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Screening Fitokimia Awal (Analisis Qualitative) Pada Daun Gambir (Uncaria Gambir Roxb) Asal Siguntur Muda
Pub Date : 2022-12-12 DOI: 10.24036/p.v11i3.114575
M. Melati, Hesty Parbuntari
— Gambir ( Uncaria gambir Roxb ) belongs to the family Rubiaceae and belongs to the genus Uncaria. Gambir is commonly used as traditional medicine by the surrounding community. This proves that gambir has secondary metabolite compounds. In this study, Phytochemical screening was conducted to determine the secondary metabolite compound contained in Uncaria gambir Roxb. The result of phytochemical screening showed that Uncaria gambir Roxb contain secondary metabolite of alkaloids, flavonoid, terpenoid and saponins, but do not contained steroid compound.
-甘茅属(Uncaria Gambir Roxb)属于茜草科,属于钩藤属。甘比尔通常被周围社区用作传统药物。这证明冈比亚具有次生代谢产物化合物。本研究通过植物化学筛选,确定了钩藤(Uncaria gambir Roxb)的次生代谢产物。植物化学筛选结果表明,钩藤含有生物碱、黄酮类、萜类和皂苷等次生代谢产物,不含甾类化合物。
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引用次数: 0
Analisis Proksimat Karbon Aktif Kulit Langsat
Pub Date : 2022-12-12 DOI: 10.24036/p.v11i3.116189
Annisa Nabila Rahma, Desy Kurniawati
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引用次数: 0
Pengaruh Pengadukan Pada Degradasi Methylene Blue Menggunakan Katalis ZnO Terdoping Cu 使用催化剂ZnO Terdoping Cu对甲基亚甲基的腐蚀作用
Pub Date : 2022-12-12 DOI: 10.24036/p.v11i3.115089
Nafika Nurullita, Rahadian Zainul
— Methylene blue is one of the heterocyclic synthetic dyes used in textile industry, but has a negative impact on water quality and the surrounding environment. This study aims to degrade methylene blue using the photocatalytic method. The catalyst used for degradation is nano ZnO doped Cu 10%. In this study, the degradation process applies sunlight using a hexagonal mobile reactor and the light intensity is a measured used a luxmeter. The degradation process was carried out with variation of stirring at 1500 rpm and without stirring at 1,2,3, and 4 hours. Degradation results were measured using UV-Vis spectrophotometer to see adsorption before and after degradation. Results of this study obtained that the degradation using stirring has a higher percentage of degradation than without stirring. The maximum percentage of degradation obtained in study was 64,4% with a stirring speed of 1500 rpm for 4 hours irradiation.
-亚甲基蓝是纺织工业中使用的杂环合成染料之一,但对水质和周围环境有负面影响。本研究旨在利用光催化方法降解亚甲基蓝。用于降解的催化剂是掺杂10% Cu的纳米ZnO。在这项研究中,降解过程使用六角形移动反应器施加阳光,光强度是使用luxmeter测量的。降解过程在1500 rpm转速下进行,在1、2、3和4小时不进行搅拌。用紫外可见分光光度计测定降解结果,观察降解前后的吸附情况。研究结果表明,使用搅拌的降解比不使用搅拌的降解率更高。在1500 rpm的搅拌速度下,辐照4小时,最大降解率为61.4%。
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引用次数: 0
Peningkatan Kemampuan Degradasi ZnO Terhadap Rhodamin B Dengan Impregnasinya Pada Karbon Aktif Dari Ampas Tebu 通过在甘蔗渣活性炭上浸渍氧化锌提高罗丹明 B 的降解能力
Pub Date : 2022-12-12 DOI: 10.24036/p.v11i3.115994
Winda Anisa, M. Khair
— Research has been carried out with the aim of knowing the characteristics of activated carbon made from bagasse waste to be used as a support for zinc oxide (ZnO) catalysts using the impregnation method and the ability of the catalyst to degrade Rhodamin B dyes. Activated carbon is impregnated with Zn(NO 3 ) 2 .6H 2 O with variations activated carbon 5%, 10%, 15%, 20%, and 25% to 15 gram mass of Zn(NO 3 ) 2 .6H 2 O. The impregnated KA/ZnO was then contacted with 10 ppm Rhodamine B dye with a degradation time of 120 minutes. The mass of KA/ZnO used was 25 mg, 50 mg and 75 mg. The FTIR (Fourier Transform Infra Red) results of the KA/ZnO catalyst show that Zn-O molecules have entered into the pores of the activated carbon marked by the appearance of absorption peaks at wavelengths of 426.28 cm-1, 419.52 cm-1, and 437.85 cm-1 . The results of UV-Vis spectrophotometer measurements obtained the highest degradation percentage of Rhodamin B dye, namely 88.23% at 10% KA/ZnO with a catalyst mass of 75 mg.
-研究的目的是了解由甘蔗渣废料制成的活性炭的特性,用浸渍法作为氧化锌催化剂的载体,以及催化剂降解罗丹明B染料的能力。将不同浓度的Zn(no3) 2.6 h2o浸渍活性炭,分别为5%、10%、15%、20%和25%至15 g Zn(no3) 2.6 h2o,然后将浸渍后的KA/ZnO与10 ppm罗丹明B染料接触,降解时间为120分钟。KA/ZnO用量分别为25 mg、50 mg和75 mg。KA/ZnO催化剂的FTIR(傅里叶变换红外光谱)结果表明,Zn-O分子进入了活性炭的孔隙,在426.28 cm-1、419.52 cm-1和437.85 cm-1波长处出现了吸收峰。紫外可见分光光度计测定结果表明,在KA/ZnO浓度为10%、催化剂质量为75 mg时,罗丹明B染料的降解率最高,为88.23%。
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引用次数: 0
Uji Fitokimia Ekstrak Metanol Bunga Tumbuhan Bunga Pagoda (Clerodendrum paniculatum L.)
Pub Date : 2022-12-12 DOI: 10.24036/p.v11i3.114971
Teuku Muhamad Khairudin, S. Etika, Melindra Mulia
— Research has been carried out on phytochemical screening on the flowers of the pagoda flower plant ( Clerodendrum paniculatum L.). This study aims to determine the content of secondary metabolites in the flowers of the pagoda flower plant. The secondary metabolites tested in this study were alkaloid, flavonoid, steroid, triterpenoid, and saponin. The results showed that the flowers of the pagoda flower plant ( Clerodendrum paniculatum L.) contained secondary metabolites, namely alkaloid, flavonoid, and saponin.
——开展宝塔花(Clerodendrum paniculatum L.)花的植物化学筛选研究。本研究旨在测定宝塔花中次生代谢产物的含量。本研究检测的次生代谢物有生物碱、类黄酮、类固醇、三萜和皂苷。结果表明,宝塔花中含有次生代谢产物,即生物碱、类黄酮和皂苷。
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引用次数: 0
Isolasi, Uji Fitokimia Dan Aktivitas Antibakteri Jamur Endofit Bunga Sambiloto (Andrographis Paniculata) 分离,植物化学测试和真菌抗菌活性为Sambiloto花(锥体Paniculata)
Pub Date : 2022-12-12 DOI: 10.24036/p.v11i3.116134
Rani Aulia Suhanah, Suryelita Thaher, Melindra Mulia
Endophytic fungi are microorganisms that live in plant tissues without harming the host plant. One of the plants that have potential as a host for endophytic fungi is the flower of the bitter plant (Andrographis paniculata) which contains secondary metabolites and has biological activity. The purpose of this study was to obtain fungal isolates and identify the content of secondary metabolites and antibacterial activity. The results of the isolation of endophytic fungi produced isolates of endophytic fungi with isolate code BS. Microscopic observation of BS isolates belonging to Chrysosporium spp. The results of the phytochemical test of the ethyl acetate extract were positive for terpenoid compounds marked with a pink color and the FTIR spectrum containing a dimethyl gem group. BS extract also could inhibit the growth of all test bacteria, namely E. coli and S. aureus at concentrations of 1%, 3%, and 5%.
内生真菌是生活在植物组织中而不伤害寄主植物的微生物。具有内生真菌寄主潜力的植物之一是苦植物(穿心莲)的花,它含有次生代谢物并具有生物活性。本研究的目的是获得真菌分离株,并鉴定其次生代谢物的含量和抗菌活性。对内生真菌进行分离,得到分离物代码为BS的内生真菌。对黄孢杆菌分离物的显微观察。乙酸乙酯提取物的植物化学检测结果显示,其萜类化合物呈粉红色,FTIR光谱显示含有二甲基宝石基团。BS提取物在1%、3%和5%浓度下均能抑制大肠杆菌和金黄色葡萄球菌的生长。
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引用次数: 0
Dedradasi Metilen Biru Secara Fotolisis Dengan Katalis Cdots Doping Au 蓝色Metilen的脱色与bdots Doping Au催化剂相辉映
Pub Date : 2022-12-12 DOI: 10.24036/p.v11i3.115918
S. Budiman, Hary Sanjaya, Isnaeni Isnaeni, Umar Kalmar Nizar, Edi Nasra
— The degradation of methylene blue was carried out by photolysis method with the help of a Cdots/Au catalyst. This study aims to determine the optimum concentration of dopen Au for Cdots and the optimum time for degradation of methylene blue with the help of a Cdots/Au catalyst. The photolysis method was carried out in a reactor equipped with 3 15 watt lamps with a UV wavelength of 254 nm. The absorption of methylene blue was measured using a spectrophotometerUV-Vis. The optimum Au dopen results were obtained at a concentration of 25 ppm with a degradation percentage of 39.94% and the optimum time for photolysis degradation was 6 hours of irradiation with a degradation percentage of 70.28%.
在Cdots/Au催化剂的帮助下,采用光解法对亚甲基蓝进行了降解。本研究旨在确定Cdots/Au催化剂降解亚甲基蓝的最佳浓度和最佳时间。光解法在配有3盏15瓦灯的反应器中进行,紫外波长为254 nm。用紫外-可见分光光度计测定亚甲基蓝的吸收率。在25 ppm的浓度下,Au的最佳降解率为39.94%;光照6 h的最佳光解降解时间为70.28%。
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引用次数: 0
Pengaruh Penambahan Gum Arab Terhadap Pembuatan Plastik Biodegradable dari Air Kelapa
Pub Date : 2022-12-12 DOI: 10.24036/p.v11i3.116214
Norma Wahyunita, Ananda Putra, Umar Kalmar Nizar, Fajriah Azra
— Plastic is a polymer that we use a lot in everyday life, but it has a bad impact on the environment because it is difficult to degrade in nature. Therefore, a study was carried out to make plastic that is more environmentally friendly, namelyplastic Biodegradable that utilizes bacterial cellulose from Acetobacter xylinum with old coconut water as a medium with the addition of a plasticizer in the form of Polyethylene Glycol (PEG) and the addition of gum arabic additives with variations in the mass of gum arabic, namely 0g , 1g, 3g, 5g and 7g. The bacterial cellulose plastic PEG gum arabic produced was characterized includingwater content, degree ofswelling,testtensile strength, elongation, elasticity, ability biodegradation, functional group analysis (FTIR) and crystallinity test (XRD). The results of testing the water content and degree of swelling on PEG gum arabic bacterial cellulose plastic, obtained plastic with the more mass of gum arabic added, the greater the percentage of water content and degree of swelling. The results of mechanical testing showed an increase in the value of tensile strength and elasticity along with the amount of gum arabic added but the elongation value decreased. In the biodegradation test, it was found that the more gum arabic which was added, the biodegradation ability increased. The analysis of the plastic functional groups showed that there were no new groups formed. Crystallinity analysis showed that the addition of gum arabic can reduce the percentage of crystallinity.
-塑料是一种聚合物,我们在日常生活中使用很多,但它对环境有不好的影响,因为它在自然界中很难降解。因此,我们进行了一项研究,以制造更环保的塑料,即生物可降解塑料,该塑料利用木醋杆菌的细菌纤维素和老椰子水为介质,加入聚乙二醇(PEG)形式的增塑剂和阿拉伯胶添加剂,阿拉伯胶的质量不同,分别为0克、1克、3克、5克和7克。对制备的细菌纤维素塑料PEG阿拉伯胶的含水量、溶胀度、试验拉伸强度、伸长率、弹性、生物降解能力、官能团分析(FTIR)和结晶度测试(XRD)进行了表征。结果对PEG阿拉伯胶细菌纤维素塑料的含水量和溶胀度进行了测试,得到的塑料中加入的阿拉伯胶质量越多,含水量百分比和溶胀度越大。力学试验结果表明,随着阿拉伯胶添加量的增加,材料的抗拉强度和弹性值有所增加,而延伸率有所下降。在生物降解试验中发现,阿拉伯胶的加入量越大,其生物降解能力越强。塑性官能团分析表明,未形成新的官能团。结晶度分析表明,阿拉伯胶的加入可以降低结晶度。
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引用次数: 0
Preparasi Poli Tanin Untuk Meningkatkan Efisiensi Dye-Sensitized Solar Cell (DSSC) Preparasi Poli Tanin untuk Meningkatkan Efisiensi Dye-Sensitized Solar Cell (DSSC)
Pub Date : 2022-12-12 DOI: 10.24036/p.v11i3.114985
Annisa Ade Putri, Hardeli Hardeli, Fajriah Azra, Minda Azhar
— DSSC ( Dye-Sensitized Solar Cell ) is a type of third-generation solar cell based on dye as a photon absorber that has been widely used. In this study, modifications were made to tannin dyes to increase double bonds. Modifications were also carried out on the semiconductor by means of TiO 2 -CuO doping. TiO 2 -CuO doping can reduce the energy gap thereby increasing the TiO 2 conductivity. The dyes were characterized using FTIR and GC-MS, while the TiO 2 -CuO doping was characterized using a UV-DRS Spectrophotometer. The results of FTIR characterization of poly tannin dyes have shown specific groups of polymerization of polytannin glutaraldehyde resin. The characterization of TiO 2 -CuO doping showed a decrease in the energy gap of 3,2 eV to 3,01 eV. The highest efficiency was produced at 90 minutes polymer time with a tannin monomer concentration of 0,4 M of 8,332%.
染料敏化太阳能电池(dye - sensitized Solar Cell, DSSC)是一种基于染料作为光子吸收剂的第三代太阳能电池,已得到广泛应用。在本研究中,对单宁染料进行了改性以增加双键。用tio2 -CuO掺杂的方法对半导体进行了修饰。tio2 -CuO掺杂可以减小能隙,从而提高tio2的电导率。用FTIR和GC-MS对染料进行了表征,用UV-DRS对tio2 -CuO掺杂进行了表征。对聚单宁染料的FTIR表征结果显示了聚单宁戊二醛树脂的特定聚合基团。tio2 -CuO掺杂表征表明,tio2 -CuO掺杂能隙从3.2 eV减小到3.1 eV。当单宁单体浓度为0.4 M时,聚合时间为90分钟,效率为8,332%。
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引用次数: 0
Pengaruh Kecepatan Pengadukan dan Waktu Kontak Terhadap Penyerapan Fenol Menggunakan Adsorben C-SinamalKaliks[4]Resorsinarena Hasil Sintesis Limbah Minyak Kayu Manis (Cinnamomum burmanii) 用C-SinamalKaliks合成废肉桂废液所产生的冲积速度和接触时间的影响
Pub Date : 2022-12-12 DOI: 10.24036/p.v11i3.115255
Dewi Kristina, S. Etika, Edi Nasra, Budhi Oktavia
— Phenol is included in hazardous waste so that its presence in the environment needs to be controlled. Phenol contamined water can cause liver damage, diarrhea, dark urine, and red blood cell breakdown. To overcome this environmental problem, the adsorption method can be applied using synthesized compounds such as C-CinnamalCalix[4]Resorcinarene (CCCR). CCCR is a derivative of Calix[4]Resorcinarene which can act as a host for cations, anions, and neutral molecules. It has a unique shape that has an active group, which can form hydrogen bonding with phenol solution. The purpose of this study was to determine the optimum conditions with variation in stirring speeds of 50, 100, 150, 200, and 250 rpm and contact times of 45, 60, 75, 105, and 150 minutes. Phenol was analyzed using a UV-Vis spectrophotometer (Specord 210). Adsorption phenol with CCCR obtained optimum conditions at stirring speeds of 200 rpm with an adsorption capacity of 2.016 mg/g and contact times of 60 minutes with an adsorption capacity of 2.079 mg/g.
-有害废物中含有苯酚,因此需要控制其在环境中的存在。被苯酚污染的水会导致肝损伤、腹泻、尿色变深和红细胞分解。为了克服这一环境问题,可以使用合成的化合物如C-CinnamalCalix[4]间苯二甲酸(CCCR)进行吸附。CCCR是杯状杯间苯二烯的衍生物,可以作为阳离子、阴离子和中性分子的宿主。它具有独特的形状,具有活性基团,可与苯酚溶液形成氢键。本研究的目的是确定搅拌速度为50、100、150、200和250 rpm,接触时间为45、60、75、105和150分钟时的最佳条件。用紫外可见分光光度计(Specord 210)分析苯酚。CCCR吸附苯酚的最佳条件为搅拌转速为200 rpm,吸附量为2.016 mg/g,接触时间为60 min,吸附量为2.079 mg/g。
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引用次数: 0
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Jurnal Periodic Jurusan Kimia UNP
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