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2022 IEEE International Conference on Flexible and Printable Sensors and Systems (FLEPS)最新文献

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Flexible Inkjet Printed Gold based Electrochemical Sensor for Aqueous Lead Detection 用于水铅检测的柔性喷墨印刷金电化学传感器
Pub Date : 2022-07-10 DOI: 10.1109/fleps53764.2022.9781482
Annatoma Arif, Robert C. Roberts
This work presents a novel simple, flexible, cost-effective, sensitive, and disposable inkjet printed (IP) electrochemical sensor on PPG Teslin SP600 substrate for aqueous lead (II) detection. The electrochemical cell contains a gold (Au) working electrode (WE), Au counter electrode (CE), and integrated silver chloride (AgCl) reference electrode (RE). The lateral dimension and area of the fabricated inkjet printed flexible (IPF) electrochemical sensor are 12×8×0.52 mm3 and 3.41 mm2 respectively. The reported sensor is initially IP using silver (Ag) nanoparticle conductive ink. The Au WE and CE are obtained with 24K brush Au-plating technology. AgCl formation occurred with dilute sodium hypochlorite (3%) immersion of the sintered Ag RE. The electrochemical sensor is characterized with 3mM of lead (II) contaminated optimized drinking water (0.1 M HCl). The fabricated novel IPF sensor is further utilized for 14.4 µg/L lead (II) contaminated optimized drinking water which is below the United States Environmental Protection Agency approved lead (II) level in the drinking water – 15 µg/L. The fabrication and characteristics/performance of the IPF electrochemical sensor were analyzed using scanning electron micrograph (SEM) images/ energy dispersive X-ray spectroscopy (EDS) and cyclic voltammetry (CV) electrochemical analyses respectively.
本研究提出了一种新颖、简单、灵活、经济、敏感的一次性喷墨印刷电化学传感器,用于PPG Teslin SP600衬底上的水铅(II)检测。该电化学电池由金(Au)工作电极(WE)、金对电极(CE)和集成氯化银(AgCl)参比电极(RE)组成。制备的喷墨印刷柔性电化学传感器的横向尺寸和面积分别为12×8×0.52 mm3和3.41 mm2。报道的传感器最初是IP使用银(Ag)纳米颗粒导电油墨。采用24K电刷镀金工艺获得了Au WE和CE。用稀次氯酸钠(3%)浸泡烧结的Ag RE,可以形成AgCl。电化学传感器的特征是3mM铅(II)污染的优化饮用水(0.1 M HCl)。制备的新型IPF传感器进一步用于14.4µg/L铅(II)污染的优化饮用水,低于美国环境保护局批准的饮用水中铅(II)水平- 15µg/L。利用扫描电镜(SEM)图像、x射线能谱(EDS)和循环伏安(CV)电化学分析对IPF电化学传感器的制备和性能进行了分析。
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引用次数: 1
Inkjet-printed flexible oxide photodetectors for scalable user interfaces 用于可扩展用户界面的喷墨印刷柔性氧化物光电探测器
Pub Date : 2022-07-10 DOI: 10.1109/fleps53764.2022.9781586
Georgios Bairaktaris, F. Khan, R. Sporea
In today’s world of connectivity and automation, novel user interfaces are used to incorporate technology into our lives in a seamless way. Printed electronics provide the tools for making flexible and conformable electronic systems that can augment the functionality of everyday objects. However, compared to conventional, off-the-shelf devices, their performance is insufficient to obtain a functional and robust fully printed system. In this work, we are developing purpose-built photodetectors (PDs) for their use in an augmented paper platform, the Magic Bookmark. The developed PDs exhibit an on/off ratio of 0.2, resulting in a voltage swing of 200 mV, when connected to external circuitry, indicating suitability for the Magic Bookmark within high tolerances due to the readout scheme selected.
在当今连接和自动化的世界中,新颖的用户界面被用来将技术无缝地融入我们的生活。印刷电子产品提供了制造灵活和兼容的电子系统的工具,可以增强日常物品的功能。然而,与传统的现成设备相比,它们的性能不足以获得功能强大的全印刷系统。在这项工作中,我们正在开发用于增强纸平台Magic Bookmark的专用光电探测器(pd)。开发的pd具有0.2的开/关比,当连接到外部电路时,电压摆幅为200 mV,表明由于选择的读出方案,在高容差范围内适合Magic Bookmark。
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引用次数: 0
Electrochemical sensor for phosphate ions based on laser scriber reduced graphene oxide 基于激光划线机还原氧化石墨烯的磷酸离子电化学传感器
Pub Date : 2022-07-10 DOI: 10.1109/fleps53764.2022.9781533
B. Patella, Federico Gitto, Michele Russo, G. Aiello, A. O’Riordan, R. Inguanta
This preliminary work shows a new and innovative way to produce laser scribed reduced graphene oxide (LSGO) electrodes using different porous substrates (ranging from paper to plastic and fabric). The obtained electrodes were also tested as electrochemical sensors towards the detection of phosphate ions in water. To obtain the electrodes, a water suspension of GO was filtered on top of substrate (such as Whatman® filter paper) and a complete sensor was obtained from its reduction using a CO2 laser. The electrode is composed of working and counter electrodes made of LSGO and a reference electrode of a Ag/AgCl obtained by using a commercial AgCl conductive paste. Phosphate ions were detected by exploiting the reaction between molybdate and phosphate ions in acidic media (known in literature as molybdenum blue method). This chemical reaction produces the Keggin-type complex (PMo12O40)3−, that can be reduced under applied potential. The obtained results show that phosphate ions can be detected in a wide linear range, from 0.001 mM to 1mM, in presence of 1mM molybdate with a very satisfying selectivity. We also tried to pre-treatment the paper substrate with acidic molybdate ions in order to obtain a ready-made sensor directly usable for the detection of phosphate ions in situ avoiding any kind of real sample manipulation For this aim, the paper substrate was soaked with sulphuric acid and molybdate solution and dried in order to desorb these chemicals directly into the water sample to be analyzed. Preliminary results, shows that the process of absorption and desorption can be carried out by optimizing the volume and concentration of the absorbed solution and thus can be used to obtain a portable, easy to use and fast phosphate sensor for in situ and real time monitoring of water quality.
这项初步工作展示了一种新的创新方法,可以使用不同的多孔基材(从纸到塑料和织物)生产激光刻写还原氧化石墨烯(LSGO)电极。所制备的电极还作为电化学传感器对水中磷酸盐离子的检测进行了测试。为了获得电极,在衬底(如Whatman®滤纸)上过滤氧化石墨烯的水悬浮液,并使用CO2激光从其还原中获得完整的传感器。该电极由由LSGO制成的工作电极和反电极以及由商用AgCl导电浆料制成的Ag/AgCl参比电极组成。磷酸盐离子的检测是利用钼酸盐和磷酸盐离子在酸性介质中的反应(文献中称为钼蓝法)。该化学反应产生keggin型络合物(PMo12O40)3−,该络合物可以在外加电位下还原。结果表明,在1mM钼酸盐存在下,磷酸盐离子在0.001 ~ 1mM的宽线性范围内可被检测到,并且具有非常满意的选择性。我们还尝试用酸性钼酸盐离子对纸质底物进行预处理,以获得可直接用于原位检测磷酸盐离子的现成传感器,避免任何类型的实际样品操作。为此,将纸质底物用硫酸和钼酸盐溶液浸泡并干燥,以便将这些化学物质直接解吸到待分析的水样中。初步结果表明,通过优化吸附溶液的体积和浓度,可以进行吸附和解吸过程,从而可以获得一种便携式、易于使用和快速的磷酸盐传感器,用于现场和实时监测水质。
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引用次数: 2
Electrochemical Investigation of Self-Assembling Monolayers toward Ultrasensitive Sensing 超灵敏传感自组装单层膜的电化学研究
Pub Date : 2022-07-10 DOI: 10.1109/fleps53764.2022.9781585
Angelo Tricase, Anna Imbriano, E. Macchia, R. Picca, D. Blasi, L. Torsi, P. Bollella
In this paper we report a combined theoretical and experimental approach for analyzing Self Assembled Monolayers (SAMs) modified electrodes. Three different SAMs were compared, consisting in a mixed SAMs of amides and carboxylic groups (Deactivated SAMs), a SAM functionalized with an antibody (Anti-IgG SAMs), and SAM functionalized with two different proteins, Anti-IgG and Bovine Serum Albumin (BSA). Each of these samples is used to describe a different component of a SAMs modified gold electrode implemented in an Electrolyte Gated – Organic Field Effect Transistor Biosensor, where the presence of a diffuse hydrogen bonding between SAMs chains plays a key role for reaching the performance of this device, able to reach the single molecule limit of detection.
本文报道了一种结合理论和实验的方法来分析自组装单层(SAMs)修饰电极。比较了三种不同的SAMs,包括酰胺和羧基的混合SAMs(失活SAMs),用抗体功能化的SAMs(抗igg SAMs),以及用两种不同的蛋白质功能化的SAM,抗igg和牛血清白蛋白(BSA)。这些样品中的每一个都用于描述在电解质门控有机场效应晶体管生物传感器中实现的SAMs修饰金电极的不同组成部分,其中SAMs链之间弥漫性氢键的存在对于达到该设备的性能起着关键作用,能够达到单分子检测极限。
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引用次数: 0
Adaptive Dielectric Thin Film Transistors: Device Physics and Modeling 自适应介电薄膜晶体管:器件物理与建模
Pub Date : 2022-07-10 DOI: 10.1109/fleps53764.2022.9781528
P. Ranjan, P. Bhattacharya, S. Sambandan
The adaptive dielectric thin film transistor (adTFT) shows a high pass response thereby offering interesting possibilities for front-end circuits e.g. low leakage electrostatic discharge protection, filtering etc. The architecture is similar to a conventional thin film transistor but with the dielectric composed of an insulator-semiconductor-insulator stack. Here we develop analytical and TCAD models describing the physics of the device.
自适应介质薄膜晶体管(adTFT)显示出高通响应,从而为前端电路提供了有趣的可能性,例如低泄漏静电放电保护,滤波等。其结构类似于传统的薄膜晶体管,但电介质由绝缘体-半导体-绝缘体堆叠而成。在这里,我们开发了描述器件物理特性的分析模型和TCAD模型。
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引用次数: 0
V2O5 nanowires coated yarn based temperature sensor for smart textiles 基于V2O5纳米线涂层纱线的智能纺织品温度传感器
Pub Date : 2022-07-10 DOI: 10.1109/fleps53764.2022.9781524
G. Khandelwal, A. Dahiya, R. Dahiya
Smart textiles can sense different stimuli such as pressure, temperature etc., to allow users to react and adapt. Such features are accomplished through integration of various fiber-based sensors and electronic components in textile structures. Yarn is 1-dimensional structure which can be modified to behave as a sensor and can further be integrated with other sensors or electronics to form smart textile by techniques like weaving, knitting, and braiding. In this work, a flexible temperature sensor is reported by modifying a stainless-steel yarn with V2O5 nanowires. The current profile and temperature sensing performance is measured from 5 to 50 °C. The device exhibits sensitivity of 3.7 %/°C and response time of ~9s. The present work demonstrates the potential of using yarn as a flexible temperature sensor that can be used to realize smart textile for wearable and healthcare applications.
智能纺织品可以感知不同的刺激,如压力、温度等,让用户做出反应和适应。这些特征是通过在纺织结构中集成各种基于纤维的传感器和电子元件来实现的。纱线是一种一维结构,可以被修改为传感器,并可以进一步与其他传感器或电子设备集成,通过编织、针织和编织等技术形成智能纺织品。本文报道了一种用V2O5纳米线修饰不锈钢纱线的柔性温度传感器。电流分布和温度传感性能可在5至50°C范围内测量。该器件灵敏度为3.7% /°C,响应时间为~9s。目前的工作展示了使用纱线作为柔性温度传感器的潜力,可用于实现可穿戴和医疗保健应用的智能纺织品。
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引用次数: 1
A hybrid casting and screen-printing based manufacturing method for flexible sensors 一种基于混合铸造和丝网印刷的柔性传感器制造方法
Pub Date : 2022-07-10 DOI: 10.1109/fleps53764.2022.9781558
S. Khan, J. Kosel
A hybrid manufacturing method is presented using a combination of screen printing and casting, which are commonly used and widely accepted industrial manufacturing processes, to create multi-layered flexible sensors. The method enables the efficient fabrication of sensors that consist of conductive metallic pastes and silicone polymers. The feasibility of the manufacturing method is demonstrated for a parallel plate capacitive pressure sensor. The top and bottom metallic layers of the sensor are made using screen-printed nanoparticle-based silver conductive paste, while the pressure-sensitive silicone layer is formed by casting Ecoflex.
提出了一种采用丝网印刷和铸造这两种工业制造工艺相结合的混合制造方法来制造多层柔性传感器。该方法能够有效地制造由导电金属糊和硅树脂聚合物组成的传感器。并对平行板电容式压力传感器的制造方法进行了验证。传感器的顶部和底部金属层由丝网印刷的纳米颗粒银导电浆料制成,而压敏硅层由铸造Ecoflex制成。
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引用次数: 1
MoS2 modified screen printed carbon electrode based flexible sensor for detection of Copper 基于二硫化钼改性丝网印刷碳电极的铜检测柔性传感器
Pub Date : 2022-07-10 DOI: 10.1109/fleps53764.2022.9781564
D. K. Neethipathi, Priyanka Ganguly, Ajay Beniwal, M. Scott, Adrian M. Bass, R. Dahiya
Monitoring of heavy metal ions in aquatic environment can be a tedious process, especially in harsh, logistically challenging field conditions. This work demonstrates the detection of copper ions in water using a low-cost screen printed 2D molybdenum disulfide (MoS2) nanoparticle based electrochemical sensor. To deal with the common field-testing challenges, an easily disposable, flexible, compact sized reliable sensor was fabricated using a screen-printing technique. The developed sensor shows an excellent performance with a linear range of 5 µM to 1000 µM, a low limits of detection (LOD) value of just 0.3125 µM, and high repeatability with standard deviation less than 0.5%. With this performance and attractive attributes such as flexible form factor, low-cost fabrication and disposability etc. the presented sensor shows a great potential for practical applications in soil and water monitoring.
在水生环境中监测重金属离子可能是一个繁琐的过程,特别是在恶劣的、具有后勤挑战性的现场条件下。这项工作展示了使用低成本的丝网印刷二维二硫化钼(MoS2)纳米颗粒电化学传感器检测水中铜离子。为了应对常见的现场测试挑战,使用丝网印刷技术制造了一种易于丢弃,灵活,紧凑尺寸可靠的传感器。该传感器具有良好的性能,线性范围为5µM ~ 1000µM,低检出限(LOD)值仅为0.3125µM,重复性高,标准偏差小于0.5%。该传感器具有良好的性能和灵活的外形、低成本的制造和可丢弃性等优点,在土壤和水监测方面具有巨大的实际应用潜力。
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引用次数: 3
Torsional and bending endurance analysis of screen-printed interconnects on various flexible substrates 各种柔性基板上丝网印刷互连的扭弯耐久性分析
Pub Date : 2022-07-10 DOI: 10.1109/fleps53764.2022.9781508
Rudra Mukherjee, A. Dahiya, R. Dahiya
Additive manufacturing is an economic and resource efficient route for development of flexible electronics for applications such as robotics, wearables, and real-time health monitoring systems. Although the 2-D and 3-D printing are mature technologies , their application in flexible electronics is still in early stage and comes with challenges such as poor reliability under repeated bending conditions. This is because the level of mechanical stresses that various components of a flexible electronic module must endure is substantially high. For example, the interconnects experience a large part of bending and twisting stresses, which can affect their conductivity and decrease the responsivity and reliability of the electronic module. In this paper, we assess the base resistance and endurance of screen-printed silver interconnects on commonly used soft and flexible substrates for up to 4000 bending and twisting cycles. It is observed that the base resistance and endurance of screen-printed silver interconnects are heavily dependent on the substrate. The endurance analysis present here will benefit applications such as smart tags, where screen printed interconnects or metal lines are extensively used.
对于机器人、可穿戴设备和实时健康监测系统等应用而言,增材制造是一种经济且资源高效的柔性电子产品开发途径。虽然2-D和3-D打印是成熟的技术,但它们在柔性电子产品中的应用仍处于早期阶段,并且面临着反复弯曲条件下可靠性差等挑战。这是因为柔性电子模块的各种组件必须承受的机械应力水平非常高。例如,互连经历了很大一部分弯曲和扭转应力,这可能会影响它们的导电性,降低电子模块的响应性和可靠性。在本文中,我们评估了丝网印刷银互连在常用软基板和柔性基板上高达4000次弯曲和扭转循环的基电阻和耐久性。观察到丝网印刷银互连的基极电阻和耐用性在很大程度上取决于衬底。这里介绍的耐久性分析将有利于智能标签等广泛使用丝网印刷互连或金属线的应用。
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引用次数: 2
Highly Conductive Flexible Printed PEDOT:PSS films for Green Humidity Sensing Applications 高导电柔性印刷PEDOT:PSS薄膜绿色湿度传感应用
Pub Date : 2022-07-10 DOI: 10.1109/fleps53764.2022.9781556
Junjie Shi, Mahmoud Wagih, S. Beeby
Over the past decades, humidity sensors have been an important sensing component in climate monitoring, agriculture, medical diagnostics and industrial process control systems. With emerging applications such as wearable devices and the internet of things in 5G scenarios, there is a growing demand for accurate humidity measurements, low-cost manufacturing processes for high-volume, high-performance sensors with flexible form factors, and the use of environmentally friendly materials. We present a simple, fast, and cost-effective method for the large-scale fabrication of highly-conductive, all-polymer, and bio-degradable humidity sensors on flexible organic polymer (polyimide) and paper substrates. We investigate the resistive properties of different thicknesses of poly(3,4-ethylenedioxythiophehe) polystyrene sulfonate (PEDOT:PSS) on Kapton and paper substrates in response to humidity, demonstrating a 3—8 Ω/square sheet resistance, suitable for all-polymer circuits. A relative resistance variation of 36.3% at levels of relative humidity ranging from 20% to 80% is demonstrated for a pristine sample, along with 1-month ageing tests to investigate the lifetime of the proposed sensor.
在过去的几十年里,湿度传感器一直是气候监测、农业、医疗诊断和工业过程控制系统中重要的传感组件。随着5G场景下可穿戴设备和物联网等新兴应用的出现,对精确湿度测量、大批量低成本制造工艺、具有灵活外形因素的高性能传感器以及使用环保材料的需求不断增长。我们提出了一种简单、快速、经济高效的方法,用于在柔性有机聚合物(聚酰亚胺)和纸基上大规模制造高导电性、全聚合物和可生物降解的湿度传感器。我们研究了不同厚度的聚(3,4-乙烯二氧噻吩)聚苯乙烯磺酸盐(PEDOT:PSS)在Kapton和纸质衬底上对湿度的响应,证明了3 - 8 Ω/平方片的电阻,适用于全聚合物电路。对于原始样品,在相对湿度范围为20%至80%的水平下,相对电阻变化为36.3%,并进行了1个月的老化测试,以研究所建议的传感器的寿命。
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引用次数: 1
期刊
2022 IEEE International Conference on Flexible and Printable Sensors and Systems (FLEPS)
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