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Effect of grain size on the deformation mechanism and fracture behavior of a non-equiatomic CoCrNi alloy with low stacking fault energy 晶粒尺寸对具有低堆积断层能的非等原子 CoCrNi 合金的变形机制和断裂行为的影响
IF 9.4 1区 材料科学 Q1 ENGINEERING, MECHANICAL Pub Date : 2024-09-12 DOI: 10.1016/j.ijplas.2024.104129

Manipulation of stacking fault energy (SFE) plays a significant role in microstructure control and in turn mechanical properties of advanced alloys. In this work, we present the influence of grain size on the mechanical properties and fracture behavior of a non-equiatomic CoCrNi alloy with low SFE. Specimens with controlled grain sizes ranging from 0.61 to 6.4 µm were fabricated through rolling and annealing. A novel SFs-dominated plastic deformation mechanism was discovered. Tensile strength decreases monotonically with increasing grain size, while ductility achieves a peak value at the medium grain size, contradicting with the typical behavior observed in most single-phase face-centered cubic (FCC) metallic materials deformed primarily by dislocation slips and/or twinning. The fracture behavior changes from void coalescence to quasi cleavage with grain coarsening, and the fracture mechanisms were analyzed. Additionally, the evolution of SFs and phase transformation is explored at various deformation strains.

堆积断层能(SFE)的控制在微观结构控制以及先进合金的机械性能方面发挥着重要作用。在这项研究中,我们介绍了晶粒大小对低 SFE 非等原子 CoCrNi 合金的机械性能和断裂行为的影响。我们通过轧制和退火制作了晶粒大小在 0.61 到 6.4 µm 之间的试样。发现了一种以 SFs 为主导的新型塑性变形机制。拉伸强度随着晶粒尺寸的增大而单调降低,而延展性则在中等晶粒尺寸时达到峰值,这与大多数单相面心立方(FCC)金属材料主要通过位错滑移和/或孪晶变形所观察到的典型行为相矛盾。断裂行为随着晶粒的粗化而从空隙凝聚变为准劈裂,并对断裂机制进行了分析。此外,还探讨了各种变形应变下 SFs 的演变和相变。
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引用次数: 0
Revealing the fatigue strengthening and damage mechanisms of surface-nanolaminated gradient structure 揭示表面氨化梯度结构的疲劳强化和损伤机理
IF 9.4 1区 材料科学 Q1 ENGINEERING, MECHANICAL Pub Date : 2024-09-10 DOI: 10.1016/j.ijplas.2024.104128

Extending the fatigue life of metals is a critical concern for maintaining material and component integrity in engineering systems. The integration of gradient structures within materials represents a highly promising approach to enhance the fatigue properties in metallic materials, while a detailed mechanistic understanding of the fatigue damage evolution of such structures is yet to be developed. Here, we report that the surface-nanolaminated gradient structure comprised of nanolaminates and hierarchical twins imparts remarkable resistance to both low-cycle and high-cycle fatigue. A dislocation-based strain gradient crystal plasticity model is developed to investigate the strengthening and damage mechanisms of our gradient structure. The size dependence of the initial dislocation density, its evolution and back stress hardening are taken into account and verified by the experimental data. The simulation results reveal that the strain delocalization and back stress hardening induced by the structure gradient significantly mitigate the fatigue damage accumulation. Additionally, in contrast to conventional gradient structures, the mechanical stability of the present structure enables these strengthening mechanisms to persist until crack initiation. These effects, combined with the sequential toughening mechanisms activated in the surface-nanolaminated gradient structure, ensure a marked life extension under low-cycle fatigue (by a factor of four), outperforming conventional gradient and other microstructural design strategies. Finally, a multiscale anti-fatigue design principal for damage homogenization is given based on the prior quantitative analysis.

延长金属的疲劳寿命是保持工程系统中材料和部件完整性的关键问题。在材料中集成梯度结构是增强金属材料疲劳性能的一种极具前景的方法,但对此类结构疲劳损伤演变的详细机理理解尚待开发。在这里,我们报告了由纳米层压板和分层孪晶组成的表面层压梯度结构对低循环和高循环疲劳都具有显著的抗性。我们建立了基于位错的应变梯度晶体塑性模型,以研究梯度结构的强化和损伤机制。该模型考虑了初始位错密度的尺寸依赖性、其演变和背应力硬化,并通过实验数据进行了验证。模拟结果表明,结构梯度引起的应变分散和背应力硬化显著减轻了疲劳损伤的累积。此外,与传统的梯度结构相比,本结构的机械稳定性使这些强化机制能够持续到裂纹产生为止。这些效应与表面消除层梯度结构中激活的连续增韧机制相结合,确保了在低循环疲劳条件下显著延长寿命(4 倍),优于传统梯度结构和其他微结构设计策略。最后,基于先前的定量分析,给出了损伤均质化的多尺度抗疲劳设计原理。
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引用次数: 0
A polycrystal plasticity-cellular automaton integrated modeling method for continuous dynamic recrystallization and its application to AA2196 alloy 连续动态再结晶的多晶塑性-细胞自动机集成建模方法及其在 AA2196 合金中的应用
IF 9.4 1区 材料科学 Q1 ENGINEERING, MECHANICAL Pub Date : 2024-09-08 DOI: 10.1016/j.ijplas.2024.104127

Continuous dynamic recrystallization usually dominates the microstructural evolution in hot working of aluminum alloys, in which the high-angle grain boundaries of new grains mainly originate from the gradual increase in subgrain misorientation angles. In this work, an integrated computational method is proposed to simulate continuous dynamic recrystallization process of aluminum alloys by coupling three-dimensional cellular automaton and visco-plastic self-consistent models. The stress response, dislocation accumulation and recovery, and evolution of crystal orientations are computed in the context of polycrystal plasticity; the formation and rotation of subgrains, followed by stored energy and curvature-driven boundary migration, are captured and visualized by cellular automaton. The non-octahedral slip mode {110}<110> is additionally introduced to capture the 〈001〉 texture during hot compression. A universal cell topology deformation method is adopted to achieve an effective track of grain morphology evolution during plastic deformation. The proposed simulation framework is validated through simulating the isothermal uniaxial compression process of AA2196 alloy under different temperatures and strain rates. The orientation dependence of CDRX during compression is numerically reproduced by correlating the subgrain formation and rotation process with the activation state of slip systems. The simulated macroscopic flow stress, 3D microstructure and inherent microstructural characteristics such as subgrain size, subgrain boundaries and textures are in good agreement with the experimental results. The proposed method provides an effective and efficient tool for multi-scale simulation of hot forming process of aluminum alloys.

连续动态再结晶通常主导着铝合金热加工过程中的微观结构演变,其中新晶粒的高角度晶界主要源于亚晶粒错位角的逐渐增大。本研究提出了一种综合计算方法,通过耦合三维细胞自动机和粘塑性自洽模型来模拟铝合金的连续动态再结晶过程。在多晶体塑性的背景下,计算了应力响应、位错累积和恢复以及晶体取向的演变;细胞自动机捕捉并可视化了亚晶粒的形成和旋转,以及随之而来的储能和曲率驱动的边界迁移。此外,还引入了非八面体滑移模式{110},以捕捉热压过程中的〈001〉纹理。采用通用的单元拓扑变形方法,可有效跟踪塑性变形过程中的晶粒形态演变。通过模拟 AA2196 合金在不同温度和应变率下的等温单轴压缩过程,验证了所提出的模拟框架。通过将亚晶粒的形成和旋转过程与滑移系统的激活状态相关联,在数值上再现了压缩过程中 CDRX 的取向依赖性。模拟的宏观流动应力、三维微观结构和固有微观结构特征(如亚晶粒尺寸、亚晶粒边界和纹理)与实验结果非常吻合。所提出的方法为铝合金热成形过程的多尺度模拟提供了有效的工具。
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引用次数: 0
A generalised framework for modelling anisotropic creep-ageing deformation and strength evolution of 2xxx aluminium alloys 2xxx 铝合金各向异性蠕变时效变形和强度演变建模的通用框架
IF 9.4 1区 材料科学 Q1 ENGINEERING, MECHANICAL Pub Date : 2024-09-07 DOI: 10.1016/j.ijplas.2024.104114
The 2xxx aluminium alloys are extensively applied in the aerospace industry due to their lightweight and balanced performance characteristics. However, a comprehensive method for modelling both the anisotropic creep deformation and strengthening behaviour in creep age forming (CAF) for 2xxx aluminium alloys remains lacking. This paper presents a generalised framework for establishing constitutive models capable of describing the anisotropic creep deformation coupled with the microstructure and material strength evolutions during creep-ageing of both the original and the pre-deformed 2xxx series Al alloys. This framework extends the rolling direction-based material model to anisotropic scenarios at varying angles between the loading and rolling directions, by employing the non-uniform rational B-splines (NURBS). The details about the anisotropic model calibration and numerical simulation implementation are demonstrated. The feasibility of this method was verified by its application to various 2xxx series aluminium alloys with or without pre-deformation, through constitutive modelling and numerical simulation, with satisfactory agreements between prediction and experimental data. For the first time, the proposed framework provides a generalised routine for establishing anisotropic creep-ageing models for various 2xxx aluminium alloys.
2xxx 铝合金因其重量轻、性能均衡等特点而被广泛应用于航空航天工业。然而,对于 2xxx 铝合金的各向异性蠕变变形和蠕变时效成形 (CAF) 中的强化行为,仍然缺乏一种全面的建模方法。本文提出了一个通用框架,用于建立能够描述原始和预变形 2xxx 系列铝合金蠕变时效过程中各向异性蠕变变形以及微观结构和材料强度演变的构成模型。该框架通过采用非均匀有理 B-样条曲线(NURBS),将基于轧制方向的材料模型扩展到加载方向和轧制方向之间不同角度的各向异性情况。演示了各向异性模型校准和数值模拟实现的细节。通过构造建模和数值模拟,将该方法应用于有或无预变形的各种 2xxx 系列铝合金,验证了该方法的可行性,并在预测和实验数据之间取得了令人满意的一致。所提出的框架首次为建立各种 2xxx 铝合金的各向异性蠕变时效模型提供了通用方法。
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引用次数: 0
Atomistic analysis of the mechanisms underlying irradiation-hardening in Fe–Ni–Cr alloys 铁-镍-铬合金辐照硬化机理的原子分析
IF 9.4 1区 材料科学 Q1 ENGINEERING, MECHANICAL Pub Date : 2024-09-06 DOI: 10.1016/j.ijplas.2024.104118

This work presents a comprehensive examination of the physical mechanisms driving hardening in irradiated face-centered cubic FeNiCr alloys. The evolution of irradiation-induced defects during shear deformation is modeled by atomistic simulations through overlapping cascade simulations, where the nucleation and evolution of dislocation loops is validated by transmission electron microscopy images obtained from irradiated FeNiCr alloys using tandem accelerator. The effect of different shear rates on the microstructure of irradiated materials with a specific focus on the changes in the density of voids and dislocation loops induced by irradiation was analyzed. Additionally, the fundamental interaction processes between single irradiation-induced defects contributing to irradiation hardening, such as voids and dislocation loops in the alloy are explained. The analysis at atomic level indicates that both the dislocation loops and the voids exhibit strengthening effects. Furthermore, the nanometric voids are much stronger obstacles than dislocation loops of comparable size. The mechanism of cutting the voids leads to an increase of voids density and thus contributes to an increase in irradiation hardening. The mechanism of collapse of small voids into dislocation loops leads to decrease of voids density and at the same time increase of loops density. The coupling effect between the density of voids and dislocation loops is determined. Finally, the novel, physical mechanisms-based model of irradiation hardening and dislocation-radiation defect reaction kinetics are developed, which consider the mechanisms of void cutting, void shrink and void collapse to dislocation loop.

这项研究全面考察了辐照面心立方铁镍铬合金硬化的物理机制。通过重叠级联模拟,以原子模拟的方式模拟了剪切变形过程中辐照诱导的缺陷演变,并通过串联加速器辐照铁镍铬合金后获得的透射电子显微镜图像验证了位错环的成核和演变。分析了不同剪切速率对辐照材料微观结构的影响,重点是辐照引起的空隙密度和位错环的变化。此外,还解释了导致辐照硬化的单一辐照诱导缺陷(如合金中的空洞和位错环)之间的基本相互作用过程。原子层面的分析表明,位错环和空隙都表现出强化效应。此外,纳米空隙比大小相当的差排环更能起到强化作用。切割空隙的机制导致空隙密度增加,从而有助于提高辐照硬化。小空隙塌缩为差排环的机制导致空隙密度降低,同时差排环密度增加。确定了空隙密度和差排环密度之间的耦合效应。最后,建立了基于物理机制的新型辐照硬化模型和位错-辐照缺陷反应动力学模型,其中考虑了空隙切割、空隙收缩和空隙塌缩为位错环的机制。
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引用次数: 0
Tailoring Mechanical Properties of Pearlitic Steels through Size Regulation of Multiscale Microstructures: Experiments and Simulations 通过多尺度微结构的尺寸调节定制珠光体钢的机械性能:实验与模拟
IF 9.4 1区 材料科学 Q1 ENGINEERING, MECHANICAL Pub Date : 2024-09-06 DOI: 10.1016/j.ijplas.2024.104110
Pearlitic steels possess excellent mechanical properties due to their multiscale microstructures, yet this configuration introduces complex size and interface effects, impeding the elucidation of their microscopic deformation mechanisms. In this study, a predictive framework that combines a high-resolution reconstruction algorithm with a strain gradient crystal plasticity model was developed to investigate the relationship between local deformation behaviors in nodules, colonies, and lamellae of various sizes and their mechanical properties. This approach effectively reconstructs the multiscale structures of pearlite and accurately tracks the dynamic mechanical responses. The integrated experimental and computational findings highlight the critical role of microstructure sizes in regulating strain delocalization and dislocation dynamics, which, through strain partitioning and interface density, are vital for optimizing mechanical properties. Notably, a decrease in lamellar spacing and nodule size significantly enhances both strength and toughness, while smaller nodules and colonies promote increased plasticity. Finally, a dual-parameter Hall-Petch equation incorporating lamellar spacing and nodule size is introduced, enabling precise quantification of the impact of all microstructures in pearlite on mechanical properties with robust predictive capabilities.
珠光体钢因其多尺度微观结构而具有优异的机械性能,但这种结构带来了复杂的尺寸和界面效应,阻碍了其微观变形机制的阐明。本研究开发了一个预测框架,该框架将高分辨率重建算法与应变梯度晶体塑性模型相结合,用于研究不同尺寸的结核、菌落和薄片的局部变形行为与其力学性能之间的关系。这种方法有效地重建了珠光体的多尺度结构,并准确地跟踪了动态力学响应。实验和计算的综合结果凸显了微观结构尺寸在调节应变分散和位错动力学中的关键作用,而应变分散和位错动力学通过应变分配和界面密度对优化机械性能至关重要。值得注意的是,减少薄片间距和结节尺寸可显著提高强度和韧性,而较小的结节和菌落则可提高塑性。最后,介绍了包含片层间距和结核尺寸的双参数霍尔-佩奇方程,从而能够精确量化珠光体中所有微结构对力学性能的影响,并具有强大的预测能力。
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引用次数: 0
A flexible yield criterion for strength modeling from biaxial compression to biaxial tension 用于从双轴压缩到双轴拉伸强度建模的灵活屈服准则
IF 9.4 1区 材料科学 Q1 ENGINEERING, MECHANICAL Pub Date : 2024-09-05 DOI: 10.1016/j.ijplas.2024.104113

Accurate strength modeling from equi-biaxial tension (EBT) to equi-biaxial compression (EBC) is critical for the plastic behavior prediction covering the wide-range of stress triaxiality encountered in sheet metal forming. To date, however, few yield criteria are available that can precisely model the initial yield and hardening behavior under six typical stress states between EBC and EBT, simultaneously. Furthermore, there is still a lack of a unified yield criterion for accurate strength modeling across various stress state ranges. To address the issues, a theoretical framework for constructing yield criteria dependent on stress states is provided and a new analytically described isotropic yield criterion is presented in this study. The flexibility in terms of the yield locus and application range is thoroughly explored to make the new yield criterion general. Subsequently, the isotropic yield criterion is extended into an analytically described anisotropic-asymmetric yield criterion. Furthermore, the extended yield criterion is applied to capture the initial yield behavior of DP980, AA5754-O, and AZ31 sheets, and the strain hardening behavior of QP1180 sheets at various stress states ranging from EBC to EBT along different loading directions. The predicted results from the extended criterion agree well with the corresponding experimental findings. The applications demonstrate that the proposed anisotropic-asymmetric yield criterion can effectively model the initial yield and hardening behavior of HCP, BCC, and FCC metal sheets under EBT, EBC, uniaxial tension (UT), plane strain tension (PST), shear (SH), and uniaxial compression (UC) in an analytical way.

从等轴拉伸(EBT)到等轴压缩(EBC)的精确强度建模对于塑性行为预测至关重要,它涵盖了金属板材成型过程中遇到的各种应力三轴性。然而,迄今为止,很少有屈服标准能同时精确模拟 EBC 和 EBT 之间六种典型应力状态下的初始屈服和硬化行为。此外,目前仍缺乏统一的屈服标准,无法对各种应力状态范围进行精确的强度建模。为了解决这些问题,本研究提供了一个构建依赖于应力状态的屈服准则的理论框架,并提出了一个新的分析描述各向同性屈服准则。研究深入探讨了屈服点和应用范围的灵活性,使新的屈服准则具有通用性。随后,将各向同性屈服准则扩展为分析描述的各向异性-不对称屈服准则。此外,扩展屈服准则还用于捕捉 DP980、AA5754-O 和 AZ31 板材的初始屈服行为,以及 QP1180 板材沿不同加载方向从 EBC 到 EBT 的各种应力状态下的应变硬化行为。扩展准则的预测结果与相应的实验结果非常吻合。这些应用表明,所提出的各向异性-不对称屈服准则可以有效地模拟 HCP、BCC 和 FCC 金属板在 EBT、EBC、单轴拉伸 (UT)、平面应变拉伸 (PST)、剪切 (SH) 和单轴压缩 (UC) 下的初始屈服和硬化行为。
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引用次数: 0
Local element segregation-induced cellular structures and dominant dislocation planar slip enable exceptional strength-ductility synergy in an additively-manufactured CoNiV multicomponent alloy with ageing treatment 局部元素偏析诱导的蜂窝状结构和主要位错平面滑移使经过时效处理的添加式制造 CoNiV 多组分合金具有卓越的强度-电导率协同效应
IF 9.4 1区 材料科学 Q1 ENGINEERING, MECHANICAL Pub Date : 2024-09-03 DOI: 10.1016/j.ijplas.2024.104112

We proposed an additively manufactured equiatomic CoNiV multicomponent alloy (MCA) using a conventional laser powder bed fusion (LPBF) method, and an exceptional strength-ductility synergy of the alloy was attained through a simple post-ageing treatment. Pronounced hierarchical microstructures were achieved in our printed alloys, including heterogeneous grain structures, and intragranular cellular structures composed of interior domain with limited dislocations and cell walls led by significant vanadium local segregation. Besides the outstanding mechanical properties at room temperature of 298 K, a giga-pascal yielding strength (> 1.1 GP) and over 40% uniform elongation were attained in the aged specimen deformed at a cryogenic temperature of 77 K, predominating the mechanical properties of many alloys reported in previous works. Such exceptional performance of the aged alloy can be mainly ascribed to considerable local chemical orders (LCOs), aggravated elemental fluctuation in the alloy matrix, and intensified vanadium segregation at walls of intragranular cellular structures which can strongly interact with dislocations. As a result, a planar slip array of dislocations with an extremely high density, namely large numbers of slip bands that can sustain and transfer high strains, dominates the deformation microstructures, thus efficiently strengthening and toughening the aged alloy, especially at a low temperature like 77 K. The above post-ageing strategy is readily and low-costly employed on additively manufactured MCAs with relatively high stacking fault energy (SFE) and proved as a feasible method to produce high-performance structural materials for extreme conditions.

我们利用传统的激光粉末床熔融(LPBF)方法提出了一种添加式制造的等原子 CoNiV 多组分合金(MCA),并通过简单的后时效处理实现了合金的优异强度-电导率协同效应。我们的打印合金实现了明显的分层微结构,包括异质晶粒结构,以及由具有有限位错的内部畴和由显著的钒局部偏析导致的细胞壁组成的粒内细胞结构。除了在 298 K 室温下具有出色的机械性能外,在 77 K 低温下变形的老化试样还达到了千兆帕屈服强度(1.1 GP)和超过 40% 的均匀伸长率,这在之前报告的许多合金的机械性能中占主导地位。老化合金之所以具有如此优异的性能,主要归因于大量的局部化学有序(LCOs)、合金基体中元素波动加剧以及晶内蜂窝结构壁上的钒偏析加剧,而钒偏析会与位错产生强烈的相互作用。因此,具有极高密度的位错平面滑移阵列(即大量可承受和传递高应变的滑移带)主导了变形微结构,从而有效地强化和韧化了老化合金,尤其是在 77 K 这样的低温条件下。
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引用次数: 0
Influence of textural variability on plastic response of porous crystal embedded in polycrystalline aggregate: A crystal plasticity study 纹理变化对嵌入多晶骨料的多孔晶体塑性响应的影响:晶体塑性研究
IF 9.4 1区 材料科学 Q1 ENGINEERING, MECHANICAL Pub Date : 2024-09-03 DOI: 10.1016/j.ijplas.2024.104117

Damage evolution in polycrystalline aggregates is complicated by the intricate interplay of crystallographic orientation of the porous grain and the surrounding anisotropic matrix. Therefore, formulation of design rules and damage models for polycrystalline materials proves daunting due to relative lack of thorough understanding of the underlying heterogeneity at the mesoscale. This work explores the orientation dependent void growth in a porous crystal embedded in an anisotropic polycrystalline matrix with different initial textures. Polycrystalline face-centered cubic based aggregate is simulated within the framework of crystal plasticity finite element method. Porosity is first modeled in the form of a single pre-existing spherical void in the central grain of the randomly oriented polycrystal. One-hundred crystallographic orientations of the central grain in three-dimensional Euler space are analyzed to reveal the orientation dependent trends of the porous grain. To account for textural variability, the analysis is repeated for polycrystals exhibiting preferred textures like Cube, Brass, Copper and Goss. In this manner, interesting orientation dependent trends in basic tenets of void growth like yield strength, coalescence strain and porosity evolution are unraveled across various polycrystalline textures. To account for spatial heterogeneity as well, porosity in the central grain is then re-distributed and the aforementioned analysis is repeated for all the crystallographic orientations of the central grain embedded in polycrystals with different textures. Owing to the large amount of data thus generated, statistical analysis is invoked to identify stimulating trends and key statistical variables governing the strength and toughness. Consequently, a statistical void growth model is also presented by assessing the CP simulation results and identifying suitable distribution function governing the growth of voids in polycrystals. The modeling framework is expected to inform porous plasticity models aimed at capturing damage evolution in porous grains embedded in polycrystalline materials exhibiting topological and crystallographic anisotropy.

由于多孔晶粒的晶体学取向与周围各向异性基体之间错综复杂的相互作用,多晶聚集体中的损伤演化非常复杂。因此,由于对中观尺度的基本异质性缺乏透彻的了解,为多晶材料制定设计规则和损伤模型显得十分困难。这项研究探索了嵌入各向异性多晶基体中的多孔晶体中与取向相关的空隙生长,其初始纹理各不相同。在晶体塑性有限元法框架内模拟了基于面心立方的多晶骨料。多孔性首先以随机取向多晶体中心晶粒中单个预先存在的球形空隙形式建模。通过分析中央晶粒在三维欧拉空间中的 100 种晶体学取向,揭示了多孔晶粒的取向趋势。为了考虑纹理的可变性,还对多晶体的首选纹理(如立方体、黄铜、铜和戈斯)进行了重复分析。通过这种方式,我们揭示了各种多晶质地的空隙生长基本原理的有趣取向依赖趋势,如屈服强度、凝聚应变和孔隙率演变。为了考虑空间异质性,中心晶粒中的孔隙率将重新分布,并对嵌入不同质地多晶体中的中心晶粒的所有晶体学取向重复上述分析。由于由此产生了大量数据,因此需要进行统计分析,以确定影响强度和韧性的刺激趋势和关键统计变量。因此,通过评估 CP 模拟结果和确定支配多晶体中空隙增长的合适分布函数,还提出了一个统计空隙增长模型。该建模框架有望为多孔塑性模型提供信息,该模型旨在捕捉嵌入多晶材料中的多孔晶粒的损伤演变,这些多晶材料表现出拓扑和晶体学各向异性。
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引用次数: 0
Automated analysis framework of strain partitioning and deformation mechanisms via multimodal fusion and computer vision 通过多模态融合和计算机视觉自动分析应变分区和变形机制的框架
IF 9.4 1区 材料科学 Q1 ENGINEERING, MECHANICAL Pub Date : 2024-09-03 DOI: 10.1016/j.ijplas.2024.104119

Simultaneously investigating strain partitioning and the underlying deformation mechanisms for both the grain interior and the grain boundary (GB) is essential for understanding the complex plastic deformation of hexagonal close-packed metals. To this end, an automated analysis framework based on high-resolution digital image correlation (HRDIC) and electron backscatter diffraction (EBSD) data fusion and computer vision, integrating nanoscale resolution and a large field of view, is proposed. This framework consists of: (1) HRDIC-EBSD data fusion; (2) Segmenting the strain field into individual grains each with a core and a mantle; (3) Data clustering of the Matrix and slip bands (SBs) for each grain; (4) Full slip system (SS) identification and SS assignment to the SBs. The capabilities of this framework were demonstrated on Mg-10Y during compression. The strain field data, which was segmented into different clusters, including grain mantle, grain core, Matrix, and SBs, was analyzed statistically and quantitatively. The pixel-based slip activity, which considers the SB morphology, was obtained from a statistical perspective. Inter-granular accommodating mechanisms, including GB strain, slip transfer, and GB sliding, were quantitatively analyzed. Overall, this analysis framework, which can be applied to other materials, can automatically and statistically evaluate both nanoscale strain fields and underlying intra- and inter-granular deformation mechanisms grain-by-grain. This work provides valuable experimental insights into plastic deformation and accommodation mechanisms for polycrystals.

同时研究晶粒内部和晶粒边界(GB)的应变分配和基本变形机制对于理解六方紧密堆积金属的复杂塑性变形至关重要。为此,我们提出了一种基于高分辨率数字图像相关(HRDIC)和电子反向散射衍射(EBSD)数据融合以及计算机视觉的自动分析框架,该框架集成了纳米级分辨率和大视场。该框架包括(1) HRDIC-EBSD 数据融合;(2) 将应变场划分为单个晶粒,每个晶粒都有一个核心和一个地幔;(3) 对每个晶粒的矩阵和滑移带 (SB) 进行数据聚类;(4) 对 SB 进行全滑移系统 (SS) 识别和 SS 分配。该框架的功能在 Mg-10Y 压缩过程中得到了验证。应变场数据被分割成不同的群组,包括晶粒地幔、晶粒核心、矩阵和 SB,并进行了统计和定量分析。从统计角度获得了基于像素的滑移活动,其中考虑了 SB 形态。定量分析了晶粒间的容纳机制,包括 GB 应变、滑移转移和 GB 滑动。总之,该分析框架可应用于其他材料,能自动并以统计方式评估纳米级应变场以及潜在的逐晶粒内部和晶粒间变形机制。这项工作为多晶体的塑性变形和容纳机制提供了宝贵的实验见解。
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引用次数: 0
期刊
International Journal of Plasticity
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