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Microscopic and microanalytical study on Sasanian metal objects from Western Iran: A case study 伊朗西部萨珊王朝金属器物的显微和微量分析研究:一个案例研究
Pub Date : 2017-10-25 DOI: 10.1080/20548923.2017.1384175
Omid Oudbashi, Ata Hasanpour, A. Jahanpoor, Zahra Rahjoo
ABSTRACT Recent archaeological excavation in western Iran discovered a Sasanian palace called Ghaleh Guri (Qela Gowri) beside of the Seimarreh River. As part of the archaeometric studies on the site, five metallic objects (a coin, a disc, a vessel, a decorated strip and some pieces with no specific function) were sampled and analysed using OM and SEM-EDS to determine alloy composition and microstructure. The results showed that strip is made of copper, disc, vessel and unidentifiable object are tin bronze and the coin is made of silver-copper alloy. Tin content in the vessel is about 30 wt% and may be classified as high-tin bronze. The microstructure of samples also revealed that the amount of working and the heat treatment was variable, most likely due to their different compositions.
最近在伊朗西部的考古发掘中,在seimarh河旁发现了一座名为Ghaleh Guri (Qela Gowri)的萨珊王朝宫殿。作为考古研究的一部分,五个金属物体(一枚硬币,一个圆盘,一个容器,一个装饰条和一些没有特定功能的碎片)被取样并使用OM和SEM-EDS分析,以确定合金成分和微观结构。结果表明,铜条为铜质,圆盘、容器及不明物品为锡青铜,硬币为银铜合金。容器中的锡含量约为30 wt%,可归类为高锡青铜。样品的微观结构也表明,加工量和热处理是不同的,很可能是由于它们的不同成分。
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引用次数: 7
Methods for developing 3D visualizations of archaeological data: a case study of the early bronze age Helike Corridor House 开发考古数据三维可视化的方法:以早期青铜器时代赫里克走廊屋为例
Pub Date : 2017-10-05 DOI: 10.1080/20548923.2017.1372934
Mariza Kormann, D. Katsonopoulou, S. Katsarou, G. Lock
ABSTRACT The Digital Helike Project aims at the digitization of archaeological data from the Helike Project, Achaia, Greece. This paper advances understanding of Early Bronze Age house building techniques with focus on corridor houses. The Helike Corridor House is a fine example of an architectural style of the Early Helladic period EH II/Early EH III on the Greek mainland and it is used here as a case study. A methodology for 3D reconstruction is described supporting both structural integrity simulations and advanced visualization studies. The paper focuses on three aspects: firstly, it highlights technological innovations in the Bronze Age period by drawing attention to structural integrity studies recently carried out by the research team; secondly, it describes a methodology for building fully geo-referenced 3D models supporting structural integrity studies and visualization on GIS-Geographic Information Systems; and thirdly, it leads to the universal access of data and visualization over the Internet through the selection of appropriate open source, open standards and freely available tools and applications. The methodologies proposed here deepen insights on archaeological data enabling new inferences and knowledge to be gained through the implementation of universally shared low cost applications.
数字Helike项目旨在将希腊亚该亚Helike项目中的考古数据数字化。本文对早期青铜器时代的房屋建造技术进行了深入的了解,重点是走廊房屋。Helike Corridor House是希腊大陆早期Helladic时期EH II/ EH III早期建筑风格的典范,这里将其作为案例研究。描述了一种支持结构完整性模拟和高级可视化研究的三维重建方法。本文主要关注三个方面:首先,通过关注研究小组最近进行的结构完整性研究,突出了青铜器时代的技术创新;其次,描述了一种建立完全地理参考的三维模型的方法,该模型支持在gis地理信息系统上进行结构完整性研究和可视化;第三,它通过选择适当的开源、开放标准和免费提供的工具和应用程序,导致数据和可视化在互联网上的普遍访问。这里提出的方法加深了对考古数据的见解,通过实施普遍共享的低成本应用程序,可以获得新的推论和知识。
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引用次数: 7
The geochemical characterization of two long distance chert tracers by ED-XRF and LA-ICP-MS. Implications for Magdalenian human mobility in the Pyrenees (SW Europe) 两种长距燧石示踪剂的ED-XRF和LA-ICP-MS地球化学表征。对比利牛斯山脉(欧洲西南部)抹大拉时期人类迁移的影响
Pub Date : 2017-09-26 DOI: 10.1080/20548923.2017.1370842
Marta Sánchez de la Torre, François‐Xavier Le Bourdonnec, S. Dubernet, B. Gratuze, Xavier Mangado, J. Fullola
ABSTRACT We geochemically characterize two chert formations outcropping in the Pyrenees and presenting similar characteristics at the visual and microscopic scale: The Montgaillard flysch cherts and the Montsaunès cherts. Cherts presenting identical textural and micropalaeontological features as both types have been found in several Magdalenian Pyrenean sites. We are face to a long distance chert type whose geochemical characterization is essential for knowing where the tracer comes from. Analyses have been done using Energy-dispersive X-ray fluorescence (ED-XRF) and laser ablation inductively-coupled plasma mass spectrometry (LA-ICP-MS). Results show that despite obtaining similar data concerning major and minor elements, differences have been observed regarding trace elements. The establishment of differences between both formations at the geochemical level has allowed specifying the origin of this chert type recovered at the Magdalenian levels of Parco Cave (Alòs de Balaguer, Spain). Results demonstrate long lithic raw material circulation and thus, human mobility in the Pyrenees during the Upper Palaeolithic.
摘要/ ABSTRACT摘要:我们对比利牛斯山两个裸露的燧石组进行了地球化学表征,并在视觉和微观尺度上表现出相似的特征:Montgaillard复理燧石组和montsaun燧石组。在马格达莱尼亚比利牛斯山脉的几个遗址中发现了两种类型的燧石,它们具有相同的结构和微古生物学特征。我们面对的是一种长距离燧石类型,其地球化学特征对于了解示踪剂的来源至关重要。利用能量色散x射线荧光(ED-XRF)和激光烧蚀电感耦合等离子体质谱(LA-ICP-MS)进行了分析。结果表明,尽管在主、微量元素方面获得了相似的数据,但在微量元素方面却存在差异。在地球化学水平上建立两种地层之间的差异,可以确定在Parco洞穴(Alòs de Balaguer, Spain)的马格达莱期水平上发现的这种燧石类型的起源。结果表明,在旧石器时代晚期,在比利牛斯山脉有长期的石器原料流通,因此,人类的流动性。
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引用次数: 14
Neutron based archaeometallurgical investigation of Picenan and Roman age metal objects from the Academia Georgica Treiensis collection (Italy) 意大利Georgica Treiensis收藏的Picenan和罗马时代金属物品的中子考古冶金学研究
Pub Date : 2017-09-21 DOI: 10.1080/20548923.2017.1372933
Massimo Rogante, László Rosta, G. Káli, Z. Kasztovszky, Z. Kis, Imre Kovács, B. Maróti, Z. Szőkefalvi-Nagy
ABSTRACT Non-destructive prompt gamma activation analysis (PGAA), neutron radiography (NR) and high resolution time-of-flight neutron diffraction (TOF-ND) have been applied to investigate metal archaeological artefacts belonging to the Academia Georgica Treiensis (AGT) collection. 8 archaeological items have been analysed, by using the facilities of the Budapest Neutron Centre (BNC). Some of these objects mostly dating back probably to the VI-IV century B.C. and presumed to be discovered in the Marche Region, Italy. The primary goal of the analyses was to advance the correct technological and material description of the objects, providing scientific data for further and more comprehensive comparative analyses also covering the find material from the close archaeological sites. The neutron investigations allowed determining the bulk composition, also providing either a qualitative and quantitative assessment of the phase composition and the structural properties of the constituents, or radiographic images, which would finally help to identify possible manufacturing techniques. Additional examinations, carried out by external milli-beam particle induced X-ray emission spectroscopy (PIXE), provided quantitative analyses of major and trace elements (e.g., Fe, Pb and As) in order to recognize the constitutive alloys and to supply information on the near-surface elemental composition, complementary to the data characteristic for the bulk. The obtained results, thought to be useful to set up a classification according to the chemical composition, and this way allow achieving important information related to the possible provenance of the objects.
采用非破坏性提示γ活化分析(PGAA)、中子射线照相(NR)和高分辨率飞行时间中子衍射(TOF-ND)技术对格鲁吉亚科学院(AGT)收藏的金属考古文物进行了研究。利用布达佩斯中子中心(BNC)的设施,对8件考古物品进行了分析。其中一些物品可能可以追溯到公元前六至四世纪,据推测是在意大利马尔凯地区发现的。分析的主要目标是促进对这些物品的正确技术和材料描述,为进一步和更全面的比较分析提供科学数据,也包括从近考古遗址发现的材料。中子调查可以确定整体成分,也可以提供相组成和成分结构特性的定性和定量评估,或射线照相图像,这将最终有助于确定可能的制造技术。通过外部毫米束粒子诱导x射线发射光谱(PIXE)进行的额外检查,提供了主要和微量元素(例如,Fe, Pb和As)的定量分析,以识别本构合金并提供近表面元素组成的信息,补充了大块的数据特征。所获得的结果,被认为是根据化学成分建立分类的有用的,这种方式允许获得与物体可能的来源有关的重要信息。
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引用次数: 1
p-XRF analysis of multi-period Impasto and Cooking Pot wares from the excavations at Stromboli-San Vincenzo, Aeolian Islands, Italy 意大利伊奥利亚群岛斯特龙博利-圣文森佐发掘的多时期Impasto和炊具的p-XRF分析
Pub Date : 2017-06-10 DOI: 10.1080/20548923.2017.1329918
V. Cannavò, E. Photos-Jones, S. Levi, D. Brunelli, P. Fragnoli, Giacomo Lomarco, F. Lugli, M. Martinelli, M. Sforna
ABSTRACT This exploratory study focuses on the elemental analysis by p-XRF (portable X-Ray Fluorescence Analyser) of 62 samples of coarse wares, consisting of Bronze Age handmade burnished ware, so-called Impasto, and of Cooking ware (dated from the Roman period to Modern times). All wares originate from the site of San Vincenzo, Stromboli, and Aeolian Islands. The question addressed here is whether it is possible to differentiate between local (Aeolian) and imported (non-Aeolian) fabrics with the use of the p-XRF; 42 of the 62 samples were also subjected to petrographic analysis as a way of testing our hypothesis. Our results show that p-XRF analysis can clearly assist in distinguishing between Aeolian vs. non-Aeolian wares. Analyses can take place in the field and large quantities of sherds can be processed as a result. We suggest that no further demands should be made of the technique in providing answers to more detailed provenance questions. This is because finer separation in subgroups (as achieved recently by combined petrographic and EPMA analysis on select samples) is not possible given the nature of coarse pottery and the limitations of the technique in measuring key light elements (Na, Mg). Furthermore, for some elements (e.g Cr) accuracy is below acceptable levels in which case results for these particular elements are considered semi-quantitative.
本探索性研究的重点是使用p-XRF(便携式x射线荧光分析仪)对62个粗糙陶器样品进行元素分析,包括青铜器时代手工抛光器,即所谓的Impasto,以及炊具(从罗马时期到现代)。所有的商品都来自圣文森佐、斯特隆博利和风利亚群岛。这里讨论的问题是,使用p-XRF是否有可能区分本地(风成)和进口(非风成)织物;62个样品中的42个还进行了岩石学分析,作为检验我们假设的一种方式。我们的研究结果表明,p-XRF分析可以清楚地帮助区分风沙和非风沙。分析可以在现场进行,结果可以处理大量碎片。我们建议,在提供更详细的来源问题的答案时,不应再对该技术提出要求。这是因为考虑到粗陶的性质和测量关键轻元素(Na, Mg)技术的局限性,在亚组中进行更精细的分离是不可能的(正如最近通过对选定样品进行岩石学和EPMA结合分析所实现的那样)。此外,对于某些元素(例如Cr),精度低于可接受的水平,在这种情况下,这些特定元素的结果被认为是半定量的。
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引用次数: 6
The identification of archaeological eggshell using peptide markers 利用肽标记对考古蛋壳进行鉴定
Pub Date : 2017-01-01 DOI: 10.1080/20548923.2018.1424300
S. Presslee, Julie Wilson, Jos Woolley, Julia Best, D. Russell, A. Radini, R. Fischer, B. Kessler, R. Boano, M. Collins, B. Demarchi
ABSTRACT Avian eggshell survives well in alkaline and neutral soils, but its potential as an archaeological resource remains largely unexplored, mainly due to difficulties in its identification. Here we exploit the release of novel bird genomes and, for the first time on eggshell, use MALDI-ToF (matrix-assisted laser desorption ionisation-time of flight) mass spectrometry in combination with peptide sequencing by LC-MS/MS. The eggshell proteome is revealed as unexpectedly complex, with 5755 proteins identified for a reference collection comprising 23 bird species. We determined 782 m/z markers useful for eggshell identification, 583 of which could be assigned to known eggshell peptide sequences. These were used to identify eggshell fragments recovered from a medieval site at Freeschool Lane, Leicester. We discuss the specificity of the peptide markers and highlight the importance of assessing the level of taxonomic identification achievable for archaeological interpretation.
禽蛋壳在碱性和中性土壤中生存良好,但其作为考古资源的潜力尚未得到充分开发,主要原因是其鉴定困难。在此,我们利用新的鸟类基因组的释放,并首次在蛋壳上使用MALDI-ToF(基质辅助激光解吸电离飞行时间)质谱法结合LC-MS/MS的肽测序。蛋壳蛋白质组出人意料地复杂,在包含23种鸟类的参考集合中鉴定出5755种蛋白质。我们确定了782个可用于蛋壳鉴定的m/z标记,其中583个可分配给已知的蛋壳肽序列。这些被用来鉴定从莱斯特的自由学校巷的中世纪遗址中发现的蛋壳碎片。我们讨论了肽标记的特异性,并强调了评估考古解释可实现的分类鉴定水平的重要性。
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引用次数: 31
From the field to the laboratory: Controlling DNA contamination in human ancient DNA research in the high-throughput sequencing era 从野外到实验室:高通量测序时代人类古代DNA研究中的DNA污染控制
Pub Date : 2017-01-01 DOI: 10.1080/20548923.2016.1258824
B. Llamas, Guido Valverde, Lars Fehren-Schmitz, L. Weyrich, A. Cooper, W. Haak
Abstract High-Throughput DNA Sequencing (HTS) technologies have changed the way in which we detect and assess DNA contamination in ancient DNA studies. Researchers use computational methods to mine the large quantity of sequencing data to detect characteristic patterns of DNA damage, and to evaluate the authenticity of the results. We argue that unless computational methods can confidently separate authentic ancient DNA sequences from contaminating DNA that displays damage patterns under independent decay processes, prevention and control of DNA contamination should remain a central and critical aspect of ancient human DNA studies. Ideally, DNA contamination can be prevented early on by following minimal guidelines during excavation, sample collection and/or subsequent handling. Contaminating DNA should also be monitored or minimised in the ancient DNA laboratory using specialised facilities and strict experimental procedures. In this paper, we update recommendations to control for DNA contamination from the field to the laboratory, in an attempt to facilitate communication between field archaeologists, anthropologists and ancient DNA researchers. We also provide updated criteria of ancient DNA authenticity for HTS-based studies. We are confident that the procedures outlined here will increase the retrieval of higher proportions of authentic genetic information from valuable archaeological human remains in the future.
高通量DNA测序(HTS)技术已经改变了我们在古代DNA研究中检测和评估DNA污染的方式。研究人员利用计算方法挖掘大量的测序数据来检测DNA损伤的特征模式,并评估结果的真实性。我们认为,除非计算方法能够自信地将真实的古代DNA序列与在独立衰变过程中显示损伤模式的污染DNA分离开来,否则DNA污染的预防和控制应该仍然是古代人类DNA研究的核心和关键方面。理想情况下,DNA污染可以通过在挖掘,样本采集和/或随后的处理过程中遵循最小的指导方针来早期预防。古DNA实验室也应使用专门的设备和严格的实验程序监测或尽量减少DNA污染。在本文中,我们更新了从现场到实验室控制DNA污染的建议,试图促进现场考古学家,人类学家和古代DNA研究人员之间的交流。我们还为基于hts的研究提供了古代DNA真实性的最新标准。我们相信,这里概述的程序将来将增加从有价值的考古人类遗骸中检索更高比例的真实遗传信息。
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引用次数: 120
The effect of trophic level on individual amino acid δ15N values in a terrestrial ruminant food web 营养水平对陆生反刍动物食物网中氨基酸δ15N值的影响
Pub Date : 2017-01-01 DOI: 10.1080/20548923.2018.1459361
Iain P. Kendall, Michael R. F. Lee, R. Evershed
ABSTRACT Bulk collagen δ15N analysis is widely used to investigate past diet and trophic positions, but these values average the δ15N values of the constituent amino acids. Compound–specific isotope analysis of amino acids (AAs) can help elucidate the complex metabolic effects underpinning bulk δ15N values. Although trophic level effects on individual AA δ15N values have been investigated in aquatic and terrestrial invertebrate food webs, most archaeological applications involve terrestrial herbivores, hence a greater understanding of these effects between diet and consumer in this food chain is required. The North Wyke Farm Platform provided baseline nitrogen isotope information for cattle grazing on a Lolium perenne-dominated pasture. Bulk dentine δ15N values show a shift expected for a one trophic level increase, but obscure insight into the underlying metabolic processes that cause this change in value. However, determination of AA δ15N values of hydrolysable plant protein and cattle tooth dentine clarifies the trophic effect on consumer AA δ15N values. The observed trophic shift in the studied system is different from previously studied food webs, with a trophic enrichment factor, based on the δ15N values of glutamate and phenylalanine, of 4.0‰ compared to 7.6‰ commonly used in ecological and archaeological studies. This emphasises the need to understand the trophic shifts in the particular food web being investigated in order to apply isotopic investigations in archaeological contexts.
散装胶原蛋白δ15N分析被广泛用于研究过去的饮食和营养地位,但这些值是组成氨基酸δ15N值的平均值。氨基酸(AAs)的化合物特异性同位素分析有助于阐明支撑体δ15N值的复杂代谢效应。虽然在水生和陆生无脊椎动物食物网中已经研究了营养水平对个体AA δ15N值的影响,但大多数考古应用都涉及陆生食草动物,因此需要对食物链中饮食和消费者之间的这些影响有更深入的了解。北威克农场平台为在一个以黑穗草为主的多年生牧草上放牧的牛提供了基本的氮同位素信息。总体牙本质δ15N值显示了一个营养级增加的预期变化,但对导致这种值变化的潜在代谢过程的见解模糊。然而,通过测定可水解植物蛋白和牛牙本质的AA δ15N值,阐明了对消费者AA δ15N值的营养效应。研究系统的营养转移与先前研究的食物网不同,基于谷氨酸和苯丙氨酸的δ15N值的营养富集因子为4.0‰,而生态学和考古学研究通常使用的是7.6‰。这强调需要了解正在调查的特定食物网中的营养变化,以便在考古背景下应用同位素调查。
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引用次数: 26
Strontium concentration, radiogenic (87Sr/86Sr) and stable (δ88Sr) strontium isotope systematics in a controlled feeding study 对照投料研究中锶浓度、放射性成因(87Sr/86Sr)和稳定同位素(δ88Sr)系统
Pub Date : 2017-01-01 DOI: 10.1080/20548923.2017.1303124
J. Lewis, A. Pike, C. Coath, R. Evershed
ABSTRACT Transhumance and palaeodiet are two central themes in archaeology and using chemical analysis of bones and teeth to reconstruct trends and patterns in diet and mobility has become a cornerstone of bioarchaeology. This study has investigated strontium concentration ([Sr]), radiogenic (87Sr/86Sr) and stable strontium (δ88Sr) isotope systematics in a controlled feeding experiment on domestic pigs designed to simulate terrestrial versus marine protein consumption. The results of the radiogenic (87Sr/86Sr) analysis offer a validation of the strontium isotope methodology. The study confirms that the radiogenic strontium isotope composition of dental enamel does represent the radiogenic strontium isotope composition of the diet. The results of the δ88Sr analysis have revealed a distinct shift of 0.322 ± 0.060 ‰ towards isotopically light Sr with trophic level. The magnitude of this shift is consistent with the predictions from the analogous shift observed in calcium isotopes. This is the first time that trophic level fractionation in δ88Sr has been identified in a controlled setting. Although still in its infancy, δ88Sr analysis has great potential to inform on trophic level systematics, to investigate dietary trends in early life and is potentially useful in examining diagenetic alteration.
迁移和古饮食是考古学的两个核心主题,利用骨骼和牙齿的化学分析来重建饮食和活动的趋势和模式已成为生物考古学的基石。为了模拟陆地和海洋蛋白质消耗,本研究对家猪进行了对照饲养试验,研究了锶浓度([Sr])、放射性源(87Sr/86Sr)和稳定锶(δ88Sr)同位素系统。放射性成因(87Sr/86Sr)分析结果验证了锶同位素方法。研究证实,牙釉质的放射性锶同位素组成确实代表了饮食中的放射性锶同位素组成。δ88Sr分析结果显示,富营养化水平向轻同位素Sr偏移0.322±0.060‰。这种变化的幅度与在钙同位素中观察到的类似变化的预测一致。这是首次在控制条件下鉴定出δ88Sr的营养级分异。虽然δ88Sr分析仍处于起步阶段,但它在营养级系统学研究、早期生活饮食趋势研究和成岩变化研究方面具有很大的潜力。
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引用次数: 82
Differing modes of animal exploitation in North-Pontic Eneolithic and Bronze Age Societies 北岸新石器时代和青铜时代社会中不同的动物开发模式
Pub Date : 2017-01-01 DOI: 10.1080/20548923.2018.1443547
Simona Mileto, E. Kaiser, Y. Rassamakin, H. Whelton, R. Evershed
ABSTRACT This paper presents new results of an interdisciplinary investigation of the diet and subsistence strategies of populations living in the North-Pontic region during the Eneolithic and the Early Bronze Age (ca. 3800 BC to the 2500 BC). New organic residue analyses of >200 sherds from five Eneolithic sites and two Early Bronze Age settlements are presented. The molecular and stable isotope results are discussed in relation to zooarchaeological evidence. Overall, the findings suggest that each community relied on either a hunting- or a husbandry-based subsistence strategy dependent upon the ecosystem in which they settled; horses and wild animals dominated subsistence in the forest-steppe communities in contrast to ruminant husbandry in the steppe.
摘要:本文介绍了新石器时代和早期青铜时代(约公元前3800年至公元前2500年)生活在北蓬蒂克地区的人群的饮食和生存策略的跨学科调查的新结果。对来自5个新石器时代遗址和2个早期青铜时代定居点的200多块碎片进行了新的有机残留物分析。分子和稳定同位素结果讨论了动物考古证据。总体而言,研究结果表明,每个社区都依赖于基于狩猎或畜牧业的生存策略,这取决于他们定居的生态系统;与草原上的反刍动物饲养相比,在森林草原群落中,马和野生动物是主要的生计来源。
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引用次数: 4
期刊
STAR: Science & Technology of Archaeological Research
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