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Near-α titanium alloy dwell load-induced deformation twinning to coordinate the deformation mechanism associated with crack initiation 耳-α钛合金停留在载荷诱导的变形孪晶中,以协调与裂纹萌发相关的变形机制
IF 9.4 1区 材料科学 Q1 ENGINEERING, MECHANICAL Pub Date : 2024-09-02 DOI: 10.1016/j.ijplas.2024.104116

In this study, we identified a specific phenomenon of coordinated deformation of twins in near-α titanium alloys during dwell fatigue (DF). The main crack source regions and internal cracks in the micro-texture region (MTR) and no-MTR samples with inconsistent orientation characteristics were characterized. The results demonstrate that the main cracks in all specimens are aligned with the (0001) basal plane, which is associated with basal slip. Notably, twins are found and confirmed to be involved in the DF crack initiation process in high Al content near-α Ti60 alloys where deformation twins are rare, and tend to nucleate at the DF basal cracks. Further in-situ dwell investigation reveals and proposes that the dislocation pile-up and prismatic-basal (PB) interfacial features between soft/hard grains lead to deformation twin nucleation and growth from hard grain boundaries. Concurrently, the pyramidal 〈c+a〉 dislocation slip is observed to be in concurrent operation with the induced twins. These findings suggest that deformation twins not only coordinate basal grain deformation but also hinder the initiation and propagation of basal cracks caused by basal 〈a〉 slip. Moreover, a high density of pyramidal 〈c+a〉 dislocations within the twin and their dissociation to form basal stacking faults (SFTs) with a specific nanometric spacing make the twinning process accompanied by significant lattice distortions inside the twin. These newly formed nanotwin boundaries and SFTs act as barriers to dislocation motion, enhancing the strength and DF lifetime of near-α Ti60 alloys and effectively reducing the dwell sensitivity of no-MTR alloys. Our findings extend the understanding of the coordinated roles of dislocation slip, twin nucleation and formation of basal SFTs in near-α titanium alloys in dwell fatigue.

在这项研究中,我们发现了近α钛合金在驻留疲劳(DF)过程中孪生体协调变形的特殊现象。我们对具有不一致取向特征的微纹理区 (MTR) 和无 MTR 试样中的主要裂纹源区域和内部裂纹进行了表征。结果表明,所有试样的主要裂纹都与 (0001) 基底面对齐,这与基底滑移有关。值得注意的是,在高铝含量的近α Ti60 合金中,孪晶被发现并证实参与了 DF 裂纹的萌生过程,在这种合金中,变形孪晶非常罕见,而且往往在 DF 基底裂纹处成核。进一步的原位驻留研究发现并提出,软/硬晶粒之间的位错堆积和棱柱基底(PB)界面特征导致变形孪晶从硬晶粒边界成核和生长。与此同时,还观察到金字塔形位错滑移与诱导孪晶同时发生作用。这些发现表明,变形孪晶不仅能协调基底晶粒变形,还能阻碍由基底滑移引起的基底裂纹的产生和扩展。此外,孪晶内金字塔形位错的高密度及其解离形成了具有特定纳米间距的基底堆积断层(SFT),使得孪晶过程伴随着孪晶内部显著的晶格畸变。这些新形成的纳米孪晶边界和 SFT 起到了阻碍位错运动的作用,从而提高了近α Ti60 合金的强度和 DF 寿命,并有效降低了无 MTR 合金的驻留敏感性。我们的研究结果扩展了对近α钛合金在驻留疲劳中位错滑移、孪晶成核和基底 SFT 形成的协调作用的理解。
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引用次数: 0
Exceptional strength-ductility synergy in the novel metastable FeCoCrNiVSi high-entropy alloys via tuning the grain size dependency of the transformation-induced plasticity effect 通过调整转变诱导塑性效应的晶粒尺寸相关性,在新型可蜕变铁铬镍硅高熵合金中实现优异的强度-韧性协同效应
IF 9.4 1区 材料科学 Q1 ENGINEERING, MECHANICAL Pub Date : 2024-09-02 DOI: 10.1016/j.ijplas.2024.104115

In-depth knowledge of the coupling between grain refinement and the transformation-induced plasticity (TRIP) effect in metastable alloys is a viable approach for the improvement of strength-ductility synergy, which needs systematic research with consideration of commercial austenitic stainless steels and novel high-entropy alloys (HEAs). Accordingly, in the present work, two Si-containing metastable HEAs in the Fe47Co30Cr10Ni5V8-xSix system (x = 3 and 6 at.%) were designed, and the TRIP-assisted AISI 304L stainless steel was also considered for comparison. The alloys were processed by cold rolling and annealing to obtain different grain sizes. Reducing the stacking fault energy (SFE) through adjusting chemical composition contributes to minimizing the detrimental effect of grain refinement on the ductility of TRIP alloys, while extremely low SFE must be avoided owing to the fast kinetics of deformation-induced martensitic phase transformation, which leads to the deterioration of ductility. In contrast to AISI 304L stainless steel, a strong TRIP effect was maintained upon grain refinement in the Fe47Co30Cr10Ni5V2Si6 HEA due to the remaining apparent SFE in the appropriate TRIP range. The tuned kinetics of martensitic transformation was found to be responsible for the exceptional ductility (∼65 %) of Fe47Co30Cr10Ni5V2Si6 HEA at an ultrahigh tensile strength of ∼1230 MPa. Therefore, considering the identical trend of SFE with grain size, an appropriate initial SFE value is important for tuning the grain size dependency of the TRIP effect. Moreover, the ultrahigh strength was attributed to the high volume fraction of α΄-martensite as well as the high strength of the martensite phase due to the high Si content. Accordingly, for achieving strong-yet-ductile HEAs, a high Si content is recommended to benefit from solid solution strengthening in the martensite phase, a specially-designed chemical composition is needed for attaining a high volume fraction of α΄-martensite, and SFE should be in a desirable range to tune the kinetics of martensitic phase transformation.

深入了解可代谢合金中晶粒细化与转化诱导塑性(TRIP)效应之间的耦合关系是提高强度-电导率协同效应的可行方法,这需要对商业奥氏体不锈钢和新型高熵合金(HEAs)进行系统研究。因此,在本研究中,设计了 Fe47Co30Cr10Ni5V8-xSix 体系(x = 3 和 6 at.%)中的两种含 Si- 的易析出高熵合金,并将 TRIP 辅助的 AISI 304L 不锈钢作为比较对象。合金经过冷轧和退火处理,以获得不同的晶粒大小。通过调整化学成分降低堆叠错能(SFE)有助于最大限度地减少晶粒细化对 TRIP 合金延展性的不利影响,同时必须避免极低的 SFE,因为形变引起的马氏体相变的动力学速度很快,会导致延展性恶化。与 AISI 304L 不锈钢相比,Fe47Co30Cr10Ni5V2Si6 HEA 在晶粒细化后仍能保持较强的 TRIP 效应,这是因为在适当的 TRIP 范围内仍存在表观 SFE。经过调整的马氏体转变动力学被认为是 Fe47Co30Cr10Ni5V2Si6 HEA 在 1230 MPa 的超高拉伸强度下具有优异延展性(∼65 %)的原因。因此,考虑到 SFE 随晶粒尺寸变化的相同趋势,适当的初始 SFE 值对于调整 TRIP 效应的晶粒尺寸依赖性非常重要。此外,超高强度还归因于α΄-马氏体的高体积分数以及高硅含量导致的马氏体相的高强度。因此,要获得强度高但韧性好的 HEA,建议采用高硅含量,以受益于马氏体相的固溶强化;需要专门设计的化学成分,以获得高体积分数的 α΄-马氏体;SFE 应在理想范围内,以调整马氏体相变的动力学。
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引用次数: 0
Excellent strength-ductility synergy assisted by dislocation dipole-induced plasticity in Co-free precipitate-strengthened medium-entropy alloy 在无钴沉淀强化中熵合金中,位错偶极子诱导塑性可实现卓越的强度-电导率协同作用
IF 9.4 1区 材料科学 Q1 ENGINEERING, MECHANICAL Pub Date : 2024-08-31 DOI: 10.1016/j.ijplas.2024.104109

Precipitation strengthening is one of the most effective approaches for developing advanced structural materials with outstanding strength-ductility combinations. However, most compositional designs of precipitate-strengthened HEAs/MEAs compromise the cost-property tradeoff owing to the addition of expensive Co element. In this study, a Co-free FeCrNi-based precipitate-strengthened medium entropy alloy (denoted as Al0.2Cr0.9FeNi2.2Ti0.2) with a near-equiatomic FeCrNi matrix and a high content (∼ 35 %) L12 nanoprecipitates was designed using a mixing strategy. The microstructural features, mechanical performance, deformation substructure evolution, and strengthening mechanisms were systematically investigated using EBSD, TEM, and APT. Tensile tests indicated that the current alloy aged within a moderate temperature range achieved an exceptional strength-ductility combination compared to existing Co-containing and Co-free HEAs/MEAs. Particularly, the alloy aged at 700 ℃ (denoted as 700A) demonstrated a high ultimate tensile strength of 1606 MPa and a large ductility of 25 %, benefiting from both precipitation hardening and an unusual strain-hardening sustainability. Such anomalous strain-hardening sustainability can be attributed to the dislocation dipole-induced plasticity. High-density dislocation dipoles can simultaneously provide additional strain hardening by reducing the dislocation mean free path and enhance plastic deformation compatibility by acting as stress delocalization origins, thereby contributing to excellent strength-ductility synergy. These findings will not only open a new door for the future development of high-performance Co-free precipitate-strengthened HEAs/MEAs, but also deepen the understanding of the work-hardening mechanisms in these alloys.

沉淀强化是开发具有出色强度-性能组合的先进结构材料的最有效方法之一。然而,由于添加了昂贵的钴元素,大多数沉淀强化 HEAs/MEAs 的成分设计在成本-性能权衡方面都大打折扣。在本研究中,采用混合策略设计了一种无 Co 的铁铬镍基沉淀强化中熵合金(记为 Al0.2Cr0.9FeNi2.2Ti0.2),其基体为接近等原子的铁铬镍,并含有高含量(∼ 35 %)的 L12 纳米沉淀物。利用 EBSD、TEM 和 APT 系统地研究了微观结构特征、机械性能、变形亚结构演变和强化机制。拉伸试验表明,与现有的含 Co 和不含 Co 的 HEA/MEAs 相比,在中等温度范围内老化的现有合金实现了优异的强度-电导率组合。尤其是在 700 ℃ 下老化的合金(记为 700A),受益于沉淀硬化和异常应变硬化的持续性,极限拉伸强度高达 1606 兆帕,延展性高达 25%。这种异常的应变硬化持续性可归因于位错偶极子引发的塑性。高密度位错偶极子可同时通过降低位错平均自由路径来提供额外的应变硬化,并通过作为应力分散源来增强塑性变形兼容性,从而促进卓越的强度-电导率协同作用。这些发现不仅为未来开发高性能无钴沉淀强化 HEA/MEAs 打开了一扇新的大门,而且加深了对这些合金中加工硬化机制的理解。
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引用次数: 0
Effect of plastic deformability and fracture behaviour on interfacial toughening mechanism at Fe/Ni interfaces 塑性变形能力和断裂行为对铁/镍界面增韧机制的影响
IF 9.4 1区 材料科学 Q1 ENGINEERING, MECHANICAL Pub Date : 2024-08-31 DOI: 10.1016/j.ijplas.2024.104107

Fracture at interface causes plastic deformation in the vicinity region. Conventional plastic energy dissipation theory indicates that ductile vicinity toughens the interface by absorbing plastic deformation energy. However, the microstructure in the vicinity directly affects local plastic deformability and fracture behaviour, implying a more complicated toughening mechanism. In this study, the effect of microstructure and hardness on fracture behaviour of Fe/Ni interface was investigated. By experimental approach, interfaces with and without dynamic recrystallization (DRX) were fabricated by controlling the bonding conditions. It showed that compression-induced plastic deformation is the main source of the hardening behaviour in the vicinity. Moreover, the interfaces with hardened DRX vicinities exhibited improved fracture toughness, which is inconsistent with the plastic energy dissipation theory. To clarify this observation, the crystal plasticity finite element method (CPFEM) approach was employed to distinguish the effects of plastic deformation and interfacial microstructure. The result showed that although higher plastic deformability in the vicinity absorbs more dissipated plastic energy, severe stress concentration at the interface leads to early fracture and poor toughness. On the other hand, the interfacial hardened DRXed grains disperse interfacial stress distribution and provide potential sub-crack sites. A combined result of uniform plastic deformation and fracture energy dissipation is responsible for the improved toughness at interfaces with DRXed grains.

界面断裂会引起附近区域的塑性变形。传统的塑性能量耗散理论认为,韧性邻区通过吸收塑性变形能量来增韧界面。然而,邻近区域的微观结构会直接影响局部塑性变形能力和断裂行为,这意味着一种更为复杂的增韧机制。本研究探讨了微观结构和硬度对铁/镍界面断裂行为的影响。通过实验方法,控制结合条件,制备了有动态再结晶(DRX)和无动态再结晶(DRX)的界面。结果表明,压缩引起的塑性变形是附近区域硬化行为的主要来源。此外,DRX 附近硬化的界面表现出更好的断裂韧性,这与塑性能量耗散理论不符。为了澄清这一观点,我们采用了晶体塑性有限元法(CPFEM)来区分塑性变形和界面微结构的影响。结果表明,虽然附近较高的塑性变形吸收了更多的耗散塑能,但界面上严重的应力集中会导致早期断裂和韧性变差。另一方面,界面硬化的 DRX 化晶粒分散了界面应力分布,并提供了潜在的次裂缝位置。均匀塑性变形和断裂能量耗散的综合结果是导致带有 DRX 化晶粒的界面韧性提高的原因。
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引用次数: 0
An anisotropic damage visco-hyperelastic model for multiaxial stress-strain response and energy dissipation in filled rubber 填充橡胶多轴应力-应变响应和能量耗散的各向异性损伤粘-超弹性模型
IF 9.4 1区 材料科学 Q1 ENGINEERING, MECHANICAL Pub Date : 2024-08-30 DOI: 10.1016/j.ijplas.2024.104111

In this article, we introduce a novel physically-based anisotropic damage visco-hyperelastic model designed to predict the history-dependent inelastic behavior of multiaxially stretched filled rubber. The model integrates both the anisotropic Mullins effect and intrinsic viscosity through the consideration of internal physics, represented by two distinct networks: an elastic ground network and a superimposed viscous network. The rupture of molecular bonds within the elastic network chain backbone is modeled using statistical mechanics, while the effects of anisotropy-induced chain orientation at the upper scale are addressed through a microsphere-based scale transition method. The intrinsic viscosity is represented by the viscous network, which is governed by time-dependent equations to account for the viscous overstress. The influence of fillers is captured through the concept of strain amplification, applied to the two networks within the rubber matrix. The effectiveness of the model in capturing the biaxial behavior of filled rubber is evaluated by comparing its outputs with experimental data from a filled rubber system. This assessment specifically considers the impact of pre-stretching under various loading conditions and across a wide range of filler concentrations. Notably, it successfully predicts anisotropic stress-strain response and energy dissipation, and the coupled effects of damage and viscosity.

本文介绍了一种基于物理的新型各向异性损伤粘-超弹性模型,旨在预测多轴拉伸填充橡胶的历史非弹性行为。该模型通过考虑内部物理因素,将各向异性的穆林斯效应和固有粘度整合在一起,由两个不同的网络表示:一个弹性地面网络和一个叠加的粘性网络。弹性网络链骨架内分子键的断裂采用统计力学建模,而各向异性引起的链取向在上尺度的影响则通过基于微球的尺度转换方法来解决。本征粘度由粘性网络表示,粘性网络受时间相关方程控制,以考虑粘性过应力。填充物的影响通过应变放大的概念来捕捉,应用于橡胶基质内的两个网络。通过将模型输出与填充橡胶系统的实验数据进行比较,评估了模型在捕捉填充橡胶双轴行为方面的有效性。该评估特别考虑了在各种加载条件下和广泛的填充物浓度范围内预拉伸的影响。值得注意的是,它成功预测了各向异性应力-应变响应和能量耗散,以及损伤和粘度的耦合效应。
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引用次数: 0
Atomic-resolution investigations on dislocation-assisted evolution of {101¯3} twin boundaries in a magnesium alloy 镁合金中{101¯3}孪生边界位错辅助演化的原子分辨率研究
IF 9.4 1区 材料科学 Q1 ENGINEERING, MECHANICAL Pub Date : 2024-08-27 DOI: 10.1016/j.ijplas.2024.104108

{101¯3}3032 twinning is usually activated at the later stage of plastic deformation of Mg alloys, which is closely relevant to their fracture behavior. Reactions between slip dislocations and twin boundaries (TBs) are suggested to facilitate TB migration, retarding the premature TB cracking. Here, dislocation-assisted evolution of {101¯3} TBs in a Mg alloy subjected to cyclic deformation were studied and modeled, according to transmission electron microscopy observations, theoretical analyses of interfacial defects, and molecular dynamics simulations. Atomic-resolution experimental observations showed that symmetric tilt grain boundaries (STGBs) near the {101¯3} twin orientation with steps were generated in the deformed Mg alloy. Theoretical analyses and atomistic simulations indicated that transformation of {101¯3} TBs into the STGBs could occur by reactions with incident basal a60 dislocations in pairs from the twin and matrix respectively under the normal stress. STGB steps would be produced by reactions of individual basal a60 dislocations with GB dislocations at the STGB. Importantly, resultant steps could further emit {101¯3} twinning dislocations to facilitate the STGB migration. Moreover, STGBs near the {101¯3} twin orientation could evolve back into {101¯3} TBs either by reactions with an array of basal a60 dislocations, or by a GB sliding of b = 3032 theoretically. Our results may provide insights into the mechanisms of {101¯3} TB evolution in Mg alloys, which plays important roles in their plastic deformation and plasticity.

{101¯3}〈303‾2‾〉孪晶通常在镁合金塑性变形的后期阶段被激活,这与其断裂行为密切相关。滑移位错与孪晶边界(TBs)之间的反应被认为可促进TB迁移,延缓TB过早开裂。在这里,位错辅助{101¯3}的演化在此,根据透射电子显微镜观察、界面缺陷理论分析和分子动力学模拟,研究了循环变形下镁合金中{101¯3}位错辅助孪晶的演化并建立了模型。原子分辨率实验观察结果表明,在变形镁合金中产生了靠近{101¯3}孪晶取向的对称倾斜晶界(STGB)。理论分析和原子模拟表明,{101¯3} TBs 转变为 STGBsTBs 转变为 STGBs 的过程可能是在法向应力作用下分别与孪晶和基体的成对基底〈a60〉位错发生反应。在STGB处,单个基底〈a60〉位错与GB位错发生反应,从而产生STGB台阶。重要的是,由此产生的阶梯会进一步释放出{101¯3}孪生位错,从而促进STGB的迁移。此外,靠近{101¯3}孪晶取向的 STGB 可能会演化回{101¯3}TB,或者通过与基底〈a60〉位错阵列的反应,或者通过b = 〈303‾2‾〉理论上的GB滑动。我们的研究结果可能有助于深入了解镁合金中{101¯3}在镁合金的塑性变形和塑性中起重要作用。
{"title":"Atomic-resolution investigations on dislocation-assisted evolution of {101¯3} twin boundaries in a magnesium alloy","authors":"","doi":"10.1016/j.ijplas.2024.104108","DOIUrl":"10.1016/j.ijplas.2024.104108","url":null,"abstract":"<div><p>{10<span><math><mover><mn>1</mn><mo>¯</mo></mover></math></span>3}<span><math><mrow><mo>〈</mo><mn>30</mn><mover><mrow><mn>3</mn></mrow><mo>‾</mo></mover><mspace></mspace><mover><mrow><mn>2</mn></mrow><mo>‾</mo></mover><mo>〉</mo></mrow></math></span> twinning is usually activated at the later stage of plastic deformation of Mg alloys, which is closely relevant to their fracture behavior. Reactions between slip dislocations and twin boundaries (TBs) are suggested to facilitate TB migration, retarding the premature TB cracking. Here, dislocation-assisted evolution of {10<span><math><mover><mn>1</mn><mo>¯</mo></mover></math></span>3} TBs in a Mg alloy subjected to cyclic deformation were studied and modeled, according to transmission electron microscopy observations, theoretical analyses of interfacial defects, and molecular dynamics simulations. Atomic-resolution experimental observations showed that symmetric tilt grain boundaries (STGBs) near the {10<span><math><mover><mn>1</mn><mo>¯</mo></mover></math></span>3} twin orientation with steps were generated in the deformed Mg alloy. Theoretical analyses and atomistic simulations indicated that transformation of {10<span><math><mover><mn>1</mn><mo>¯</mo></mover></math></span>3} TBs into the STGBs could occur by reactions with incident basal <span><math><mrow><mo>〈</mo><msub><mi>a</mi><mn>60</mn></msub><mo>〉</mo></mrow></math></span> dislocations in pairs from the twin and matrix respectively under the normal stress. STGB steps would be produced by reactions of individual basal <span><math><mrow><mo>〈</mo><msub><mi>a</mi><mn>60</mn></msub><mo>〉</mo></mrow></math></span> dislocations with GB dislocations at the STGB. Importantly, resultant steps could further emit {10<span><math><mover><mn>1</mn><mo>¯</mo></mover></math></span>3} twinning dislocations to facilitate the STGB migration. Moreover, STGBs near the {10<span><math><mover><mn>1</mn><mo>¯</mo></mover></math></span>3} twin orientation could evolve back into {10<span><math><mover><mn>1</mn><mo>¯</mo></mover></math></span>3} TBs either by reactions with an array of basal <span><math><mrow><mo>〈</mo><msub><mi>a</mi><mn>60</mn></msub><mo>〉</mo></mrow></math></span> dislocations, or by a GB sliding of <strong><em>b</em></strong> = <span><math><mrow><mo>〈</mo><mn>30</mn><mover><mrow><mn>3</mn></mrow><mo>‾</mo></mover><mspace></mspace><mover><mrow><mn>2</mn></mrow><mo>‾</mo></mover><mo>〉</mo></mrow></math></span> theoretically. Our results may provide insights into the mechanisms of {10<span><math><mover><mn>1</mn><mo>¯</mo></mover></math></span>3} TB evolution in Mg alloys, which plays important roles in their plastic deformation and plasticity.</p></div>","PeriodicalId":340,"journal":{"name":"International Journal of Plasticity","volume":null,"pages":null},"PeriodicalIF":9.4,"publicationDate":"2024-08-27","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142095939","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":1,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Study of the dynamic impact spalling of ductile materials based on Gurson-type phase-field model 基于古尔森型相场模型的韧性材料动态冲击剥落研究
IF 9.4 1区 材料科学 Q1 ENGINEERING, MECHANICAL Pub Date : 2024-08-26 DOI: 10.1016/j.ijplas.2024.104106

The formation of void damage and spalling failure in ductile metallic materials under strong impact is a well-established phenomenon. In aerospace and defense technology engineering design, understanding the spalling failure process and related mechanisms is of utmost importance. This paper develops an explicit Gurson-type phase-field model that can simulate the void evolution and spalling damage of three-dimensional ductile metallic materials under high-velocity impacts based on the study of Aldakheel et al.. The model incorporates the Gurson-type void evolution equation and the phase-field approach while taking into account the pressure-dependent bulk modulus and inertia effects. This model is used to study the main processes and mechanisms of impacted layer cracking of metals in different dimensions. Meanwhile based on the study of complex spallation cracking processes in metals in two and three dimensions, observing and proposing the formation mechanism of complex spallation cracking modes in materials due to lateral and edge (base angle) rarefied effects.

韧性金属材料在强冲击力作用下形成空洞损伤和剥落破坏是一种公认的现象。在航空航天和国防技术工程设计中,了解剥落破坏过程和相关机理至关重要。本文以 Aldakheel 等人的研究为基础,建立了一个明确的 Gurson 型相场模型,可以模拟三维韧性金属材料在高速冲击下的空洞演化和剥落破坏。该模型结合了 Gurson 型空隙演化方程和相场方法,同时考虑了与压力相关的体积模量和惯性效应。该模型用于研究不同尺寸金属的冲击层开裂的主要过程和机理。同时,基于二维和三维金属复杂剥落开裂过程的研究,观察并提出了横向和边缘(基角)稀疏效应导致的材料复杂剥落开裂模式的形成机理。
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引用次数: 0
Nanostructured amorphous Al2O3-ZrO2 (La2O3) ceramics with plastic deformation via interface inducing hierarchical shear bands 通过界面诱导分层剪切带产生塑性变形的纳米结构非晶 Al2O3-ZrO2 (La2O3) 陶瓷
IF 9.4 1区 材料科学 Q1 ENGINEERING, MECHANICAL Pub Date : 2024-08-21 DOI: 10.1016/j.ijplas.2024.104103

Ionic-bonded ceramics are featured by their thermal stability, corrosion resistance, hardness and strength, but their applications are limited by the inherent brittleness. Ceramics are composed of strong chemical bonding and intricate crystal structures, making plastic deformation by dislocation slip highly challenging. A nanostructured amorphous Al2O3-ZrO2 ceramic comprising nanoscale amorphous particles and amorphous interfaces between particles was achieved in practice, where the amorphous interface is in scale of approximately 2.34 nm and amorphous particles is in width of approximately 6.75 nm. Based on nano-indentation tests, the shear transformation zone (STZ) volumes of nanostructured amorphous ceramics hot-pressed under various conditions are calculated, suggesting attenuation of free volume with the increase in pressure and temperature. The medium-temperature compression test of the samples exhibits a permanent plastic deformation of 14.6 %, with the presence of hierarchical shear bands in the deformed samples. The main shear bands (MSBs) in width of 0.84–9.15 μm are generated by the stress concentration in crystal-amorphous interface, and the small shear bands (SSBs) of 31–428 nm are related to abundant free volumes in the interface between amorphous particles.

离子键陶瓷具有热稳定性、耐腐蚀性、硬度和强度等特点,但其固有的脆性限制了其应用。陶瓷由强化学键和错综复杂的晶体结构组成,通过位错滑移实现塑性变形极具挑战性。在实践中获得了一种由纳米级非晶粒子和粒子间非晶界面组成的纳米结构非晶 Al2O3-ZrO2 陶瓷,其中非晶界面的尺度约为 2.34 纳米,非晶粒子的宽度约为 6.75 纳米。根据纳米压痕测试,计算了在不同条件下热压纳米结构非晶陶瓷的剪切转化区(STZ)体积,表明自由体积随压力和温度的增加而减小。样品的中温压缩试验显示出 14.6% 的永久塑性变形,变形样品中存在分层剪切带。宽度为 0.84-9.15 μm 的主剪切带(MSBs)是由晶体-非晶体界面的应力集中产生的,而宽度为 31-428 nm 的小剪切带(SSBs)则与非晶体颗粒之间界面丰富的自由体积有关。
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引用次数: 0
Interpretation of the stress dip test as a means of characterizing backstress: Experiments and backstress-aided crystal plasticity modeling of polycrystalline tantalum 将应力浸渍测试作为表征背应力的一种手段:多晶钽的实验和背应力辅助晶体塑性建模
IF 9.4 1区 材料科学 Q1 ENGINEERING, MECHANICAL Pub Date : 2024-08-21 DOI: 10.1016/j.ijplas.2024.104089

Backstresses, associated with certain dislocation arrangements and their inter-dislocation long-range stresses, are known to contribute significantly to deformation response of metals, including kinematic hardening, the Bauschinger effect (BE) and the Hall-Petch effect. Various methods have been employed to quantify these backstresses at the macro-scale. One of these approaches, which has received relatively little attention, is the stress dip test. The strain rate observed during a load dip and hold, after previous plastic deformation, can be positive or negative, depending upon the level at which the load is held, and the relative magnitudes of competing friction and backstresses. The most direct interpretation of previously reported tests indicates a surprisingly high level of backstress in common materials, and which is generally also higher than the value extracted from an unload-reload test. In this paper, stress dip tests are performed on pure polycrystalline tantalum, along with unload-reload tests. A plateau is seen in the strain rate observed during the stress dip test, which has not been previously reported. If the backstress is interpreted to correspond with the stress level associated with the middle point of the plateau, in line with the friction/backstress model of the unload-reload test, the resulting backstress obtained from both tests are very similar. A novel crystal plasticity model, incorporating backstress, reversible dislocations and non-Schmid effects, is used to help justify this new approach. The model predicts the observed plateau in strain rate, and provides a slip-level interpretation of the macroscopically observed backstress. The slip-level backstress (when considered as a fraction of the stress prior to the dip) is reasonably similar to the values interpreted from the dip test experiment. The ∼23% lower value in the simulation may be due to the lack of certain aspects of the actual physics in the model.

众所周知,背应力与某些位错排列及其位错间的长程应力有关,对金属的变形响应有重大影响,包括运动硬化、鲍辛格效应(Bauschinger effect,BE)和霍尔-佩奇效应(Hall-Petch effect)。人们采用了各种方法来量化这些宏观尺度的背应力。其中一种方法是应力浸渍试验,这种方法受到的关注相对较少。在之前的塑性变形之后,在载荷浸入和保持期间观察到的应变率可能是正的,也可能是负的,这取决于保持载荷的水平以及竞争摩擦力和背应力的相对大小。对以前报告的试验的最直接解释表明,普通材料的背应力水平出奇地高,通常也高于从卸载-重载试验中提取的值。本文对纯多晶钽进行了应力浸渍测试和卸载-重载测试。在应力浸渍试验中观察到的应变率出现了高原现象,这是以前从未报道过的。如果根据卸载-重载试验的摩擦/背应力模型,将背应力解释为与高原中点相关的应力水平,则两种试验得到的背应力非常相似。为了证明这种新方法的合理性,我们使用了一个包含背应力、可逆位错和非施密特效应的新型晶体塑性模型。该模型预测了观察到的应变速率高原,并对宏观观察到的反应力提供了滑移级解释。滑移级反应力(当被视为倾覆前应力的一部分时)与倾覆测试实验的解释值相当相似。模拟值低 23%可能是由于模型中缺少某些实际物理因素。
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引用次数: 0
Texture and lattice strain evolution in a pearlitic steel during shear deformation: An in situ synchrotron X-ray diffraction study 剪切变形过程中珠光体钢的纹理和晶格应变演变:同步辐射 X 射线衍射原位研究
IF 9.4 1区 材料科学 Q1 ENGINEERING, MECHANICAL Pub Date : 2024-08-20 DOI: 10.1016/j.ijplas.2024.104083

In-situ synchrotron X-ray diffraction experiments were conducted on the pearlitic steel sample with a carbon content of 0.74% by weight. Specimens were subjected to uniaxial loading that induced shear deformation and two-dimensional diffraction patterns were acquired. The evolution of the lattice microstrain and the strain-resolved crystallographic texture development of both ferrite (α-BCC) and cementite (θ-orthorhombic) phases were followed. The analysis revealed that the texture changed from {110}<113>α to {113}<121>α component and then, stabilized at {013}<uvw>α orientations. The θ phase exhibited a weak texture in the {100, 010, and 001}θ family planes. Additionally, it was revealed that the nucleation of interfacial defects at the α/θ interface promotes the amorphization of cementite and the activation of slip systems in less densely packed {310}α planes. The influence of microstructural changes on mechanical properties is discussed.

对含碳量为 0.74% (重量百分比)的珠光体钢样品进行了原位同步辐射 X 射线衍射实验。对试样进行单轴加载,诱发剪切变形,并获取二维衍射图样。对铁素体(α-BCC)和雪明石(θ-正方体)两相的晶格微应变演变和应变分辨结晶纹理发展进行了跟踪。分析表明,纹理从{110}<113>α转变为{113}<121>α成分,然后稳定在{013}<uvw>α取向。θ相在{100、010和001}θ族平面上表现出微弱的纹理。此外,研究还发现,α/θ界面上界面缺陷的成核促进了雪明碳酸盐的非晶化,并激活了密度较低的{310}α平面上的滑移系统。本文讨论了微观结构变化对力学性能的影响。
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International Journal of Plasticity
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