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Determining the Uncertainty of Frequency Measurements Referenced to GPS Disciplined Oscillators GPS规范振荡器频率测量不确定度的确定
Pub Date : 2013-07-15 DOI: 10.51843/wsproceedings.2013.34
M. Lombardi
GPS disciplined oscillators (GPSDOs) are commonly used as references for frequency calibrations. Over long intervals, a GPSDO is an inherently accurate source of frequency because it is continuously adjusted to agree with the Coordinated Universal Time (UTC) time scale maintained by the United States Naval Observatory (USNO). However, most frequency calibrations last for intervals of one day or less, and it can be difficult for metrologists to determine the uncertainty of a GPSDO during a short interval, and even more difficult to prove their uncertainty claims to skeptical laboratory assessors. This paper can serve as a guide to metrologists and laboratory assessors who work with GPSDOs as frequency standards. It describes the relationship between GPS time and Coordinated Universal Time (UTC) and explains why GPS time is traceable to the SI. It discusses how a GPSDO utilizes the GPS signals to control the frequency of its local oscillator. It explains how to estimate frequency stability, and how to apply estimates of frequency stability to determine the uncertainty of a GPSDO used as the reference for a frequency calibration.
GPS规范振荡器(gpsdo)通常用作频率校准的参考。在很长的时间间隔内,GPSDO是一个固有的精确频率源,因为它不断调整以符合美国海军天文台(USNO)维持的协调世界时(UTC)时间尺度。然而,大多数频率校准持续的间隔为一天或更短,计量学家很难在短间隔内确定GPSDO的不确定度,甚至更难以向持怀疑态度的实验室评估人员证明其不确定度声明。本文可以作为使用gpsdo作为频率标准的计量学家和实验室评估人员的指南。介绍了GPS时间与协调世界时(UTC)的关系,并解释了GPS时间可溯源到SI的原因。讨论了GPSDO如何利用GPS信号控制其本地振荡器的频率。它解释了如何估计频率稳定性,以及如何应用频率稳定性估计来确定用作频率校准参考的GPSDO的不确定度。
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引用次数: 0
The NIST Quality System for Measurement Services: A look at its Past Decade and a Gaze towards its Future NIST测量服务质量体系:回顾过去十年,展望未来
Pub Date : 2013-05-08 DOI: 10.51843/wsproceedings.2013.38
S. S. Bruce
A Look at its Past Decade and a Gaze towards its Future. As the National Metrology Institute (NMI) for the United States, the National Institute of Standards and Technology (NIST), formerly the National Bureau of Standards, has provided measurement services, both calibrations and reference materials, for more than 100 years. Through these services, our customers have benefitted from our measurement capabilities and expertise in many areas, including amount of substance; dimensional metrology; electricity and magnetism; ionizing radiation; mass and related quantities; photometry and radiometry; thermodynamics; and time and frequency. NIST’s customers have also had access to some of the lowest measurement uncertainties available and a dependable way to establish traceability to the International System of Units (SI) [http://www.nist.gov/pml/wmd/metric/si-units.cfm].In response to the signing of the International Committee for Weights and Measures (CIPM) Mutual Recognition Arrangement (MRA), NIST first established an institution-wide quality system for the measurement services 10 years ago [http://www.bipm.org/en/cipm-mra/objectives.html]. NIST’s Quality System for Measurement Services has advanced the quality of service and measurements we provide our customers by fostering an environment in which NIST management and staff work towards continual improvement in the development and delivery of NIST measurement services. This paper describes NIST’s Quality System for the Measurement Services and its relevance to international standards of quality, such as the International Organization for Standardization and the International Electrotechnical Commission (ISO/IEC) 17025 standard and ISO Guide 34 [http://www.nist.gov/nistqs/]. It also provides a history of this quality system and a glimpse of future goals for improving its implementation.
回顾过去十年,展望未来。作为美国的国家计量研究所(NMI),美国国家标准与技术研究所(NIST),前身是国家标准局,提供测量服务,包括校准和参考材料,已有100多年的历史。通过这些服务,我们的客户受益于我们在许多领域的测量能力和专业知识,包括物质量;空间计量;电、磁;电离辐射;质量及相关量;光度学和辐射学;热力学;时间和频率。NIST的客户也有机会获得一些最低的测量不确定度,并有一个可靠的方法来建立对国际单位制(SI)的可追溯性[http://www.nist.gov/pml/wmd/metric/si-units.cfm]。10年前,NIST首次为测量服务建立了一个机构范围的质量体系[http://www.bipm.org/en/cipm-mra/objectives.html]。NIST的测量服务质量体系提高了我们为客户提供的服务和测量的质量,营造了一个环境,在这个环境中,NIST的管理层和员工致力于持续改进NIST测量服务的开发和交付。本文描述了NIST的测量服务质量体系及其与国际质量标准的相关性,例如国际标准化组织和国际电工委员会(ISO/IEC) 17025标准和ISO指南34 [http://www.nist.gov/nistqs/]。它还提供了该质量体系的历史和对改进其实施的未来目标的一瞥。
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引用次数: 5
Introduction to Agile and Testing Best Practices for Distributed Software Teams with Hardware Dependencies 针对具有硬件依赖性的分布式软件团队的敏捷和测试最佳实践介绍
Pub Date : 1900-01-01 DOI: 10.51843/wsproceedings.2013.27
Logan Kunitz
There is no shortage of literature on how to use Agile and Scrum to speed up software development and deploy working code more frequently, however many of the concepts presented these days are geared toward pure software solutions, that are often web-based, where testing can be fully automated. This paper will address using Scrum and Agile software development practices in solutions that have hardware and/or regulatory dependencies, and a distributed development team. The hardware and regulatory dependencies, and distributed development team, can complicate the use of these development practices and limit the frequency of deploying working code due to the time consuming testing that is often involved • sometimes delaying a release for months. This is very different than with some pure software solutions, developed locally, that strive to be able to deploy working software “continuously” through the use of automated testing. This paper will attempt to reconcile the issues around using Agile and Scrum for developing HW and regulatory dependent software solutions that are not fully addressed in many agile / scrum literature and presentations. We’ll start by revisiting the core principles around agile / scrum development, and testing best practices. Then, we’ll look at examples from our own development processes at National Instruments, where we’ve adopted an agile process for the development of our software application that is used to automate the calibration of NI’s many hardware products, for both our internal service laboratory and 3rd party metrology laboratories. This application presents a number of challenges that should resonate for any software group that has a large number of hardware dependencies or regulatory requirements on their applications. For example, the broad portfolio of NI products and instrument standards that this application supports, makes regression testing for large changes an extremely time consuming task. Finally, we will address some of the challenges with using scrum with a global team, as we have developers split between Austin, TX and Hungary.
关于如何使用敏捷和Scrum来加速软件开发和更频繁地部署工作代码的文献并不缺乏,然而,最近提出的许多概念都是面向纯软件解决方案的,这些解决方案通常是基于web的,测试可以完全自动化。本文将讨论在具有硬件和/或法规依赖性的解决方案中使用Scrum和敏捷软件开发实践,以及分布式开发团队。硬件和法规依赖关系,以及分布式开发团队,可能会使这些开发实践的使用复杂化,并限制部署工作代码的频率,因为经常涉及耗时的测试,有时会将发布推迟数月。这与一些本地开发的纯软件解决方案非常不同,后者努力能够通过使用自动化测试“连续”地部署工作软件。本文将试图调和使用敏捷和Scrum来开发硬件和依赖法规的软件解决方案的问题,这些问题在许多敏捷/ Scrum文献和演讲中没有得到充分解决。我们将从重新审视敏捷/ scrum开发的核心原则开始,并测试最佳实践。然后,我们将看看我们自己在国家仪器公司的开发过程中的例子,在那里我们采用了一个敏捷的过程来开发我们的软件应用程序,用于自动校准NI的许多硬件产品,为我们的内部服务实验室和第三方计量实验室。这个应用程序提出了许多挑战,对于任何在其应用程序上有大量硬件依赖性或法规要求的软件组来说,这些挑战都应该引起共鸣。例如,该应用程序支持的NI产品和仪器标准的广泛组合,使得大变化的回归测试成为一项极其耗时的任务。最后,我们将解决在全球团队中使用scrum的一些挑战,因为我们的开发人员分散在德克萨斯州的奥斯汀和匈牙利。
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引用次数: 0
Low Frequency Accelerometer Calibration Chalenges and Improvements 低频加速度计校准的挑战和改进
Pub Date : 1900-01-01 DOI: 10.51843/wsproceedings.2013.51
M. Schiefer, Eric J. Seller, P. Timmons
Low Frequency accelerometer calibration is generally time consuming and requires special considerations and excitation techniques. A new class of reference standard and excitation shaker for use in low frequency accelerometer calibration is introduced. This exciter and reference standard addresses these low frequency challenges and reduces uncertainty to near 1% and throughput by a factor of 3. This paper also outlines challenges of low frequency calibration and details principal sources of error. New developments in low frequency accelerometer calibration excitation technology are introduced. Comparison to manufacturer’s primary calibration of an artifact as well as comparison to primary means is presented.
低频加速度计的校准通常是耗时的,需要特殊的考虑和激励技术。介绍了一种用于低频加速度计标定的新型参考标准和激振器。该激振器和参考标准解决了这些低频挑战,并将不确定性降低到接近1%,吞吐量降低了3倍。本文还概述了低频校准的挑战,并详细说明了主要的误差来源。介绍了低频加速度计标定激励技术的最新进展。给出了与制造商对工件的初次标定的比较以及与初次标定方法的比较。
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引用次数: 1
Digitally Gernerated AC Reference Source 数字生成的交流参考源
Pub Date : 1900-01-01 DOI: 10.51843/wsproceedings.2013.29
M. Bailey
The design of an AC voltage reference source using a digital to analogue converter controlled by microcontroller to produce a calculable RMS AC voltage reference with accuracy suitable for calibrating high performance Digital multimeters.
设计了一种交流电压基准源,采用单片机控制的数模转换器产生可计算的有效值交流电压基准源,其精度适用于校准高性能数字万用表。
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引用次数: 0
Best Practices for Pipette Calibration Uncertainty Budgets and CMC Determination 移液器校准不确定度预算和CMC测定的最佳实践
Pub Date : 1900-01-01 DOI: 10.51843/wsproceedings.2013.50
G. Rodrigues
With unit sales in excess of one million pieces per year, pipettes are ubiquitous devices and found in a wide variety of laboratories. Applications vary from non-quantitative uses (such as mixing or decanting) to highly quantitative uses such as dispensing of standards and preparation of accurate serial dilutions. Because pipettes are used extensively in critical laboratory tests such as quality control assay of injectable drugs and DNA analysis which results in conviction or exoneration, proper calibration of pipettes is important and the consequences of poor calibrations can be severe. There is a definite upward trend in the number of pipette calibration laboratories and service organizations which have obtained accreditation to ISO/IEC 17025:2005. Each of these laboratories will have performed an uncertainty analysis and calculated their calibration measurement capability (CMC).In this paper, the available scopes of accreditation from forty different pipette calibration laboratories are compiled, compared and contrasted. The various formats were translated into a common basis and then plotted to show how CMCs vary with pipette volume and vary between laboratories. One of the most notable differences is the significant variation in the CMCs among laboratories, which can vary by factors of 100 or more. There appears to be little correlation between a published pipette CMC and other laboratory variables such as experience in the discipline, equipment, reference standards, environmental controls, and capabilities in related disciplines such as mass or volumetrics. To understand the reasons behind these differences in CMC, pipette uncertainty budgets from some leading laboratories were compared. Based on this evaluation, the authors conclude that laboratory practices for establishing pipette calibration CMCs are not well standardized, and the largest source of variation seems to be practice in how the repeatability contribution from the pipette unit under test (UUT) is evaluated and considered. ILAC policy P-14 [1] defines CMC and establishes general policy regarding inclusion of repeatability and reproducibility of the “best existing device”. In practice, there is currently no consensus on which sources of variation in the pipette calibration process should be included in the CMC evaluation, nor is there agreement on how to apply the concept of a best existing pipette. This paper attempts to begin filling this gap by providing recommendations for a best practice in evaluating and communicating the uncertainty of a pipette calibration and for evaluating the CMC of a pipette calibration laboratory. The important questions of reporting measurement uncertainty and the impact it has on evaluating inter-laboratory comparisons and determining compliance with tolerances are also discussed.
随着单位销售量每年超过一百万件,移液器是无处不在的设备,并在各种各样的实验室中发现。应用范围从非定量用途(如混合或滗析)到高度定量用途,如标准品的分配和精确系列稀释的制备。由于移液器广泛用于关键的实验室测试,例如注射药物的质量控制分析和导致定罪或无罪的DNA分析,因此正确校准移液器很重要,校准不良的后果可能很严重。获得ISO/IEC 17025:2005认证的移液器校准实验室和服务机构的数量有明显的上升趋势。每个实验室都将进行不确定度分析并计算其校准测量能力(CMC)。本文对40个不同的移液器校准实验室现有的认可范围进行了汇编、比较和对比。各种格式被翻译成一个共同的基础,然后绘制以显示cmc如何随移液器体积和实验室之间的变化而变化。最显著的差异之一是实验室之间cmc的显著差异,其差异可达100倍或更多。已公布的移液器CMC与其他实验室变量(如学科经验、设备、参考标准、环境控制和相关学科的能力,如质量或体积)之间似乎没有什么相关性。为了了解CMC差异背后的原因,比较了一些领先实验室的移液器不确定度预算。基于这一评价,作者得出结论,建立移液器校准cmc的实验室实践没有很好地标准化,最大的差异来源似乎是如何评估和考虑被测移液器(UUT)的重复性贡献的实践。ILAC政策P-14[1]定义了CMC,并建立了关于“最佳现有设备”的可重复性和再现性的一般政策。在实践中,目前对于移液器校准过程中的哪些变异源应包括在CMC评估中没有达成共识,也没有就如何应用最佳现有移液器的概念达成一致。本文试图通过提供评估和沟通移液器校准不确定性的最佳实践以及评估移液器校准实验室CMC的建议,开始填补这一空白。报告测量不确定度的重要问题及其对评估实验室间比较和确定符合公差的影响也进行了讨论。
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引用次数: 0
Nonconformities Analysis According to ISO/IEC 17025 in Brazil 根据巴西ISO/IEC 17025进行不合格分析
Pub Date : 1900-01-01 DOI: 10.51843/wsproceedings.2013.36
Morgana Pizzolato, Filipe Medeiros Albano
This paper presents the analysis of nonconformities found in auditing of testing and calibration laboratories in accordance with ISO/IEC 17025. This International Standard specifies the general requirements for the competence to carry out tests and/or calibrations. It covers testing and calibration performed using standard methods, non-standard methods, and laboratory-developed methods. The auditing was conducted by auditors from Rede Metrológica RS (RMRS). The RMRS is a nonprofit association of technical and scientific nature that acts as an articulator in metrology and quality in Brazil. The main objective of this research was to identify the ISO/IEC 17025 requirements that have a higher number of non-conformities. We collected data on laboratory auditing performed in 2008, 2009, 2010, 2011 and 2012 years that represent about 500 laboratories audits. The data analyses were conducted clustering the laboratories by calibration and test area, by ISO/IEC 17025 requirements and by year. The areas of calibration laboratories were: acoustic; length, electricity, force, torque and hardness, mass, optical, pressure, flow and level, temperature and humidity, time and frequency, viscosity, volume. The areas of testing laboratories were: chemistry and physical chemistry, microbiological, biological and toxicological, mechanical and biochemistry. In the analysis were considered separately the percentages of non-conformities in technical and management requirements and also joint. Among the technical requirements with the highest number of non-conformities are Test and calibration methods and method validation (5.4) and Measurement traceability (5.6). Among the management requirements are Document control (4.3) and Control of records (4.13). Was also possible to identify which area of calibration or test showed a higher number of non-conformities. The calibration areas that had the highest number of non-conformities were pressure, flow and level, temperature and humidity and length. The testing areas that had the highest number of non-conformities were chemistry and physical chemistry and microbiological. Finally, one can see the trend of nonconformities in assessments of laboratories in accordance with the ISO/IEC 17025 requirements using the result of five years.
本文介绍了根据ISO/ iec17025审核检测和校准实验室时发现的不符合项的分析。本标准规定了进行测试和/或校准能力的一般要求。它涵盖了使用标准方法、非标准方法和实验室开发的方法进行的测试和校准。审核由Rede Metrológica RS (RMRS)的审核员进行。RMRS是一个非营利性的技术和科学性质的协会,在巴西的计量和质量方面发挥着明确的作用。本研究的主要目的是识别有较多不符合项的ISO/IEC 17025要求。我们收集了2008年、2009年、2010年、2011年和2012年进行的实验室审计的数据,这些数据代表了大约500个实验室的审计。数据分析按校准和测试区域、ISO/IEC 17025要求和年份对实验室进行聚类。校正实验室的范围包括:声学;长度、电、力、扭矩和硬度、质量、光学、压力、流量和液位、温度和湿度、时间和频率、粘度、体积。测试实验室的领域包括:化学和物理化学、微生物学、生物和毒理学、机械和生物化学。在分析中分别考虑了技术和管理要求中不符合项的百分比,也联合考虑了不符合项的百分比。在不符合项数量最多的技术要求中,测试和校准方法及方法验证(5.4)和测量可追溯性(5.6)。管理要求包括文件控制(4.3)和记录控制(4.13)。还可以确定哪个校准或测试区域显示了更多的不符合项。不符合项数量最多的校准区域是压力、流量和液位、温度和湿度以及长度。不符合项数量最多的测试领域是化学、物理化学和微生物学。最后,使用五年的结果,可以看到实验室按照ISO/IEC 17025要求进行评估的不合格趋势。
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引用次数: 0
Calibration of Coordinate Measuring Machines Meeting the Requirements of ISO 10360-2:2009 at the Standards and Calibration Laboratory 在标准及校正实验室校正符合ISO 10360-2:2009要求的三坐标测量机
Pub Date : 1900-01-01 DOI: 10.51843/wsproceedings.2013.24
Dennis W.K. Lee, Francis S.Y. Wong, C. K. Fung
A coordinate measuring machine (CMM) is a measuring system, with the means to move a probe system, to determine spatial coordinates on a work piece surface. It is a 3-dimensional measuring device for determining the physical geometrical characteristics of objects. To verify the performance of a CMM, it is essential to carry out acceptance tests and with subsequent periodic checks to it in accordance with ISO 10360-2, which is an international geometrical product specification standard for CMM testing. At Standards and Calibration Laboratory (SCL), a calibration method, meeting the requirements of the latest edition of ISO 10360-2, is developed using precision step gauges as the reference standards to calibrate CMMs with measurement results traceable to the unit of length (i.e. the metre). Method for estimation of measurement uncertainty is also developed in accordance with the JCGM 100:2008 (Guide to the Expression of Uncertainty in Measurement), ISO/TS 15530-1:2011 and ISO/TS 15530-3:2011 (Guidelines for the Evaluation of CMM Test Uncertainty).Learning Objectives: To develop methods for CMM calibration meeting ISO 10360-2:2009 and uncertainty evaluation in accordance with JCGM 100:2008.
三坐标测量机(CMM)是一种测量系统,通过移动测头系统来确定工件表面的空间坐标。它是一种用于确定物体物理几何特征的三维测量装置。为了验证三坐标测量机的性能,必须按照ISO 10360-2进行验收测试和随后的定期检查,这是三坐标测量机测试的国际几何产品规格标准。标准及校正实验所(下称“实验所”)以精密步进规为参考标准,发展一套符合最新版ISO 10360-2要求的校正方法,校正三坐标测量机,测量结果可追溯至长度单位(即米)。测量不确定度的估计方法也根据JCGM 100:2008(测量不确定度表达指南),ISO/TS 15530-1:2011和ISO/TS 15530-3:2011 (CMM测试不确定度评估指南)开发。学习目标:开发符合ISO 10360-2:2009的三坐标测量机校准方法,并根据JCGM 100:2008进行不确定度评估。
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引用次数: 0
Reevaluating the NIST Uncertainties for AC-DC Voltage Transfer Difference 重新评估交直流电压传递差的NIST不确定性
Pub Date : 1900-01-01 DOI: 10.51843/wsproceedings.2013.17
T. E. Lipe
Determination of ac-dc difference of thermal voltage converters has traditionally been done by range-to-range scaling techniques, beginning at the voltage level and optimal frequency of the primary standards, and continuing until the parameter space has been completed. Range-to-range scaling propagates uncertainties of the measurement process at each step, so that the uncertainties become larger at values away from the primary standards, with the magnitude determined largely from the number of scaling steps. At the National Institute of Standards and Technology (NIST), we have recently fabricated multi junction thermal converters with exceptional properties over a large range of voltages and frequencies. Coupled with the use of an ac voltage standard based on quantum effects, we have reevaluated the NIST uncertainty matrix for ac-dc voltage transfer difference, and have made significant reductions in the uncertainties at all voltage and frequency levels.
热电压变换器的交直流差的测定传统上是通过量程到量程缩放技术来完成的,从主要标准的电压水平和最佳频率开始,一直持续到参数空间完成。范围到范围的标度在每一步都传播测量过程的不确定性,因此,在远离主要标准的值处,不确定性变得更大,其大小主要由标度步骤的数量决定。在美国国家标准与技术研究院(NIST),我们最近制造了在大电压和频率范围内具有优异性能的多结热转换器。结合使用基于量子效应的交流电压标准,我们重新评估了NIST交直流电压转移差的不确定性矩阵,并在所有电压和频率水平上显著降低了不确定性。
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引用次数: 2
Calibration of Rogowski Coils at High Pulsed Currents 高脉冲电流下Rogowski线圈的校准
Pub Date : 1900-01-01 DOI: 10.51843/wsproceedings.2013.01
B. Djokic
Calibration of Rogowski Coils at High Pulsed Currents. The many applications of Rogowski coils include their use as current sensors in AC resistance welding. Weld quality depends on monitoring/controlling the welding currents. The accuracy of these current sensors matters, and so does the accuracy of their calibration. A high-accuracy system for calibrating Rogowski coils at continuous AC currents was previously developed at NRC. However, in AC resistance welding, high pulsed currents are used. A new calibration system was developed to calibrate current sensors and related equipment under high pulsed currents.
高脉冲电流下Rogowski线圈的校准。Rogowski线圈的许多应用包括它们在交流电阻焊接中用作电流传感器。焊接质量取决于对焊接电流的监控。这些电流传感器的精度很重要,它们的校准精度也很重要。NRC先前开发了一种高精度系统,用于在连续交流电流下校准Rogowski线圈。然而,在交流电阻焊接中,使用高脉冲电流。开发了一种新的校准系统,用于高脉冲电流下的电流传感器及相关设备的校准。
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引用次数: 0
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NCSL International Workshop & Symposium Conference Proceedings 2013
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