的堆焊表面上可以观察到凹坑、划痕和犁痕。Ni-WC-Co 复合材料的侵蚀磨损机制为韧性-脆性混合,侵蚀率总体较低。
{"title":"Characterization and erosion wear behavior of Ni-13%WC8Co microwave clad on AISI-316 steel","authors":"Manavendra Mishra, SB Mishra, DK Shukla","doi":"10.1177/14644207241266661","DOIUrl":"https://doi.org/10.1177/14644207241266661","url":null,"abstract":"A microwave hybrid heating technique was used to develop a protective composite cladding of Ni-13%WC8Co over AISI-316 stainless steel. The metallurgical and mechanical characterizations were done using XRD, SEM, EDS, and Vickers microhardness testers. The erosion wear was assessed at impact angles of 30°, 45°, 60°, and 90° and a velocity of 40 m/s. The dilution of clad material with steel resulted in good metallurgical bonding between the two. The SEM images have shown the hard cemented carbides within the soft nickel matrix. The diffraction pattern indicated the formation of WC, NiW, FeNi<jats:sub>3</jats:sub>, Co<jats:sub>2</jats:sub>C, and Co<jats:sub>3</jats:sub>W<jats:sub>3</jats:sub>C<jats:sub>2</jats:sub> phases. Ni-13%WC8Co clad has a microhardness value of 1000.8 HV and a four times lower erosion rate than AISI-316 stainless steel. The craters, scratches and plowing marks are observed on the eroded clad surface. The erosion wear mechanism of Ni-WC-Co clad was mixed ductile-brittle, with an overall lower erosion rate.","PeriodicalId":20630,"journal":{"name":"Proceedings of the Institution of Mechanical Engineers, Part L: Journal of Materials: Design and Applications","volume":"19 1","pages":""},"PeriodicalIF":2.4,"publicationDate":"2024-08-02","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"141887148","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Flutter behavior of quadrilateral auxetic core sandwich plate with bio-inspired three-phase composite facings numerical analysis and experimental verification 带有生物启发三相复合材料面层的四边形辅助夹芯夹层板的扑翼行为数值分析与实验验证
IF 2.4 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-08-02 DOI: 10.1177/14644207241265465
Vinay Kumar Prajapati, Jeyaraj Pitchaimani
Flutter characteristics of auxetic core quadrilateral sandwich plates with three-phase bio-inspired laminated composite facings are presented. The core is made of aluminum, while the facings are made of graphene nanoplatelets dispersed in bio-inspired glass fiber/epoxy laminates. The equations of motion are obtained using Reissner-Mindlin plate theory and Hamilton’s approach and then solved with the help of differential quadrature method. Experimental verification of free vibration is done for isotropic and hexagonal honeycomb core sandwich panels. Influences of core parameters (aspect ratio, inclined angle, and thickness-to-width ratio), mass fraction of graphene nanoplatelets and fibers, various graphene nanoplatelet distribution patterns, the geometry and aspect ratio of the plate, and bio-inspired layup scheme of laminated facings on the flutter characteristic are explored. The critical aerodynamic pressure is not sensitive to the core parameters and the dispersion pattern of graphene nanoplatelets. Critical aerodynamic pressure of the panel increases significantly with increase in the mass fractions of fiber and graphene nanoplatelet. Furthermore, the increase in the plate angles results in reduced critical aerodynamic pressure. Facing laminate made of helicoidal type bio-inspired lay-up scheme with lower rotation angle enhances the critical aerodynamic pressure compared to the conventional uni-directional, cross-ply, and quasi-isotropic lay-ups.
本文介绍了带有三相生物启发层压复合材料面层的辅助磁芯四边形夹层板的扑翼特性。板芯由铝制成,板面由分散在生物启发玻璃纤维/环氧层压板中的石墨烯纳米片制成。利用 Reissner-Mindlin 板理论和 Hamilton 方法获得了运动方程,然后借助微分正交法进行了求解。对各向同性和六边形蜂窝芯夹层板的自由振动进行了实验验证。研究探讨了夹芯参数(长宽比、倾斜角和厚宽比)、石墨烯纳米片和纤维的质量分数、各种石墨烯纳米片分布模式、板的几何形状和长宽比以及层压面的生物启发分层方案对扑翼特性的影响。临界气动压力对核心参数和石墨烯纳米片的分散模式并不敏感。随着纤维和石墨烯纳米片质量分数的增加,面板的临界气动压力显著增加。此外,板角的增加也会降低临界空气动力压力。与传统的单向层压、交叉层压和准各向同性层压相比,采用旋转角度较小的螺旋型生物启发层压方案制成的面层板可提高临界空气动力压力。
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引用次数: 0
Interfacial microstructure and mechanical properties in diffusion bonded Inconel 718 to austenitic stainless-steel joints 扩散键合 Inconel 718 与奥氏体不锈钢接头的界面微观结构和机械性能
IF 2.4 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-08-02 DOI: 10.1177/14644207241269012
Salman Khan, Massab Junaid, Tauheed Shehbaz, Al-Badrawy Abo El-Nasr, Hafiz T Ali, Uzair Khaleeq Uz Zaman
Diffusion bonding (DB) of Inconel (IN718) with Austenitic Stainless Steel (SS-304L) was conducted by varying the bonding temperatures and times at 5 MPa of pressure under vacuum. The optimized joint interface was evaluated for its mechanical, nanomechanical, microstructural, and compositional analyses using shear and Vickers hardness tests, optical and scanning electron microscopy (OM & SEM) equipped with energy dispersive spectroscopy (EDS), X-ray diffraction (XRD) and nanoindentation. The results showed that the optimized bonding parameters for achieving a stable joint interface were 950 °C for 90 min of holding time. It was observed that the joint interface was comprised of NbC, Cr23C7, Fe2Nb, and δ-Ni3Nb. The maximum nanohardness of 3.5 GPa occurred in the joint interface which was 10% and 35% higher as compared to the base metals (BM) of IN718 and SS-304L, respectively. Lastly, maximum joint strength of 143 MPa was achieved with a joint efficiency of 37%.
在 5 兆帕真空压力下,通过改变粘接温度和时间,实现了铬镍铁合金(IN718)与奥氏体不锈钢(SS-304L)的扩散粘接(DB)。采用剪切和维氏硬度测试、配备能量色散光谱仪(EDS)的光学和扫描电子显微镜(OM & SEM)、X 射线衍射(XRD)和纳米压痕法对优化后的接合界面进行了机械、纳米机械、微观结构和成分分析评估。结果表明,实现稳定接合界面的优化接合参数为 950 °C、90 分钟保温时间。据观察,接合界面由 NbC、Cr23C7、Fe2Nb 和 δ-Ni3Nb 组成。接合界面的最大纳米硬度为 3.5 GPa,分别比 IN718 和 SS-304L 的贱金属 (BM) 高出 10%和 35%。最后,接头强度达到最大值 143 兆帕,接头效率为 37%。
{"title":"Interfacial microstructure and mechanical properties in diffusion bonded Inconel 718 to austenitic stainless-steel joints","authors":"Salman Khan, Massab Junaid, Tauheed Shehbaz, Al-Badrawy Abo El-Nasr, Hafiz T Ali, Uzair Khaleeq Uz Zaman","doi":"10.1177/14644207241269012","DOIUrl":"https://doi.org/10.1177/14644207241269012","url":null,"abstract":"Diffusion bonding (DB) of Inconel (IN718) with Austenitic Stainless Steel (SS-304L) was conducted by varying the bonding temperatures and times at 5 MPa of pressure under vacuum. The optimized joint interface was evaluated for its mechanical, nanomechanical, microstructural, and compositional analyses using shear and Vickers hardness tests, optical and scanning electron microscopy (OM &amp; SEM) equipped with energy dispersive spectroscopy (EDS), X-ray diffraction (XRD) and nanoindentation. The results showed that the optimized bonding parameters for achieving a stable joint interface were 950 °C for 90 min of holding time. It was observed that the joint interface was comprised of NbC, Cr<jats:sub>23</jats:sub>C<jats:sub>7</jats:sub>, Fe<jats:sub>2</jats:sub>Nb, and δ-Ni<jats:sub>3</jats:sub>Nb. The maximum nanohardness of 3.5 GPa occurred in the joint interface which was 10% and 35% higher as compared to the base metals (BM) of IN718 and SS-304L, respectively. Lastly, maximum joint strength of 143 MPa was achieved with a joint efficiency of 37%.","PeriodicalId":20630,"journal":{"name":"Proceedings of the Institution of Mechanical Engineers, Part L: Journal of Materials: Design and Applications","volume":"48 1","pages":""},"PeriodicalIF":2.4,"publicationDate":"2024-08-02","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"141883954","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Effect of various weld length ratios on the curvature and distortion of a double-side edge welded fin plate: A study using SYSWELD 不同焊缝长度比对双侧边缘焊接鳍板曲率和变形的影响:使用 SYSWELD 进行的研究
IF 2.4 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-08-02 DOI: 10.1177/14644207241268877
V Sudharsanam, C Sathiya Narayanan, B Shanmugarajan, L Prakash
In this study, finite element modelling (FEM) of gas metal arc welding on two edges of a fin plate was performed, using SYSWELD software. The fin plate material is SA 387 Gr. 12 Cl 2 and its size is 1200 mm × 50 mm × 6 mm. The weld length, L1 on the first edge of the plate was fixed as 400 mm. The weld length, L2 on the second edge was chosen so as to result in five distinct L2/L1 ratios namely 1.00, 1.25, 1.50, 1.75 and 2.00. FEM of welding on the two edges of the fin, one after the other was performed for each ratio and the results on weld distortion and curvature were studied. It was found that increasing the L2/L1 ratio results in higher offset of weld distortion caused by first weld and for L2/L1 = 1.4, the mid-span distortion becomes near-zero. However, the net curvature of first weld segment (L1) stays constant for all L2/L1 ratios. The FEM results, in respect of temperature, strain and distortion for the case of L2/L1 = 1.50 matched well with the corresponding results obtained experimentally, thereby confirming the accuracy of the FEM procedure.
本研究使用 SYSWELD 软件对鳍板两边缘的气体金属弧焊进行了有限元建模(FEM)。鳍板材料为 SA 387 Gr. 12 Cl 2,尺寸为 1200 mm × 50 mm × 6 mm。鳍板第一条边缘的焊接长度 L1 定为 400 毫米。第二边缘的焊接长度 L2 被选择为 5 个不同的 L2/L1 比率,即 1.00、1.25、1.50、1.75 和 2.00。针对每个比率对鳍片的两个边缘逐一进行了焊接有限元分析,并研究了焊接变形和曲率的结果。结果发现,L2/L1 比值越大,第一道焊缝造成的焊接变形偏移越大,当 L2/L1 = 1.4 时,跨中变形接近零。然而,在所有 L2/L1 比率下,第一条焊缝(L1)的净曲率保持不变。在 L2/L1 = 1.50 的情况下,温度、应变和变形方面的有限元分析结果与相应的实验结果非常吻合,从而证实了有限元分析程序的准确性。
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引用次数: 0
Nanoceramic particle reinforced high alloying Al-Zn-Mg-Cu composites 纳米陶瓷颗粒增强高合金化铝-锌-镁-铜复合材料
IF 2.4 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-08-02 DOI: 10.1177/14644207241269595
Hailong Cong, Zhen Zhang, Zefan Cheng, Haichao Li, Pei Wang, Wanting Sun
In the metal matrix composites (MMCs) reinforced with nanoparticles, the enhancement of composite performance is often closely associated with the types of nanoparticles. It is vital to explore the influences and differences of various nanoparticles on the microstructure evolution and mechanical properties of highly alloyed aluminum-based composites. This study is the first to employ hot pressing for preparing Al-Zn-Mg-Cu composite materials reinforced with SiC and Al2O3 nano-ceramic particles, respectively. By employing hot extrusion and T6 heat treatment techniques, a systematic investigation was conducted on the effects of the addition of nano-ceramic particles on the microstructure evolution and mechanical properties of the Al-Zn-Mg-Cu composites, and a comparative analysis was performed on the two types of composite materials. The experimental results demonstrated that the Mg atoms in the α-Al matrix were consumed by the addition of SiC/Al2O3 nano-ceramic particles, and thereby the grain size primary η’ (MgZn2) strengthening phase was refined, leading to an enhanced overall mechanical performance of the Al-Zn-Mg-Cu composite. In particular, the Mg2Si phase was generated by the addition of SiC nanoceramic particles, through the interfacial reactions, and thus with the synergistic effects of precipitation strengthening and Orowan strengthening, the ultimate compressive strength and compressibility of Al-Zn-Mg-Cu composite can be increased to 844 MPa and 27.5%, respectively. On the other hand, the addition of Al2O3 nanoceramic particles can bring about the formation of an oxygen-rich phase and refined precipitates at grain boundaries. Accordingly, the elongation is increased to 43.5% while a high ultimate compressive strength in the composites can be maintained. It is anticipated that nanoceramic particle-reinforced Al-based metal composites have significant potential for achieving both high strength and exceptional ductility for the application in the industry field.
在用纳米颗粒增强的金属基复合材料(MMC)中,复合材料性能的提高往往与纳米颗粒的种类密切相关。探索各种纳米粒子对高合金铝基复合材料微观结构演变和力学性能的影响和差异至关重要。本研究首次采用热压工艺制备了分别以 SiC 和 Al2O3 纳米陶瓷颗粒增强的 Al-Zn-Mg-Cu 复合材料。通过热挤压和 T6 热处理技术,系统研究了纳米陶瓷颗粒的添加对铝锌镁铜复合材料微观结构演变和力学性能的影响,并对两种复合材料进行了对比分析。实验结果表明,SiC/Al2O3 纳米陶瓷颗粒的加入消耗了 α-Al 基体中的镁原子,从而细化了晶粒尺寸初级 η'(MgZn2)强化相,提高了 Al-Zn-Mg-Cu 复合材料的整体力学性能。其中,SiC 纳米陶瓷颗粒的加入通过界面反应生成了 Mg2Si 相,在沉淀强化和奥罗旺强化的协同作用下,Al-Zn-Mg-Cu 复合材料的极限抗压强度和压缩性分别提高到了 844 兆帕和 27.5%。另一方面,Al2O3 纳米陶瓷颗粒的加入可在晶界形成富氧相和细化析出物。因此,复合材料的伸长率提高到 43.5%,同时还能保持较高的极限抗压强度。预计纳米陶瓷颗粒增强铝基金属复合材料在实现高强度和优异延展性方面具有巨大潜力,可应用于工业领域。
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Proceedings of the Institution of Mechanical Engineers, Part L: Journal of Materials: Design and Applications
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