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A hybrid numerical approach for characterising airflow and temperature distribution in a ventilated pallet of heat-generating products: Application to cheese 用于描述发热产品通风托盘中气流和温度分布的混合数值方法:应用于奶酪
IF 5.3 2区 农林科学 Q1 ENGINEERING, CHEMICAL Pub Date : 2024-09-18 DOI: 10.1016/j.jfoodeng.2024.112323
Dihia Aguenihanai , Denis Flick , Steven Duret , Jean Moureh

Temperature control throughout the cold chain is of crucial importance in the preservation of the quality of cheese. As a result of cheese heat generation, both natural and forced convection need to be considered. This numerical study aimed to characterise the airflow and temperature fields within a ventilated pallet of heat-generating cheeses. An original computational fluid dynamics (CFD) hybrid approach was developed. This approach is based on a combination of a porous media approach for the contents of the boxes and a direct CFD approach for the outer cardboard walls, including vent size and position. The computational domain is limited to one pallet level. The simulations were conducted on a steady state for two upwind air velocities 0.31 m/s and 0.73 m/s and three generated heat fluxes 0.05 W, 0.15 W, and 0.3 W per product item (250 g). The model was validated by comparison with experimental results related to velocity and product temperature profiles obtained on a full-scale experimental set-up. The hybrid approach shows good accuracy while reducing the mesh size and the computational time in comparison with the direct CFD approach.

整个冷链的温度控制对奶酪质量的保持至关重要。由于奶酪会产生热量,因此需要考虑自然对流和强制对流。这项数值研究旨在确定发热奶酪通风托盘内气流和温度场的特征。研究开发了一种独创的计算流体动力学(CFD)混合方法。该方法结合了多孔介质方法和直接 CFD 方法,前者适用于箱内物品,后者适用于纸板外壁,包括通风口的大小和位置。计算域仅限于一个托盘层。模拟在两种上风速 0.31 米/秒和 0.73 米/秒以及每件产品(250 克)产生 0.05 瓦、0.15 瓦和 0.3 瓦三种热通量的稳定状态下进行。通过与在全尺寸实验装置上获得的速度和产品温度曲线相关实验结果进行比较,对模型进行了验证。与直接 CFD 方法相比,混合方法在减少网格尺寸和计算时间的同时,显示出良好的精确性。
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引用次数: 0
Engineering effects of hydrocolloids on drying kinetics, powder characteristics, and antioxidant preservation in grape powder 水胶体对葡萄粉干燥动力学、粉末特性和抗氧化剂保存的工程学影响
IF 5.3 2区 农林科学 Q1 ENGINEERING, CHEMICAL Pub Date : 2024-09-17 DOI: 10.1016/j.jfoodeng.2024.112319
Amanda Nascimento, Alexandre Lúcio, Ana Nery, Rogério Andrade, Ana Maria Sarinho, Janaina Lima, Leonardo Batista, Hugo M. Lisboa
This study explores the preservation of bioactive compounds in grape powder via encapsulation using spray drying, focusing on the impact of hydrocolloids—whey protein isolate (WPI), gum arabic, and high methoxy pectin—on critical engineering parameters. The research analyzes the effects of these encapsulants on rheological properties, drying kinetics, droplet formation, and drying curves, all of which influence the powder's morphology and antioxidant retention. Drying times ranged from 1.05 to 1.14 s, with distinct drying curves reflecting the relationship between moisture content and time, correlating with key powder properties such as bulk and tap density, flowability, and compressibility. Dimensionless numbers, including Peclet and Reynolds numbers, showed significant correlations with both powder characteristics and bioactive retention, highlighting the role of efficient heat and mass transfer in preserving phenolic content. The study concludes that optimal formulations, particularly those combining WPI and pectin, result in uniform droplet sizes, faster drying rates, and enhanced bioactive stability, providing insights for optimizing spray drying processes to produce high-quality, stable food powders.
本研究探讨了通过喷雾干燥封装技术保存葡萄粉中生物活性化合物的方法,重点研究了水胶体--分离乳清蛋白(WPI)、阿拉伯树胶和高甲氧基果胶--对关键工程参数的影响。研究分析了这些封装剂对流变特性、干燥动力学、液滴形成和干燥曲线的影响,所有这些都会影响粉末的形态和抗氧化剂的保留。干燥时间从 1.05 秒到 1.14 秒不等,不同的干燥曲线反映了水分含量与时间之间的关系,并与关键的粉末特性(如体积密度和敲击密度、流动性和可压缩性)相关联。包括佩克莱特数和雷诺数在内的无量纲数与粉末特性和生物活性保留率都有显著的相关性,凸显了高效传热和传质在保存酚类物质含量方面的作用。研究得出结论,最佳配方,尤其是结合了 WPI 和果胶的配方,能产生均匀的液滴大小、更快的干燥速率和更强的生物活性稳定性,为优化喷雾干燥工艺以生产高质量、稳定的食品粉末提供了启示。
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引用次数: 0
Fabrication of pH-responsive whey protein/sodium alginate composite hydrogel beads for theaflavins 制造具有 pH 响应性的乳清蛋白/海藻酸钠复合水凝胶珠,用于生产茶黄素
IF 5.3 2区 农林科学 Q1 ENGINEERING, CHEMICAL Pub Date : 2024-09-17 DOI: 10.1016/j.jfoodeng.2024.112324
Yeexuan Tan , Sookwah Chan , Beiqi Wu , Hongxin Wang , Zaixiang Lou

In this study, pH-responsive whey protein (WP)/sodium alginate (SA) composite hydrogel beads using the ionic gelation method were described and evaluated for their potential as delivery carriers for theaflavin (TF). Fourier transform infrared spectroscopy (FTIR) confirmed the interaction between WP and SA in the hydrogel beads is driven primarily by the strong intermolecular interactions, including hydrogen bonding and electrostatic attractions. The swelling ratio of the beads possesses good pH dependence and pH reversibility, effectively preventing the release of TF in the gastric environment. The encapsulation efficiency (EE) of TF in hydrogel beads ranged from 94.995 ± 0.03 to 95.709 ± 0.14, with a loading capacity (LC) of 27–34 mg/g. In in vitro digestion simulations, owing to the pH responsiveness, hydrogel beads released minimal TF throughout gastric digestion and were fully released in the intestine phase. Additionally, the release kinetics of TF from the beads were further examined in a simulated intestinal environment. These findings suggest that the hydrogel bead system is a promising carrier for encapsulating TF, offering a theoretical and experimental basis for its future application in the food industry.

本研究采用离子凝胶法描述并评估了pH响应型乳清蛋白(WP)/海藻酸钠(SA)复合水凝胶珠作为茶黄素(TF)递送载体的潜力。傅立叶变换红外光谱(FTIR)证实,水凝胶珠中可湿性粉剂和海藻酸盐之间的相互作用主要由分子间的强相互作用(包括氢键和静电吸引)驱动。珠子的溶胀率具有良好的 pH 依赖性和 pH 可逆性,可有效防止 TF 在胃环境中的释放。TF在水凝胶珠中的包封效率(EE)为94.995 ± 0.03至95.709 ± 0.14,负载能力(LC)为27-34 mg/g。在体外消化模拟中,由于 pH 值响应性,水凝胶珠在整个胃消化过程中释放的 TF 极少,而在肠道阶段完全释放。此外,还在模拟肠道环境中进一步研究了水凝胶珠释放 TF 的动力学。这些研究结果表明,水凝胶珠系统是一种很有前景的封装 TF 的载体,为其未来在食品工业中的应用提供了理论和实验基础。
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引用次数: 0
Sustained-release effect of eggshell powder microcapsules on lavender essential oil 蛋壳粉微胶囊对薰衣草精油的缓释作用
IF 5.3 2区 农林科学 Q1 ENGINEERING, CHEMICAL Pub Date : 2024-09-16 DOI: 10.1016/j.jfoodeng.2024.112322
Ziwei Zhang , Yanlong Liu , Ying Gao , Jiaying Huo , Shijian Dong , Liya Liu , Shugang Li

Eggshells are rich in Ca2+ and organic compounds, which can be taken as coupling agents for sustained-release materials. Essential oils are widely applied due to their excellent volatility, but poor sustained-release stability has limited their development. The study aimed to develop a novel eggshell powder (EP) sustained-release microcapsule, providing a new approach to protect the active ingredients of Lavender essential oil (LEO), and investigated the reasons for EP to regulate protein-polysaccharide microcapsule structure. Experimental results showed when the addition ratio of EP and Whey protein (WPI) was 1: 3, the dosage of LEO was 25%, the microcapsule displayed smooth and porous spherical structure. XRD and FT-IR indicated that a dense and orderly network structure was formed via the cross-linking reaction between eggshell powder and wall materials, which induced protein and polysaccharide to form special spherical hollow sustained-release shell structure through the calcium bridge (-COO-Ca-COO-), then achieved the sustained-release effect on LEO.

蛋壳富含 Ca2+ 和有机化合物,可用作缓释材料的偶联剂。精油因其优良的挥发性而被广泛应用,但其缓释稳定性较差,限制了其发展。本研究旨在开发一种新型蛋壳粉(EP)缓释微胶囊,为保护薰衣草精油(LEO)的有效成分提供一种新方法,并研究蛋壳粉调节蛋白质-多糖微胶囊结构的原因。实验结果表明,当 EP 与乳清蛋白(WPI)的添加比例为 1:3,LEO 的用量为 25%时,微胶囊呈现出光滑多孔的球形结构。XRD和FT-IR表明,蛋壳粉与壁材发生交联反应形成了致密有序的网络结构,通过钙桥(-COO-Ca-COO-)诱导蛋白质和多糖形成特殊的球形中空缓释壳结构,从而实现了LEO的缓释效果。
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引用次数: 0
Can rheometer be used for determination of baking stability of cocoa based filling creams 流变仪能否用于测定可可基馅奶油的烘焙稳定性
IF 5.3 2区 农林科学 Q1 ENGINEERING, CHEMICAL Pub Date : 2024-09-13 DOI: 10.1016/j.jfoodeng.2024.112320
Burcu Utku Aktar , Arzu Karakaş İshak , Duygu Ozmen , Halide Ezgi Tuna Ağırbaş , Ozer Atıl , Omer Said Toker

Bake stable filling creams are important for some products such as biscuits, cakes, cookies, etc. In the present study, a rheometer-based method for determining the baking stability of the cream fillings was developed considering the consistency and fluidity of the fillings after baking. For this aim, the heating and cooling process was simulated depending on the temperature of the filling reached during the baking process of cookies. Three bake-stable and three bake-unstable filling creams were obtained from the market. Rheological, textural, and baking stability analysis were performed on the samples. Change in the apparent viscosity values of the samples was observed at temperature values from 20 °C to 105 °C and from 105 °C to 30 °C using rheometer. The percentage of viscosity change at 30 °C before and after the heating process was calculated. This value for stable samples was 67%, 73% and 9%. Fluctuation observation during the measurement is also important for stability. Unstable fillings have many fluctuations in the temperature versus apparent viscosity curve as their viscosity change value was lower. The absence of fluctuations on the temperature versus viscosity graph indicates the stability of the filling creams. The findings of the study indicated that a rheometer can be used as an effective tool for determining the baking stability of the creams with minimal effort, labor, sample requirement, and time.

对于饼干、蛋糕、曲奇等一些产品来说,烘焙稳定的奶油馅非常重要。在本研究中,考虑到烘焙后馅料的稠度和流动性,开发了一种基于流变仪的方法来确定奶油馅料的烘焙稳定性。为此,根据饼干烘焙过程中馅料达到的温度,模拟了加热和冷却过程。从市场上获得了三种烘焙稳定型和三种烘焙不稳定型馅料奶油。对样品进行了流变学、质地和烘焙稳定性分析。使用流变仪观察了样品在 20 °C 至 105 °C 和 105 °C 至 30 °C 温度值下表观粘度值的变化。计算了加热过程前后 30 °C 下粘度变化的百分比。稳定样品的这一数值分别为 67%、73% 和 9%。测量过程中的波动观察对稳定性也很重要。不稳定的填料在温度与表观粘度曲线上会有很多波动,因为它们的粘度变化值较低。温度与表观粘度曲线图上没有波动说明填充膏具有稳定性。研究结果表明,流变仪可以作为一种有效的工具,以最小的工作量、人力、样品要求和时间来确定奶油的烘焙稳定性。
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引用次数: 0
Quantifying rheology and texture of chocolate products with oleogels using fractional calculus 利用分数微积分量化含油凝胶巧克力产品的流变性和质地
IF 5.3 2区 农林科学 Q1 ENGINEERING, CHEMICAL Pub Date : 2024-09-13 DOI: 10.1016/j.jfoodeng.2024.112321
Yumin Yang , Jinghu Yu , Shanhua Qian , Fangyong Zhu

Oleogels, a novel technology for structuring fats, show great potential for partially or completely replacing solid fats in chocolate products containing unhealthy saturated fatty acids. However, how to maintain similar rheological properties and sensory texture attributes is a major challenge. Given the lack of a concise and effective mathematical framework, simulating the rheological response and quantifying the textural parameters of the hybrid oleogel-dispersed chocolate products, is complicated. In this work, the rheological power law behavior of hybrid oleogel-dispersed chocolate products is accurately captured by using a fractional constitutive mathematical framework with few constitutive parameters. The sensory texture parameter firmness is quantified on the basis of creep response. The rheological response and firmness index are linked together on the basis of the fractional derivative model. This work helps provide heuristic insights into the structure-texture engineering of this food type. Such insights may, in turn, guide the formulation and design of food products.

油凝胶是一种新颖的脂肪结构技术,在部分或完全替代含有不健康饱和脂肪酸的巧克力产品中的固体脂肪方面显示出巨大的潜力。然而,如何保持相似的流变特性和感官质地属性是一大挑战。由于缺乏简明有效的数学框架,模拟混合油凝胶分散巧克力产品的流变响应和量化质构参数的工作十分复杂。在这项工作中,通过使用少量构成参数的分数构成数学框架,准确捕捉了混合油凝胶分散巧克力产品的流变幂律行为。在蠕变响应的基础上,对感官质地参数 "坚固度 "进行了量化。在分数导数模型的基础上,将流变响应和坚固指数联系在一起。这项工作有助于为这种食品的结构-质地工程提供启发式见解。这些见解反过来又可以指导食品的配方和设计。
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引用次数: 0
Potential of acoustic sensors for real-time monitoring of physicochemical properties of milk protein concentrate during ultrafiltration 声学传感器在超滤过程中实时监测浓缩牛奶蛋白理化特性的潜力
IF 5.3 2区 农林科学 Q1 ENGINEERING, CHEMICAL Pub Date : 2024-09-12 DOI: 10.1016/j.jfoodeng.2024.112314
Guangya Xu , John T. Tobin , Hanieh Amani , Surabhi Subhir , Colm P. O'Donnell , Norah O'Shea

Ultrafiltration (UF) is the step for concentrating protein in milk and whey prior to evaporation and drying in dairy ingredient production, e.g. milk protein concentrate (MPC). To optimize UF process, it is important to monitor changes in product/process parameters. Two in-line sensors with outputs: 1. bulk acoustic wave (BAW), acoustic viscosity (AV); 2. surface acoustic wave (SAW), acoustic impedance (AI) and acoustic transmission (AT), were evaluated to measure MPC physicochemical properties (total solids (TS), density, protein and apparent viscosity) during UF. Trials were quintuplicated in a UF membrane pilot-plant, to concentrate feed (TS 11.36–19.10%). Models for predicting MPC physicochemical properties developed by acoustic parameters performed well, especially by AI and AT, with R2 > 0.963, SEP <1.076 to predict apparent viscosity, and R2 > 0.980, SEP <0.627 for all other properties’ prediction. This study demonstrated the potential of both acoustic sensors for UF process monitoring.

超滤(UF)是在乳制品配料生产(如牛奶浓缩蛋白(MPC))过程中,在蒸发和干燥之前浓缩牛奶和乳清中蛋白质的步骤。为了优化超滤工艺,监测产品/工艺参数的变化非常重要。两个在线传感器具有以下输出1. 体积声波 (BAW)、声粘度 (AV);2. 表面声波 (SAW)、声阻抗 (AI) 和声透射 (AT)。在超滤膜中试工厂进行了五次试验,以浓缩饲料(TS 11.36-19.10%)。通过声学参数建立的 MPC 理化特性预测模型表现良好,尤其是 AI 和 AT,预测表观粘度的 R2 > 为 0.963,SEP <为 1.076,预测所有其他特性的 R2 > 为 0.980,SEP <为 0.627。这项研究证明了这两种声学传感器在监测 UF 过程方面的潜力。
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引用次数: 0
3D printing food flow in different extruders based on crazy and adaptive salp swarm algorithm-deep extreme learning machine improved-lattice Boltzmann method 基于疯狂和自适应萨尔普群算法的 3D 打印食品在不同挤出机中的流动--深度极端学习机改进的格子波尔兹曼法
IF 5.3 2区 农林科学 Q1 ENGINEERING, CHEMICAL Pub Date : 2024-09-12 DOI: 10.1016/j.jfoodeng.2024.112318
Weiwei Wu, Minheng Gu, Xin Liu, Zhongyi Shan, Shuang Ding, Yanjun Zhang, Wenhan Yang

Extrusion is significant in achieving 3D printing emulsion. The piston and screw extruders are the common structures to achieve the extrusion. The chocolate emulsion is taken for example, two extruders are numerically investigated and compared based on the fluid dynamic analysis. To conduct the simulations, the crazy and adaptive salp swarm algorithm-deep extreme learning machine (CASSA-DELM) is proposed to predict the viscosity of the chocolate emulsion, which is used to replace the traditional fitted model. The built model can avoid non-consistency in the whole shearing rate range. Then, an improved lattice Boltzmann method (I-LBM) is introduced to process the non-Newtonian behavior of the emulsion. In the simulation, the CASSA-DELM model provides the viscosities for each iteration in I-LBM based on the obtained shearing rates. Because the attachment(s) may be generated on the walls, the no-attachment and with-attachment(s) cases are explored, and the necessary results are obtained, which indicate that the piston extruder is more suitable for extruding the single component of food fluid. The screw extruder is recommended for the multiple components of food fluid because the vortex in the X-Y cross-section contributes to further mixing action for the emulsion containing different materials, such as the investigated chocolate emulsion. The indirect experiments are conducted to validate the above conclusions. The current work can contribute to improving the extruding theory of material extrusion technologies.

挤压对于实现三维打印乳化非常重要。活塞挤压机和螺杆挤压机是实现挤压的常见结构。以巧克力乳液为例,基于流体动力学分析对两种挤出机进行了数值研究和比较。为了进行仿真,提出了疯狂自适应萨尔普群算法-深度极端学习机(CASSA-DELM)来预测巧克力乳液的粘度,用来替代传统的拟合模型。建立的模型可避免整个剪切速率范围内的不一致性。然后,引入改进的晶格玻尔兹曼法(I-LBM)来处理乳液的非牛顿行为。在模拟过程中,CASSA-DELM 模型根据获得的剪切速率为 I-LBM 的每次迭代提供粘度。由于壁上可能会产生附着物,因此对无附着物和有附着物的情况进行了探讨,并得出了必要的结果。对于多组分食品流体,建议使用螺杆挤出机,因为 X-Y 截面上的漩涡有助于进一步混合含有不同材料的乳液,如所研究的巧克力乳液。间接实验验证了上述结论。目前的工作有助于改进材料挤压技术的挤压理论。
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引用次数: 0
Dynamic mechanism and structural property analysis of microfluidic-obtained pea protein fiber 微流控获得豌豆蛋白纤维的动力机制和结构特性分析
IF 5.3 2区 农林科学 Q1 ENGINEERING, CHEMICAL Pub Date : 2024-09-11 DOI: 10.1016/j.jfoodeng.2024.112316
Ren Li , Yulin Feng , Sen Zhang , Huijuan Zhang , Feiyue Ren , Jie Liu , Jing Wang

Although protein-based fibers have been developed, the preparation of inexpensive, safe and environmentally friendly plant protein fibers is still a hot topic. Herein, we constructed the microfluidic chip to produce protein fiber using pea protein and a small amount of cellulose nanofibers. The results demonstrated that compared to pea protein alone, the pea protein-based fiber produced through microfluidic spinning exhibited a smooth and dense surface structure, good thermal stability, higher Zeta potential and antioxidant activity, and lower surface hydrophobicity and sensitization. Furthermore, we comprehensively revealed the dynamic formation mechanism of pea protein-based fiber. During the fiber preparation process, hydrodynamics led the protein and cellulose nanofibers to align gradually along the flow direction, enhancing their molecular orientation. Additionally, strong hydrodynamic shear force altered the protein structure, transitioning its spatial structure from random coil and α-helix to β-sheet, and promoting a binding of protein to cellulose nanofibers. This research may offer theoretical guidance for the application of pea protein-based fiber in the preparation of hypoallergenic protein-based fibers and the construction of foodborne delivery materials.

虽然蛋白基纤维已被开发出来,但制备廉价、安全、环保的植物蛋白纤维仍是一个热门话题。在此,我们利用豌豆蛋白和少量纤维素纳米纤维构建了制备蛋白纤维的微流控芯片。结果表明,与单独使用豌豆蛋白相比,通过微流控纺丝生产的豌豆蛋白基纤维具有光滑致密的表面结构、良好的热稳定性、更高的Zeta电位和抗氧化活性、更低的表面疏水性和敏化性。此外,我们还全面揭示了豌豆蛋白基纤维的动态形成机理。在纤维制备过程中,流体力学使蛋白质和纤维素纳米纤维沿流动方向逐渐排列,增强了它们的分子取向。此外,强大的流体动力剪切力改变了蛋白质的结构,使其空间结构从随机线圈和α-螺旋过渡到β-片状,促进了蛋白质与纤维素纳米纤维的结合。这项研究可为豌豆蛋白基纤维在制备低过敏性蛋白基纤维和构建食源性递送材料方面的应用提供理论指导。
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引用次数: 0
Effect of carboxymethyl cellulose binder on physical, thermal, and rheological properties of milk protein isolate/guar gum mixture powder 羧甲基纤维素粘合剂对分离乳蛋白/瓜尔胶混合物粉末的物理、热和流变特性的影响
IF 5.3 2区 农林科学 Q1 ENGINEERING, CHEMICAL Pub Date : 2024-09-11 DOI: 10.1016/j.jfoodeng.2024.112317
Jun-Hwan Oh, Wonjae Lee, Juneha Bak, Byoungseung Yoo

This study examined the effect of fluidized-bed agglomeration with a carboxymethyl cellulose (CMC) binder on the physical, thermal, and rheological properties of agglomerated milk protein isolate (MPI)-guar gum (GG) mixtures (AMGs). The agglomeration process produced larger and more porous particles, improving solubility and powder flowability. An exothermic event followed by an endothermic event was observed in DSC thermograms. These thermal events tended to occur at a higher temperature with lower enthalpy values as the binder concentration increased. All samples exhibited shear-thinning behavior, with apparent viscosity at 100 s−1 values (0.27–0.29 Pa s) for AMGs being lower than for non-agglomerated MPI-GG mixture (NAMG; 0.34 Pa s). Viscoelastic moduli values showed similar trends. Additionally, compared to NAMG, larger and more guar gum lumps occurred in the AMGs. These findings suggest that the agglomeration process with CMC promoted depletion interactions between the protein and polysaccharide components in the mixture system.

本研究考察了使用羧甲基纤维素(CMC)粘合剂进行流化床团聚对团聚牛奶蛋白分离物(MPI)-瓜尔胶(GG)混合物(AMGs)的物理、热和流变特性的影响。团聚过程产生了更大更多孔的颗粒,提高了溶解性和粉末流动性。在 DSC 热图中观察到一个放热事件,随后是一个内热事件。随着粘合剂浓度的增加,这些热事件往往发生在温度较高且焓值较低的地方。所有样品都表现出剪切稀化行为,AMG 在 100 s-1 时的表观粘度值(0.27-0.29 Pa s)低于非胶结 MPI-GG 混合物(NAMG;0.34 Pa s)。粘弹性模量值也呈现出类似的趋势。此外,与 NAMG 相比,AMG 中的瓜尔胶块更大、更多。这些发现表明,使用 CMC 的聚结过程促进了混合物体系中蛋白质和多糖成分之间的耗竭相互作用。
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引用次数: 0
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Journal of Food Engineering
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