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PROCEEDINGS OF THE INTERNATIONAL CONFERENCE ON ADVANCED MATERIALS WITH HIERARCHICAL STRUCTURE FOR NEW TECHNOLOGIES AND RELIABLE STRUCTURES 2019最新文献

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Tribological properties of copper-titanium polymetals obtained by the additive manufacturing 增材制造获得的铜钛多金属摩擦学性能
D. Gurianov, E. Khoroshko, A. Gusarova, A. Chumaevskii
The structure and tribological properties of polymetallic products from Cu-Ti system are investigated. The results of the work show that in the material obtained by successive deposition of titanium and copper filaments on the substrate, a complex structure is formed from a mixture of intermetallic phases with different composition. Friction tests show high tribological properties paired with a steel counterbody. Besides the hardened state associated with the presence of Cu4Ti intermetallic particles, the material of the samples is characterized by the plasticity preservation of the copper matrix, which increases the tribological properties of the finished product.
研究了Cu-Ti体系多金属制品的结构和摩擦学性能。研究结果表明,在基底上连续沉积钛和铜长丝得到的材料中,不同成分的金属间相混合形成了复杂的结构。摩擦试验表明,与钢衬体搭配具有较高的摩擦学性能。除了与Cu4Ti金属间颗粒的存在相关的硬化状态外,样品材料的特点是铜基体的塑性保存,这增加了成品的摩擦学性能。
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引用次数: 0
Risks of pollution of Arctic territories by oil and oil products 石油和石油产品污染北极地区的风险
M. Alekseeva, L. I. Svarovskaya, I. Yashchenko
A special place in the Arctic zone of Russia is occupied by the shelf of the Barents Sea. Russian official sources estimate the oil reserves of the Barents Sea at around 400 million tons of which only a quarter, about 100 million tons, is confirmed [1]. Industrial development of oil fields in the Arctic zone takes place in the most difficult conditions and requires the use of new unique technologies. Poor compliance with oil spill prevention measures has already led to large-scale environmental pollution in the Arctic zone of Russia. The cause of pollution is the operation of marine stationary platforms, accompanied by the construction of shore-based terminals, hydrocarbon storage facilities, offshore pipeline lay, drilling operations, and increased shipping.A special place in the Arctic zone of Russia is occupied by the shelf of the Barents Sea. Russian official sources estimate the oil reserves of the Barents Sea at around 400 million tons of which only a quarter, about 100 million tons, is confirmed [1]. Industrial development of oil fields in the Arctic zone takes place in the most difficult conditions and requires the use of new unique technologies. Poor compliance with oil spill prevention measures has already led to large-scale environmental pollution in the Arctic zone of Russia. The cause of pollution is the operation of marine stationary platforms, accompanied by the construction of shore-based terminals, hydrocarbon storage facilities, offshore pipeline lay, drilling operations, and increased shipping.
巴伦支海的大陆架占据了俄罗斯北极地区一个特殊的地方。俄罗斯官方资料估计巴伦支海的石油储量约为4亿吨,其中只有四分之一,约1亿吨得到确认[1]。北极地区油田的工业开发是在最困难的条件下进行的,需要使用新的独特技术。石油泄漏预防措施执行不力已经导致俄罗斯北极地区的大规模环境污染。造成污染的原因是海上固定平台的运行,伴随着岸上码头的建设、碳氢化合物储存设施、海上管道铺设、钻井作业和航运的增加。巴伦支海的大陆架占据了俄罗斯北极地区一个特殊的地方。俄罗斯官方资料估计巴伦支海的石油储量约为4亿吨,其中只有四分之一,约1亿吨得到确认[1]。北极地区油田的工业开发是在最困难的条件下进行的,需要使用新的独特技术。石油泄漏预防措施执行不力已经导致俄罗斯北极地区的大规模环境污染。造成污染的原因是海上固定平台的运行,伴随着岸上码头的建设、碳氢化合物储存设施、海上管道铺设、钻井作业和航运的增加。
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引用次数: 2
Strain rate effect on the deformation and fracture in different zones of friction stir welded aluminum 应变速率对铝搅拌摩擦焊不同区域变形和断裂的影响
R. Balokhonov, V. Romanova, M. Sergeev
Deformation and fracture of polycrystalline microstructures typical for different zones of friction stir welds are numerically investigated. A phenomenological physically-based dislocation model is used to describe the dynamic behavior of aluminum. The ordinary differential constitutive equation is solved to determine the model parameter for the Al6061-T6 alloy. Using this equation, two-dimensional calculations are carried out for aluminum specimens subjected to tension at different strain rates, with the polycrystalline microstructure observed in the nugget and thermo-mechanically affected zone on the advancing side of the weld being taken into account in an explicit form. Convergence of the numerical solution is proved. Fracture patterns are shown to depend on the strain rate.Deformation and fracture of polycrystalline microstructures typical for different zones of friction stir welds are numerically investigated. A phenomenological physically-based dislocation model is used to describe the dynamic behavior of aluminum. The ordinary differential constitutive equation is solved to determine the model parameter for the Al6061-T6 alloy. Using this equation, two-dimensional calculations are carried out for aluminum specimens subjected to tension at different strain rates, with the polycrystalline microstructure observed in the nugget and thermo-mechanically affected zone on the advancing side of the weld being taken into account in an explicit form. Convergence of the numerical solution is proved. Fracture patterns are shown to depend on the strain rate.
对搅拌摩擦焊不同区域典型多晶组织的变形和断裂进行了数值研究。采用基于现象学物理的位错模型来描述铝的动态行为。通过求解常微分本构方程,确定了Al6061-T6合金的模型参数。利用该方程对不同应变速率下受拉伸的铝试样进行二维计算,并以显式形式考虑焊缝推进侧熔核和热机械影响区中观察到的多晶显微组织。证明了数值解的收敛性。断裂模式取决于应变速率。对搅拌摩擦焊不同区域典型多晶组织的变形和断裂进行了数值研究。采用基于现象学物理的位错模型来描述铝的动态行为。通过求解常微分本构方程,确定了Al6061-T6合金的模型参数。利用该方程对不同应变速率下受拉伸的铝试样进行二维计算,并以显式形式考虑焊缝推进侧熔核和热机械影响区中观察到的多晶显微组织。证明了数值解的收敛性。断裂模式取决于应变速率。
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引用次数: 0
Thermobaric studies of multifunctional composition based on surfactants 基于表面活性剂的多功能组合物的热压研究
D. Filatov, E. A. Rozhdestvenskiy, L. Altunina
The multifunctional chemical composition based on surfactants and possessing both oil-driving and flow-diverting properties has been developed at the IPC SB RAS. The investigation of the physicochemical properties of the composition performed at 100°С at three pressure values 7.5, 9.5, and 12 MPa and three carbon dioxide concentrations 20, 40, and 60 mol % has revealed that the pattern of changes in physicochemical properties of the composition are almost the same as when the composition was thermostated without CO2. The low temperature composition has a low interfacial tension at the boundary with oil. The urea is partially hydrolyzed during the thermostating. The pH rises and initiates a hydrolysis of aluminum ions. Upon completion of the hydrolytic polycondensation reaction aluminum hydroxide sols are formed. The degree of urea hydrolysis decreases with increasing concentration of CO2 in the reactor. This occurs regardless of the time of thermostating, as with an increase in the concentration of the product of urea hydrolysis reaction—CO2, the equilibrium shifts towards the reverse reaction, that is, towards the formation of urea. Based on the studies performed, it can be concluded that the injection of a multifunctional chemical composition together with carbon dioxide into the reservoir can significantly enhance the oil recovery.The multifunctional chemical composition based on surfactants and possessing both oil-driving and flow-diverting properties has been developed at the IPC SB RAS. The investigation of the physicochemical properties of the composition performed at 100°С at three pressure values 7.5, 9.5, and 12 MPa and three carbon dioxide concentrations 20, 40, and 60 mol % has revealed that the pattern of changes in physicochemical properties of the composition are almost the same as when the composition was thermostated without CO2. The low temperature composition has a low interfacial tension at the boundary with oil. The urea is partially hydrolyzed during the thermostating. The pH rises and initiates a hydrolysis of aluminum ions. Upon completion of the hydrolytic polycondensation reaction aluminum hydroxide sols are formed. The degree of urea hydrolysis decreases with increasing concentration of CO2 in the reactor. This occurs regardless of the time of thermostating, as with an increase in the concentration of the pr...
以表面活性剂为基础,具有驱油和导流双重性能的多功能化学成分在IPC SB RAS得到了发展。在100°С下,在7.5、9.5和12 MPa的压力值和20、40和60 mol %的二氧化碳浓度下,对该组合物的理化性质进行了研究,结果表明,该组合物的理化性质的变化模式与不含CO2的热态组合物的变化模式几乎相同。低温组分在与油交界处具有较低的界面张力。在恒温过程中尿素被部分水解。pH值上升,引发铝离子的水解。水解缩聚反应完成后,形成氢氧化铝溶胶。尿素水解程度随反应器中CO2浓度的增加而降低。这与恒温时间无关,因为随着尿素水解反应产物- co2浓度的增加,平衡向逆反应方向转移,即向尿素的形成方向转移。根据所进行的研究,可以得出结论,将多功能化学成分与二氧化碳一起注入储层可以显着提高石油采收率。以表面活性剂为基础,具有驱油和导流双重性能的多功能化学成分在IPC SB RAS得到了发展。在100°С下,在7.5、9.5和12 MPa的压力值和20、40和60 mol %的二氧化碳浓度下,对该组合物的理化性质进行了研究,结果表明,该组合物的理化性质的变化模式与不含CO2的热态组合物的变化模式几乎相同。低温组分在与油交界处具有较低的界面张力。在恒温过程中尿素被部分水解。pH值上升,引发铝离子的水解。水解缩聚反应完成后,形成氢氧化铝溶胶。尿素水解程度随反应器中CO2浓度的增加而降低。这与恒温时间无关,就像pr浓度的增加一样。
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引用次数: 0
Fracture characteristics of titanium alloy samples obtained by electron beam additive manufacturing 电子束增材制造钛合金试样的断裂特征
K. Kalashnikov, K. Osipovich
In this work, the fracture features of a titanium alloy Ti-6Al-4V samples obtained using the electron beam wire-feed additive manufacturing have been investigated. Studies have shown that the main character of sample fracture is viscous, with an in-grained dimple rupture observed. The strongest samples are characterized by the absence of defects in the fracture structure. For some samples, there are pores with sufficiently large sizes. Sample tests show a low dependence of mechanical properties on the direction of the applied load. Mechanical properties of the whole series of samples vary within the range of 3 – 6 %.In this work, the fracture features of a titanium alloy Ti-6Al-4V samples obtained using the electron beam wire-feed additive manufacturing have been investigated. Studies have shown that the main character of sample fracture is viscous, with an in-grained dimple rupture observed. The strongest samples are characterized by the absence of defects in the fracture structure. For some samples, there are pores with sufficiently large sizes. Sample tests show a low dependence of mechanical properties on the direction of the applied load. Mechanical properties of the whole series of samples vary within the range of 3 – 6 %.
本文研究了采用电子束喂丝增材制造获得的Ti-6Al-4V钛合金试样的断裂特征。研究表明,试样断裂的主要特征是粘性断裂,并观察到晶内韧窝断裂。最强试样的特点是断口结构中没有缺陷。对于某些样品,存在足够大的孔隙。样品试验表明,机械性能对施加载荷方向的依赖性较低。整个系列样品的力学性能在3 - 6%的范围内变化。本文研究了采用电子束喂丝增材制造获得的Ti-6Al-4V钛合金试样的断裂特征。研究表明,试样断裂的主要特征是粘性断裂,并观察到晶内韧窝断裂。最强试样的特点是断口结构中没有缺陷。对于某些样品,存在足够大的孔隙。样品试验表明,机械性能对施加载荷方向的依赖性较低。整个系列样品的力学性能在3 - 6%的范围内变化。
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引用次数: 0
Influence of the phase composition of Al-Mg alloys on the propagation of deformation bands Al-Mg合金相组成对变形带扩展的影响
D. Yuzbekova, Y. Borisova, A. Mogucheva
The influence of phase composition on the manifestations of the Portevin–Le Chatelier effect was studied in Al-Mg alloys using the digital image correlation technique. The smooth deformation curves were observed for Al-3Mg and Al-4.57Mg-0.35Mn-0.2Sc-0.09Zr alloys, whereas type A serration can be distinguished on the deformation curve of Al-5.4Mg-0.52Mn-0.1Zr alloy. At the same time, both the smooth plastic deformation and the stress serration are related to the propagation of a deformation band. The band velocity and the band passed distance for investigated alloys were estimated.
采用数字图像相关技术研究了Al-Mg合金中相组成对波特文-勒夏特列效应表现的影响。Al-3Mg和Al-4.57Mg-0.35Mn-0.2Sc-0.09Zr合金的变形曲线较为光滑,而Al-5.4Mg-0.52Mn-0.1Zr合金的变形曲线呈现A型锯齿形。同时,光滑塑性变形和应力锯齿都与变形带的扩展有关。估计了所研究合金的能带速度和能带通过距离。
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引用次数: 0
Study of structural features of monolithic TiNi-based alloy to produce porous monolithic structures 制备多孔整体式镍基合金的结构特征研究
M. Kaftaranova, N. Artyukhova, S. Anikeev, A. Garin, A. Monogenov, V. Gunther
Structural features of TiNi-based alloys with different Ti contents in the B2 matrix phase were studied at the stage of production of a porous monolithic structure. It was shown that the main feature of the alloys is homogeneity of the structure formed, which enabled their use for production of a porous monolithic structure. The study showed the efficiency of additional mechanical grinding of the monolithic plate surface to provide a more developed surface. It was found that at the boundary of transition of the porous zone to the monolithic one, powder particles are sintered to a monolithic TiNi plate, and its structure does not show an increase in the concentration of particles of the secondary phases Ti2Ni and Ti4Ni2 (O, N, C) and softening of the structure formed.Structural features of TiNi-based alloys with different Ti contents in the B2 matrix phase were studied at the stage of production of a porous monolithic structure. It was shown that the main feature of the alloys is homogeneity of the structure formed, which enabled their use for production of a porous monolithic structure. The study showed the efficiency of additional mechanical grinding of the monolithic plate surface to provide a more developed surface. It was found that at the boundary of transition of the porous zone to the monolithic one, powder particles are sintered to a monolithic TiNi plate, and its structure does not show an increase in the concentration of particles of the secondary phases Ti2Ni and Ti4Ni2 (O, N, C) and softening of the structure formed.
研究了不同Ti含量的B2基体Ti基合金在制备多孔整体结构阶段的组织特征。结果表明,该合金的主要特征是形成的组织均匀性,这使其能够用于生产多孔整体结构。研究表明,单片表面附加机械磨削的效率可以提供一个更发达的表面。研究发现,在多孔区向整体区过渡的边界处,粉末颗粒烧结成整体TiNi板,其结构没有表现出二次相Ti2Ni和Ti4Ni2 (O, N, C)颗粒浓度的增加和所形成的结构的软化。研究了不同Ti含量的B2基体Ti基合金在制备多孔整体结构阶段的组织特征。结果表明,该合金的主要特征是形成的组织均匀性,这使其能够用于生产多孔整体结构。研究表明,单片表面附加机械磨削的效率可以提供一个更发达的表面。研究发现,在多孔区向整体区过渡的边界处,粉末颗粒烧结成整体TiNi板,其结构没有表现出二次相Ti2Ni和Ti4Ni2 (O, N, C)颗粒浓度的增加和所形成的结构的软化。
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引用次数: 0
Tensile behavior of friction stir welded Al-Mg-Si alloy
I. Vysotskiy, S. Malopheyev, S. Mironov, R. Kaibyshev
In this work, digital image correlation technique was applied to examine evolution of strain distribution during transverse tensile tests of friction stir welded (FSW) Al-Mg-Si alloy. Due to sharp thermal- as well as strain gradients inherent to FSW process, the microstructure distribution within the joints is usually heterogeneous and thus the mechanical response is expected to be not uniform. Indeed, the tensile strain was found to preferentially concentrate in a heat-affected zone, presumably due coarsening of strengthening precipitates in this microstructural region and the concomitant material softening. With subsequent tensile deformation, however, the strain also expanded to a relatively hard stir zone and this observation was attributed to a work hardening effect. Nevertheless, the tensile strain was shown to have highly localized character and this resulted in premature failure of the joints.In this work, digital image correlation technique was applied to examine evolution of strain distribution during transverse tensile tests of friction stir welded (FSW) Al-Mg-Si alloy. Due to sharp thermal- as well as strain gradients inherent to FSW process, the microstructure distribution within the joints is usually heterogeneous and thus the mechanical response is expected to be not uniform. Indeed, the tensile strain was found to preferentially concentrate in a heat-affected zone, presumably due coarsening of strengthening precipitates in this microstructural region and the concomitant material softening. With subsequent tensile deformation, however, the strain also expanded to a relatively hard stir zone and this observation was attributed to a work hardening effect. Nevertheless, the tensile strain was shown to have highly localized character and this resulted in premature failure of the joints.
本文采用数字图像相关技术,研究了搅拌摩擦焊接Al-Mg-Si合金横向拉伸试验中应变分布的演变规律。由于摩擦摩擦焊过程中固有的尖锐的热梯度和应变梯度,接头内的微观组织分布通常是不均匀的,因此预计力学响应不是均匀的。事实上,拉伸应变被发现优先集中在热影响区,可能是由于强化相在该显微组织区域的粗化和伴随的材料软化。然而,随着随后的拉伸变形,应变也扩展到相对坚硬的搅拌区,这一观察结果归因于加工硬化效应。然而,拉伸应变显示出高度局部化的特征,这导致了关节的过早失效。本文采用数字图像相关技术,研究了搅拌摩擦焊接Al-Mg-Si合金横向拉伸试验中应变分布的演变规律。由于摩擦摩擦焊过程中固有的尖锐的热梯度和应变梯度,接头内的微观组织分布通常是不均匀的,因此预计力学响应不是均匀的。事实上,拉伸应变被发现优先集中在热影响区,可能是由于强化相在该显微组织区域的粗化和伴随的材料软化。然而,随着随后的拉伸变形,应变也扩展到相对坚硬的搅拌区,这一观察结果归因于加工硬化效应。然而,拉伸应变显示出高度局部化的特征,这导致了关节的过早失效。
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引用次数: 0
Fracture incubation time and scale invariance of dynamic crack propagation in brittle solids 脆性固体中动态裂纹扩展的断裂孕育时间和尺度不变性
A. Grigoriev, E. Shilko
In the paper, we theoretically studied the dynamics of mode II crack propagation in brittle solids with taking into account the finite duration of incubation of local fracture. The study was carried out by computer simulation using the movable cellular automaton method. We analyzed the influence of the magnitude of fracture incubation time on the fulfillment of the scale-invariance condition of dynamic crack propagation. We proposed a definition of this condition in terms of fracture incubation time and introduced a new physically based criterion to classify structural levels of fracture in brittle materials.
本文从理论上研究了考虑局部断裂孕育时间有限的脆性固体中II型裂纹扩展动力学。采用可移动元胞自动机方法进行计算机仿真。分析了断裂孕育时间大小对满足动态裂纹扩展尺度不变条件的影响。我们从断裂孕育时间的角度提出了这一条件的定义,并引入了一种新的基于物理的标准来分类脆性材料的断裂结构水平。
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引用次数: 1
Structural-phase state of the Zr-Y-O layer in the Zr-Y-O/Si Al-N coating at long annealing using «in-situ» observation 原位观察Zr-Y-O/Si Al-N涂层长时间退火时Zr-Y-O层的结构相状态
M. Fedorischeva, A. Nikonenko, M. Kalashnikov, I. Bozhko, V. Sergeev
TEM research of the structure of the multilayered coatings consisting of the alternating Si-Al-N and Zr-Y-O layers an equal thickness was carried out. The Zr-Y-O layers in the Zr-Y-O / Si-Al-N multilayer coating have a columnar structure, the diameter of a column reaches 80 nm, the column height is about 1000 nm, which, in this case, corresponds to the thickness of the deposited layer. The structure of the Si-Al-N layers is amorphous. High temperature annealing at 900 °С for 20-120 min leads to a change in the structural-phase state. The untransformable t’ phase appears at a temperature of 900 °С after a 20 minute exposure, the grain size reaches its maximal value after a 70 minute exposure and does not change further.TEM research of the structure of the multilayered coatings consisting of the alternating Si-Al-N and Zr-Y-O layers an equal thickness was carried out. The Zr-Y-O layers in the Zr-Y-O / Si-Al-N multilayer coating have a columnar structure, the diameter of a column reaches 80 nm, the column height is about 1000 nm, which, in this case, corresponds to the thickness of the deposited layer. The structure of the Si-Al-N layers is amorphous. High temperature annealing at 900 °С for 20-120 min leads to a change in the structural-phase state. The untransformable t’ phase appears at a temperature of 900 °С after a 20 minute exposure, the grain size reaches its maximal value after a 70 minute exposure and does not change further.
用透射电镜对等厚度Si-Al-N和Zr-Y-O交替多层涂层的结构进行了研究。Zr-Y-O / Si-Al-N多层涂层中的Zr-Y-O层呈柱状结构,柱的直径达到80 nm,柱的高度约为1000 nm,对应沉积层的厚度。Si-Al-N层的结构是非晶态的。900°С温度下20-120 min的高温退火导致结构相态发生变化。暴露20分钟后,在900°С温度下出现不可转变的t′相,暴露70分钟后晶粒尺寸达到最大值,不再发生变化。用透射电镜对等厚度Si-Al-N和Zr-Y-O交替多层涂层的结构进行了研究。Zr-Y-O / Si-Al-N多层涂层中的Zr-Y-O层呈柱状结构,柱的直径达到80 nm,柱的高度约为1000 nm,对应沉积层的厚度。Si-Al-N层的结构是非晶态的。900°С温度下20-120 min的高温退火导致结构相态发生变化。暴露20分钟后,在900°С温度下出现不可转变的t′相,暴露70分钟后晶粒尺寸达到最大值,不再发生变化。
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引用次数: 0
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PROCEEDINGS OF THE INTERNATIONAL CONFERENCE ON ADVANCED MATERIALS WITH HIERARCHICAL STRUCTURE FOR NEW TECHNOLOGIES AND RELIABLE STRUCTURES 2019
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