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Journal of Applied Crystallography最新文献

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Compact sextupole permanent magnet lens: a practical approach to focusing pulsed neutrons 紧凑型六极永磁透镜:聚焦脉冲中子的实用方法
IF 2.8 3区 材料科学 Q2 CHEMISTRY, MULTIDISCIPLINARY Pub Date : 2025-09-18 DOI: 10.1107/S1600576725007496
Taisen Zuo, Zhangjiang Lu, Hong Zhu, Zehua Han, Changdong Deng, Yongcheng He, Long Tian, Tianhao Wang, Songwen Xiao, Zhengqiang He, Xiong Lin, Changli Ma, He Cheng

The focusing of pulsed neutrons can increase neutron current, reduce sample volume and enable access to smaller scattering angles. Consequently, it represents a critical challenge for next-generation spallation neutron sources. The primary difficulty stems from the inherent chromatic aberration of white neutrons. Here, a new compact nested rotating sextupole permanent magnet (Nest-Rotating-SPM) lens, with a total length of 200 mm, was developed and tested on the very small angle neutron scattering instrument at the China Spallation Neutron Source. Through synchronization of the outer sextupole lens rotation with the neutron pulse from the source, we achieved aberration-free focusing of neutrons with wavelengths between 11.0 and 15.5 Å for the first time. The implementation of water cooling and carbon fibre winding ensures both magnetic field stability and mechanical robustness of the inner sextupole. The compact design incorporating bridge sextupoles enables modular assembly of multiple lens units for focusing pulsed neutrons with wavelengths shorter than 10.0 Å, making it practically useful in a pulsed neutron instrument to enhance neutron current or access lower scattering vectors. Additional research is required to mitigate background noise.

脉冲中子的聚焦可以增加中子电流,减小样品体积,并使散射角更小。因此,它代表了下一代散裂中子源的一个关键挑战。主要的困难来自于白中子固有的色差。在中国散裂中子源的极小角中子散射仪上,研制了一种总长度为200mm的新型紧凑嵌套旋转六极永磁透镜(nest - rotation - spm)。通过外六极透镜旋转与源源中子脉冲同步,首次实现了波长在11.0 ~ 15.5 Å之间的中子的无像差聚焦。水冷却和碳纤维缠绕确保了内部六极的磁场稳定性和机械坚固性。紧凑的设计结合了桥式六极,使多个透镜单元的模块化组装能够聚焦波长小于10.0 Å的脉冲中子,使其在脉冲中子仪器中实际有用,以增强中子电流或访问低散射矢量。需要进一步的研究来减轻背景噪音。
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引用次数: 0
IF 2.8 3区 材料科学 Q2 CHEMISTRY, MULTIDISCIPLINARY Pub Date : 2025-09-18
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引用次数: 0
IF 2.8 3区 材料科学 Q2 CHEMISTRY, MULTIDISCIPLINARY Pub Date : 2025-09-18
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引用次数: 0
Insights on the textural and crystallographic properties of calcite obtained through MICP using advanced synchrotron diffraction imaging 利用先进的同步加速器衍射成像技术,通过MICP获得方解石的结构和晶体学特性
IF 2.8 3区 材料科学 Q2 CHEMISTRY, MULTIDISCIPLINARY Pub Date : 2025-09-12 DOI: 10.1107/S1600576725007010
Michela La Bella, Marilyn Sarkis, Christian Geindreau, Fabrice Emeriault, Haixing Fang, Jonathan P. Wright, Catherine Noiriel, Antoine Naillon

The microbially induced calcite precipitation (MICP) technique is used to turn sand into a cohesive medium by inducing the precipitation of calcite crystals in the pores. This work presents, for the first time, a comprehensive study of the morphological and crystallographic properties of bio-induced calcite using scanning 3D X-ray diffraction and phase contrast tomography, highlighting possible implications of the calcite precipitation process on the microstructure of biocemented sand. The combined approach of diffraction and imaging techniques with laboratory characterization tools revealed the link between morphology and crystallinity of bio-induced calcite crystals and the preferred orientation of crystals at the surface of sand grains. These results provide useful insights not only into the role of the crystallographic properties of calcite in determining the microstructure of biocemented sand but also on the influence of Sporosarcina Pasteurii on the precipitation process. The potential of scanning 3D X-ray diffraction in tackling challenges related to construction and geomaterials is demonstrated.

微生物诱导方解石沉淀(MICP)技术是通过诱导孔隙中方解石晶体的沉淀,将砂土转化为黏结介质。这项工作首次利用扫描3D x射线衍射和相衬断层扫描技术对生物诱导方解石的形态和晶体学特性进行了全面研究,强调了方解石沉淀过程对生物胶结砂微观结构的可能影响。结合衍射和成像技术以及实验室表征工具,揭示了生物诱导方解石晶体的形态和结晶度与沙粒表面晶体的首选取向之间的联系。这些结果不仅为方解石的晶体学性质在确定生物胶结砂微观结构中的作用提供了有用的见解,而且还为巴氏孢杆菌对沉淀过程的影响提供了有用的见解。扫描三维x射线衍射在解决与建筑和岩土材料相关的挑战方面的潜力被证明。
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引用次数: 0
IF 2.8 3区 材料科学 Q2 CHEMISTRY, MULTIDISCIPLINARY Pub Date : 2025-09-12
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引用次数: 0
IF 2.8 3区 材料科学 Q2 CHEMISTRY, MULTIDISCIPLINARY Pub Date : 2025-09-12
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引用次数: 0
IF 2.8 3区 材料科学 Q2 CHEMISTRY, MULTIDISCIPLINARY Pub Date : 2025-09-12
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引用次数: 0
IF 2.8 3区 材料科学 Q2 CHEMISTRY, MULTIDISCIPLINARY Pub Date : 2025-09-12
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引用次数: 0
IF 2.8 3区 材料科学 Q2 CHEMISTRY, MULTIDISCIPLINARY Pub Date : 2025-09-04
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引用次数: 0
IF 2.8 3区 材料科学 Q2 CHEMISTRY, MULTIDISCIPLINARY Pub Date : 2025-09-04
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引用次数: 0
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Journal of Applied Crystallography
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