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Chemical comparison and Trichomes types of Salvia species growing in Anbar Governorate – Iraq 伊拉克安巴尔省鼠尾草种类的化学比较和毛状体类型
Pub Date : 2023-06-25 DOI: 10.25130/tjps.v28i3.1419
Khader Alzawi, I. Abdulrazzaq, Majed Aldobaissi, A. O. Alfalahi
The trichomes and chemical composition of three species of the genus Salvia wild-grown (Salvia lanigera, Salvia spinosa) and cultured (Salvia officinalis) were studied in the Anbar governate, the chemical components of the stem and leaves were studied by Gas chromatography–mass spectrometry(GC-MS), in addition to studying the trichomes of the epidermis in the stem and leaves (upper and lower epidermis) by Light microscope. Important differences appeared to us in the chemical study, where it was found that some compounds were found in species without others, which gives them taxonomic importance, also, the trichomes were important in distinguishing the studied species, the species S. spinosa was distinguished by the presence of glandular trichome with funnel form head on the lower epidermis of the leaves and absence non-glandular multicellular-uniseriate flagellated trichomes. S. officinalis was distinguished by the density of non-glandular multicellular-uniseriate –flagellated trichomes, while S. lanigera was distinguished by non-glandular multicellular-uniseriate –branched trichomes, addition to the presence non-glandular multicellular-uniseriate – straight, curved and glandular trichome with globular head in all studied species.
研究了安巴尔省三种野生鼠尾草属(Salvia lanigera, Salvia spinosa)和人工鼠尾草属(Salvia officinalis)的毛状体和化学成分,采用气相色谱-质谱联用技术(GC-MS)对其茎叶的化学成分进行了研究,并在光镜下对其茎叶表皮(上表皮和下表皮)的毛状体进行了研究。我们在化学研究中发现了重要的差异,其中发现一些化合物在物种中没有发现其他化合物,这使得它们在分类上具有重要意义,此外,毛状体对于区分所研究的物种很重要,刺叶草的种类是由叶片下表皮上有漏斗状头的腺状毛状体和没有非腺状多细胞单毛鞭毛状体来区分的。officinalis以非腺状多细胞单毛鞭毛的密度来区分,而S. lanigera则以非腺状多细胞单毛分枝毛的密度来区分,并且在所有被研究物种中都存在非腺状多细胞单毛的直毛、弯毛和球状头腺毛。
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引用次数: 0
Compute Nano topology by used the programing language python 利用python编程语言计算纳米拓扑结构
Pub Date : 2023-06-25 DOI: 10.25130/tjps.v28i3.1437
Nawfal N. Abed, A. Shihab
The research aims to Compute the Nano topologies of any set, consisting of five or less elements, through the Python programming language, with finding the necessary algorithms for the solution steps, We explain the mechanism of action: In first we will find the equivalence relations on set, and then we must compute the nano topology, and end know who set was semi-open, alpha-open,beta-open Regular open ,pre open and gamma-open set .
本研究的目的是通过Python编程语言计算任何由五个或五个以下元素组成的集合的纳米拓扑,并找到求解步骤所需的算法。我们解释了作用机制:首先我们将找到集合上的等价关系,然后我们必须计算纳米拓扑,最后知道哪个集合是半开、α开、β开、正则开、预开和γ开集合。
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引用次数: 0
Ecology, Morphology and Molecular Confirmation of Chaetogaster limnaei (Annelida: Naididae) retrieved from freshwater snail Physa acuta from Greater Zab River, Iraq. 伊拉克大扎布河淡水蜗牛尖裂螺(Physa acuta)的生态学、形态学和分子鉴定。
Pub Date : 2023-06-25 DOI: 10.25130/tjps.v28i3.1421
Shwan Khursheed Bashê
The present study is concerned with the Chaetogaster limnaei retrieved from the freshwater snail Physa acuta collected from (March-October 2021) from various locations near Chama-dubz village on the Greater Zab River, Erbil province, Iraq. Some Physicochemical variables, like water temperature, pH, Dissolved Oxygen, and Calcium ion experiment on a freshwater snail. The result showed statistically significant differences among Monthly variations with variables (number of snails, water temperature, pH and DO, and Calcium ion). In addition, isolated the Chaetogaster limnaei from Physa acuta with a prevalence was 5.75% (33/574), which has no dorsal and ventral chaeta approximately 14 to 20 per bundle, lack in segments 3 to 5, and chaetae and a vestige of a prostomium with sharply bent teeth. The identified morphologically and molecularly confirmed by using a COI sequence marker confirmed a 100% match to species with accession number (KF952336.1). As a result, the current study is the first report of Chaetogaster limnaei in Iraq, supported by phylogenetic analysis using Maximum Likelihood and Maximum Parsimony Methods.
本研究涉及从伊拉克埃尔比勒省大扎布河Chama-dubz村附近不同地点采集的淡水蜗牛Physa acuta中提取的Chaetogaster limnaei(2021年3月至10月)。一些物理化学变量,如水温,pH值,溶解氧,钙离子对淡水蜗牛的实验。结果表明,钉螺数量、水温、pH和DO、钙离子等变量的月变化具有统计学意义。此外,从尖裂Physa actuta中分离到的Chaetogaster limnaei患病率为5.75%(33/574),每束无背侧和腹侧毛羽,约14 ~ 20个,3 ~ 5节缺毛羽,有残残的原口,齿尖弯曲。利用COI序列标记对鉴定的物种进行形态和分子鉴定,证实与加入号(KF952336.1)的物种100%匹配。因此,目前的研究是伊拉克Chaetogaster limnaei的第一份报告,采用最大似然法和最大简约法进行系统发育分析。
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引用次数: 0
Study the change of some physical and chemical properties of TiN under high pressure 研究了TiN在高压下某些理化性质的变化
Pub Date : 2023-06-25 DOI: 10.25130/tjps.v28i3.1427
Nashwa Salhuddin Sultan, Raed Hashim AL-Saqa, Siham J. AL-Faris
The pressure equation of state of Titanium nitrate TiN was investigated in the current work using two equations of state (EOS) from the literature, including the Barden EOS and the Birch-Murnaghan EOS, whereas the Bardeen EOS, which is based on interstellar atomic potentials, and the Birch-Murnaghan EOS, which is based on the solid mechanics notion of finite strain. The EOSs were processed to identify the impacts of high pressure on the bulk modulus B, Debye temperature θD and lattice constant a, which are characterizations of TiN. Ultimately, a fair comparison of the current findings with the first principle approximation and the generalized gradient approximation approach was conducted, and a perfect agreement was found. It was demonstrated that TiN EOS can be used to calibrate high pressure for chemical compound TiN .
本文采用Barden状态方程和Birch-Murnaghan状态方程,即基于星际原子势的Bardeen状态方程和基于有限应变固体力学概念的Birch-Murnaghan状态方程,研究了硝酸钛TiN的压力状态方程。对eos进行了处理,以确定高压对TiN的体积模量B、Debye温度θD和晶格常数a的影响。最后,将目前的发现与第一原理近似和广义梯度近似方法进行了公平的比较,并发现了完全一致的结果。结果表明,TiN EOS可用于化合物TiN的高压标定。
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引用次数: 0
Ion-Pair Complex of Trimethoprim with Alizarin Yellow and its Determination and Extraction by LLE and DLLME 甲氧苄啶与茜素黄的离子对配合物及其液相色谱法和液相色谱法的测定与提取
Pub Date : 2023-06-25 DOI: 10.25130/tjps.v28i3.1422
Araf I. Jabbar, Mohammed Z. Thani, Ali I. Khaleel
For the analysis of trimethoprim medication in its pure form and pharmaceutical formulations, precise and accurate microextraction techniques with UV-Vis measurement have been developed and confirmed. In this study, LLE and DLLME procedures were utilized for the separation, pre-concentration, and evaluation of trimethoprim in pure form and pharmaceutical preparations by UV-Vis spectroscopy at 390 nm. The method was validated and applied to the evaluation of trimethoprim in pharmaceutical formulations. Several experimental factors containing the type of dispersive and extraction solvents and their volumes, pH, temperature, and centrifuging time were carried out. Under the ideal conditions, the procedures were linear in the range of 2–45 and 1-10 mg/L, with a coefficient of determination (R2) of 0.9961 and 0.9992 for LLE and DLLME, respectively. The limit of detection (LOD) was 1.52 and 0.21 mg/L. Recovery of the target analyte in pharmaceutical formulations was 99.3%-104.9%.
为了分析甲氧苄氨嘧啶药物的纯形式和药物配方,已经开发并确认了精确和准确的紫外可见微提取技术。在本研究中,采用LLE和DLLME方法对甲氧苄啶纯品和药物制剂进行分离、预富集和390 nm紫外可见光谱评价。验证了该方法的有效性,并将其应用于复方甲氧苄啶的质量评价。考察了分散溶剂和萃取溶剂的种类及其体积、pH、温度和离心时间等实验因素。在理想条件下,LLE和DLLME在2 ~ 45和1 ~ 10 mg/L范围内呈线性关系,决定系数(R2)分别为0.9961和0.9992。检出限分别为1.52和0.21 mg/L。目的分析物在制剂中的回收率为99.3% ~ 104.9%。
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引用次数: 0
Validity of the Lower Zab River Sediments for Road and Asphalt Works - Southwest of Kirkuk/Northern Iraq 下扎布河沉积物用于道路和沥青工程的有效性-基尔库克西南部/伊拉克北部
Pub Date : 2023-04-27 DOI: 10.25130/tjps.v28i2.1334
Ibrahim Mustafa Hassan, Mohammed Rashid Abood, Lafta Salman Kadhim
In this study, a geotechnical assessment of gravel and sand deposits were conducted on both sides of the Lower Zab River in the southwest of Kirkuk Governorate/Northern Iraq. geologically the sediment related to Quaternary age and tectonically located at the  unstable zone. 5 samples were collected from the study area for the purpose of conducting various geotechnical tests on them and their validity for road works to the sub-base layer and the base layer for asphalt works. The results of the physical tests were shown by grain size analysis of thes aggregates for the samples of the study area, and it was found that they are identical to class (A) According to the American Standard [1], and suitable for use in road works for the sub-base layer. The moisture ratio ranging between (1.95 - 4.26) %. The tests of flatness and elongation showed that the highest percentage of flat-shaped particles was (29%) and longitudinal-shaped particles (19%). The laboratory tests results showed the durability tests such as - Los Angeles test the highest percentage of weight loss was (20.06%), and thus it is valid according to the Iraqi Standard Specification [2] for use in road works. the highest result of test the aggregate impact value of samples is 7.8%, It conforms to the requirements of specifications that must be provided for road works for a sub base layer. Accordingly it is valid for road works. It was found from Proctor test for (5) samples from the study area that the values of the maximum dry density ranged between (2.14-2.28 gm/cm3), and the values of the optimum moisture content ranged between (3.1-2.41%). An asphalt typical mixture was designed for the base layer from the aggregate of the first station S1 as represent station consisting of coarse crushed aggregate 12%, medium crushed aggregate 22%, fine crushed aggregate 20%, river sand 40% and the proportion of filler 6%. The results of the asphalt tests for the ideal station S1 showed that the ideal percentage of asphalt from the weight of the mixture in the asphalt mixture is 4.1, which is within the limits of the specification Roads and Bridges [3]. The percentage of asphalt to the weight of the aggregate after adding the ideal percentage of asphalt showed that its value was 4.3%, As for the stability test result (Marshall), it reached 11.4 kN, and the result of the creep test (Marshall) reached 2.9 mm, and the density was 2.362  
在这项研究中,对基尔库克省西南/伊拉克北部的下扎布河两岸的砾石和砂石沉积物进行了地质技术评价。地质上与第四纪有关,构造上位于不稳定带。我们在研究区内收集了5个样本,对样本进行各种岩土测试,以及测试样本在道路工程至次基层和沥青工程基层的有效性。对研究区样品进行粒度分析,得出物理试验结果,符合美国标准[1](A)级,适合用于道路工程的次基层。含水率在(1.95 - 4.26)%之间。平整度和伸长率试验表明,平板状颗粒比例最高(29%),纵向状颗粒比例最高(19%)。实验室试验结果表明,洛杉矶试验等耐久性试验的减重率最高(20.06%),因此根据伊拉克标准规范[2]适用于道路工程。试验结果最高,样品的总冲击值为7.8%,符合次基层道路工程必须提供的规范要求。因此,它适用于道路工程。通过对研究区5个样品的Proctor检验发现,最大干密度为(2.14 ~ 2.28 gm/cm3),最佳含水量为(3.1 ~ 2.41%)。以第一站S1为代表站,以粗碎骨料12%、中碎骨料22%、细碎骨料20%、河砂40%、填料比例6%为基层设计沥青典型混合料。理想站S1的沥青试验结果表明,沥青混合料在沥青混合料中的理想沥青重量百分比为4.1,在《路桥规范》的限制范围内[3]。加入理想沥青百分比后,沥青占骨料重量的百分比值为4.3%,稳定性试验结果(马歇尔)达到11.4 kN,蠕变试验结果(马歇尔)达到2.9 mm,密度为2.362
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引用次数: 0
2D Electrical Resistivity Imaging to delineate the exact boundary and true thickness of granular aquifers 利用二维电阻率成像技术精确圈定颗粒含水层的边界和真实厚度
Pub Date : 2023-04-27 DOI: 10.25130/tjps.v28i2.1337
B. Q. Aziz, Zana M. Rughzai
Electrical resistivity imaging (ERI) is one of the best geophysical techniques for studying subsurface and groundwater aquifer investigations. In clastic sediments, determining the exact boundary between different layers on the inverse section of ERI is not an easy task due to gradual changes in resistivity between surrounding layers and the granular aquifers. Therefore, the main aim of the study is to indicate a more precise boundary of the granular aquifers (true thickness of aquifers) on the inverse section. Two different models were used: the field model and the laboratory model, in the field model, four different locations were selected. They are located in (Kalar, Chamchamal, Bazyan, and Piramagroon), within the Sulaymaniyah Governorate, NE Iraq. Two-dimensional (2D) electrical resistivity imaging was carried out along four profiles of 355 m length with a five-meter electrode spacing. The Wenner-Schlumberger array was used for recording the data. For the lab model, a laboratory geological model was constructed has length, height, and width equal to 192, 65, and 45 cm, respectively. Two synthetic profiles were carried out on this model, they have lengths of 190 cm with electrode spacing of 10 cm. The field results indicated that aquifers in clastic sediments on inverse sections always showed anomalies with apparent thicknesses larger than their true thicknesses, which were obtained from the geological column of the wells. In the four studied locations, aquifers' average true thickness is approximately 68.2% of the apparent thicknesses on the inverse sections. The result of the laboratory geological model also showed that the true thickness of the unsaturated gravel is approximately equal to 59.7% of the apparent thickness of the anomaly, which is formed by the dry gravel layer. Also, the true thickness of the saturated gravel is about 57.1% of the apparent thickness of the anomaly, which is formed by the saturated gravel layer. Moreover, the geological model showed that the higher resistivity layer (dry gravel) creates a narrower transitional resistivity zone between clay and gravel than saturated gravel of lower resistivity.
电阻率成像(ERI)是研究地下和地下水含水层的最佳地球物理技术之一。在碎屑沉积物中,由于周围层与颗粒含水层之间的电阻率逐渐变化,在ERI逆剖面上确定不同层之间的确切边界并非易事。因此,研究的主要目的是在逆剖面上指示更精确的颗粒含水层边界(含水层的真实厚度)。采用两种不同的模型:现场模型和实验室模型,在现场模型中,选择了四个不同的位置。它们位于伊拉克东北部苏莱曼尼亚省(Kalar、Chamchamal、Bazyan和Piramagroon)。二维(2D)电阻率成像沿着四条355 m长的剖面进行,电极间距为5米。温纳-斯伦贝谢阵列用于记录数据。对于实验室模型,构建了一个长192、高65、宽45 cm的实验室地质模型。在该模型上进行了两个合成廓形,它们的长度为190 cm,电极间距为10 cm。现场结果表明,碎屑沉积物含水层在反剖面上的表观厚度异常总是大于其真实厚度的异常,这是由井的地质柱得到的。在研究的4个地点,含水层的平均真实厚度约为反剖面表观厚度的68.2%。室内地质模型结果还表明,非饱和砾石的真实厚度约为异常视厚度的59.7%,由干砾石层形成。饱和砾石的真实厚度约为异常视厚度的57.1%,由饱和砾石层形成。此外,地质模型表明,高电阻率层(干砾石)与低电阻率饱和砾石相比,在粘土与砾石之间形成了更窄的电阻率过渡带。
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引用次数: 0
Investigate shielding of standard materials and glass for stopping 662 KeV gamma ray penetrations 研究阻挡662 KeV伽马射线穿透的标准材料和玻璃屏蔽
Pub Date : 2023-04-27 DOI: 10.25130/tjps.v28i2.1274
Berun N. Ghafoor, Y. Shwan
Calculations on shielding are required for the building of a gamma ray radiography exposure room to ensure worker exposure to radiation. A measurement used to evaluate the radiation diffusive and absorption characteristics of a medium is the linear attenuation coefficient ( ). Despite the fact that, as radiation moves through a medium, its absorption is influenced by the wavelength of the radiation as well as the thickness and composition of the medium, the linear absorption coefficient is crucial in the interaction of radiation with matter. This research uses a variety of materials as a shield for a gamma radiation source of  emitted by Cs-137. The results obtained using a gamma source with a scintillation counter showed that the Half Value Thickness (HVT) of glass and aluminum were 3.57 cm, and 3.39 cm while for standard materials (concrete, iron, and lead) were 2.98 cm, 1.195 cm, and 0.58 cm respectively.
为了确保工作人员暴露在辐射中,需要对屏蔽进行计算。用来评价介质辐射扩散和吸收特性的一种测量方法是线性衰减系数()。尽管辐射在介质中运动时,其吸收受到辐射波长以及介质的厚度和成分的影响,但在辐射与物质的相互作用中,线性吸收系数是至关重要的。本研究使用多种材料作为屏蔽由铯-137发射的伽马辐射源。利用带闪烁计数器的伽马源得到的结果表明,玻璃和铝的半值厚度分别为3.57 cm和3.39 cm,而标准材料(混凝土、铁和铅)的半值厚度分别为2.98 cm、1.195 cm和0.58 cm。
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引用次数: 1
Modify PRESENT Algorithm by New technique and key Generator by External unit 采用新技术对现有算法进行改进,并利用外部单元实现密钥生成
Pub Date : 2023-04-27 DOI: 10.25130/tjps.v28i2.1340
Ahmed Abdullah Khalil, Awny Muhammed Kaftan, Maytham Mustafa Hammoud
Recently, the widespread use of devices in the field of electronics has caused people to worry about safety. Using traditional cryptographic algorithms to build a complete cryptographic environment for embedded applications or the Internet of Things (IoT) will not be possible due to space, power, and speed limitations. The focus is on lightweight encryption to overcome these problems. In this paper, we have developed the (PRESENT) algorithm, which is among the lightweight algorithms that are used in the IOT and that keeps pace with the requirements of communication speed at the present time. We also used a physical part with the developed algorithm (an external unit that is a USB and using it as a fingerprint for the system) to generate the key while ensuring that the system does not work until after the external unit is connected to the calculator to provide more security for the system from breaches. The developed algorithm achieved a high speed of execution faster than the original algorithm and passed standard tests for various files (text, image, audio, video). In addition to increasing the degree of complexity than the original algorithm.
最近,电子设备在电子领域的广泛使用引起了人们对安全的担忧。由于空间、功率和速度的限制,使用传统的加密算法为嵌入式应用程序或物联网(IoT)构建完整的加密环境是不可能的。重点是轻量级加密,以克服这些问题。在本文中,我们开发了(PRESENT)算法,它是物联网中使用的轻量级算法之一,符合当前对通信速度的要求。我们还使用了一个具有开发算法的物理部分(一个外部单元,它是一个USB,并将其用作系统的指纹)来生成密钥,同时确保系统在外部单元连接到计算器之后才工作,从而为系统提供更大的安全性。所开发的算法实现了比原算法更快的高执行速度,并通过了各种文件(文本、图像、音频、视频)的标准测试。除了比原算法增加了复杂度之外。
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引用次数: 0
Preparation, Characterization, Anti-cancer and Antibacterial Evaluation of New Schiff base and Tetrazole Derivatives 新型希夫碱和四唑衍生物的制备、表征、抗癌和抗菌评价
Pub Date : 2023-04-27 DOI: 10.25130/tjps.v28i2.1333
Yuosra Khalaf Alasadi, Fawzi Hameed Jumaa, Mohammed Ghanam Mukhlif, , Safa Mahmood Shawkat
This work involved the synthesis of tetrazole derivatives 4,4'-(((sulfonylbis(4,1-phenylene))bis(diazene-2,1-dil))bis(2-(1-(4-R)phenyl]-4),5-Dihydro-1H-tetrazol-5-yl(phenol) (where R = OH or OCH3) through the reaction of the substituted amine in THF as a solvent, with sodium azide. FT-IR 1H-NMR Spectrophotometric methods were used to characterize the prepared compounds, the antibacterial activity against four types of bacteria have been studied where it has been proven that tetrazole compounds are more effective than the compounds from which it was derived, and the anticancer activity measured against MCF-7 strains of human breast cells of the synthesized compounds.
这项工作涉及通过取代胺在四氢呋喃中作为溶剂与叠氮化钠反应合成四氮唑衍生物4,4'-(((磺酰基双(4,1-苯))双(二氮-2,1-二))双(2-(1-(4-R)苯基)-4),5-二氢- 1h -四氮-5-基(苯酚)(其中R = OH或OCH3)。利用FT-IR - 1H-NMR分光光度法对所制备的化合物进行了表征,研究了其对四种细菌的抗菌活性,证明了四唑类化合物比其衍生化合物更有效,并测定了所合成化合物对人乳腺MCF-7菌株的抗癌活性。
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引用次数: 0
期刊
Tikrit Journal of Pure Science
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