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The influence of mineral inclusion on the effective strength of rock-like geomaterials 矿物包裹体对类岩土工材料有效强度的影响
IF 9.4 1区 材料科学 Q1 ENGINEERING, MECHANICAL Pub Date : 2024-08-17 DOI: 10.1016/j.ijplas.2024.104104

The influences of microstructure on the macroscopic mechanical behavior of a composite with a porous matrix reinforced by mineral inclusions are investigated in the present work by both numerical and theoretical methods. The mineral inclusions are embedded at the mesoscopic scale and much bigger than the pores which are located at the microscopic scale. In order to consider the properties of the studied rock-like geomaterials, such as the dissymmetry between tension and compression, the solid phase at the microscopic scale is assumed to obey to a Drucker–Prager criterion. Based on the studied microstructure, the Fast Fourier Transform (FFT) based numerical method is firstly adopted to investigate the macroscopic plastic yield stress of the studied composite. Different microstructure having different volume fraction of inclusion, micro-porosity and frictional coefficient of the solid phase are considered. Based on these numerical results, the existing theoretical yield criterion is estimated. One finds that it should be improved for the case of a microstructure having a high inclusion content. Then, a new macroscopic yield criterion is constructed in the present work by using the modified secant method. This criterion ameliorates fundamentally the one proposed in Shen et al. (2013), specially for the case of a deviatoric loading. It is then estimated and validated by comparing with the FFT based numerical results which were carried out in this work with different volume fractions of heterogeneous phase.

本研究采用数值和理论方法研究了微观结构对矿物夹杂物增强多孔基体复合材料宏观力学行为的影响。矿物夹杂物嵌入在中观尺度上,比位于微观尺度上的孔隙大得多。为了考虑所研究的类岩石土工材料的特性,如拉伸和压缩之间的不对称,假定微观尺度上的固相服从德鲁克-普拉格准则。基于所研究的微观结构,首先采用基于快速傅立叶变换(FFT)的数值方法研究了所研究复合材料的宏观塑性屈服应力。不同的微观结构具有不同的夹杂物体积分数、微孔率和固相摩擦系数。根据这些数值结果,对现有的理论屈服准则进行了估算。结果发现,在微结构中夹杂物含量较高的情况下,应该对该标准进行改进。然后,本研究利用修正的正割法构建了一个新的宏观屈服准则。该准则从根本上改进了 Shen 等人(2013 年)提出的准则,特别是在偏差加载的情况下。然后,通过与基于 FFT 的数值结果进行比较,对其进行估算和验证。
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引用次数: 0
Uncovering all possible dislocation locks in face-centered cubic materials 揭示面心立方材料中所有可能的位错锁
IF 9.4 1区 材料科学 Q1 ENGINEERING, MECHANICAL Pub Date : 2024-08-16 DOI: 10.1016/j.ijplas.2024.104101

Dislocation reactions and locks play an important role in the plastic deformation and mechanical behavior of crystalline materials. Various types of dislocation locks in face-centered cubic (FCC) materials have been reported in the literature pertaining to material-specific molecular-dynamic simulations and high-resolution transmission electron microscopy observations. However, it is unknown how many dislocation locks are possible, and how immobile all the dislocation locks are, with respect to each other. Here we present a discrete mathematics-based approach to reveal all possible dislocation locks in the FCC crystal structure. Totally eight types of dislocation locks are uncovered, resulting from all possible reactions of mobile/glissile (namely, perfect and Shockley partial) dislocations with (a) non-coplanar Burgers vectors which reside on two slip planes intersecting at both obtuse and acute angles and (b) coplanar Burgers vectors. We redefine the degree of dislocation lock immobility based on misorientations between non-close-packed lock planes and close-packed {111} slip planes. The subsequently derived sequences for the dislocation lock immobility and formation tendency are rationalized by the reported experimental and dislocation-dynamics simulation results.

位错反应和位错锁在晶体材料的塑性变形和机械行为中发挥着重要作用。有关材料特定的分子动力学模拟和高分辨率透射电子显微镜观察的文献报道了面心立方(FCC)材料中的各种差排锁。然而,究竟有多少个位错锁是可能的,以及所有位错锁相互之间的固定程度如何,目前尚不得而知。在此,我们提出了一种基于离散数学的方法来揭示 FCC 晶体结构中所有可能的位错锁。我们总共发现了八种类型的位错锁,它们是由移动/裂隙(即完全位错和肖克利部分位错)位错与(a)非共面伯格斯矢量(位于钝角和锐角相交的两个滑移面上)和(b)共面伯格斯矢量的所有可能反应所产生的。我们根据非紧密堆积锁定平面和紧密堆积{111}滑移平面之间的错位重新定义了差排锁定不动度。随后得出的差排锁定不流动性和形成趋势的序列与所报告的实验和差排动力学模拟结果相吻合。
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引用次数: 0
Enhancing plasticity in BCC Mg-Li-Al alloys through controlled precipitation at grain boundaries 通过控制晶界析出提高 BCC 镁-锂-铝合金的塑性
IF 9.4 1区 材料科学 Q1 ENGINEERING, MECHANICAL Pub Date : 2024-08-15 DOI: 10.1016/j.ijplas.2024.104105

This study investigates the improvement of plasticity in body-centered cubic magnesium (Mg)-lithium (Li)-aluminum (Al) alloys, crucial for lightweight structural applications. The ternary Mg-Li-Al alloys exhibits high strength but low ductility. Precipitates at grain boundaries in these alloys, linked to reduced plasticity, are examined for their crystal structure and composition. Advanced microscopic techniques reveal the transformation of precipitates and the development of specific structures at grain boundaries. Thermodynamics of element diffusion at grain boundaries are explored through first-principles calculations, and a phase-field simulation models precipitate evolution. Molecular dynamics simulations elucidate nanoscale mechanisms governing the transition from brittle to ductile fracture modes during artificial aging. The D03−Mg3Al at grain boundaries is a brittle phase, and through a 170 °C aging treatment, it induces the precipitation of lamellar α-Mg phase with D03−Mg3Al as nucleation sites. The occupancy energy of Al atoms at Li sites in α-Mg is found to be lower than that in D03−Mg3Al, leading to the dissolution of D03−Mg3Al. The α-Mg, characterized by a stronger metallic nature, exhibits a better-matched modulus with the matrix and enhanced dislocation mobility. The precipitation of α-Mg plays a pivotal role in significantly improving the ductility of the alloy. This work contributes to the understanding of the complex interplay between alloy composition, grain boundary precipitates, and plasticity, as well as brings insights to guide interfacial control in the development of advanced Mg-Li-Al alloys for structural applications.

本研究探讨了如何改善体心立方镁(Mg)-锂(Li)-铝(Al)合金的塑性,这对轻质结构应用至关重要。三元镁-锂-铝合金具有高强度和低延展性。这些合金晶界处的析出物与塑性降低有关,我们对其晶体结构和成分进行了研究。先进的显微技术揭示了析出物的转变和晶界特定结构的发展。通过第一原理计算探索了元素在晶界扩散的热力学,并通过相场模拟建立了沉淀演变模型。分子动力学模拟阐明了人工老化过程中从脆性断裂模式向韧性断裂模式过渡的纳米级机制。晶界处的 D03-Mg3Al 是一种脆性相,通过 170 °C 老化处理,它诱导了以 D03-Mg3Al 为成核点的片状 α-Mg 相的析出。研究发现,α-Mg 中 Al 原子在 Li 位点的占据能低于 D03-Mg3Al,从而导致 D03-Mg3Al 的溶解。α-镁的特点是金属性更强,与基体的模量匹配性更好,位错迁移率更高。α-Mg的析出在显著改善合金延展性方面发挥了关键作用。这项研究有助于理解合金成分、晶界析出物和塑性之间复杂的相互作用,并为开发先进的镁-锂-铝合金结构应用提供了界面控制指导。
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引用次数: 0
Crack-tip plasticity mediated grain refinement and its resisting effect on the fatigue short crack growth 裂纹尖端塑性介导的晶粒细化及其对疲劳短裂纹增长的抑制作用
IF 9.4 1区 材料科学 Q1 ENGINEERING, MECHANICAL Pub Date : 2024-08-15 DOI: 10.1016/j.ijplas.2024.104102

Fatigue short crack growth governed by the crack-tip plasticity dominates the fatigue life and strength of metallic materials or structural components. Here, for the first time, we discover a new mechanism of resisting fatigue short crack growth by grain refinement near the crack-tip driven by dynamic recrystallization in a Ni-based superalloy during high-cycle fatigue. The local cumulative plastic strain plays a determining role in the crack-tip grain refinement and concurrent dissolution of nanoprecipitation. Comprehensive microstructural analysis provides the evidence that the refined grains reduce the plastic micro-strain gradient in the vicinity of the crack-tip, which causes the crack blunting and deflection towards the interface of coarse-fine grains, hence decelerating the short crack growth. Although the grain refinement reduces the local stress threshold in the fine-grained areas (FGA), the dominant effects of FGA are identified to provide additional microstructural resistance to the propagation of short cracks.

受裂纹尖端塑性支配的疲劳短裂纹增长对金属材料或结构组件的疲劳寿命和强度起着主导作用。在这里,我们首次发现了一种新的机制,即在高循环疲劳过程中,镍基超合金在动态再结晶的驱动下,通过裂纹尖端附近的晶粒细化来抵抗疲劳短裂纹的增长。局部累积塑性应变在裂纹尖端晶粒细化和同时发生的纳米沉淀溶解中起着决定性作用。全面的微观结构分析表明,细化晶粒降低了裂纹尖端附近的塑性微应变梯度,导致裂纹钝化并向粗-细晶粒界面偏转,从而减慢了短裂纹的增长速度。虽然晶粒细化降低了细晶粒区域(FGA)的局部应力阈值,但确定了 FGA 的主要作用是为短裂纹的扩展提供额外的微结构阻力。
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引用次数: 0
High-temperature creep mechanism of Ti-Ta-Nb-Mo-Zr refractory high-entropy alloys prepared by laser powder bed fusion technology 激光粉末床熔融技术制备的 Ti-Ta-Nb-Mo-Zr 高熵难熔合金的高温蠕变机理
IF 9.4 1区 材料科学 Q1 ENGINEERING, MECHANICAL Pub Date : 2024-08-14 DOI: 10.1016/j.ijplas.2024.104080

Creep resistance, which is one of the most important deformation modes, is rarely reported for refractory high entropy alloys (RHEAs). The experiment investigated the high-temperature creep mechanism of Ti-Ta-Nb-Mo-Zr RHEA prepared by laser powder bed fusion (LPBF) technology. The high cooling rate of LPBF suppresses most of the elemental segregation, but there are still over-solidified precipitates and a few continuous precipitates (CP). In the range of 923–1023 K, the stress exponent and activation energy were determined to be 3.2–3.4 and 261.5 ± 19.5 kJ/mol, respectively. Compared with other conventional alloys and HEAs, a large reduction of the minimum creep rate is found in the LPBF-built Ti1.5Ta0.5NbZrMo0.5 RHEA, indicating a significant improvement in high-temperature properties. The dislocation tangles at the interface is formed during the creep process and new Zr-rich CP phases are generated in the dislocation tangles region. The interfacial dislocation tangles is the result of the interaction between dislocations and two-phase mismatch stresses. The dislocation tangles prevents dislocations from further cutting the matrix phase, which is very favorable to the high-temperature creep performance. At the same time, the formation of this dislocation tangles greatly accelerates the nucleation process and growth rate of the new CP phase. The present work provides a pathway to design novel HEAs with improved high-temperature creep resistance.

抗蠕变性是最重要的变形模式之一,但对于难熔高熵合金(RHEAs)却鲜有报道。本实验研究了采用激光粉末床熔融(LPBF)技术制备的 Ti-Ta-Nb-Mo-Zr RHEA 的高温蠕变机理。LPBF 的高冷却速率抑制了大部分元素偏析,但仍存在过固结析出物和少量连续析出物(CP)。在 923-1023 K 范围内,应力指数和活化能分别为 3.2-3.4 和 261.5 ± 19.5 kJ/mol。与其他传统合金和 HEA 相比,LPBF 构建的 TiTaNbZrMo RHEA 的最小蠕变速率大大降低,表明其高温性能得到显著改善。蠕变过程中形成了界面位错缠结,并在位错缠结区域生成了新的富 Zr CP 相。界面差排缠结是差排与两相错配应力相互作用的结果。位错缠结阻止了位错进一步切割基体相,这对高温蠕变性能非常有利。同时,这种位错缠结的形成也大大加快了新 CP 相的成核过程和生长速度。本研究为设计具有更高抗高温蠕变性能的新型 HEA 提供了一条途径。
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引用次数: 0
Crystal plasticity-phase–field based analyses of interfacial microstructural evolution during dynamic recrystallization in a dual phase titanium alloy 基于晶体塑性相场的双相钛合金动态再结晶过程中界面微结构演变分析
IF 9.4 1区 材料科学 Q1 ENGINEERING, MECHANICAL Pub Date : 2024-08-12 DOI: 10.1016/j.ijplas.2024.104087

In this study, an integrated crystal plasticity finite element–phase–field (CPFE–PF) model is developed to examine dynamic recrystallization (DRX) in a dual phase Ti alloy. The CP framework is coupled with PF by updating the free energy density with energy contributions due to plasticity. The evolution of grain boundaries through evolving non-conserved order parameters in the PF model is tracked using the Allen–Cahn equation. Nucleation is allowed to occur if the dislocation density exceeds a critical value. DRX is studied in various Ti morphologies such as an αTi single crystal containing a stiff elastoplastic particle, α-Ti bicrystals with low and high misorientation between grains, an αβ bicrystal and a globular αβ Ti structure with β phase at αα interfaces. For an αTi bicrystal, a high misorientation facilitates the onset of DRX at the αα interface at a significantly lower strain than the bicrystal with low misorientation. In an αβ bicrystal, DRX is only observed at the αβ interface. For the globular morphology, nucleation is observed at both αβ interfaces and inside α grains, which is consistent with previous experimental observations for a similar morphology. Nucleation inside α grains is explained by the correlation between SSD density and misorientation indicators such as KAM and GROD at the nucleus site. To correlate slip activity with nucleation propensity immediately prior to different nucleation events, the dislocation density, shear rate and Schmid factors on different slip systems are evaluated at nucleation sites.

本研究开发了一种集成晶体塑性有限元-相场(CPFE-PF)模型,用于研究双相钛合金中的动态再结晶(DRX)。CP 框架与 PF 相耦合,通过更新自由能密度与塑性导致的能量贡献来实现。使用 Allen-Cahn 方程跟踪 PF 模型中通过非保留阶次参数演变的晶界演化。如果位错密度超过临界值,则允许发生成核。DRX 在不同的钛形态中进行了研究,如含有刚性弹塑性颗粒的 α-Ti 单晶、晶粒间具有低和高错位取向的 α-Ti 双晶、α-β 双晶和在α-α 接口处具有 β 相的球状 α-β Ti 结构。对于α-Ti 双晶,高取向错位有助于在α-α界面上发生 DRX,其应变明显低于低取向错位的双晶。在 α-β 双晶中,只有在 α-β 界面才能观察到 DRX。对于球状形态,在 α-β 界面和 α 晶粒内部都能观察到成核现象,这与之前对类似形态的实验观察结果一致。α晶粒内部的成核可通过核部位的SSD密度与KAM和GROD等错取向指标之间的相关性来解释。为了将不同成核事件发生前的滑移活动与成核倾向相关联,在成核点评估了不同滑移系统上的位错密度、剪切速率和施密德因子。
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引用次数: 0
Direct application of elasto-visco-plastic self-consistent crystal plasticity model to U-draw bending and springback of dual-phase high strength steel 弹塑性自洽晶体塑性模型在双相高强度钢 U 型拉伸弯曲和回弹中的直接应用
IF 9.4 1区 材料科学 Q1 ENGINEERING, MECHANICAL Pub Date : 2024-08-12 DOI: 10.1016/j.ijplas.2024.104098

The incremental elasto-visco-plastic self-consistent polycrystal model (ΔEVPSC) was utilized to describe the constitutive behavior of dual-phase 980 (DP980) steel. A simple baseline modeling approach was chosen: the hardening behavior of each constituent phase in the DP980 steel was described by a simple Voce hardening law without explicitly considering the back stress; and it was assumed that using the same single crystal elastic modulus for ferrite and martensite is sufficiently representative. The adequacy of this baseline modeling approach was evaluated by comparing various mechanical experimental data with model predictions in terms of the stress vs. strain curves obtained from uniaxial tension, tension-compression, and loading-unloading-loading (LUL) tests. Additionally, the evolution of experimental lattice strain data reported in literature was used to validate the phase-specific Voce hardening parameters. Despite its minimalistic modeling description, the baseline ΔEVPSC model successfully captured key features: 1) the Bauschinger effect, 2) the decrease in chord modulus, and 3) the non-linearity in the stress vs. strain curves resulting from the LUL test. All three mentioned characteristics are crucial for accurate prediction of springback in sheet metals. The ΔEVPSC model, interfaced with a finite element solver (Abaqus/standard) as the user material subroutine, was employed to simulate the Numisheet93 benchmark problem. The strip of DP980 was first U-drawn followed by springback. The model-predicted springback profile aligned well with the experimental results only when stress relaxation was properly considered, resulting in improved predictive accuracy compared to predictions based on a distortional plasticity model.

增量弹塑性自洽多晶体模型(ΔEVPSC)用于描述双相 980(DP980)钢的构成行为。我们选择了一种简单的基准建模方法:DP980 钢中各组成相的硬化行为由简单的 Voce 硬化定律来描述,而不明确考虑背应力;并且假定对铁素体和马氏体使用相同的单晶弹性模量具有足够的代表性。通过比较单轴拉伸、拉伸-压缩和加载-卸载-加载(LUL)试验获得的应力与应变曲线,将各种机械实验数据与模型预测进行比较,从而评估了这种基准建模方法的适当性。此外,文献中报道的实验晶格应变数据的演变也用于验证特定相位的 Voce 硬化参数。尽管建模描述非常简单,但基线 ΔEVPSC 模型成功地捕捉到了以下关键特征:1) 鲍辛格效应;2) 弦模量的降低;3) LUL 试验产生的应力与应变曲线的非线性。上述三个特征对于准确预测金属板材的回弹至关重要。ΔEVPSC 模型作为用户材料子程序与有限元求解器(Abaqus/标准)连接,用于模拟 Numisheet93 基准问题。首先对 DP980 带材进行 U 型拉伸,然后进行回弹。只有在适当考虑应力松弛的情况下,模型预测的回弹曲线才能与实验结果很好地吻合,从而与基于变形塑性模型的预测相比提高了预测精度。
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引用次数: 0
Strong and ductile low carbon low alloy steels with multiphase bimodal microstructure 具有多相双峰微观结构的高强度、延展性低碳低合金钢
IF 9.4 1区 材料科学 Q1 ENGINEERING, MECHANICAL Pub Date : 2024-08-11 DOI: 10.1016/j.ijplas.2024.104097

Restrained by the strength-ductility tradeoff, it is still challenging to develop advanced high-strength low carbon low alloy (LCLA) steels with superior strength-ductility combinations and cost-effectiveness to satisfy industry demands. In this study, an innovative 2-cyclic quenching and partitioning (Q&P) heat treatment was developed to produce a novel LCLA steel with the optimized microstructure, in which a bimodal grain size distribution across various constituent phases was achieved. Tensile test results show that the 2-cyclic Q&P LCLA steel exhibits excellent mechanical properties with a uniform elongation, close to 18 %, nearly triple that of conventional Q&P LCLA steel while maintaining a tensile strength above 1 GPa. To reveal the underlying mechanisms of such exceptional strength-elongation synergy, the detailed deformation behaviors of the developed LCLA steel were characterized while the evolution of hetero-deformation-induced (HDI) stress and effective stress was investigated from the perspective of the dislocation model. It is indicated that, with increasing strain, the heterogeneous structures promote strong strain partitioning which leads to extensive geometrically necessary dislocations (GNDs) pile-ups at hetero-interface and persistently strong HDI strengthening effect, and produce the coordinated deformation among constituent phases to realize dislocation forest strengthening, collectively contributing to the enhanced work hardening capacity and hence overcoming the strength-ductility tradeoff. This study provides a new processing strategy for developing strong and ductile LCLA steels.

受限于强度-电导率的权衡,开发具有优异的强度-电导率组合和成本效益的先进高强度低碳低合金钢(LCLA)以满足工业需求仍是一项挑战。本研究开发了一种创新的双循环淬火和分区(Q&P)热处理方法,用于生产具有优化微观结构的新型 LCLA 钢,在这种钢中,各组成相的晶粒尺寸分布呈双峰分布。拉伸试验结果表明,双循环 Q&P LCLA 钢具有优异的机械性能,均匀伸长率接近 18%,几乎是传统 Q&P LCLA 钢的三倍,同时抗拉强度保持在 1 GPa 以上。为了揭示这种优异的强度-伸长协同作用的内在机制,研究人员对所开发的 LCLA 钢的详细变形行为进行了表征,同时从位错模型的角度研究了异变形诱导应力(HDI)和有效应力的演变。结果表明,随着应变的增加,异质结构促进了强应变分区,导致异质界面出现大量几何必要位错(GNDs)堆积和持续的强 HDI 强化效应,并在各组成相之间产生协调变形,实现位错林强化,共同促进了加工硬化能力的提高,从而克服了强度-电导率折衷问题。这项研究为开发强度高、韧性好的 LCLA 钢提供了一种新的加工策略。
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引用次数: 0
Discerning the duality of H in Mg: H-induced damage and ductility 辨别镁中 H 的二重性:H 诱导的损伤和延展性
IF 9.4 1区 材料科学 Q1 ENGINEERING, MECHANICAL Pub Date : 2024-08-10 DOI: 10.1016/j.ijplas.2024.104084

Prone H reduction is considered an important factor in the poor corrosion resistance of Mg and its alloys, while the reduced H simultaneously impacts their mechanical properties whose mechanism is still unclear. It can be experimentally found that the elongation of Mg charged with atomic H is 2.76 % greater than that in air. To reveal the underlying physics, multi-scale modeling combining first-principle calculation, molecular dynamic/static (MD/MS) simulation, and crystal plasticity finite element method (CPFEM) is first employed to elaborate the influence of H on Mg at different length scales. The first-principle results show that the Prism-I {101¯0} exhibits the most corrosive nature with an effective H adsorption density that reaches 18 nm−2 and its diffusion barrier is only 0.156 eV H−1. Conversely, the Basal {0001} has the best surficial H resistance. After H infiltration into the Mg matrix, the generalized stacking fault energies of most twining planes decrease by 2.26 % ∼18.49 %. Especially for the Basal {0001}, the H not only lowers its stacking fault energy to -7.13 J m−2, but also impedes its cleavage cracking along [101¯0] according to the MD/MS simulation. The presence of H within the grains induces early initiation of stacking fault and elevates the critical stress at the crack tips. The CPFEM modeling reveals that the difference in twining growth is concentrated within 4 % strain. The H addition promotes the twining of Mg, however, following 4 % strain, the relative activity of planes in the Mg/Mg-H models is consistent.

镁及其合金耐腐蚀性差的一个重要因素是氢的还原,而还原的氢同时也影响了它们的机械性能,其机理尚不清楚。实验发现,带原子氢的镁的伸长率比在空气中的伸长率高 2.76%。为了揭示其基本物理原理,研究人员首先结合第一性原理计算、分子动力学/静态(MD/MS)模拟和晶体塑性有限元法(CPFEM)进行了多尺度建模,以阐述不同长度尺度上 H 对镁的影响。第一原理结果表明,Prism-I {101¯0} 具有最强的腐蚀性,其有效 H 吸附密度达到 18 nm-2,扩散势垒仅为 0.156 eV H-1。相反,Basal {0001} 的表面抗 H 能力最强。H 渗入镁基体后,大多数缠绕平面的广义堆积断层能降低了 2.26 % ∼ 18.49 %。特别是对于基底{0001},根据 MD/MS 模拟,H 不仅使其堆积断层能降低到 -7.13 J m-2,而且还阻碍了其沿 [101¯0] 的劈裂开裂。晶粒中 H 的存在诱导了堆叠断层的早期发生,并提高了裂纹尖端的临界应力。CPFEM 模型显示,缠绕增长的差异集中在 4% 应变范围内。H 的加入促进了镁的缠绕,然而,在 4% 应变之后,镁/镁-H 模型中平面的相对活性是一致的。
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引用次数: 0
Creep-fatigue damage level evaluation based on the relationship between microstructural evolution and mechanical property degradation 基于微结构演变与机械性能退化之间关系的蠕变疲劳损伤等级评估
IF 9.4 1区 材料科学 Q1 ENGINEERING, MECHANICAL Pub Date : 2024-08-08 DOI: 10.1016/j.ijplas.2024.104086

Creep-fatigue interaction is identified as a primary failure mode for components operating under high temperatures. As operational durations extend, this interaction not only alters the material's microstructures but also initiates a gradual degradation in mechanical properties, significantly impacting its deformation and damage behaviors. In this work, the dynamic microstructural evolution of GH4169 superalloy during creep-fatigue was elucidated via qualitative characterization, and damage level evaluation method was subsequently developed by bridging microstructure degradation to mechanical property degradation. Creep-fatigue tests were performed at 650 °C with various tensile holding times and were interrupted at lifetime fractions of 10 %, 50 % and 80 % for further analysis and tensile evaluations. Results revealed that the prolonged exposure to holding times induced the coarsening of γ precipitates alongside an increase in low-angle grain boundaries, culminating a reduction in creep-fatigue strength. The development of voids and cracks exacerbated the degradation of elongation, leading to a hybrid fracture mode encompassing both intergranular and transgranular cracking paths. Synthesizing microstructural evolutions to qualitatively categorize diverse degradation levels imparted a robust physical basis for damage evaluation. A mapping model was established to correlate the average kernel average misorientation (micro-degradation indicator) with the tensile plastic strain energy density (macro-degradation indicator). The damage level evaluation method was endowed with quantitative metrics utilizing this model, and its generality was additionally validated in P92 steel. This work offers an insight into the quantitative damage evaluations of creep-fatigue-induced degradations in materials, thereby providing a theoretical basis for the development of operation management and inspection plans of components.

蠕变-疲劳相互作用被认为是在高温下工作的部件的主要失效模式。随着工作时间的延长,这种相互作用不仅会改变材料的微观结构,还会引发机械性能的逐渐退化,对材料的变形和损伤行为产生重大影响。在这项工作中,通过定性表征阐明了 GH4169 超合金在蠕变疲劳过程中的动态微结构演变,随后通过将微结构退化与机械性能退化联系起来,开发了损伤程度评估方法。蠕变疲劳试验在 650 °C、不同拉伸保持时间下进行,并在寿命分数为 10%、50% 和 80% 时中断,以进行进一步分析和拉伸评估。结果表明,长时间暴露于保持时间下会导致γ″析出物变粗,同时低角度晶界增加,最终导致蠕变疲劳强度降低。空隙和裂纹的产生加剧了伸长率的下降,导致了一种包含晶间和跨晶开裂途径的混合断裂模式。综合微观结构演变对不同的退化程度进行定性分类,为损伤评估提供了可靠的物理基础。建立了一个映射模型,将平均核平均错向(微观降解指标)与拉伸塑性应变能量密度(宏观降解指标)相关联。利用该模型为损伤程度评估方法赋予了量化指标,并在 P92 钢中对其通用性进行了额外验证。这项研究深入探讨了材料蠕变疲劳诱导退化的定量损伤评估,从而为制定部件运行管理和检测计划提供了理论依据。
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International Journal of Plasticity
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