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Investigation of the media tightness of a microform-fitted plastic/light metal composite 微成型塑料/轻金属复合材料的介质密封性研究
IF 3.8 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-09-14 DOI: 10.1016/j.jajp.2024.100253
Moritz Mascher, Pia Wagner, Christian Hopmann

Plastic/metal hybrid components made of amorphous thermoplastics such as polycarbonate and light metals such as aluminum offer potential to be used in modern automotive headlights to meet the high requirements for tolerances and surface quality. A microform-fit joining approach is used to join plastics and metals, which combines the advantages of material-fit and form-fit joining processes while at the same time avoiding some of the disadvantages of the respective joining approaches, such as stress peaks or the use of additional chemicals. For this purpose, the light metal component is microstructured through laser ablation. To ensure the functional safety of electrical components, the media tightness of the hybrid component is tested with a pressure drop test. An influence of the structure arrangement, the structure spacing and the molding compound on the media tightness can be determined. The highest media tightness can be achieved with a ring-shaped structural arrangement in which the microstructures are orientated orthogonally to the outlet direction of the test medium. The media permeability of a ring-shaped structure arrangement with a structure spacing of 500 µm is 0.42 cm3/s for test specimens made of aluminum and polycarbonate. As the value is below the threshold value of 12 cm3/s, watertightness up to an overpressure of at least 0.5 bar can be concluded.

由聚碳酸酯等无定形热塑性塑料和铝等轻金属制成的塑料/金属混合组件有望用于现代汽车前大灯,以满足对公差和表面质量的高要求。塑料和金属的接合采用了微成型接合方法,它结合了材料接合和成型接合工艺的优点,同时避免了各自接合方法的一些缺点,如应力峰值或使用额外的化学品。为此,可通过激光烧蚀对轻金属元件进行微结构处理。为确保电气元件的功能安全,混合元件的介质密封性通过压降试验进行测试。可以确定结构排列、结构间距和模塑化合物对介质密封性的影响。环形结构布置的介质密封性最高,其中微结构的方向与测试介质的出口方向正交。对于由铝和聚碳酸酯制成的测试样本,结构间距为 500 微米的环形结构布置的介质渗透率为 0.42 立方厘米/秒。由于该值低于 12 立方厘米/秒的临界值,因此可以断定在至少 0.5 巴的超压条件下不会漏水。
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引用次数: 0
Characterization and modeling of laser transmission welded polyetherketoneketone (PEKK) joints: Influence of process parameters and annealing on weld properties 激光透射焊接聚醚酮酮 (PEKK) 接头的表征和建模:工艺参数和退火对焊接性能的影响
IF 3.8 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-09-10 DOI: 10.1016/j.jajp.2024.100252
Marcela Matus-Aguirre , Benoît Cosson , Christian Garnier , Fabrice Schmidt , André Chateau Akué-Asséko , France Chabert

Welding high-performance thermoplastics has gained popularity across various industries such as automotive, aerospace, and medical. Laser transmission welding (LTW) has emerged as an effective method for joining thermoplastic parts due to its precise control and high joint quality. PAEK (polyaryletherketone) are wide spreading over various industrial applications as a substitute to metals and thermosets when high durability and performance are required. Polyetherketoneketone (PEKK) is one of these PAEK and it has received less attention than PEEK until now. PEKK, being a semi-crystalline thermoplastic, requires additional care during processing due to its propensity to crystallize. This study presents both experimental and numerical investigations into LTW of PEKK molded parts, aiming to understand the influence of welding parameters and crystallinity on weld joint morphology and mechanical properties. PEKK plates, prepared in amorphous and semi-crystalline states, are subjected to LTW using a 975 nm diode laser. Material characterization confirms differences in crystallinity between the samples, which affect their thermal and optical properties, which are crucial for welding. Welding tests are conducted with varying laser power (between 75 and 95 W) and semi-transparent part thickness (2 and 4 mm). The morphology of joints is analysed. Assemblies undergo post-weld annealing treatment to examine its influence on weld crystallinity and consequent mechanical properties. Results reveal an anisotropic distribution of crystallinity within the heat-affected zone (HAZ). The depths of the molten layer (ML) and semi-crystalline layer (scL) vary with laser power and assembly type. A notable decrease in weld strength with laser power is highlighted, while annealing leads to enhanced crystallinity and improved weld strength. Despite variations, high weld strengths are achieved with annealing. Computational modelling elucidates the complex interplay between laser irradiation, temperature distribution, and crystallization kinetics observed experimentally. Overall, this comprehensive investigation provides valuable insights into optimizing LTW parameters for PEKK parts.

焊接高性能热塑性塑料在汽车、航空航天和医疗等各行各业越来越受欢迎。激光传输焊接(LTW)因其精确的控制和较高的焊接质量,已成为连接热塑性塑料部件的有效方法。PAEK(聚芳基醚酮)作为金属和热固性塑料的替代品,在要求高耐用性和高性能的各种工业应用中得到了广泛的推广。聚醚醚酮(PEKK)是 PAEK 的一种,但到目前为止,它受到的关注还不如 PEEK 多。PEKK 是一种半结晶热塑性塑料,由于容易结晶,因此在加工过程中需要格外小心。本研究对 PEKK 模制件的 LTW 进行了实验和数值研究,旨在了解焊接参数和结晶度对焊点形态和机械性能的影响。在无定形和半结晶状态下制备的 PEKK 板材使用 975 nm 的二极管激光器进行 LTW。材料表征证实了样品之间结晶度的差异,这种差异会影响样品的热性能和光学性能,而这些性能对焊接至关重要。焊接测试在不同的激光功率(75 至 95 W)和半透明部件厚度(2 至 4 mm)下进行。对接头的形态进行了分析。组装件经过焊后退火处理,以检查其对焊接结晶度和由此产生的机械性能的影响。结果显示,热影响区(HAZ)内的结晶度呈各向异性分布。熔融层(ML)和半结晶层(scL)的深度随激光功率和装配类型而变化。随着激光功率的增加,焊接强度明显降低,而退火可提高结晶度并改善焊接强度。尽管存在差异,但通过退火可获得较高的焊接强度。计算建模阐明了实验观察到的激光辐照、温度分布和结晶动力学之间复杂的相互作用。总之,这项综合研究为优化 PEKK 零件的 LTW 参数提供了宝贵的见解。
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引用次数: 0
Dual-mode laser beam welding of similar and dissimilar material tab-to-busbar for electric vehicle battery pack 双模激光束焊接电动汽车电池组中的同类和异类材料接片与母线
IF 3.8 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-09-06 DOI: 10.1016/j.jajp.2024.100250
Nikhil Kumar , Venkat Vivek Pamarthi , Christopher Harris , Elliot Burbidge , Iain Masters

The escalation in electric vehicle (EV) adoption necessitates advanced laser joining techniques for critical battery pack components. However, using a standard Gaussian single-mode laser for joining similar and dissimilar material combinations e.g. aluminium/aluminium (Al/Al), aluminium/copper (Al/Cu) for tab-to-busbar connections often led to defects such as cracks and intermetallic compound (IMC) formation. This paper investigates using a dual-mode laser consisting of a core and ring to overcome these issues. In this research, 0.3 mm Al and Cu tabs were welded with 1.5 mm Al and Cu busbars using a 6 kW IPG dual-mode laser at a high welding speed of 1 m s-1. The study focussed on the effects of dual-mode parameters (i.e. core and ring beam power) and welding speed on tab-to-busbar connections, analysing the interplay between electrical contact resistance, temperature and IMC formation through electrical resistance tests, elemental and strength analysis. The results show, that using the ring beam along with the core beam reduces excessive melting and evaporation of Al and minimises the intermixing of Al and Cu solid solutions in the joint. In the Cu tab-to-Al busbar joint, increasing the ring beam intensity effectively reduces the convexity defect found with single-mode beam attributed to improved keyhole stability. Overall, in dual-mode laser welding, the ring beam protects the keyhole and reduces the IMC formation, while the core beam, with its high peak intensities, controls the penetration depth. This necessitates balancing both core and ring beam intensities for optimal weld quality. Further, the joint resistance for Cu tab-to-Cu busbar (51.90 μΩ) joint was the lowest followed by Cu tab-to-Al busbar (68.38 μΩ) joint, Al tab-to-Cu busbar (84.44 μΩ) joint and Al tab-to-Al busbar (114.12 μΩ) joint.

随着电动汽车(EV)的普及,电池组关键部件需要采用先进的激光连接技术。然而,使用标准的高斯单模激光器来连接类似和不同的材料组合,例如铝/铝(Al/Al)、铝/铜(Al/Cu)的凸片与母线连接,往往会导致裂纹和金属间化合物(IMC)形成等缺陷。本文研究使用由核心和环组成的双模激光器来克服这些问题。在这项研究中,使用 6 kW IPG 双模激光器,以 1 m s-1 的高速焊接,将 0.3 mm 铝和铜焊片与 1.5 mm 铝和铜母线焊接在一起。研究的重点是双模参数(即核心和环形光束功率)和焊接速度对片与母线连接的影响,并通过电阻测试、元素和强度分析来分析电接触电阻、温度和 IMC 形成之间的相互作用。结果表明,在使用芯梁的同时使用环梁可减少铝的过度熔化和蒸发,并最大限度地减少接头中铝和铜固溶体的混合。在铜片与铝母线的焊接中,环形光束强度的增加有效地减少了单模光束下的凸凹缺陷,这归功于键孔稳定性的提高。总之,在双模激光焊接中,环形光束可保护键孔并减少 IMC 的形成,而具有高强度峰值的核心光束则可控制穿透深度。这就需要平衡核心光束和环形光束的强度,以获得最佳焊接质量。此外,铜片对铜母线(51.90 μΩ)接头的接头电阻最小,其次是铜片对铝母线(68.38 μΩ)接头、铝片对铜母线(84.44 μΩ)接头和铝片对铝母线(114.12 μΩ)接头。
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引用次数: 0
An energetic approach to the statistical analysis and optimization of friction welding processes applied to an aluminum-steel-joint 对铝-钢接头摩擦焊接工艺进行统计分析和优化的能量方法
IF 3.8 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-09-04 DOI: 10.1016/j.jajp.2024.100251
M. Winkler , C. Rößler , N. Harriehausen , S. Jüttner , D. Schmicker , F. Trommer

The present publication deals with an energy-oriented approach to the statistical analysis of rotational friction welding processes. To illustrate the methodological approach, it is applied to investigate the effects of energy flow on material flow behavior and joint quality during friction welding of an AA6060 alloy with a low-alloy 16MnCr5 filler steel. The influences of the setting parameters on the energetic states are first analyzed by means of an initial screening. The evaluation using process simulation and statistical methods enables the generation of regressive response surfaces for the friction power, the friction time and the resulting induced friction energy. Based on these findings, a second experimental field is formed and evaluated, which considers the interaction between the energy input of the frictioning stage and the workpiece forging. This new approach results in the functional separation of the frictioning and forging stage, which eliminates the usual statistical interaction effects and thus facilitates analysis and optimization. The qualitative result variable required for the purpose of interpreting the results is the ultimate tensile strength of the friction-welded joint. Additionally determined hardness curves provide information about the properties of the thermally influenced zone and strength-relevant process sequences. The result is that, in addition to the amount of energy induced, the frictional power with which the former is induced also has a considerable influence on the joint strength, as it influences the material flow and the properties of the joining zone.

本出版物涉及一种以能量为导向的旋转摩擦焊接过程统计分析方法。为说明该方法,本文应用该方法研究了 AA6060 合金与低合金 16MnCr5 填充钢摩擦焊接过程中能量流对材料流动行为和接头质量的影响。首先通过初步筛选分析了设定参数对能量状态的影响。通过使用过程模拟和统计方法进行评估,得出了摩擦功率、摩擦时间和由此产生的诱导摩擦能的回归响应面。基于这些发现,形成并评估了第二个实验领域,该领域考虑了摩擦阶段的能量输入与工件锻造之间的相互作用。这种新方法将摩擦阶段和锻造阶段的功能分开,消除了通常的统计交互效应,从而便于分析和优化。解释结果所需的定性结果变量是摩擦焊接接头的极限拉伸强度。此外,测定的硬度曲线还提供了有关热影响区特性和强度相关工艺顺序的信息。结果表明,除了诱导的能量外,前者诱导的摩擦力对接头强度也有相当大的影响,因为它会影响材料流动和接合区的特性。
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引用次数: 0
Fe/polymer joining via Fe/TiB2 composite structures via in-situ laser-induced reaction of Fe-Ti-B system: Effect of powder composition 通过原位激光诱导 Fe-Ti-B 系统反应,在 Fe/TiB2 复合结构中加入铁/聚合物:粉末成分的影响
IF 3.8 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-09-02 DOI: 10.1016/j.jajp.2024.100249
Shaoyun Zhou, Koki Omiya, Yuto Ueda, Asuka Suzuki, Naoki Takata, Makoto Kobashi

Achieving strong direct joining between steel and polymers through mechanical interlocking is crucial for developing multi-material structures, particularly in the automotive and aerospace industries. This study synthesized micro-scale structures on a pure Fe substrate (simulating interstitial-free (IF) steel) for mechanical interlocking with thermoplastic parts. Numerous submillimeter-scale Fe/TiB2 composite particles were in-situ synthesized by laser scanning on the Fe-Ti-B powder mixture and well-bonded with the Fe substrate. The effects of powder composition (TiB2 volume fraction) on the morphology, microstructure, and joint strength with PA6 were investigated. A TiB2 volume fraction over 60 % was essential for the formation of the composite particles promoted by a TiB2 skeletal structure. Higher TiB2 volume fractions increased the area fraction of the composite particles and decreased the bonding ratio (adhesive) of the particles with the substrate due to poor adhesiveness at the edge of the laser-scanning line. A wider high-temperature region was generated at a higher TiB2 volume fraction, suggesting that the reaction heat to form TiB2 assisted the bonding of the particles with the substrate at the edge of the laser scanning line. The Fe/PA6 joint strength increased to approximately 30 MPa with increasing the TiB2 volume fraction to 100 % and showed a linear correlation with the product of particle area fraction and bonding ratio. A higher TiB2 volume fraction was preferable for enhancing the joint strength via the micro-scale structures synthesized by laser scanning on the Fe-Ti-B powder mixture. A combination of the micro-structuring process using a high fraction of TiB2 with advanced joining technologies will contribute to manufacturing high-strength Fe/polymer hybrid parts.

通过机械互锁实现钢与聚合物之间的强力直接连接对于开发多材料结构至关重要,尤其是在汽车和航空航天工业领域。本研究在纯铁基底(模拟无间隙(IF)钢)上合成了微尺度结构,用于与热塑性部件进行机械联锁。通过激光扫描在 Fe-Ti-B 粉末混合物上原位合成了大量亚毫米级的 Fe/TiB2 复合材料颗粒,并与铁基材很好地结合在一起。研究了粉末成分(TiB2 体积分数)对形态、微观结构以及与 PA6 的接合强度的影响。TiB2 体积分数超过 60% 对形成由 TiB2 骨架结构促进的复合颗粒至关重要。较高的 TiB2 体积分数增加了复合材料颗粒的面积分数,但由于激光扫描线边缘的粘合性较差,降低了颗粒与基材的粘合率(粘合力)。TiB2 体积分数越高,产生的高温区域越宽,这表明形成 TiB2 的反应热有助于颗粒与激光扫描线边缘基底的粘合。随着 TiB2 体积分数增加到 100%,Fe/PA6 接头强度增加到约 30 兆帕,并且与颗粒面积分数和结合率的乘积呈线性相关。较高的 TiB2 体积分数更有利于通过激光扫描在 Fe-Ti-B 粉末混合物上合成的微尺度结构来提高接头强度。将使用高比例 TiB2 的微结构工艺与先进的连接技术相结合,将有助于制造高强度的铁/聚合物混合零件。
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引用次数: 0
Interfacial inhomogeneous plastic deformation during rotary friction welding of dissimilar AA2219-SS321 joint combination with AA6061 interlayer 带有 AA6061 中间膜的异种 AA2219-SS321 接头旋转摩擦焊接过程中的界面不均匀塑性变形
IF 3.8 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-08-30 DOI: 10.1016/j.jajp.2024.100245
Neeraj Kumar Mishra , S.G.K. Manikandan , Amber Shrivastava

This research investigates the inherent radial non-uniformity within the rotary friction welding process, particularly concerning microstructure attributes like grain size, grain boundaries, misorientation angles, and interlayer presence along the radial axis. SS321-AA2219 rotary friction welding was carried out with and without an AA6061 interlayer. The numerical thermal model suggests increase in temperatures from the center to the periphery, due to non-uniform heat generation. Also, dissimilar material across the interface resulted in an asymmetric temperature profile along axial direction. Plastic deformation on the Aluminum side suggests dynamic recrystallization and grain refinement, whereas pronounced low-angle grain boundary (LAGB) formation near the SS side interface validates dynamic recovery. A radial non-uniformity in microstructure is observed, with metrics such as average grain size, LAGB fraction, and misorientation showing an increase from the center towards the periphery. The insertion of an interlayer alters process dynamics, manifesting in reduced temperatures and heightened forces, resulting in a more consolidated joint by enhancing the strength by 31 %. Interdiffusion of elements across the interface formed Fe-Al intermetallic compounds (IMC) confirmed with X ray diffraction. Fractography analysis elucidates the presence of rubbing marks and facet surfaces in interlayer-less joints, while joints with interlayer display sticking and dimples.

本研究调查了旋转摩擦焊过程中固有的径向不均匀性,特别是沿径向轴线的晶粒尺寸、晶界、错位角和夹层存在等微观结构属性。在有 AA6061 夹层和没有 AA6061 夹层的情况下进行了 SS321-AA2219 旋转摩擦焊。数值热模型表明,由于发热不均匀,温度从中心向周边升高。此外,界面上的异种材料导致沿轴向的温度分布不对称。铝侧的塑性变形表明了动态再结晶和晶粒细化,而 SS 侧界面附近明显的低角度晶界(LAGB)形成则验证了动态恢复。观察到微观结构的径向不均匀性,平均晶粒大小、LAGB 分数和取向偏差等指标显示出从中心向外围增加的趋势。中间层的插入改变了工艺动态,表现为温度降低和作用力增加,从而使接头更加牢固,强度提高了 31%。X 射线衍射证实,元素在界面上的相互扩散形成了铁铝金属间化合物(IMC)。碎裂分析表明,无夹层的接合处存在摩擦痕迹和刻面,而有夹层的接合处则出现粘连和凹陷。
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引用次数: 0
Loosening phenomenon on thin plates bolted joint due to offset load 偏载导致薄板螺栓连接处出现松动现象
IF 3.8 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-08-28 DOI: 10.1016/j.jajp.2024.100247
Naoki Yamamoto , Takehiro Ohno , Shinji Hashimura

In this study, the new loosening behavior was discovered and investigated when offset loads were repeatedly applied to both ends of a bolted joint initially tightened to a thin plate made of high-tensile steel. In the experiments, the impact of offset distance on reduction of clamp force was investigated through multiple applications of symmetric offset axial load to the bolted joint assembly. The experimental results showed that even a slight offset load reduced the clamp force, and the larger the offset distance, the greater the reduction of the clamp force. It was also found that the decrease in clamp force depends not on the number of times the offset load is applied but on the magnitude of the offset load. Until now even if the thin plate bolted joint was subjected to an offset load, as long the plates do not deform significantly due to plastic deformation, it has been generally recognized that the clamp force is not reduced. This loosening phenomenon is new and its mechanism has not been elucidated yet. In order to clarify the mechanism that may lower the clamp force, this study conducted FE analysis using a simplified model of a bolted joint. In the FE model, the bolt and nut are considered as a single unit and the effect of slippage between the thread surfaces and the effect of plastic deformation is ignored by using elastic analysis. The results of the FE analysis showed that the main factor causing the reduction in clamp force was slippage between the thin plates to be joined, which was caused by offset load, and that the slippage didn't return to the original position resulting in the reduction in clamp force.

在本研究中,我们发现并研究了一种新的松动行为,即在最初拧紧在高强度钢薄板上的螺栓连接两端反复施加偏置载荷。在实验中,通过对螺栓连接组件多次施加对称偏置轴向载荷,研究了偏置距离对夹紧力降低的影响。实验结果表明,即使是轻微的偏移载荷也会降低夹紧力,而且偏移距离越大,夹紧力的降低幅度越大。实验还发现,夹紧力的减小并不取决于施加偏置载荷的次数,而是取决于偏置载荷的大小。迄今为止,即使薄板螺栓连接承受了偏置载荷,只要薄板没有因塑性变形而发生显著变形,夹紧力就不会降低,这一点已得到普遍认可。这种松动现象是一种新现象,其机理尚未阐明。为了阐明可能降低夹紧力的机理,本研究使用螺栓连接的简化模型进行了有限元分析。在有限元模型中,螺栓和螺母被视为一个整体,通过弹性分析,忽略了螺纹表面之间的滑动效应和塑性变形效应。有限元分析的结果表明,导致夹紧力降低的主要因素是由偏移载荷引起的待连接薄板之间的滑动,而这种滑动不会恢复到原来的位置,从而导致夹紧力降低。
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引用次数: 0
Friction weldability of ultrafine-grained titanium grade 2 超细晶粒钛 2 级的摩擦焊接性
IF 3.8 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-08-26 DOI: 10.1016/j.jajp.2024.100246
Beata Skowrońska , Tomasz Chmielewski , Michał Baranowski , Mariusz Kulczyk , Jacek Skiba

The paper presents the results of an experimental study of the friction weldability of Titanium Grade 2 with ultrafine-grained (UFG) microstructure obtained by hydrostatic extrusion and rotary swaging (HE+RS). High-speed friction welding with different rotational speed (n) values was used as a joining method. The best properties were obtained for n=7000 rpm. Metallographic observations confirmed the formation of a continuous friction joint with a changed microstructure of the base material in the thermal-mechanical affected zone (TMAZ) and a friction weld (FW). The results of the mechanical properties showed the greatest decrease in hardness in the TMAZ. The friction welded joint had an 18 % lower tensile strength value than initial state UFG Titanium Grade 2 after the HE+RS process (with UTS=1050 MPa).

本文介绍了通过静水挤压和旋转锻造(HE+RS)获得的具有超细晶粒(UFG)微观结构的 2 级钛的摩擦焊接性实验研究结果。采用不同转速(n)值的高速摩擦焊作为连接方法。n=7000 rpm 时获得了最佳性能。金相学观察证实,在热机械影响区(TMAZ)和摩擦焊缝(FW)中形成了母材微观结构发生变化的连续摩擦接头。机械性能结果表明,TMAZ 的硬度下降幅度最大。在 HE+RS 工艺(UTS=1050 兆帕)之后,摩擦焊接接头的抗拉强度值比初始状态的 UFG 钛 2 级低 18%。
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引用次数: 0
Improvements in manufacturability, bonding strength, and curing efficiency of a silicone adhesive 提高硅酮粘合剂的可制造性、粘合强度和固化效率
IF 3.8 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-08-20 DOI: 10.1016/j.jajp.2024.100243
Ye Yang , Jinfeng Xu , Xusheng Chen , Wang Yang , Lina Si , Hongjuan Yan , Zhaoliang Dou , Fengbin Liu , Huanxiong Xia

Two-component room temperature vulcanizing silicone adhesive RTV566 with a lower elastic modulus has been widely used in precision optomechanical products such as remote sensors and aerospace infrared cameras. However, the silicone adhesive is of poor manufacturability due to its extremely high viscosity, and the bonded joint usually exhibits low bonding strength and requires a long curing time. This paper investigates a way to improve both the adhesion strength and curing efficiency of Invar alloy and optical glass with RTV566 through single-lap experiments. It is found that adding small amounts of acetone and water can significantly reduce the viscosity, enhance the bonding strength, and shorten the curing time. The viscosity can be reduced by 63.4 % and the bonding strength can be improved by 136.4 % with the weight ratio of adhesive to acetone being 20:2. Moreover, a little amount of water in the weight ratio of 100:10:0.1 (adhesive: acetone: water) can shorten the curing time from 7 days to 4 days without harms to the bonding strength and elastic modulus. As to the mechanism, the silicone adhesive can be dissolved by acetone and its sulfuration reaction can be enhanced by water, resulting in good manufacturability and high curing efficiency. This work contributes a novel and easy-to-use method to greatly improve the performances of the bonding process of precision optical structures.

具有较低弹性模量的双组分室温硫化硅酮粘合剂 RTV566 已广泛应用于遥感器和航空红外摄像机等精密光机械产品。然而,这种硅胶粘合剂由于粘度极高,可制造性差,粘接接头通常粘接强度低,固化时间长。本文通过单圈实验研究了一种用 RTV566 提高因瓦合金和光学玻璃的粘接强度和固化效率的方法。实验发现,添加少量丙酮和水可显著降低粘度,提高粘接强度,缩短固化时间。粘合剂与丙酮的重量比为 20:2,粘度可降低 63.4%,粘合强度可提高 136.4%。此外,以 100:10:0.1(粘合剂:丙酮:水)的重量比加入少量水,可将固化时间从 7 天缩短至 4 天,而不会影响粘合强度和弹性模量。在机理方面,丙酮可溶解硅酮粘合剂,水可促进其硫化反应,因此具有良好的可制造性和较高的固化效率。这项工作提供了一种新颖易用的方法,大大提高了精密光学结构粘接工艺的性能。
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引用次数: 0
Fracture toughness and microstructural analysis of rotary friction welded S355J2 and SS316L steels for critical applications 用于关键应用的旋转摩擦焊接 S355J2 和 SS316L 钢的断裂韧性和微观结构分析
IF 3.8 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-08-19 DOI: 10.1016/j.jajp.2024.100244
Rajkumar Das , Giribaskar Sivaswamy , Himanshu Lalvani , Ajit Pal Singh

Dissimilar metal welding is seeing growing adoption across industries to enhance structural functionality and efficiency. Achieving high-quality, defect-free dissimilar weld joints requires a comprehensive understanding of the interrelationships between the welding-induced microstructural changes and the material's performance characteristics, particularly its fracture-related properties. This study investigates the impact of microstructural changes on the fracture toughness of dissimilar welds between structural low-carbon steel (S355J2) and austenitic stainless steel (SS316L) prepared using the Rotary Friction Welding (RFW) technique. Welding preforms were created from respective pipe pup pieces. The evaluation involves microstructural analysis, tensile testing, hardness testing, and fracture toughness testing using compact tension specimens derived from various zones of the weld joints. Results revealed significant microstructural differences across the weld joint. The weld region exhibited stable hardness with a maximum of 208 HV1 in S355J2′s thermo-mechanically affected zone (TMAZ). High tensile strength (Ultimate Tensile Strength 540 MPa, Yield Strength 367 MPa) with failures mainly on the S355J2 side. The fracture toughness (KQ) matched parent metal values, with the RFW weld centre line (WCL) showing superior crack tip opening displacement (CTOD) of 0.35 mm. Fractography generally indicates ductile failure.

各行各业越来越多地采用异种金属焊接来提高结构功能和效率。要实现高质量、无缺陷的异种焊接接头,需要全面了解焊接引起的微观结构变化与材料性能特征之间的相互关系,特别是与断裂有关的性能。本研究探讨了微观结构变化对使用旋转摩擦焊(RFW)技术制备的低碳钢(S355J2)和奥氏体不锈钢(SS316L)异种焊缝断裂韧性的影响。焊接预型件是由各自的管件制作而成的。评估包括微观结构分析、拉伸测试、硬度测试和断裂韧性测试,使用的是来自焊点不同区域的紧凑拉伸试样。结果显示,整个焊点的微观结构存在明显差异。焊缝区域显示出稳定的硬度,S355J2 热机械影响区(TMAZ)的最大硬度为 208 HV1。抗拉强度高(极限抗拉强度 540 兆帕,屈服强度 367 兆帕),主要在 S355J2 一侧出现破坏。断裂韧性(KQ)与母体金属值相匹配,RFW 焊接中心线(WCL)显示出 0.35 毫米的优异裂纹尖端张开位移(CTOD)。断口形貌一般显示为韧性破坏。
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Journal of Advanced Joining Processes
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