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OPTICAL TRAPPING OF A SINGLE CHLOROFORM MICRODROPLET IN WATER 水中单个三氯甲烷微滴的光学捕获
IF 0.7 Q3 ENGINEERING, MULTIDISCIPLINARY Pub Date : 2023-04-19 DOI: 10.11113/jurnalteknologi.v85.19303
Muhamad Safuan Mat Yeng, S. K. Ayop, K. Sasaki
The study aims to optically trap a single chloroform (CHCl3) microdroplet in water using optical tweezers. The study also investigates the effect of the preparation procedure by sonication on the chloroform microdroplet size and its stability in water. This microdroplet can potentially act as a carrier containing active molecules and for sensor applications in a fluid. The chloroform is sonicated in deionized water to produce a chloroform microdroplet solution. The size of the resultant microdroplets is observed under the optical microscope. The stability of the chloroform microdroplets in water was studied by monitoring the absorption spectra within a specified duration of time for 1 hour. A single chloroform microdroplet in the water is trapped using a 976 nm continuous laser beam with optical tweezers. The finding shows that the average size of the produced chloroform microdroplets does not vary significantly when the sonication time is less than 10 minutes. Furthermore, Chloroform microdroplets in water were stable within an hour of monitoring time. This study confirmed that a single chloroform microdroplet could be stably trapped using optical tweezers. It implies that the chloroform can form stable microdroplets in water and can be optically trapped under a focused laser.
该研究旨在使用光学镊子在水中光学捕获单个氯仿(CHCl3)微滴。研究了超声制备工艺对氯仿微滴粒径及其在水中稳定性的影响。这种微液滴可以潜在地作为含有活性分子的载体,并用于流体中的传感器应用。氯仿在去离子水中超声产生氯仿微滴溶液。在光学显微镜下观察所得微滴的大小。通过监测氯仿微滴在水中1小时内的吸收光谱,研究了其在水中的稳定性。使用带有光学镊子的976 nm连续激光束捕获水中的单个氯仿微滴。结果表明,当超声时间小于10分钟时,制备的氯仿微滴的平均大小变化不明显。此外,水中氯仿微滴在1小时的监测时间内是稳定的。本研究证实了利用光镊可以稳定地捕获单个氯仿微滴。这意味着氯仿可以在水中形成稳定的微滴,并且可以在聚焦激光下被光学捕获。
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引用次数: 0
SCREENING THE EFFECT OF THE EXPRESSION MEDIUM AND GROWTH CONDITIONS ON THE PERFORMANCE OF ENGINEERED XYLANASE PRODUCED BY IMMOBILIZED RECOMBINANT E. COLI 筛选表达培养基和生长条件对固定化重组大肠杆菌生产工程木聚糖酶性能的影响
IF 0.7 Q3 ENGINEERING, MULTIDISCIPLINARY Pub Date : 2023-04-19 DOI: 10.11113/jurnalteknologi.v85.18143
S. F. Z. Mohamad Fuzi, Nur Atiqah Lyana Nor Ashikin, Low Kheng Oon
Escherichia coli is the most prevalent host organism for the production of recombinant en-zymes. This was feasible due to the possibility of genetic modification and the availability of multiple E. coli strains as recombinant systems. The primary disadvantage of using E. coli as a host, however, is bacterial cell lysis due to tension build-up in the periplasmic space caused by the overexpression of the recombinant enzyme. Therefore, immobilization is preferable to cytoplasmic excretion for directing the expression of recombinant enzymes into the culture medium. This research investigated the effect of graphene oxide (GO) on the xylanase and β-galactosidase activity of immobilized recombinant E. coli. The effect of culture conditions (expression medium, IPTG, post induction temperature, post induction duration, agitation rate, and pH) on xylanase excretion and cell survival of an immobilized cell was studied using the one factor at a time (OFAT) method. After 24 hours of induction, using terrific broth (TB) as a medium increased xylanase excretion to 0.060 U/ml and resulted in decreased β-galactosidase activity (1.218 U/ml). Apart from that, a lower concentration of isopropyl -D-1-thiogalactopyranoside (IPTG) at 0.01 mM, a lower post-induction temperature (25°C), a 5-hour post-induction time, neutral pH, and 150 rpm significantly increased the xylanase excretion of immobilized cells with low β-galactosidase activity. This study established that immobilizing recombinant E. coli on GO may be advantageous for the excretion of recombinant proteins with a high cell viability.
大肠杆菌是生产重组酶最普遍的宿主生物。这是可行的,因为有可能进行基因修饰,并且可以使用多种大肠杆菌菌株作为重组系统。然而,使用大肠杆菌作为宿主的主要缺点是,由于重组酶的过表达导致周质空间中的张力积聚,细菌细胞裂解。因此,为了将重组酶的表达引导到培养基中,固定化比细胞质排泄更可取。研究了氧化石墨烯(GO)对固定化重组大肠杆菌木聚糖酶和β-半乳糖苷酶活性的影响。使用一次一因子(OFAT)法研究了培养条件(表达培养基、IPTG、诱导后温度、诱导后持续时间、搅拌速率和pH)对固定化细胞木聚糖酶排泄和细胞存活的影响。诱导24小时后,使用极好的肉汤(TB)作为培养基,木聚糖酶的排泄量增加到0.060U/ml,并导致β-半乳糖苷酶活性降低(1.218U/ml)。除此之外,在0.01mM、较低的诱导后温度(25°C)、5小时的诱导后时间、中性pH和150rpm下,较低浓度的异丙基-D-硫代吡喃半乳糖苷(IPTG)显著增加了具有低β-半乳糖苷酶活性的固定化细胞的木聚糖酶排泄。该研究证实,将重组大肠杆菌固定在GO上可能有利于具有高细胞活力的重组蛋白的排泄。
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引用次数: 0
ACTIVE EXTRAPOLATION OF DIMSIMS IN NORDSIECK REPRESENTATION nordsieck表示中调光量的主动外推
IF 0.7 Q3 ENGINEERING, MULTIDISCIPLINARY Pub Date : 2023-04-19 DOI: 10.11113/jurnalteknologi.v85.19511
Ali Jameel Kadhim, A. Gorgey, Noorhelyna Razali
Diagonally implicit multistage integration methods (DIMSIMs) are widely utilized in finding the solution to any problems in the subject of ordinary differential equations. These methods are selected from the general linear methods, which is considerable potential for efficient implementations. The extrapolation is derived from the stability of the explicit Runge-Kutta methods. In this paper, the combination of DIMSIMs with Richardson extrapolation of different orders shows that numerical solutions give higher accuracy when the extrapolation is applied with the base method.
对角隐式多级积分方法(DIMSIM)被广泛用于求解常微分方程中的任何问题。这些方法是从一般的线性方法中选择的,这在有效实现方面具有相当大的潜力。外推法是由显式龙格-库塔方法的稳定性导出的。在本文中,将DIMSIM与不同阶的Richardson外推相结合表明,当使用基本方法进行外推时,数值解具有更高的精度。
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引用次数: 0
ANALYSIS OF GRAVITY ON ALTITUDE CHANGES IN GRAVITY MICRO DATA USING POLYNOMIAL EQUATION APPROACH (CASE STUDIES OF MERAPI AND KELUD VOLCANOES) 用多项式方程方法分析重力微数据中重力对海拔变化的影响(以MERAPI火山和KELUD火山为例)
IF 0.7 Q3 ENGINEERING, MULTIDISCIPLINARY Pub Date : 2023-04-19 DOI: 10.11113/jurnalteknologi.v85.19488
A. Setiawan, Immanatul Huda, Richard Lewerissa
Analysis of gravity changes to altitude changes from gravity measurements at Merapi Volcano and Kelud Volcano was carried out to determine the characteristics of the two mountains based on the gravity method. Merapi Volcano and Kelud Volcano are two very active mountains in Indonesia and have different physiography, especially at the top of Kelud there is a crater filled with water. Repeated gravity surveys will be useful for studying deformation in volcanoes and providing information about changes in subsurface mass. The gravity data on Merapi Volcano is secondary data from BPPTKG (Research and Development Center for Geological Disaster Technology), and data on Kelud Volcano is obtained from the 2019 data collection survey. Volcanic monitoring using the gravity method is carried out by observing changes in gravity with changes in altitude  to study deformation in the volcano and providing information about changes in subsurface mass using a polynomial equation approach of  to  . The findings indicate that there was little variation in the gravity anomaly within Merapi Volcano between 2018 and 2019. The highest coefficient of determination, at 96%, was observed in the gravity anomaly data from inside the Kelud Volcano in 2019, after applying Bouguer corrections in the form of spherical effects. Additionally, the coefficients of the second and third order polynomials of the Merapi Volcano data had opposite signs to those of Kelud Volcano, suggesting that the internal source of the gravity anomaly within Merapi Volcano is distinct from that within Kelud Volcano.
通过对默拉皮火山和克鲁德火山的重力测量,分析了重力随海拔变化的变化,以基于重力方法确定这两座火山的特征。默拉皮火山和克鲁德火山是印度尼西亚两座非常活跃的山脉,具有不同的地貌,尤其是在克鲁德山顶有一个充满水的火山口。重复的重力调查将有助于研究火山变形,并提供有关地下质量变化的信息。默拉皮火山的重力数据是来自BPPTKG(地质灾害技术研究与发展中心)的二次数据,而克卢德火山的数据是从2019年的数据收集调查中获得的。使用重力法的火山监测是通过观察重力随海拔变化的变化来研究火山的变形,并使用到的多项式方程方法提供有关地下质量变化的信息来进行的。研究结果表明,2018年至2019年间,默拉皮火山的重力异常变化不大。在以球面效应的形式应用布格修正后,在2019年科卢德火山内部的重力异常数据中观察到了96%的最高决定系数。此外,默拉皮火山数据的二阶多项式和三阶多项式的系数与克卢德火山的系数具有相反的符号,这表明默拉皮熔岩内重力异常的内部来源与克卢德火山内重力异常不同。
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引用次数: 0
A REVIEW OF POOL BOILING HEAT TRANSFER PROPERTIES BY NANOFLUID 纳米流体池沸腾换热特性研究进展
IF 0.7 Q3 ENGINEERING, MULTIDISCIPLINARY Pub Date : 2023-04-19 DOI: 10.11113/jurnalteknologi.v85.18324
M. S. A., A. Hassan
Boiling heat transfer has maintained a high degree of interest due to the range of its applications in the energy sector. In recent years, much research has focused on improving the nucleate pool boiling by modifying the fluid properties. In this review article, the basic properties and characteristics of Al2O3 nanofluids and few other nanofluids are explored and discussed through past research findings. Next, previous studies that involved pool boiling heat transfer enhancement using Al2O3 nanofluid and its performance in terms of critical heat flux (CHF) and heat transfer coefficient (HTC) are further highlighted. These studies have employed methods that affected the performance of CHF and HTC such as electric field and surface modification. Maximum enhancement in CHF measured is approximately 200%. On the other hand, usage of prediction models to predict enhancements are also discussed thoroughly. Regardless of boiling performance enhancements with the deployment of nanofluids, several concerns must first be addressed before it is able to be deployed for practical use.
沸腾传热由于其在能源领域的广泛应用而一直备受关注。近年来,许多研究都集中在通过改变流体性质来改善核池沸腾。本文通过以往的研究成果,对Al2O3纳米流体和其他几种纳米流体的基本性质和特性进行了探讨和讨论。接下来,进一步强调了先前使用Al2O3纳米流体增强池沸腾传热的研究及其在临界热通量(CHF)和传热系数(HTC)方面的性能。这些研究采用了影响CHF和HTC性能的方法,如电场和表面改性。CHF的最大增强量约为200%。另一方面,还深入讨论了使用预测模型来预测增强。无论纳米流体的部署增强了沸腾性能,在能够部署用于实际使用之前,必须首先解决几个问题。
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引用次数: 0
STUDY OF THE DOSE CURVE TO DETERMINE THE DOSE RECEIVED BY A PATIENT ON THE DIAGNOSTIC RADIOLOGY 研究剂量曲线,以确定病人在诊断放射学上所接受的剂量
IF 0.7 Q3 ENGINEERING, MULTIDISCIPLINARY Pub Date : 2023-04-19 DOI: 10.11113/jurnalteknologi.v85.19017
M. Salam, Ayu Jati Puspitasari
A study of the dose curve to determine the dose received by a patient on the diagnostic radiology was carried out. One of the efforts to apply radiation dose optimization in diagnostic radiology is using the Diagnostic Reference Level (DRL), the dose value used as a reference for each radiological examination. The primary purpose of this study is to develop a method for determining the dose curve as a function of two variables: x-ray tube current and x-ray beam energy. Furthermore, the dose curve that has been developed can be used to estimate the value of the patient dose for each exposure factor arranged. In this study, the dose curve is determined using the polynomial model compiled using MATLAB software, and then validation is carried out using calibrated dosimeter. It shows that at a focus-to-detector distance (FDD) of 100 cm, the deviation factor is 4.89%. It meets the acceptance criteria determined, which is less than 5%. Furthermore, another validation result at FFD 50 cm shows that the average deviation value is 0.43%. In addition, the estimated dose still met the DRL criteria, where the estimated dose obtained for thorax AP and abdominal examinations are 0.26 mGy and 1.5 mGy, respectively. These values were still below the Indonesian Diagnostic Reference Level (IDRL) criteria determined by the Nuclear Energy Regulatory Agency of Indonesia (BAPETEN), which are 0.4 mGy and 10 mGy for thorax AP and abdominal, respectively.
对剂量曲线进行了研究,以确定患者在诊断放射学上接受的剂量。在诊断放射学中应用辐射剂量优化的努力之一是使用诊断参考水平(DRL),该剂量值用作每次放射学检查的参考。本研究的主要目的是开发一种确定剂量曲线的方法,该曲线是两个变量的函数:x射线管电流和x射线束能量。此外,已经开发的剂量曲线可以用于估计针对所安排的每个暴露因子的患者剂量值。在本研究中,使用MATLAB软件编制的多项式模型确定剂量曲线,然后使用校准的剂量计进行验证。结果表明,在焦点到探测器距离为100cm时,偏差因子为4.89%,符合确定的验收标准,小于5%。此外,FFD 50 cm处的另一个验证结果显示,平均偏差值为0.43%。此外,估计剂量仍然符合DRL标准,其中胸部AP和腹部检查获得的估计剂量分别为0.26 mGy和1.5 mGy。这些值仍低于印度尼西亚核能管理局(BAPETEN)确定的印度尼西亚诊断参考水平(IDRL)标准,胸部AP和腹部分别为0.4 mGy和10 mGy。
{"title":"STUDY OF THE DOSE CURVE TO DETERMINE THE DOSE RECEIVED BY A PATIENT ON THE DIAGNOSTIC RADIOLOGY","authors":"M. Salam, Ayu Jati Puspitasari","doi":"10.11113/jurnalteknologi.v85.19017","DOIUrl":"https://doi.org/10.11113/jurnalteknologi.v85.19017","url":null,"abstract":"A study of the dose curve to determine the dose received by a patient on the diagnostic radiology was carried out. One of the efforts to apply radiation dose optimization in diagnostic radiology is using the Diagnostic Reference Level (DRL), the dose value used as a reference for each radiological examination. The primary purpose of this study is to develop a method for determining the dose curve as a function of two variables: x-ray tube current and x-ray beam energy. Furthermore, the dose curve that has been developed can be used to estimate the value of the patient dose for each exposure factor arranged. In this study, the dose curve is determined using the polynomial model compiled using MATLAB software, and then validation is carried out using calibrated dosimeter. It shows that at a focus-to-detector distance (FDD) of 100 cm, the deviation factor is 4.89%. It meets the acceptance criteria determined, which is less than 5%. Furthermore, another validation result at FFD 50 cm shows that the average deviation value is 0.43%. In addition, the estimated dose still met the DRL criteria, where the estimated dose obtained for thorax AP and abdominal examinations are 0.26 mGy and 1.5 mGy, respectively. These values were still below the Indonesian Diagnostic Reference Level (IDRL) criteria determined by the Nuclear Energy Regulatory Agency of Indonesia (BAPETEN), which are 0.4 mGy and 10 mGy for thorax AP and abdominal, respectively.","PeriodicalId":47541,"journal":{"name":"Jurnal Teknologi-Sciences & Engineering","volume":" ","pages":""},"PeriodicalIF":0.7,"publicationDate":"2023-04-19","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"43224220","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
A STUDY ON THE INJECTION RATE CHARACTERISTICS OF THE SOLENOID COMMON-RAIL INJECTOR UNDER USING A HIGH-PRESSURE FUEL SYSTEM 高压燃油系统下电磁共轨喷油器喷射速率特性研究
IF 0.7 Q3 ENGINEERING, MULTIDISCIPLINARY Pub Date : 2023-04-19 DOI: 10.11113/jurnalteknologi.v85.19106
Vo Tan Chau, Tran Dang Long, Huynh Ba Vang, N. M. Hoang, N. Phuc, Nguyen Quoc Sy
The combustion of diesel engines is mainly controlled by fuel injection. Determining the fuel injection flow rate combined with the common-rail fuel injection system is a key solution to effectively improve engine performance and exhaust emissions. This work aims to investigate the influence of high injection pressures with a 6-holes-solenoid common rail injector on the injection rate characteristics in the range of 400 bar to 1600 bar, and a constant injector energizing time of 1.5 ms. The injection rate characteristics were carried out based on the pressure difference in the Zuech measuring chamber and synchronized data in real-time. The results showed that the increase of the mentioned injection pressures caused the decrease of hydraulic injection delay from 0.5 ms to 0.25 ms and expansion of the injector opening angle profile. In addition, the actual opening injection interval was prolonged as compared to the injector control signal. An increasing trend of fuel discharge coefficient was realized as higher injection pressure.
柴油机的燃烧主要由燃油喷射控制。确定燃油喷射流量与共轨燃油喷射系统相结合是有效改善发动机性能和废气排放的关键解决方案。本研究旨在研究6孔螺线管共轨喷油器在400 ~ 1600 bar范围内高喷射压力对喷油器喷射速率特性的影响,且喷油器通电时间为1.5 ms。根据Zuech测量室内的压差和实时同步数据进行注射速率特性分析。结果表明,上述喷射压力的增加使液压喷射延迟从0.5 ms减小到0.25 ms,喷油器开角轮廓增大;此外,与喷油器控制信号相比,实际开启喷射间隔延长。喷油压力越高,燃油流量系数越高。
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引用次数: 0
THE ROLE OF COMPACTION ON PYHSICOCHEMICAL PROPERTIES AND CARBON EMISSIONS OF TROPICAL PEAT SOILS: A REVIEW 压实作用对热带泥炭土理化性质及碳排放的影响
IF 0.7 Q3 ENGINEERING, MULTIDISCIPLINARY Pub Date : 2023-04-19 DOI: 10.11113/jurnalteknologi.v85.18340
M. K. Samuel, S. Evers
The peat compaction method is currently adopted by Malaysia oil palm companies to mitigate the uprising environmental issues. This method is claimed to be effective in minimising the risk of fire through enhancement of soil moisture due to capillary effect. In this review, the authors discussed on the peatland function in global perspective, the important of peat soil compaction, emergence of potential peat compaction in oil palm plantation establishment, peat compaction processes and the effects of compaction on physicochemical properties and carbon emission via peat surface and fire. Authors also found that compaction terminology on tropical peatland should be defined wisely, as it closely depends on the initial water table level and the peat quality. Thus, the retrieved information could serve as basic platform to further probe into the highlighted aspects and may as well function as a guide for management of these sensitive ecosystems, particularly in light of carbon loss mitigation.
泥炭压实法目前被马来西亚油棕公司采用,以缓解日益严重的环境问题。这种方法被认为是有效地减少火灾的风险,通过提高土壤湿度,由于毛细效应。本文综述了全球视角下泥炭地的功能、泥炭土壤压实的重要性、泥炭压实在油棕种植园建设中的潜在可能性、泥炭压实过程以及泥炭压实对泥炭表面和火的理化性质和碳排放的影响。作者还发现,热带泥炭地的压实术语应该明智地定义,因为它密切依赖于初始地下水位和泥炭质量。因此,检索到的信息可以作为进一步探讨突出方面的基本平台,也可以作为管理这些敏感生态系统的指南,特别是在减少碳损失方面。
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引用次数: 1
SPRING-BACK ANALYSIS OF THE VEE BENDING PROCESS FOR HIGH-STRENGTH STAINLESS STEEL 高强度不锈钢v形弯曲回弹分析
IF 0.7 Q3 ENGINEERING, MULTIDISCIPLINARY Pub Date : 2023-04-19 DOI: 10.11113/jurnalteknologi.v85.16614
Nana Rahdiana, Sukarman -, Khoirudin -, Amri Abdulah, A. D. Shieddieque
This study discussed the evaluation of bending process using high-strength SUS 304 (HS-SUS-304) material of high degree tolerances, and its application in a safe, strongbox, and strongroom protection system. This bending process is one of the several material-forming techniques widely used in the manufacturing industry. Moreover, incorrectly selected parameters such as the V-die punch radius, the angle of V-die bending, and the angle of machine parameters often leads to material failure and wrong final dimensions. The V-bending process was chosen for evaluation because it exhibits significant spring-back effect and has a wide range of industrial applications. The experimental method utilized HS-SUS 304 with a thickness of 3.0 mm that meets the ASTM A-240 requirement, and the input parameters used for V-die angle as well as tip punch radius were chosen in order to achieve the 90o ± 0.5o, and 50o ± 0.5o degrees of the workpieces. The V-die angle of 89o was selected with a tip punch radius of 1.0 mm and 1.2 mm. Furthermore, the spring-back effect was analyzed and evaluated to meet the standard angle requirement, and the results showed that the settings on the bending machine need to be adjusted to achieve angles within tolerances of degrees. It was observed that when the process bend angles on the machine was set at 93.75o and 52.83o with 1.0 mm V-dies tip punch radius, the spring-back factor results produce an average of 0.9609, 0.9618, and 0.9600. Meanwhile, this average increased to 0.9634, 0.9641, and 0.9655, by using 1.2 mm.
本研究探讨了高强度sus304 (HS-SUS-304)高度公差材料的弯曲工艺评价及其在安全、保险箱和保险室保护系统中的应用。这种弯曲工艺是广泛应用于制造业的几种材料成形技术之一。此外,v型模冲孔半径、v型模弯曲角度、机床参数角度等参数选择不当,往往会导致材料失效和最终尺寸错误。选择v型弯曲工艺进行评价是因为它具有显著的回弹效应,具有广泛的工业应用。实验方法采用符合ASTM a -240要求的厚度为3.0 mm的HS-SUS 304,选择v型模角度和尖端冲头半径的输入参数,以实现工件的90°±0.5°和50°±0.5°。v型模角选择为89o,尖端冲孔半径分别为1.0 mm和1.2 mm。对回弹效果进行了分析和评价,以满足标准角度要求,结果表明,需要调整弯曲机上的设置,以使角度在度的公差范围内。观察到,当机床上的工艺弯曲角度分别为93.75°和52.83°,v型模具尖端冲孔半径为1.0 mm时,回弹系数的平均值分别为0.9609、0.9618和0.9600。使用1.2 mm时,该平均值分别增加到0.9634、0.9641和0.9655。
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引用次数: 0
INFLUENCE OF DOUBLE CALCINATION-MILLING ROUTE ON THE STRUCTURAL AND MICROSTRUCTURAL PROPERTIES OF LEAD-FREE K0.5NA0.5NBO3 (KNN) CERAMICS 双烧磨工艺对无铅k0.5na0.5nbo3 (knn)陶瓷组织和显微组织性能的影响
IF 0.7 Q3 ENGINEERING, MULTIDISCIPLINARY Pub Date : 2023-04-19 DOI: 10.11113/jurnalteknologi.v85.19202
Norni Hidayawati Mat Daud, Dzetty Soraya Abdul Aziz, I. R. Ibrahim, Dayang Salyani Abang Mahmod, A. Khan, N. Ahmad, Nurul Mohd Fuad
Potassium sodium niobate (KNN) has always been one of the most potential candidates to replace lead-based piezoelectric ceramics due to its strong piezoelectric properties and environmentally friendly composition. A strong piezoelectric property is constantly influenced by the sample's densification as well as its microstructural characteristics. One of the current main issues with this KNN lead-free piezoelectric material is the difficulty in creating high-density samples by conventional preparation and sintering. Thus, KNN lead-free ceramics were synthesised using an improved solid-state method by introducing the double calcination-milling route to this process. The outcome demonstrates that, despite the presence of additional KNN secondary phases, the double calcination-milling approach contributed to the early creation of the KNN phase. When sintered pellets are subjected to a double calcination milling process, the XRD pattern revealed that the main peaks of the sample are indexed to orthorhombic K0.5Na0.5NbO3. The double calcination KNN pellet have a relative density of 90% densification which is slightly higher than that of single calcination KNN pellet which shows 88% densification.
铌酸钾钠(KNN)由于其强大的压电性能和环保的成分,一直是取代铅基压电陶瓷的最有潜力的候选者之一。试样的致密化及其微观结构特征不断影响着材料的强压电性能。目前这种KNN无铅压电材料的主要问题之一是难以通过常规制备和烧结产生高密度样品。因此,通过引入双煅烧-磨粉路线,采用改进的固态方法合成了KNN无铅陶瓷。结果表明,尽管存在额外的KNN次级相,但双重煅烧-磨粉方法有助于KNN相的早期形成。烧结球团经二次煅烧制粉后,XRD谱图显示样品的主峰为正交K0.5Na0.5NbO3。双烧KNN球团的相对密度为90%,略高于单烧KNN球团的88%。
{"title":"INFLUENCE OF DOUBLE CALCINATION-MILLING ROUTE ON THE STRUCTURAL AND MICROSTRUCTURAL PROPERTIES OF LEAD-FREE K0.5NA0.5NBO3 (KNN) CERAMICS","authors":"Norni Hidayawati Mat Daud, Dzetty Soraya Abdul Aziz, I. R. Ibrahim, Dayang Salyani Abang Mahmod, A. Khan, N. Ahmad, Nurul Mohd Fuad","doi":"10.11113/jurnalteknologi.v85.19202","DOIUrl":"https://doi.org/10.11113/jurnalteknologi.v85.19202","url":null,"abstract":"\u0000\u0000\u0000\u0000Potassium sodium niobate (KNN) has always been one of the most potential candidates to replace lead-based piezoelectric ceramics due to its strong piezoelectric properties and environmentally friendly composition. A strong piezoelectric property is constantly influenced by the sample's densification as well as its microstructural characteristics. One of the current main issues with this KNN lead-free piezoelectric material is the difficulty in creating high-density samples by conventional preparation and sintering. Thus, KNN lead-free ceramics were synthesised using an improved solid-state method by introducing the double calcination-milling route to this process. The outcome demonstrates that, despite the presence of additional KNN secondary phases, the double calcination-milling approach contributed to the early creation of the KNN phase. When sintered pellets are subjected to a double calcination milling process, the XRD pattern revealed that the main peaks of the sample are indexed to orthorhombic K0.5Na0.5NbO3. The double calcination KNN pellet have a relative density of 90% densification which is slightly higher than that of single calcination KNN pellet which shows 88% densification.\u0000\u0000\u0000\u0000","PeriodicalId":47541,"journal":{"name":"Jurnal Teknologi-Sciences & Engineering","volume":" ","pages":""},"PeriodicalIF":0.7,"publicationDate":"2023-04-19","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"48474894","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
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