首页 > 最新文献

STAR: Science & Technology of Archaeological Research最新文献

英文 中文
Methodologies for the investigation of corroded iron objects: examples from prehistoric sites in South-eastern Arabia and Western Iran 腐蚀铁器的调查方法:以阿拉伯东南部和伊朗西部的史前遗址为例
Pub Date : 2017-12-15 DOI: 10.1080/20548923.2018.1424304
I. Stepanov, L. Weeks, K. Franke, C. Cable, B. Overlaet, P. Magee, M. Händel, Yaaqoub Yousif Al Aali, Mansour Boraik Radwan, H. Zein
ABSTRACT Ancient iron objects from early Iron Age archaeological sites are almost always severely corroded, which can severely limit the possibilities for their archaeometallurgical analysis. In this paper, a range of corroded iron objects from different sites and regions of the ancient Near East are investigated with the purpose of developing an integrated scientific approach to the investigation of such materials, outlining the capabilities and major technical limitations of currently available techniques. Specific objectives of the research include: (1) Assessing the state of degradation of ancient ferrous objects in respect to the portion of remnant carburized areas preserved; (2) Identifying metallographic structures and evaluating the carbon content from the observation of remnant carburized areas; (3) Developing an understanding of the representativeness of remnant carburized areas in corroded ferrous samples; and (4) Exploring the validity and technical constraints of SEM-EDS analyses of slag inclusions in corroded iron artefacts for the determination of provenance. GRAPHICAL ABSTRACT
来自早期铁器时代考古遗址的古代铁器几乎总是被严重腐蚀,这严重限制了它们的考古冶金分析的可能性。本文对来自古代近东不同地点和地区的一系列锈蚀铁器进行了调查,目的是开发一种综合的科学方法来调查这些材料,概述了当前可用技术的能力和主要技术限制。研究的具体目标包括:(1)根据保存的残余渗碳区域的比例,评估古代含铁物体的降解状态;(2)通过观察残余渗碳区,识别金相组织,评价碳含量;(3)对腐蚀铁样品中残余渗碳区代表性的认识;(4)探讨腐蚀铁制品中矿渣夹杂物SEM-EDS分析的有效性和技术限制。图形抽象
{"title":"Methodologies for the investigation of corroded iron objects: examples from prehistoric sites in South-eastern Arabia and Western Iran","authors":"I. Stepanov, L. Weeks, K. Franke, C. Cable, B. Overlaet, P. Magee, M. Händel, Yaaqoub Yousif Al Aali, Mansour Boraik Radwan, H. Zein","doi":"10.1080/20548923.2018.1424304","DOIUrl":"https://doi.org/10.1080/20548923.2018.1424304","url":null,"abstract":"ABSTRACT Ancient iron objects from early Iron Age archaeological sites are almost always severely corroded, which can severely limit the possibilities for their archaeometallurgical analysis. In this paper, a range of corroded iron objects from different sites and regions of the ancient Near East are investigated with the purpose of developing an integrated scientific approach to the investigation of such materials, outlining the capabilities and major technical limitations of currently available techniques. Specific objectives of the research include: (1) Assessing the state of degradation of ancient ferrous objects in respect to the portion of remnant carburized areas preserved; (2) Identifying metallographic structures and evaluating the carbon content from the observation of remnant carburized areas; (3) Developing an understanding of the representativeness of remnant carburized areas in corroded ferrous samples; and (4) Exploring the validity and technical constraints of SEM-EDS analyses of slag inclusions in corroded iron artefacts for the determination of provenance. GRAPHICAL ABSTRACT","PeriodicalId":21858,"journal":{"name":"STAR: Science & Technology of Archaeological Research","volume":"99 1","pages":"270 - 284"},"PeriodicalIF":0.0,"publicationDate":"2017-12-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"85885547","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 7
Characterization of Zahari Zograph’s nave wall paintings in the church “The nativity of the virgin” of Rila Monastery (Bulgaria) by vibrational spectroscopy and SEM–EDX analysis 用振动光谱和SEM-EDX分析分析保加利亚里拉修道院教堂“圣母诞生”中殿壁画的特征
Pub Date : 2017-12-15 DOI: 10.1080/20548923.2018.1426274
D. Yancheva, S. Tapanov, E. Velcheva, B. Stamboliyska, Z. Glavcheva, S. Stoyanov, Nikifor Haralampiev, D. Fischer, A. Lederer
ABSTRACT An analytical study on the nave mural paintings of the church “The Nativity of the Virgin” of Rila monastery, Bulgaria, painted by Zahari Zograph was carried out. Vibrational spectroscopy was applied to identify the pigments and organic materials used in the mural paintings. To complement the spectral information, elemental composition of the samples was determined by SEM-EDX. The data showed that smalt with carbohydrate binder was applied for the blue background, green colour was executed by green earths and red-orange colour – by red lead. Azurite is the pigment used to paint the blue colour of the saints’ hoods. The mordant for gilding was prepared of drying oil, resin and siccative metal oxides as evidenced by SEM-EDX, ATR-FTIR and pyrolysis GC-MS analysis. The use of azurite is related to Zahari Zograph’s works as it was not found in any of the previously studied murals in the church painted by other artists.
摘要对保加利亚里拉修道院教堂中殿壁画《圣母诞生》进行分析研究,该壁画由扎哈里·佐格(Zahari Zograph)绘制。利用振动光谱法对壁画中使用的颜料和有机材料进行了鉴定。为了补充光谱信息,用SEM-EDX测定了样品的元素组成。数据表明,蓝色底色采用含碳水化合物粘结剂,绿色底色采用绿土,红橘色采用红铅。蓝铜矿是用来绘制圣徒头罩的蓝色的颜料。通过SEM-EDX、ATR-FTIR和热解GC-MS分析,确定了干燥油、树脂和干性金属氧化物作为烫金媒染剂。蓝铜矿的使用与Zahari Zograph的作品有关,因为在之前研究的其他艺术家绘制的教堂壁画中都没有发现蓝铜矿。
{"title":"Characterization of Zahari Zograph’s nave wall paintings in the church “The nativity of the virgin” of Rila Monastery (Bulgaria) by vibrational spectroscopy and SEM–EDX analysis","authors":"D. Yancheva, S. Tapanov, E. Velcheva, B. Stamboliyska, Z. Glavcheva, S. Stoyanov, Nikifor Haralampiev, D. Fischer, A. Lederer","doi":"10.1080/20548923.2018.1426274","DOIUrl":"https://doi.org/10.1080/20548923.2018.1426274","url":null,"abstract":"ABSTRACT An analytical study on the nave mural paintings of the church “The Nativity of the Virgin” of Rila monastery, Bulgaria, painted by Zahari Zograph was carried out. Vibrational spectroscopy was applied to identify the pigments and organic materials used in the mural paintings. To complement the spectral information, elemental composition of the samples was determined by SEM-EDX. The data showed that smalt with carbohydrate binder was applied for the blue background, green colour was executed by green earths and red-orange colour – by red lead. Azurite is the pigment used to paint the blue colour of the saints’ hoods. The mordant for gilding was prepared of drying oil, resin and siccative metal oxides as evidenced by SEM-EDX, ATR-FTIR and pyrolysis GC-MS analysis. The use of azurite is related to Zahari Zograph’s works as it was not found in any of the previously studied murals in the church painted by other artists.","PeriodicalId":21858,"journal":{"name":"STAR: Science & Technology of Archaeological Research","volume":"53 1","pages":"437 - 449"},"PeriodicalIF":0.0,"publicationDate":"2017-12-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"84417366","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 4
Analysis of a gilded silver sheeted bridle from Hungary – preliminary results 匈牙利镀金银片马勒的分析——初步结果
Pub Date : 2017-12-15 DOI: 10.1080/20548923.2018.1429522
Réka Ágnes Piros
ABSTRACT In this paper, I introduce the preliminary results of the archaeometrical investigation of fourth to fifth century AD harnesses of the Vor- und Frühgeschichte Museum in Berlin. The assemblage was originated from Hungary and included a pair of axe-shaped bronze/copper pendant from the bridle, covered with pressed, gilded silver plaque, as well as one piece of spoke-shaped horse bit with the similar type of ornamentation. This material was the subject of our investigation, focused on the way of the ornamentation, which can bring us closer to the problem of approximate determination of the analogies, provenance and the cultural effects that might have had an influence on the objects. To find out, we carried out a non-destructive element analysis with a Bruker’s XRF Tracer. According to the first results, some new information is available and a few earlier opinions can be refined.
本文介绍了柏林vorund fr geschichte博物馆对公元4世纪至5世纪马具的考古调查的初步结果。这个组合来自匈牙利,包括一对斧头形的青铜/铜吊坠,上面覆盖着镀金的银匾,以及一块带有类似装饰的辐条形马嚼子。这些材料是我们调查的主题,重点是装饰的方式,这可以让我们更接近近似确定类比、来源和可能对这些物品产生影响的文化影响的问题。为了找到答案,我们用布鲁克的XRF示踪剂进行了非破坏性元素分析。根据最初的结果,可以获得一些新的信息,并且可以改进一些先前的意见。
{"title":"Analysis of a gilded silver sheeted bridle from Hungary – preliminary results","authors":"Réka Ágnes Piros","doi":"10.1080/20548923.2018.1429522","DOIUrl":"https://doi.org/10.1080/20548923.2018.1429522","url":null,"abstract":"ABSTRACT In this paper, I introduce the preliminary results of the archaeometrical investigation of fourth to fifth century AD harnesses of the Vor- und Frühgeschichte Museum in Berlin. The assemblage was originated from Hungary and included a pair of axe-shaped bronze/copper pendant from the bridle, covered with pressed, gilded silver plaque, as well as one piece of spoke-shaped horse bit with the similar type of ornamentation. This material was the subject of our investigation, focused on the way of the ornamentation, which can bring us closer to the problem of approximate determination of the analogies, provenance and the cultural effects that might have had an influence on the objects. To find out, we carried out a non-destructive element analysis with a Bruker’s XRF Tracer. According to the first results, some new information is available and a few earlier opinions can be refined.","PeriodicalId":21858,"journal":{"name":"STAR: Science & Technology of Archaeological Research","volume":"40 1","pages":"253 - 257"},"PeriodicalIF":0.0,"publicationDate":"2017-12-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"78862084","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 1
An Archaic metallurgical workshop in Thasos (Greece): the case of Charitopoulos plot 萨索斯(希腊)的一个古代冶金车间:Charitopoulos情节的案例
Pub Date : 2017-12-15 DOI: 10.1080/20548923.2017.1419659
N. Nerantzis, G. Sanidas, Benjamin Jagou, T. Kozelj, Konstantina Panoussi
ABSTRACT An important archaeometallurgical context dating to the Archaic period (700-480 BC) has been excavated at Thasos (Greece). In particular a pear-shaped metallurgical furnace was revealed while its fill and surrounding area was characterized by the abundant presence of slag, fragments of crucibles and furnace lining. Based on macroscopic examination and instrumental analysis it was shown that the slags and other waste products correspond to the melting and recycling of bronze. The significance of this finding is highlighted by the fact that the workshop is located within the urban core of Thasos. Based on the analytical results it could be suggested that bronze, containing lead was melted and recycled in crucibles at this workshop. Such ternary alloys were mostly used in bronze castings during this period. The results presented here contribute to a better understanding of certain metallurgical practices which were incorporated to the long technological tradition of Thasos.
希腊萨索斯(Thasos)出土了古代(公元前700-480年)重要的考古冶金背景。特别是一个梨形的冶金炉,而它的填充物和周围地区的特点是大量存在的炉渣,坩埚碎片和炉衬。通过宏观检验和仪器分析表明,炉渣和其他废物与青铜的熔化和回收有关。该工作室位于Thasos的城市核心,这一发现的重要性得到了强调。根据分析结果,可以认为含铅的青铜在这个车间被熔化并在坩埚中回收。在这一时期,这种三元合金主要用于青铜铸件。这里提出的结果有助于更好地理解某些冶金实践,这些实践被纳入了萨索斯悠久的技术传统。
{"title":"An Archaic metallurgical workshop in Thasos (Greece): the case of Charitopoulos plot","authors":"N. Nerantzis, G. Sanidas, Benjamin Jagou, T. Kozelj, Konstantina Panoussi","doi":"10.1080/20548923.2017.1419659","DOIUrl":"https://doi.org/10.1080/20548923.2017.1419659","url":null,"abstract":"ABSTRACT An important archaeometallurgical context dating to the Archaic period (700-480 BC) has been excavated at Thasos (Greece). In particular a pear-shaped metallurgical furnace was revealed while its fill and surrounding area was characterized by the abundant presence of slag, fragments of crucibles and furnace lining. Based on macroscopic examination and instrumental analysis it was shown that the slags and other waste products correspond to the melting and recycling of bronze. The significance of this finding is highlighted by the fact that the workshop is located within the urban core of Thasos. Based on the analytical results it could be suggested that bronze, containing lead was melted and recycled in crucibles at this workshop. Such ternary alloys were mostly used in bronze castings during this period. The results presented here contribute to a better understanding of certain metallurgical practices which were incorporated to the long technological tradition of Thasos.","PeriodicalId":21858,"journal":{"name":"STAR: Science & Technology of Archaeological Research","volume":"25 1","pages":"148 - 160"},"PeriodicalIF":0.0,"publicationDate":"2017-12-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"88355899","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Metalworking Evidence from a Late Antique Context in the Forum of Grumentum 格鲁门特姆论坛中晚期古语境中的金属加工证据
Pub Date : 2017-12-15 DOI: 10.1080/20548923.2018.1479940
G. Bison, Lara Pozzan, S. Haghani, L. Anguilano
ABSTRACT This paper is a preliminary report on metallurgical activity detected in the Forum of the ancient city of Grumentum ( Basilicata, Italy). In the Late antique period, an area next to one of the most important temples of the square was turned into a metalworking structure, which has yielded a set of hearths, metallurgical remains, and some tools. The results of archaeometrical investigation on the debris are reported and discussed, together with a general analysis of the archaeological context, also in comparison with other similar evidence detected elsewhere in Italy.
本文对意大利巴西利卡塔古城格鲁门图姆(Grumentum)遗址中发现的冶金活性进行了初步报道。在古代晚期,广场上最重要的寺庙之一旁边的一块区域被改造成一个金属加工结构,在那里发现了一套炉膛、冶金遗迹和一些工具。报告和讨论了对碎片的考古调查结果,以及对考古背景的一般分析,并与在意大利其他地方发现的其他类似证据进行了比较。
{"title":"Metalworking Evidence from a Late Antique Context in the Forum of Grumentum","authors":"G. Bison, Lara Pozzan, S. Haghani, L. Anguilano","doi":"10.1080/20548923.2018.1479940","DOIUrl":"https://doi.org/10.1080/20548923.2018.1479940","url":null,"abstract":"ABSTRACT This paper is a preliminary report on metallurgical activity detected in the Forum of the ancient city of Grumentum ( Basilicata, Italy). In the Late antique period, an area next to one of the most important temples of the square was turned into a metalworking structure, which has yielded a set of hearths, metallurgical remains, and some tools. The results of archaeometrical investigation on the debris are reported and discussed, together with a general analysis of the archaeological context, also in comparison with other similar evidence detected elsewhere in Italy.","PeriodicalId":21858,"journal":{"name":"STAR: Science & Technology of Archaeological Research","volume":"79 7 1","pages":"220 - 237"},"PeriodicalIF":0.0,"publicationDate":"2017-12-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"90935229","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Complex metallographic study on Gepid bronze and silver buckles from the Great Hungarian Plain (5-6th cent.) 大匈牙利平原格皮德青铜和银扣的复杂金相研究(5-6分)
Pub Date : 2017-12-15 DOI: 10.1080/20548923.2018.1450131
B. Török, M. Benke, V. Mertinger, P. Barkóczy, Á. Kovács, K. Hoppál, Péter F. Kovács
ABSTRACT This work presents a complex metallographic examination of bronze, silver and golden artefacts from early medieval German (Gepid) cemeteries of the Hungarian Plain, focusing on the finds from Tiszapüspöki.A newly developed non-destructive X-ray diffraction method was applied on the artefacts for the first time, as a novel approach, for sampling-free residual stress measurements. Other techniques such as optical microscopy and scanning electron microscopy combined with energy dispersive spectrometry has also been used. In addition to residual stress, crystallographic texture and properties of the reflections were analysed as well. The combined application of these methods was found to be an effective tool to deduce the production technologies of the examined artefacts. In addition to defining the characteristics of the material structures and compositions on the surfaces of the artefacts, the typical traces of several technological methods as casting, forming, coating were detected which are used for making various types of artefacts.
本研究对匈牙利平原中世纪早期德国(Gepid)墓地中的青铜、银和金文物进行了复杂的金相检查,重点研究了Tiszapüspöki的发现。本文首次将新开发的无损x射线衍射法应用于工件上,作为一种新的无采样残余应力测量方法。其他技术如光学显微镜和扫描电子显微镜与能量色散光谱相结合也被使用。除残余应力外,还分析了反射光的晶体织构和性能。这些方法的结合应用被发现是一种有效的工具来推断所检查的人工制品的生产技术。除了确定人工制品表面材料结构和成分的特征外,还检测了用于制造各种类型人工制品的几种技术方法的典型痕迹,如铸造,成型,涂层。
{"title":"Complex metallographic study on Gepid bronze and silver buckles from the Great Hungarian Plain (5-6th cent.)","authors":"B. Török, M. Benke, V. Mertinger, P. Barkóczy, Á. Kovács, K. Hoppál, Péter F. Kovács","doi":"10.1080/20548923.2018.1450131","DOIUrl":"https://doi.org/10.1080/20548923.2018.1450131","url":null,"abstract":"ABSTRACT This work presents a complex metallographic examination of bronze, silver and golden artefacts from early medieval German (Gepid) cemeteries of the Hungarian Plain, focusing on the finds from Tiszapüspöki.A newly developed non-destructive X-ray diffraction method was applied on the artefacts for the first time, as a novel approach, for sampling-free residual stress measurements. Other techniques such as optical microscopy and scanning electron microscopy combined with energy dispersive spectrometry has also been used. In addition to residual stress, crystallographic texture and properties of the reflections were analysed as well. The combined application of these methods was found to be an effective tool to deduce the production technologies of the examined artefacts. In addition to defining the characteristics of the material structures and compositions on the surfaces of the artefacts, the typical traces of several technological methods as casting, forming, coating were detected which are used for making various types of artefacts.","PeriodicalId":21858,"journal":{"name":"STAR: Science & Technology of Archaeological Research","volume":"91 1","pages":"245 - 252"},"PeriodicalIF":0.0,"publicationDate":"2017-12-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"86457038","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 1
A small bronze statue from the Archaeological Museum of Thessaloniki; exploring its authenticity 塞萨洛尼基考古博物馆的一尊小铜像;探索其真实性
Pub Date : 2017-12-01 DOI: 10.1080/20548923.2018.1441696
Vasiliki A. Michalopoulou, P. Adam-Veleni, I. Karapanagiotis
ABSTRACT This study explores the authentication of a bronze statue by means of the evaluation of technical evidence and investigation of patinas formation. The statue was identified by the police as a product of illicit excavation and handed to the Archaeological Museum of Thessaloniki. The visual examination reveals technical features that are consistent with those commonly found on ancient bronze statues while the physicochemical character of the corrosion was in accordance with typical bronze corrosion mechanisms (decuprification). Original features like the metal microstructure were detected on the corrosion layers, showing the complexity and long lasting character of their formation. The metal composition was determined by XRF and the corrosion products were analysed by XRF and SEM-EDS. GRAPHICAL ABSTRACT
摘要:本研究通过技术证据评估和铜绿形成的调查来探讨铜像的鉴定。警方确认这尊雕像是非法挖掘的产物,并将其交给了塞萨洛尼基考古博物馆。视觉检查显示,这些技术特征与古代青铜雕像的常见特征一致,而腐蚀的物理化学特征符合典型的青铜腐蚀机制(脱铜)。在腐蚀层上检测到金属微观结构等原始特征,显示了腐蚀层形成的复杂性和持久性。用XRF测定了金属成分,用XRF和SEM-EDS分析了腐蚀产物。图形抽象
{"title":"A small bronze statue from the Archaeological Museum of Thessaloniki; exploring its authenticity","authors":"Vasiliki A. Michalopoulou, P. Adam-Veleni, I. Karapanagiotis","doi":"10.1080/20548923.2018.1441696","DOIUrl":"https://doi.org/10.1080/20548923.2018.1441696","url":null,"abstract":"ABSTRACT This study explores the authentication of a bronze statue by means of the evaluation of technical evidence and investigation of patinas formation. The statue was identified by the police as a product of illicit excavation and handed to the Archaeological Museum of Thessaloniki. The visual examination reveals technical features that are consistent with those commonly found on ancient bronze statues while the physicochemical character of the corrosion was in accordance with typical bronze corrosion mechanisms (decuprification). Original features like the metal microstructure were detected on the corrosion layers, showing the complexity and long lasting character of their formation. The metal composition was determined by XRF and the corrosion products were analysed by XRF and SEM-EDS. GRAPHICAL ABSTRACT","PeriodicalId":21858,"journal":{"name":"STAR: Science & Technology of Archaeological Research","volume":"138 1","pages":"303 - 313"},"PeriodicalIF":0.0,"publicationDate":"2017-12-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"74305954","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 4
Klimt artwork: red-pigment material investigation by backscattering Fe-57 Mössbauer spectroscopy, SEM and p-XRF 克里姆特艺术品:红色颜料材料的后向散射Fe-57 Mössbauer光谱,扫描电镜和p-XRF研究
Pub Date : 2017-12-01 DOI: 10.1080/20548923.2017.1399332
R. Lehmann, D. Wengerowsky, H. Schmidt, M. Kumar, A. Niebur, B. Costa, F. Dencker, G. Klingelhöfer, R. Sindelar, F. Renz
ABSTRACT Material tests were performed on a rediscovered Klimt-artwork “Trompetender Putto”. We performed studies on the red colored spots, mainly taken from non-restored parts. MIMOS II Fe-57 Mössbauer spectroscopy (novelty in art-pigment analysis) mainly reveals haematite and crystallized goethite in red colors. Electron microscopy can identify various layers of the original and overpainting of an artwork. The number of layers fluctuates between three and four chemically painted areas. The portable X-ray fluorescence analysis enables to reduce the pigment list to containing mercury (cinnabar), lead, zinc, iron and titanium. Infrared-light-irradiation visualizes the different age of the pigments.
对重新发现的克林姆特艺术作品“Trompetender Putto”进行了材料测试。我们对红色斑点进行了研究,主要取自未修复的部分。MIMOS II Fe-57 Mössbauer光谱(艺术颜料分析中的新颖性)主要显示红色的赤铁矿和结晶针铁矿。电子显微镜可以识别一件艺术品的原画和复画的不同层。层数在三到四个化学涂漆区域之间波动。便携式x射线荧光分析能够将颜料列表减少到含有汞(朱砂),铅,锌,铁和钛。红外线照射可以看到不同年龄的色素。
{"title":"Klimt artwork: red-pigment material investigation by backscattering Fe-57 Mössbauer spectroscopy, SEM and p-XRF","authors":"R. Lehmann, D. Wengerowsky, H. Schmidt, M. Kumar, A. Niebur, B. Costa, F. Dencker, G. Klingelhöfer, R. Sindelar, F. Renz","doi":"10.1080/20548923.2017.1399332","DOIUrl":"https://doi.org/10.1080/20548923.2017.1399332","url":null,"abstract":"ABSTRACT Material tests were performed on a rediscovered Klimt-artwork “Trompetender Putto”. We performed studies on the red colored spots, mainly taken from non-restored parts. MIMOS II Fe-57 Mössbauer spectroscopy (novelty in art-pigment analysis) mainly reveals haematite and crystallized goethite in red colors. Electron microscopy can identify various layers of the original and overpainting of an artwork. The number of layers fluctuates between three and four chemically painted areas. The portable X-ray fluorescence analysis enables to reduce the pigment list to containing mercury (cinnabar), lead, zinc, iron and titanium. Infrared-light-irradiation visualizes the different age of the pigments.","PeriodicalId":21858,"journal":{"name":"STAR: Science & Technology of Archaeological Research","volume":"15 1","pages":"450 - 455"},"PeriodicalIF":0.0,"publicationDate":"2017-12-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"77060480","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 2
Polished Decorative Fields in Thracian Fresco Tombs from the Hellenistic period - Archaeometrical Research 希腊化时期色雷斯壁画墓葬中的抛光装饰领域-考古研究
Pub Date : 2017-11-10 DOI: 10.1080/20548923.2017.1396723
D. Guirdzhiiska, B. Zlateva, Z. Glavcheva
ABSTRACT In order to gather information on the technological characteristics of the monochrome decorative wall plasters in some Thracian fresco tombs (4th -3rd centuries BC) found in South Bulgaria, several types of analyses have been carried out. Samples of red, yellow and white large wall-painted fields in different monuments, have been investigated using a combination of Attenuated Total Reflectance Fourier Transform Infrared Spectroscopy (ATR-FTIR) and Differential Scanning Calorimetry (DSC) to identify the organic components of the paint layer. The nature of the pigments has been determined both by X-ray diffraction (XRD) and ATR-FTIR. The obtained results point towards the recognition of final polishing processes performed on still wet plaster. This technique of creating polished wall painted surfaces in combination with organic coatings (known as stucco lustro) is traditionally associated with the Pompean frescoes and the work of roman painters. Based on the technical examination, it can be assumed that in pre-roman time, the Hellenistic paint-craftsmen in Thrace inland were also familiar to this technique. GRAPHICAL ABSTRACT
为了收集在保加利亚南部发现的一些色雷斯壁画墓(公元前4 -3世纪)中单色装饰墙面灰泥的技术特征信息,进行了几种类型的分析。利用衰减全反射傅里叶变换红外光谱(ATR-FTIR)和差示扫描量热法(DSC)相结合的方法,研究了不同古迹中红色、黄色和白色大面积涂墙场的样品,以确定油漆层的有机成分。用x射线衍射(XRD)和红外光谱(ATR-FTIR)测定了颜料的性质。所获得的结果指向对在仍湿石膏上进行的最终抛光工艺的识别。这种结合有机涂料(灰泥)创造抛光墙面的技术传统上与庞培壁画和罗马画家的作品联系在一起。根据技术检查,可以假设在前罗马时代,色雷斯内陆的希腊化油漆工匠也熟悉这种技术。图形抽象
{"title":"Polished Decorative Fields in Thracian Fresco Tombs from the Hellenistic period - Archaeometrical Research","authors":"D. Guirdzhiiska, B. Zlateva, Z. Glavcheva","doi":"10.1080/20548923.2017.1396723","DOIUrl":"https://doi.org/10.1080/20548923.2017.1396723","url":null,"abstract":"ABSTRACT In order to gather information on the technological characteristics of the monochrome decorative wall plasters in some Thracian fresco tombs (4th -3rd centuries BC) found in South Bulgaria, several types of analyses have been carried out. Samples of red, yellow and white large wall-painted fields in different monuments, have been investigated using a combination of Attenuated Total Reflectance Fourier Transform Infrared Spectroscopy (ATR-FTIR) and Differential Scanning Calorimetry (DSC) to identify the organic components of the paint layer. The nature of the pigments has been determined both by X-ray diffraction (XRD) and ATR-FTIR. The obtained results point towards the recognition of final polishing processes performed on still wet plaster. This technique of creating polished wall painted surfaces in combination with organic coatings (known as stucco lustro) is traditionally associated with the Pompean frescoes and the work of roman painters. Based on the technical examination, it can be assumed that in pre-roman time, the Hellenistic paint-craftsmen in Thrace inland were also familiar to this technique. GRAPHICAL ABSTRACT","PeriodicalId":21858,"journal":{"name":"STAR: Science & Technology of Archaeological Research","volume":"2003 1","pages":"428 - 436"},"PeriodicalIF":0.0,"publicationDate":"2017-11-10","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"86245493","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 4
A non-destructive technological study of three fresco fragments from Iklaina, Pylos, Greece 对希腊皮洛斯伊克拉纳三幅壁画碎片的非破坏性技术研究
Pub Date : 2017-10-31 DOI: 10.1080/20548923.2017.1395153
G. Tsairis, E. Palamara, N. Zacharias, M. Cosmopoulos
ABSTRACT The objective of the present study is to conduct a non-destructive characterisation analysis of three fresco fragments from Iklaina, southern Peloponnese, Greece, in order to identify their manufacture techniques. Furthermore, this study aims at using the results of the scientific and analytical analyses to produce accurate replicas of these fragments (use of similar composition mortars, pigments, and manufacture techniques), which can be used for the restoration program of the site. These replicas will be exhibited alongside the originals in the new Pylos Archaeological Museum. Due to the high archaeological value of the objects, the analytical approach we followed was completely non-destructive and was based on the parallel use of optical microscopy, p-XRF and SEM/EDS. The analyses suggest the use of Egyptian blue pigment for the backgrounds. The wavy black coil of hair was painted with an organic black pigment. The use of inorganic pigments has been revealed on the upper layers on the basis of the identification of minerals and rocks. The substrate of the wall paintings is made of aluminosilicate lime mortars. The results corroborate the suggestions of previous studies for the pigments comprising the Mycenaean artistic palette and provides further insight on the artistic and technological choices made by Mycenaean artists.
本研究的目的是对希腊伯罗奔尼撒半岛南部Iklaina的三幅壁画碎片进行非破坏性特征分析,以确定其制作技术。此外,本研究旨在利用科学和分析分析的结果(使用相似成分的砂浆、颜料和制造技术)来制作这些碎片的精确复制品,这些复制品可用于遗址的修复计划。这些复制品将在新的皮洛斯考古博物馆与原件一起展出。由于这些物品具有很高的考古价值,我们采用的分析方法是完全无损的,并且是基于光学显微镜、p-XRF和SEM/EDS的并行使用。分析表明,背景使用了埃及蓝颜料。波浪状的黑色卷发是用有机黑色颜料涂上的。在矿物和岩石鉴定的基础上,揭示了无机颜料在上层的使用。壁画的基材是由硅酸铝石灰砂浆制成的。这些结果证实了先前关于迈锡尼艺术调色板中颜料的研究,并为迈锡尼艺术家的艺术和技术选择提供了进一步的见解。
{"title":"A non-destructive technological study of three fresco fragments from Iklaina, Pylos, Greece","authors":"G. Tsairis, E. Palamara, N. Zacharias, M. Cosmopoulos","doi":"10.1080/20548923.2017.1395153","DOIUrl":"https://doi.org/10.1080/20548923.2017.1395153","url":null,"abstract":"ABSTRACT The objective of the present study is to conduct a non-destructive characterisation analysis of three fresco fragments from Iklaina, southern Peloponnese, Greece, in order to identify their manufacture techniques. Furthermore, this study aims at using the results of the scientific and analytical analyses to produce accurate replicas of these fragments (use of similar composition mortars, pigments, and manufacture techniques), which can be used for the restoration program of the site. These replicas will be exhibited alongside the originals in the new Pylos Archaeological Museum. Due to the high archaeological value of the objects, the analytical approach we followed was completely non-destructive and was based on the parallel use of optical microscopy, p-XRF and SEM/EDS. The analyses suggest the use of Egyptian blue pigment for the backgrounds. The wavy black coil of hair was painted with an organic black pigment. The use of inorganic pigments has been revealed on the upper layers on the basis of the identification of minerals and rocks. The substrate of the wall paintings is made of aluminosilicate lime mortars. The results corroborate the suggestions of previous studies for the pigments comprising the Mycenaean artistic palette and provides further insight on the artistic and technological choices made by Mycenaean artists.","PeriodicalId":21858,"journal":{"name":"STAR: Science & Technology of Archaeological Research","volume":"8 1","pages":"418 - 427"},"PeriodicalIF":0.0,"publicationDate":"2017-10-31","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"87534124","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 1
期刊
STAR: Science & Technology of Archaeological Research
全部 Acc. Chem. Res. ACS Applied Bio Materials ACS Appl. Electron. Mater. ACS Appl. Energy Mater. ACS Appl. Mater. Interfaces ACS Appl. Nano Mater. ACS Appl. Polym. Mater. ACS BIOMATER-SCI ENG ACS Catal. ACS Cent. Sci. ACS Chem. Biol. ACS Chemical Health & Safety ACS Chem. Neurosci. ACS Comb. Sci. ACS Earth Space Chem. ACS Energy Lett. ACS Infect. Dis. ACS Macro Lett. ACS Mater. Lett. ACS Med. Chem. Lett. ACS Nano ACS Omega ACS Photonics ACS Sens. ACS Sustainable Chem. Eng. ACS Synth. Biol. Anal. Chem. BIOCHEMISTRY-US Bioconjugate Chem. BIOMACROMOLECULES Chem. Res. Toxicol. Chem. Rev. Chem. Mater. CRYST GROWTH DES ENERG FUEL Environ. Sci. Technol. Environ. Sci. Technol. Lett. Eur. J. Inorg. Chem. IND ENG CHEM RES Inorg. Chem. J. Agric. Food. Chem. J. Chem. Eng. Data J. Chem. Educ. J. Chem. Inf. Model. J. Chem. Theory Comput. J. Med. Chem. J. Nat. Prod. J PROTEOME RES J. Am. Chem. Soc. LANGMUIR MACROMOLECULES Mol. Pharmaceutics Nano Lett. Org. Lett. ORG PROCESS RES DEV ORGANOMETALLICS J. Org. Chem. J. Phys. Chem. J. Phys. Chem. A J. Phys. Chem. B J. Phys. Chem. C J. Phys. Chem. Lett. Analyst Anal. Methods Biomater. Sci. Catal. Sci. Technol. Chem. Commun. Chem. Soc. Rev. CHEM EDUC RES PRACT CRYSTENGCOMM Dalton Trans. Energy Environ. Sci. ENVIRON SCI-NANO ENVIRON SCI-PROC IMP ENVIRON SCI-WAT RES Faraday Discuss. Food Funct. Green Chem. Inorg. Chem. Front. Integr. Biol. J. Anal. At. Spectrom. J. Mater. Chem. A J. Mater. Chem. B J. Mater. Chem. C Lab Chip Mater. Chem. Front. Mater. Horiz. MEDCHEMCOMM Metallomics Mol. Biosyst. Mol. Syst. Des. Eng. Nanoscale Nanoscale Horiz. Nat. Prod. Rep. New J. Chem. Org. Biomol. Chem. Org. Chem. Front. PHOTOCH PHOTOBIO SCI PCCP Polym. Chem.
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
0
微信
客服QQ
Book学术公众号 扫码关注我们
反馈
×
意见反馈
请填写您的意见或建议
请填写您的手机或邮箱
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
现在去查看 取消
×
提示
确定
Book学术官方微信
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术
文献互助 智能选刊 最新文献 互助须知 联系我们:info@booksci.cn
Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。
Copyright © 2023 Book学术 All rights reserved.
ghs 京公网安备 11010802042870号 京ICP备2023020795号-1