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Effectiveness of different surface treatments on bond strength between 3D-printed teeth and denture base. 不同表面处理对 3D 打印牙齿和义齿基托之间粘接强度的影响。
IF 3.4 2区 医学 Q1 DENTISTRY, ORAL SURGERY & MEDICINE Pub Date : 2024-09-21 DOI: 10.1111/jopr.13941
Anne Karoline de Holanda Cavalcanti Pereira, Rayanna Thayse Florêncio Costa, Rafaella de Souza Leão, Bruno Gustavo da Silva Casado, Andre Ulisses Dantas Batista, Sandra Lúcia Dantas Moraes

Purpose: To investigate the effects of different surface treatments and thermal cycling on the shear bond strength between 3D-printed teeth and denture bases.

Material and methods: For the shear bond strength (SBS) test, the specimens were the maxillary central incisors (11 × 9 × 7 mm) bonded on a cylindrical base (20 × 25 mm). The control group was heat-cured polymethylmethacrylate (PMMA) (N = 20). The printed group was divided into five subgroups (N = 20): no treatment, sandblasting with aluminum oxide (Al2O3), methyl methacrylate monomer, acetone, and adhesive with urethane dimethacrylate. Half of the samples were subjected to 2000 thermal cycling cycles, and all samples were subjected to the SBS test. The failure mode was established as adhesive, cohesive, or mixed through stereomicroscopic analysis. The surface roughness test (Sa) was performed using optical profilometry, and the rectangular specimens (14 × 14 × 2.5 mm) were divided into four groups according to the surface treatments (N = 7 per group). Paired T and Wilcoxon tests were conducted to perform comparisons within the same group. The Kruskal-Wallis and Dwass-Steel-Critchlow-Fligner post-hoc tests were conducted to compare the groups.

Results: Al2O3 sandblasting in the 3D-printed groups achieved high SBS values comparable to those of the control group in the thermal cycled (p = 0.962) and non-thermal cycled samples (p = 0.319). It was the only treatment capable of modifying the surface of the 3D-printed resin, thereby increasing the roughness (p = 0.016).

Conclusions: Sandblasting is recommended to increase the bond strength between the tooth and denture bases.

目的:研究不同表面处理和热循环对三维打印牙齿与义齿基托之间剪切粘接强度的影响:在剪切粘接强度(SBS)测试中,试样为粘接在圆柱形基托(20 × 25 毫米)上的上颌中切牙(11 × 9 × 7 毫米)。对照组为热固化聚甲基丙烯酸甲酯(PMMA)(N = 20)。印刷组分为五个子组(N = 20):未处理组、氧化铝(Al2O3)喷砂组、甲基丙烯酸甲酯单体组、丙酮组和聚氨酯二甲基丙烯酸酯粘合剂组。半数样品进行了 2000 次热循环,所有样品都进行了 SBS 测试。通过立体显微镜分析确定失效模式为粘合、内聚或混合。使用光学轮廓仪进行表面粗糙度测试(Sa),并根据表面处理将矩形试样(14 × 14 × 2.5 毫米)分为四组(每组 7 个)。同组内的比较采用配对 T 检验和 Wilcoxon 检验。对各组进行 Kruskal-Wallis 和 Dwass-Steel-Critchlow-Fligner 事后检验:结果:在热循环(p = 0.962)和非热循环(p = 0.319)样品中,3D 打印组的 Al2O3 喷砂获得了与对照组相当的高 SBS 值。这是唯一一种能够改变 3D 打印树脂表面的处理方法,从而增加了粗糙度(p = 0.016):结论:建议采用喷砂处理来增加牙齿和义齿基托之间的粘接强度。
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引用次数: 0
Effect of finishing and polishing techniques on the fit accuracy and dimensions of conventional and CAD-CAM removable partial denture frameworks. 精加工和抛光技术对传统和 CAD-CAM 可摘局部义齿框架的配合精度和尺寸的影响。
IF 3.4 2区 医学 Q1 DENTISTRY, ORAL SURGERY & MEDICINE Pub Date : 2024-09-21 DOI: 10.1111/jopr.13950
Majed S Altoman, Pooya Soltanzadeh, Montry S Suprono, Thrya S Gadah, Mathew T Kattadiyil

Purpose: The purpose of this study was to compare the effects of finishing and polishing techniques on the fit accuracy, metal loss, and surface roughness of conventional versus CAD-CAM removable partial denture (RPD) frameworks.

Materials and methods: A 3D-printed maxillary Kennedy class III modification I model served as the master cast. Forty impressions (20 conventional and 20 digital) were divided into four groups: lost-wax technique (Group I: LWT), CAD-printed (Group II: CAD-RP), CAD-printed from a stone cast (Group III: CAD-RPS), and lost-wax technique from resin-printed models (Group IV: LWTR). Various finishing and polishing techniques were applied, followed by digital scanning for fit accuracy assessment using surface matching software. Metal thickness loss and surface roughness were evaluated pre- and post-finishing and polishing. The Kruskal-Wallis test followed by the Scheffe post-hoc test were conducted to evaluate the fit accuracy between groups (α = 0.05).

Results: Color mapping revealed significant differences (p < 0.001) between conventionally casted RPD frameworks and 3D-printed groups post-finishing and polishing. The most significant gap was observed with the guide plates from printed RPD frameworks. The D-Lyte technique resulted in less metal loss compared to the conventional finishing and polishing technique (p < 0.001).

Conclusion: Within the limitations of this study, conventionally processed RPD groups exhibited better overall fit accuracy post-finishing and polishing. Both conventional cast and 3D-printed RPD frameworks showed clinically acceptable fit accuracy. The D-Lyte technique presented less metal loss and smoother surfaces compared to other groups, suggesting it as a viable alternative.

目的:本研究的目的是比较精加工和抛光技术对传统与 CAD-CAM 可摘局部义齿(RPD)框架的配合精度、金属损失和表面粗糙度的影响:以 3D 打印的上颌肯尼迪 III 类改良 I 型作为母模。40 个印模(20 个传统印模和 20 个数字印模)被分为四组:失蜡技术组(第一组:LWT)、CAD 打印组(第二组:CAD-RP)、CAD 打印铸石组(第三组:CAD-RPS)和树脂打印模型失蜡技术组(第四组:LWTR)。在采用各种精加工和抛光技术后,使用表面匹配软件进行数字扫描,以评估配合精度。对抛光前后的金属厚度损失和表面粗糙度进行了评估。采用 Kruskal-Wallis 检验和 Scheffe 事后检验来评估组间的配合精度(α = 0.05):结果:色谱显示,传统铸造的 RPD 框架与三维打印组在抛光和打磨后存在明显差异(p < 0.001)。在打印 RPD 框架的导板上观察到的差距最大。与传统的精加工和抛光技术相比,D-Lyte 技术导致的金属损失更少(p < 0.001):在本研究的限制条件下,传统加工的 RPD 组在抛光和打磨后表现出更好的整体配合精度。传统铸造和三维打印的 RPD 框架都显示出临床上可接受的密合精度。与其他组别相比,D-Lyte 技术的金属损失更少,表面更光滑,是一种可行的替代方法。
{"title":"Effect of finishing and polishing techniques on the fit accuracy and dimensions of conventional and CAD-CAM removable partial denture frameworks.","authors":"Majed S Altoman, Pooya Soltanzadeh, Montry S Suprono, Thrya S Gadah, Mathew T Kattadiyil","doi":"10.1111/jopr.13950","DOIUrl":"https://doi.org/10.1111/jopr.13950","url":null,"abstract":"<p><strong>Purpose: </strong>The purpose of this study was to compare the effects of finishing and polishing techniques on the fit accuracy, metal loss, and surface roughness of conventional versus CAD-CAM removable partial denture (RPD) frameworks.</p><p><strong>Materials and methods: </strong>A 3D-printed maxillary Kennedy class III modification I model served as the master cast. Forty impressions (20 conventional and 20 digital) were divided into four groups: lost-wax technique (Group I: LWT), CAD-printed (Group II: CAD-RP), CAD-printed from a stone cast (Group III: CAD-RPS), and lost-wax technique from resin-printed models (Group IV: LWTR). Various finishing and polishing techniques were applied, followed by digital scanning for fit accuracy assessment using surface matching software. Metal thickness loss and surface roughness were evaluated pre- and post-finishing and polishing. The Kruskal-Wallis test followed by the Scheffe post-hoc test were conducted to evaluate the fit accuracy between groups (α = 0.05).</p><p><strong>Results: </strong>Color mapping revealed significant differences (p < 0.001) between conventionally casted RPD frameworks and 3D-printed groups post-finishing and polishing. The most significant gap was observed with the guide plates from printed RPD frameworks. The D-Lyte technique resulted in less metal loss compared to the conventional finishing and polishing technique (p < 0.001).</p><p><strong>Conclusion: </strong>Within the limitations of this study, conventionally processed RPD groups exhibited better overall fit accuracy post-finishing and polishing. Both conventional cast and 3D-printed RPD frameworks showed clinically acceptable fit accuracy. The D-Lyte technique presented less metal loss and smoother surfaces compared to other groups, suggesting it as a viable alternative.</p>","PeriodicalId":49152,"journal":{"name":"Journal of Prosthodontics-Implant Esthetic and Reconstructive Dentistry","volume":" ","pages":""},"PeriodicalIF":3.4,"publicationDate":"2024-09-21","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142299355","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"医学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Comparative evaluation of the effects of laser and chemical denture disinfectants on the surface characteristics of CAD-CAM and conventional denture resins: An in vitro experimental study. 激光和化学义齿消毒剂对 CAD-CAM 和传统义齿树脂表面特性影响的比较评估:体外实验研究。
IF 3.4 2区 医学 Q1 DENTISTRY, ORAL SURGERY & MEDICINE Pub Date : 2024-09-19 DOI: 10.1111/jopr.13952
Rania Moussa, Passent Ellakany, Shaimaa M Fouda, Mai Salah El-Din

Purpose: The purpose of this study was to assess the effect of Ga-Al-Ar diode, Nd:YAG lasers, and chemical disinfectants (NaOCl, vinegar, and Corega) on surface roughness (Ra) and hardness (VHN) of polymethylmethacrylate (PMMA), thermoplastic polyamide, milled and 3D-printed denture base resins.

Materials and methods: About 432 specimens of PMMA, thermoplastic polyamide, milled, and 3D-printed resins were divided into six subgroups (n = 18): distilled water (control:C), Ga-Al-Ar diode laser (L1), Nd:YAG laser (L2), 1% sodium hypochlorite (NaOCl), vinegar (AA), and Corega (CR). Each specimen's Ra and VHN were measured. Surface topography assessment was done using scanning electron microscopy (SEM). Analysis was done using ANOVA and post hoc Tukey's test (p = 0.05).

Results: A significant difference was noted in Ra and VHN as affected by denture base materials, surface disinfectants, and their interaction (p < 0.001). Results showed a significant increase in Ra of PMMA with NaOCL (p < 0.001), AA (p = 0.005), and CR (p = 0.009), thermoplastic polyamide with L1 (p = 0.012), L2 (p = 0.015), NaOCL AA, and CR (p < 0.001 each), milled resin with AA NaOCL, and CR (p < 0.001 each), and 3D-printed resin with L1, NaOCl, AA (p < 0.001 each), and CR (p = 0.008). The VHN increased in PMMA with NaOCL (p < 0.001), AA (p = 0.044), and CR (p < 0.001), thermoplastic polyamide with L1 (p = 0.037), milled resin with L1, L2, and CR (p < 0.001 each), and 3D-printed resin with L1, NaOCl (p < 0.001 each), and decreased with CR (p = 0.007).

Conclusion: The tested properties showed variations affected by denture base material and surface disinfectants. Laser treatments induced smoother surfaces than chemical disinfectants. Laser improved the surface hardness of CAD-CAM resins, while chemical immersion improved that of PMMA.

目的:本研究旨在评估Ga-Al-Ar二极管、Nd:YAG激光和化学消毒剂(NaOCl、醋和Corega)对聚甲基丙烯酸甲酯(PMMA)、热塑性聚酰胺、铣制和3D打印义齿基底树脂表面粗糙度(Ra)和硬度(VHN)的影响:将约 432 个 PMMA、热塑性聚酰胺、研磨和 3D 打印树脂试样分为六个子组(n = 18):蒸馏水(对照组:C)、Ga-Al-Ar 二极管激光器(L1)、Nd:YAG 激光器(L2)、1% 次氯酸钠(NaOCl)、醋(AA)和 Corega(CR)。对每个试样的 Ra 和 VHN 进行了测量。使用扫描电子显微镜(SEM)对表面形貌进行评估。分析采用方差分析和事后 Tukey 检验(p = 0.05):结果:Ra 和 VHN 受义齿基托材料、表面消毒剂及其相互作用的影响存在明显差异(p < 0.001)。结果显示,PMMA 与 NaOCL(p < 0.001)、AA(p = 0.005)和 CR(p = 0.009)、热塑性聚酰胺与 L1(p = 0.012)、L2(p = 0.015)、NaOCL AA 和 CR(各 p < 0.001),研磨树脂与 AA NaOCL 和 CR(各 p < 0.001),以及 3D 打印树脂与 L1、NaOCl、AA(各 p < 0.001)和 CR(p = 0.008)。使用 NaOCL 的 PMMA(p < 0.001)、AA(p = 0.044)和 CR(p < 0.001)、使用 L1 的热塑性聚酰胺(p = 0.037)、使用 L1、L2 和 CR 的研磨树脂(p < 0.001)以及使用 L1、NaOCl 的 3D 打印树脂(p < 0.001)的 VHN 增加,而使用 CR 的 VHN 减少(p = 0.007):测试结果表明,义齿基底材料和表面消毒剂会影响测试特性。与化学消毒剂相比,激光治疗能使表面更光滑。激光提高了 CAD-CAM 树脂的表面硬度,而化学浸泡提高了 PMMA 的表面硬度。
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引用次数: 0
Comparison of full-arch mandibular reconstruction with dental implants using completely splinted or segmentally splinted prostheses with two different occlusal schemes: A finite-element analysis. 使用两种不同咬合方案的完全夹板式或分段夹板式义齿进行下颌全拱重建的比较:有限元分析。
IF 3.4 2区 医学 Q1 DENTISTRY, ORAL SURGERY & MEDICINE Pub Date : 2024-09-19 DOI: 10.1111/jopr.13954
Sarah Abrishamkar, Amirhossein Fathi, Mahsa Ghorbani, Ramin Mosharraf

Purpose: This study aimed to comparatively analyze full-arch mandibular reconstruction using dental implants. It focused on two distinct prosthesis configurations: completely splinted and segmentally splinted. These configurations were evaluated under two different occlusal schemes-group function and canine guidance-utilizing finite element analysis (FEA).

Materials and methods: The methodology involved developing three-dimensional finite element models from computed tomography data acquired from an edentulous patient. Six dental implants were utilized to complete the mandibular reconstruction. Prosthetic reconstruction was conducted with completely and segmentally splinted prostheses, each employing group function and canine guidance occlusal schemes. Consequently, four distinct models were analyzed. Following meshing, a 200 N load was applied at a 30-degree angle. Subsequent evaluation encompassed stress, strain distribution, and the overall deformation of the implants, crowns, and underlying bone structure assessment.

Results: The group function occlusal scheme generally exhibited lower stress values than the canine guidance occlusal scheme, with three-piece prostheses demonstrating even lower stress levels than one-piece prostheses. Conversely, the canine guidance occlusal scheme exhibited higher stress values overall.

Conclusion: The findings of this study may assist clinicians in selecting the most effective occlusal scheme and prosthetic configuration for implant-supported mandibular restorations, potentially enhancing treatment outcomes and reducing the risk of mechanical complications. In summary, results indicated that group function loading, irrespective of prosthesis type, offers more uniform load distribution and lower stress values, making it a preferable choice over canine guidance. Within the group function occlusal scheme, three-piece prostheses demonstrated lower stress values than one-piece prostheses, but the clinical significance of this difference appears to be minimal.

目的:本研究旨在比较分析使用牙科种植体进行全拱下颌重建的情况。研究重点是两种不同的修复体配置:完全夹板式和分段夹板式。利用有限元分析(FEA),在两种不同的咬合方案下对这些配置进行了评估--组功能和犬齿引导:研究方法包括根据从无牙颌患者身上获取的计算机断层扫描数据建立三维有限元模型。利用六颗种植体完成下颌重建。修复重建采用完全和分段夹板修复体,每种修复体都采用组功能和犬引导咬合方案。因此,对四个不同的模型进行了分析。啮合后,以 30 度角施加 200 N 的负荷。随后的评估包括应力、应变分布以及种植体、牙冠和底层骨结构的整体变形评估:结果:组功能咬合方案的应力值普遍低于犬引导咬合方案,三件式修复体的应力水平甚至低于一件式修复体。相反,犬引导咬合方案的应力值总体较高:本研究的结果可以帮助临床医生为种植体支持的下颌修复体选择最有效的咬合方案和修复体配置,从而提高治疗效果并降低机械并发症的风险。总之,研究结果表明,无论修复体类型如何,群功能加载都能提供更均匀的负荷分布和更低的应力值,因此与犬齿引导相比,群功能加载是更可取的选择。在组功能咬合方案中,三件式修复体的应力值低于一件式修复体,但这种差异的临床意义似乎微乎其微。
{"title":"Comparison of full-arch mandibular reconstruction with dental implants using completely splinted or segmentally splinted prostheses with two different occlusal schemes: A finite-element analysis.","authors":"Sarah Abrishamkar, Amirhossein Fathi, Mahsa Ghorbani, Ramin Mosharraf","doi":"10.1111/jopr.13954","DOIUrl":"https://doi.org/10.1111/jopr.13954","url":null,"abstract":"<p><strong>Purpose: </strong>This study aimed to comparatively analyze full-arch mandibular reconstruction using dental implants. It focused on two distinct prosthesis configurations: completely splinted and segmentally splinted. These configurations were evaluated under two different occlusal schemes-group function and canine guidance-utilizing finite element analysis (FEA).</p><p><strong>Materials and methods: </strong>The methodology involved developing three-dimensional finite element models from computed tomography data acquired from an edentulous patient. Six dental implants were utilized to complete the mandibular reconstruction. Prosthetic reconstruction was conducted with completely and segmentally splinted prostheses, each employing group function and canine guidance occlusal schemes. Consequently, four distinct models were analyzed. Following meshing, a 200 N load was applied at a 30-degree angle. Subsequent evaluation encompassed stress, strain distribution, and the overall deformation of the implants, crowns, and underlying bone structure assessment.</p><p><strong>Results: </strong>The group function occlusal scheme generally exhibited lower stress values than the canine guidance occlusal scheme, with three-piece prostheses demonstrating even lower stress levels than one-piece prostheses. Conversely, the canine guidance occlusal scheme exhibited higher stress values overall.</p><p><strong>Conclusion: </strong>The findings of this study may assist clinicians in selecting the most effective occlusal scheme and prosthetic configuration for implant-supported mandibular restorations, potentially enhancing treatment outcomes and reducing the risk of mechanical complications. In summary, results indicated that group function loading, irrespective of prosthesis type, offers more uniform load distribution and lower stress values, making it a preferable choice over canine guidance. Within the group function occlusal scheme, three-piece prostheses demonstrated lower stress values than one-piece prostheses, but the clinical significance of this difference appears to be minimal.</p>","PeriodicalId":49152,"journal":{"name":"Journal of Prosthodontics-Implant Esthetic and Reconstructive Dentistry","volume":" ","pages":""},"PeriodicalIF":3.4,"publicationDate":"2024-09-19","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142299329","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"医学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Effects of post‐curing light intensity on the trueness, compressive strength, and resin polymerization characteristics of 3D‐printed 3‐unit fixed dental prostheses 后固化光强度对 3D 打印三单元固定义齿的真实性、抗压强度和树脂聚合特性的影响
IF 4 2区 医学 Q1 DENTISTRY, ORAL SURGERY & MEDICINE Pub Date : 2024-09-13 DOI: 10.1111/jopr.13951
Citra Dewi Sahrir, Wei‐Shao Lin, Chin‐Wei Wang, Wei‐Chun Lin
PurposeTo investigate the effect of different post‐curing light intensities on the trueness, compressive strength, and resin polymerization of 3D‐printed 3‐unit fixed dental prostheses (FPD).Materials and MethodsA total of 60 specimens were prepared to support a 3‐unit FDP with a deep chamfer marginal design, utilizing computer‐aided design and computer‐aided manufacturing (CAD‐CAM) technology. Light‐polymerizing FDP resin with varying light intensities (105, 210, 420, and 840 mW/cm2) was employed for 10 min. Subsequently, trueness assessment, fracture load testing, scanning electron microscopy (SEM) surface examination, and Fourier‐Transform Infrared (FTIR) analysis were conducted. A one‐way analysis of variance (ANOVA) was performed to ascertain the differences between the experimental groups (p < 0.05).ResultsThe group exposed to 210 mW/cm2 showed the highest trueness (57.6 ± 2.1 µm), while the 840 mW/cm2 group had the highest deviation (79.3 ± 2.7 µm) (p < 0.001). Significant differences in fracture resistance were found between groups (p < 0.001), with mean fracture strengths of 1149.77 ± 67.81 N, 1264.92 ± 39.06 N, 1331.34 ± 53.62 N, and 1439.93 ± 34.58 N for light intensities of 105, 210, 420, and 840 mW/cm2, respectively (p < 0.001). The resin polymerization analysis shows a peak intensity surge at 3579 cm−1 for O‐H and C‐H stretching vibrations, except in samples exposed to 105 mw/cm2 light, with the lowest peak at 2890 cm−1. The performance of resin polymerization is most significant under the condition of 840 mW/cm2.ConclusionThe light intensity of 210 mW/cm2 exhibited the highest trueness, while the 840 mW/cm2 group showed the highest deviation. However, the light intensity of 840 mW/cm2 demonstrated the highest compressive strength. Furthermore, polymerization occurred at all post‐treatment light intensities except 105 mW/cm2. These findings indicate that while low‐intensity usage offers greater trueness, high‐intensity usage provides better compressive strength and polymerization. Therefore, 210 mW/cm2 could be the recommended solution for post‐curing.
材料与方法利用计算机辅助设计和计算机辅助制造(CAD-CAM)技术,制备了 60 个试样,以支持具有深倒角边缘设计的 3 单元 FDP。使用不同光强度(105、210、420 和 840 mW/cm2)的光聚合 FDP 树脂 10 分钟。随后,进行了真实性评估、断裂负荷测试、扫描电子显微镜(SEM)表面检查和傅立叶变换红外(FTIR)分析。结果210 mW/cm2 组的真实度最高(57.6 ± 2.1 µm),而 840 mW/cm2 组的偏差最大(79.3 ± 2.7 µm)(p <0.001)。光照强度为 105、210、420 和 840 mW/cm2 组的平均断裂强度分别为 1149.77 ± 67.81 N、1264.92 ± 39.06 N、1331.34 ± 53.62 N 和 1439.93 ± 34.58 N(p <0.001)。树脂聚合分析表明,O-H 和 C-H 拉伸振动的峰值强度在 3579 cm-1 处激增,但暴露于 105 mw/cm2 光的样品除外,其最低峰值在 2890 cm-1 处。在 840 mW/cm2 的条件下,树脂聚合的性能最为显著。然而,光照强度为 840 mW/cm2 的抗压强度最高。此外,除 105 mW/cm2 外,所有后处理光强度下都出现了聚合现象。这些研究结果表明,虽然低强度使用能提供更高的真实度,但高强度使用能提供更好的抗压强度和聚合度。因此,210 mW/cm2 可以作为后固化的推荐方案。
{"title":"Effects of post‐curing light intensity on the trueness, compressive strength, and resin polymerization characteristics of 3D‐printed 3‐unit fixed dental prostheses","authors":"Citra Dewi Sahrir, Wei‐Shao Lin, Chin‐Wei Wang, Wei‐Chun Lin","doi":"10.1111/jopr.13951","DOIUrl":"https://doi.org/10.1111/jopr.13951","url":null,"abstract":"PurposeTo investigate the effect of different post‐curing light intensities on the trueness, compressive strength, and resin polymerization of 3D‐printed 3‐unit fixed dental prostheses (FPD).Materials and MethodsA total of 60 specimens were prepared to support a 3‐unit FDP with a deep chamfer marginal design, utilizing computer‐aided design and computer‐aided manufacturing (CAD‐CAM) technology. Light‐polymerizing FDP resin with varying light intensities (105, 210, 420, and 840 mW/cm<jats:sup>2</jats:sup>) was employed for 10 min. Subsequently, trueness assessment, fracture load testing, scanning electron microscopy (SEM) surface examination, and Fourier‐Transform Infrared (FTIR) analysis were conducted. A one‐way analysis of variance (ANOVA) was performed to ascertain the differences between the experimental groups (<jats:italic>p</jats:italic> &lt; 0.05).ResultsThe group exposed to 210 mW/cm<jats:sup>2</jats:sup> showed the highest trueness (57.6 ± 2.1 µm), while the 840 mW/cm<jats:sup>2</jats:sup> group had the highest deviation (79.3 ± 2.7 µm) (<jats:italic>p</jats:italic> &lt; 0.001). Significant differences in fracture resistance were found between groups (<jats:italic>p</jats:italic> &lt; 0.001), with mean fracture strengths of 1149.77 ± 67.81 N, 1264.92 ± 39.06 N, 1331.34 ± 53.62 N, and 1439.93 ± 34.58 N for light intensities of 105, 210, 420, and 840 mW/cm<jats:sup>2</jats:sup>, respectively (<jats:italic>p</jats:italic> &lt; 0.001). The resin polymerization analysis shows a peak intensity surge at 3579 cm<jats:sup>−1</jats:sup> for O‐H and C‐H stretching vibrations, except in samples exposed to 105 mw/cm<jats:sup>2</jats:sup> light, with the lowest peak at 2890 cm<jats:sup>−1</jats:sup>. The performance of resin polymerization is most significant under the condition of 840 mW/cm<jats:sup>2</jats:sup>.ConclusionThe light intensity of 210 mW/cm<jats:sup>2</jats:sup> exhibited the highest trueness, while the 840 mW/cm<jats:sup>2</jats:sup> group showed the highest deviation. However, the light intensity of 840 mW/cm<jats:sup>2</jats:sup> demonstrated the highest compressive strength. Furthermore, polymerization occurred at all post‐treatment light intensities except 105 mW/cm<jats:sup>2</jats:sup>. These findings indicate that while low‐intensity usage offers greater trueness, high‐intensity usage provides better compressive strength and polymerization. Therefore, 210 mW/cm<jats:sup>2</jats:sup> could be the recommended solution for post‐curing.","PeriodicalId":49152,"journal":{"name":"Journal of Prosthodontics-Implant Esthetic and Reconstructive Dentistry","volume":"65 1","pages":""},"PeriodicalIF":4.0,"publicationDate":"2024-09-13","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142248335","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"医学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Vertical marginal gap and internal fit of virgilite-based lithium disilicate glass ceramic veneers with different preparation designs. 采用不同制备设计的病毒基二硅酸锂玻璃陶瓷贴面的垂直边缘间隙和内部密合度。
IF 3.4 2区 医学 Q1 DENTISTRY, ORAL SURGERY & MEDICINE Pub Date : 2024-09-09 DOI: 10.1111/jopr.13937
Amr Rizk, Ahmed Abdou, Amira Mohammad Samy, Nouran Mahmoud, Sarah Omar

Purpose: To evaluate and compare internal fit and marginal adaptation of conventional lithium disilicate (LDS) glass ceramics and LDS containing virgilite computer-aided design and manufacturing (CAD-CAM) blocks before and after aging.

Materials and methods: Seventy-two epoxy replicated dies from two prepared maxillary right central incisors acrylic typodont were divided into two groups of different preparation designs (n = 36): Group I, incisal butt-joint, and Group P, incisal overlap. Each group was further subdivided into two equal groups according to ceramic material (n = 18): Group E, IPS e.max CAD, and Group T, Tessera advanced lithium disilicate (ALD) CAD-CAM blocks. The replica technique was used to assess the internal fit using a stereomicroscope at 45× magnification. Laminate veneers were cemented to their corresponding epoxy dies, then the vertical marginal gap was evaluated before and after thermal cycling. Repeated measures analysis of variance (ANOVA) were used for marginal fit data and 2-way ANOVA for internal fit measurements (α = 0.05).

Results: For internal fit, there were no significant differences between tested groups. For vertical marginal gap results, two-way ANOVA showed that only aging had a significant effect on the vertical marginal gap (p < 0.001), while different CAD-CAM materials and preparation designs did not affect the vertical marginal gap.

Conclusions: The vertical marginal gap and internal fits of IPS e.max CAD and CEREC Tessera CAD for both preparation designs were comparable. Aging significantly affected the vertical marginal gap of the laminate veneers of both materials and both preparation designs; however, all were within clinically acceptable ranges before and after aging.

目的:评估和比较传统二硅酸锂(LDS)玻璃陶瓷和含有virgilite的二硅酸锂计算机辅助设计和制造(CAD-CAM)区块在老化前后的内部密合性和边缘适应性:从两颗制备好的上颌右中切牙丙烯酸类型牙中取出 72 个环氧树脂复制模,将其分为两组,每组有不同的制备设计(n = 36):I 组为切缘对接,P 组为切缘重叠。根据陶瓷材料的不同,每组又分为两个相同的小组(n = 18):E 组为 IPS e.max CAD,T 组为 Tessera 高级二硅酸锂 (ALD) CAD-CAM 块。使用 45 倍放大率的体视显微镜,采用复制技术评估内部密合度。将层压板贴面粘结到相应的环氧树脂模具上,然后评估热循环前后的垂直边缘间隙。边缘贴合数据采用重复测量方差分析(ANOVA),内部贴合测量采用双向方差分析(α = 0.05):结果:在内部贴合度方面,测试组之间没有明显差异。对于垂直边缘间隙结果,双向方差分析显示,只有年龄对垂直边缘间隙有显著影响(p 结论):IPS e.max CAD 和 CEREC Tessera CAD 两种预备设计的垂直边缘间隙和内部密合度相当。老化对两种材料和两种预备设计的层压贴面的垂直边缘间隙都有明显的影响;但是,老化前后的垂直边缘间隙都在临床可接受的范围内。
{"title":"Vertical marginal gap and internal fit of virgilite-based lithium disilicate glass ceramic veneers with different preparation designs.","authors":"Amr Rizk, Ahmed Abdou, Amira Mohammad Samy, Nouran Mahmoud, Sarah Omar","doi":"10.1111/jopr.13937","DOIUrl":"https://doi.org/10.1111/jopr.13937","url":null,"abstract":"<p><strong>Purpose: </strong>To evaluate and compare internal fit and marginal adaptation of conventional lithium disilicate (LDS) glass ceramics and LDS containing virgilite computer-aided design and manufacturing (CAD-CAM) blocks before and after aging.</p><p><strong>Materials and methods: </strong>Seventy-two epoxy replicated dies from two prepared maxillary right central incisors acrylic typodont were divided into two groups of different preparation designs (n = 36): Group I, incisal butt-joint, and Group P, incisal overlap. Each group was further subdivided into two equal groups according to ceramic material (n = 18): Group E, IPS e.max CAD, and Group T, Tessera advanced lithium disilicate (ALD) CAD-CAM blocks. The replica technique was used to assess the internal fit using a stereomicroscope at 45× magnification. Laminate veneers were cemented to their corresponding epoxy dies, then the vertical marginal gap was evaluated before and after thermal cycling. Repeated measures analysis of variance (ANOVA) were used for marginal fit data and 2-way ANOVA for internal fit measurements (α = 0.05).</p><p><strong>Results: </strong>For internal fit, there were no significant differences between tested groups. For vertical marginal gap results, two-way ANOVA showed that only aging had a significant effect on the vertical marginal gap (p < 0.001), while different CAD-CAM materials and preparation designs did not affect the vertical marginal gap.</p><p><strong>Conclusions: </strong>The vertical marginal gap and internal fits of IPS e.max CAD and CEREC Tessera CAD for both preparation designs were comparable. Aging significantly affected the vertical marginal gap of the laminate veneers of both materials and both preparation designs; however, all were within clinically acceptable ranges before and after aging.</p>","PeriodicalId":49152,"journal":{"name":"Journal of Prosthodontics-Implant Esthetic and Reconstructive Dentistry","volume":" ","pages":""},"PeriodicalIF":3.4,"publicationDate":"2024-09-09","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142156454","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"医学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Effect of cleaning solution on surface properties of 3D-printed denture materials. 清洁液对 3D 打印义齿材料表面特性的影响。
IF 3.4 2区 医学 Q1 DENTISTRY, ORAL SURGERY & MEDICINE Pub Date : 2024-09-04 DOI: 10.1111/jopr.13936
Marina Rodrigues Santi, Nadima Khodor, Michael Sekula, David Donatelli, Grace Mendonça De Souza

Purpose: To evaluate the effect of cleaning solutions on surface properties of 3D-printed resins.

Materials and methods: Seven different resin materials for denture base and teeth were used in the form of 280 half-disks. Samples were randomly assigned to two cleaning groups (FD, FreshDent; PO, Polydent), with daily 2- or 3-min immersion followed by water storage, repeated for 30 days. Samples were then cleaned in an ultrasonic bath with water and analyzed for surface roughness (Keyence, VHX-7000N) and hardness (Shimadzu, HMV-2 series). The pH of cleaning solutions was analyzed over 5-min and the surface morphology of specimens was analyzed via scanning electron microscopy (SEM). Statistical analysis used two-way ANOVA (α = 0.05).

Results: Surface roughness of base materials was significantly affected (p < 0.001), whereas roughness of teeth materials was not. As for hardness, there was a significant interaction between materials and cleaning solution for both, base (p < 0.001) and teeth (p < 0.001). For teeth materials, PO significantly increased Denture's (Dentca) hardness and decreased that of Rodin's (Pac Dent), while PO significantly increased Rodin's Base (Pac Dent) hardness. The hardness of Flexcera Ultra (Envision Tec), Glidewell (Glidewell), Lucitone (Dentsply Sirona), and NextDent (NextDent) teeth and base materials were not affected by the cleaning solution. Overall, the pH of FD averaged 7.3 and PO averaged 6.6. All the SEM images indicated surface irregularities after immersion in either FD or PO.

Conclusions: One-month of storage and cyclic cleaning of 3D- printed resins did not affect surface roughness but had a significant impact on hardness. The cleaning solutions' effect was not homogeneous among materials.

目的:评估清洁溶液对 3D 打印树脂表面特性的影响:七种不同的义齿基托和牙齿树脂材料被制成 280 个半圆盘。样品被随机分配到两个清洁组(FD,FreshDent;PO,Polydent),每天浸泡 2 或 3 分钟,然后储水,重复 30 天。然后在超声波槽中用水清洗样品,并分析表面粗糙度(Keyence,VHX-7000N)和硬度(Shimadzu,HMV-2 系列)。在 5 分钟内分析了清洁溶液的 pH 值,并通过扫描电子显微镜(SEM)分析了试样的表面形态。统计分析采用双因素方差分析(α = 0.05):结果:基底材料的表面粗糙度受到显著影响(p < 0.001),而牙齿材料的粗糙度则不受影响。至于硬度,基底(p < 0.001)和牙齿(p < 0.001)的材料与清洁液之间存在明显的交互作用。就牙齿材料而言,PO 能明显提高 Denture(Dentca)的硬度,降低 Rodin(Pac Dent)的硬度,而 PO 能明显提高 Rodin Base(Pac Dent)的硬度。Flexcera Ultra (Envision Tec)、Glidewell (Glidewell)、Lucitone (Dentsply Sirona) 和 NextDent (NextDent) 牙齿和基底材料的硬度不受清洁溶液的影响。总体而言,FD 的 pH 值平均为 7.3,PO 的 pH 值平均为 6.6。所有的 SEM 图像都显示,在 FD 或 PO 溶液中浸泡后,表面会出现不规则现象:结论:3D 打印树脂存放一个月和循环清洗不会影响表面粗糙度,但对硬度有显著影响。清洁溶液对不同材料的影响不尽相同。
{"title":"Effect of cleaning solution on surface properties of 3D-printed denture materials.","authors":"Marina Rodrigues Santi, Nadima Khodor, Michael Sekula, David Donatelli, Grace Mendonça De Souza","doi":"10.1111/jopr.13936","DOIUrl":"https://doi.org/10.1111/jopr.13936","url":null,"abstract":"<p><strong>Purpose: </strong>To evaluate the effect of cleaning solutions on surface properties of 3D-printed resins.</p><p><strong>Materials and methods: </strong>Seven different resin materials for denture base and teeth were used in the form of 280 half-disks. Samples were randomly assigned to two cleaning groups (FD, FreshDent; PO, Polydent), with daily 2- or 3-min immersion followed by water storage, repeated for 30 days. Samples were then cleaned in an ultrasonic bath with water and analyzed for surface roughness (Keyence, VHX-7000N) and hardness (Shimadzu, HMV-2 series). The pH of cleaning solutions was analyzed over 5-min and the surface morphology of specimens was analyzed via scanning electron microscopy (SEM). Statistical analysis used two-way ANOVA (α = 0.05).</p><p><strong>Results: </strong>Surface roughness of base materials was significantly affected (p < 0.001), whereas roughness of teeth materials was not. As for hardness, there was a significant interaction between materials and cleaning solution for both, base (p < 0.001) and teeth (p < 0.001). For teeth materials, PO significantly increased Denture's (Dentca) hardness and decreased that of Rodin's (Pac Dent), while PO significantly increased Rodin's Base (Pac Dent) hardness. The hardness of Flexcera Ultra (Envision Tec), Glidewell (Glidewell), Lucitone (Dentsply Sirona), and NextDent (NextDent) teeth and base materials were not affected by the cleaning solution. Overall, the pH of FD averaged 7.3 and PO averaged 6.6. All the SEM images indicated surface irregularities after immersion in either FD or PO.</p><p><strong>Conclusions: </strong>One-month of storage and cyclic cleaning of 3D- printed resins did not affect surface roughness but had a significant impact on hardness. The cleaning solutions' effect was not homogeneous among materials.</p>","PeriodicalId":49152,"journal":{"name":"Journal of Prosthodontics-Implant Esthetic and Reconstructive Dentistry","volume":" ","pages":""},"PeriodicalIF":3.4,"publicationDate":"2024-09-04","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142134204","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"医学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Influence of CAD-CAM manufacturing methods on the accuracy and mechanical properties of implant-supported prostheses: A systematic review. CAD-CAM 制造方法对种植体支撑修复体的精度和机械性能的影响:系统综述。
IF 3.4 2区 医学 Q1 DENTISTRY, ORAL SURGERY & MEDICINE Pub Date : 2024-09-04 DOI: 10.1111/jopr.13933
Passent Ellakany, Marwa Madi, Amira H Elwan, Turki Alshehri, Hussain Aljubran, Nourhan M Aly

Purpose: This systematic review aimed to provide comprehensive insights on the accuracy, fit, and mechanical characteristics of implant-supported computer-aided design and computer-aided manufacturing (CAD-CAM) prostheses, with a focus on milled and 3D-printed approaches.

Methods: The research question focused on implant-supported dental prostheses, comparing different manufacturing techniques (conventional, milled, and 3D-printed) to determine the different factors affecting the mechanical properties and fit of the CAD-CAM implant-supported prosthesis. The eligibility criteria encompassed studies involving implant-supported restorations, clear reporting of manufacturing techniques, and English-language publications from the last decade. The search was conducted across three main databases, MEDLINE, Scopus, and Web of Science in September 2023. Publication details, study characteristics, and methodological details of each included study were described.

Results: Of the initial 1964 articles, 581 met the inclusion criteria, and 104 studies were included in the final qualitative analysis. The majority of studies were conducted in the United States, Turkey, and Brazil. Fourteen studies evaluated accuracy parameters, while four studies focused on mechanical characteristics. The studies revealed variability in mechanical properties and marginal and internal fit, with fabrication methods impacting the structural integrity and stress distribution of the prostheses.

Conclusions: The findings suggest that digital manufacturing workflows, both milling and 3D printing, yield acceptable properties for implant-supported restorations with minimal variations in fit and accuracy. Notably, 3D printing and hybrid techniques demonstrate advantages in specific aspects like marginal fit and stress distribution. However, the milled prosthesis provided superior results in flexural strength and fracture resistance compared to conventional methods. Further research is needed to confirm these findings in clinical settings.

目的:本系统综述旨在提供有关种植体支持计算机辅助设计和计算机辅助制造(CAD-CAM)修复体的准确性、密合性和机械特性的全面见解,重点关注铣制和三维打印方法:研究问题聚焦于种植体支持的牙科修复体,比较不同的制造技术(传统、铣削和三维打印),以确定影响计算机辅助设计和计算机辅助制造(CAD-CAM)种植体支持修复体的机械性能和密合性的不同因素。资格标准包括涉及种植体支持修复体的研究、对制造技术的明确报告以及过去十年间的英文出版物。检索于 2023 年 9 月在 MEDLINE、Scopus 和 Web of Science 三个主要数据库中进行。对每项纳入研究的出版细节、研究特点和方法细节进行了描述:在最初的 1964 篇文章中,有 581 篇符合纳入标准,104 项研究被纳入最终的定性分析。大部分研究在美国、土耳其和巴西进行。14 项研究评估了精度参数,4 项研究侧重于机械特性。这些研究揭示了机械性能、边缘和内部配合的差异性,而制造方法会影响假体的结构完整性和应力分布:结论:研究结果表明,数字化制造工作流程(包括铣削和三维打印)可为种植体支持修复体提供可接受的特性,并且在密合性和准确性方面的变化极小。值得注意的是,三维打印和混合技术在边缘密合度和应力分布等特定方面具有优势。不过,与传统方法相比,铣制修复体在抗弯强度和抗折性方面更胜一筹。要在临床环境中证实这些发现,还需要进一步的研究。
{"title":"Influence of CAD-CAM manufacturing methods on the accuracy and mechanical properties of implant-supported prostheses: A systematic review.","authors":"Passent Ellakany, Marwa Madi, Amira H Elwan, Turki Alshehri, Hussain Aljubran, Nourhan M Aly","doi":"10.1111/jopr.13933","DOIUrl":"https://doi.org/10.1111/jopr.13933","url":null,"abstract":"<p><strong>Purpose: </strong>This systematic review aimed to provide comprehensive insights on the accuracy, fit, and mechanical characteristics of implant-supported computer-aided design and computer-aided manufacturing (CAD-CAM) prostheses, with a focus on milled and 3D-printed approaches.</p><p><strong>Methods: </strong>The research question focused on implant-supported dental prostheses, comparing different manufacturing techniques (conventional, milled, and 3D-printed) to determine the different factors affecting the mechanical properties and fit of the CAD-CAM implant-supported prosthesis. The eligibility criteria encompassed studies involving implant-supported restorations, clear reporting of manufacturing techniques, and English-language publications from the last decade. The search was conducted across three main databases, MEDLINE, Scopus, and Web of Science in September 2023. Publication details, study characteristics, and methodological details of each included study were described.</p><p><strong>Results: </strong>Of the initial 1964 articles, 581 met the inclusion criteria, and 104 studies were included in the final qualitative analysis. The majority of studies were conducted in the United States, Turkey, and Brazil. Fourteen studies evaluated accuracy parameters, while four studies focused on mechanical characteristics. The studies revealed variability in mechanical properties and marginal and internal fit, with fabrication methods impacting the structural integrity and stress distribution of the prostheses.</p><p><strong>Conclusions: </strong>The findings suggest that digital manufacturing workflows, both milling and 3D printing, yield acceptable properties for implant-supported restorations with minimal variations in fit and accuracy. Notably, 3D printing and hybrid techniques demonstrate advantages in specific aspects like marginal fit and stress distribution. However, the milled prosthesis provided superior results in flexural strength and fracture resistance compared to conventional methods. Further research is needed to confirm these findings in clinical settings.</p>","PeriodicalId":49152,"journal":{"name":"Journal of Prosthodontics-Implant Esthetic and Reconstructive Dentistry","volume":" ","pages":""},"PeriodicalIF":3.4,"publicationDate":"2024-09-04","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142134205","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"医学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Microstructural and flexural strength of various CAD-CAM lithium disilicate ceramics. 各种 CAD-CAM 二硅酸锂陶瓷的微结构和抗弯强度。
IF 3.4 2区 医学 Q1 DENTISTRY, ORAL SURGERY & MEDICINE Pub Date : 2024-09-04 DOI: 10.1111/jopr.13938
Joissi Ferrari Zaniboni, Amanda Soares Silva, Aryvelto Miranda Silva, João Felipe Besegato, Oscar Fernando Muñoz-Chávez, Edson Alves de Campos

Purpose: To analyze the microstructural and mechanical properties of various commercial trademarks of lithium disilicate ceramics for CAD-CAM systems.

Materials and methods: Specimens of different lithium disilicate ceramics were obtained and randomized into 5 groups (n = 14): EM: e.max CAD; RT: Rosetta SM; EV: Evolith; PM: Smile-Lithium CAD; and, HS: HaHaSmile. The microstructural analysis was performed by X-ray diffraction (XRD) and scanning electron microscopy (SEM); for flexural strength, the three-point bending flexure test was used. XRD and SEM data were qualitatively evaluated. Data from flexural strength were assessed with one-way ANOVA test (α = 0.05) and Weibull analysis.

Results: High peaks corresponding to the lithium metasilicate and lithium disilicate pattern with similar intensities were observed in all ceramics in the XRD analysis. SEM images showed similar patterns of crystalline structure in the EM and RT ceramics, while the other three groups presented different crystal morphologies than the previous ones and were similar to each other. No differences were found in flexural strength among the groups (p = 0.28).

Conclusions: The CAD-CAM lithium disilicate ceramics showed comparable crystalline intensities. The microstructure of the EM and RT ceramics were different from the other groups. Flexural strength was similar among all ceramics.

目的:分析用于 CAD-CAM 系统的各种二硅酸锂陶瓷商业商标的微观结构和机械性能:获得不同二硅酸锂陶瓷的试样,并随机分为 5 组(n = 14):EM:e.max CAD;RT:EV:Evolith;PM:EV:Evolith;PM:Smile-Lithium CAD;HS:HaHaSmile。微观结构分析采用 X 射线衍射(XRD)和扫描电子显微镜(SEM);抗弯强度采用三点弯曲抗弯试验。对 X 射线衍射和扫描电子显微镜数据进行了定性评估。弯曲强度数据采用单因素方差分析(α = 0.05)和 Weibull 分析进行评估:在 XRD 分析中,所有陶瓷都观察到了与偏硅酸锂和二硅酸锂模式相对应的峰值,且强度相似。扫描电子显微镜图像显示,EM 陶瓷和 RT 陶瓷的晶体结构形态相似,而其他三组陶瓷的晶体形态与前者不同,彼此相似。各组之间的抗弯强度没有差异(p = 0.28):结论:CAD-CAM 二硅酸锂陶瓷的结晶强度相当。结论:CAD-CAM 二硅酸锂陶瓷的结晶强度相当,EM 和 RT 陶瓷的微观结构与其他组不同。所有陶瓷的抗弯强度相似。
{"title":"Microstructural and flexural strength of various CAD-CAM lithium disilicate ceramics.","authors":"Joissi Ferrari Zaniboni, Amanda Soares Silva, Aryvelto Miranda Silva, João Felipe Besegato, Oscar Fernando Muñoz-Chávez, Edson Alves de Campos","doi":"10.1111/jopr.13938","DOIUrl":"https://doi.org/10.1111/jopr.13938","url":null,"abstract":"<p><strong>Purpose: </strong>To analyze the microstructural and mechanical properties of various commercial trademarks of lithium disilicate ceramics for CAD-CAM systems.</p><p><strong>Materials and methods: </strong>Specimens of different lithium disilicate ceramics were obtained and randomized into 5 groups (n = 14): EM: e.max CAD; RT: Rosetta SM; EV: Evolith; PM: Smile-Lithium CAD; and, HS: HaHaSmile. The microstructural analysis was performed by X-ray diffraction (XRD) and scanning electron microscopy (SEM); for flexural strength, the three-point bending flexure test was used. XRD and SEM data were qualitatively evaluated. Data from flexural strength were assessed with one-way ANOVA test (α = 0.05) and Weibull analysis.</p><p><strong>Results: </strong>High peaks corresponding to the lithium metasilicate and lithium disilicate pattern with similar intensities were observed in all ceramics in the XRD analysis. SEM images showed similar patterns of crystalline structure in the EM and RT ceramics, while the other three groups presented different crystal morphologies than the previous ones and were similar to each other. No differences were found in flexural strength among the groups (p = 0.28).</p><p><strong>Conclusions: </strong>The CAD-CAM lithium disilicate ceramics showed comparable crystalline intensities. The microstructure of the EM and RT ceramics were different from the other groups. Flexural strength was similar among all ceramics.</p>","PeriodicalId":49152,"journal":{"name":"Journal of Prosthodontics-Implant Esthetic and Reconstructive Dentistry","volume":" ","pages":""},"PeriodicalIF":3.4,"publicationDate":"2024-09-04","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142134206","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"医学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Effect of artificial aging on fracture toughness and hardness of 3D-printed and milled 3Y-TZP zirconia. 人工老化对 3D 打印和研磨 3Y-TZP 氧化锆断裂韧性和硬度的影响。
IF 3.4 2区 医学 Q1 DENTISTRY, ORAL SURGERY & MEDICINE Pub Date : 2024-09-03 DOI: 10.1111/jopr.13943
Abdulaziz Alhotan, Burak Yilmaz, Anna Weber, Rua Babaier, Christoph Bourauel, Ahmed Mahmoud Fouda

Purpose: This study aimed to evaluate the impact of artificial aging on the fracture toughness and hardness of three-dimensional (3D)-printed and computer-aided design and computer-aided manufacturing (CAD-CAM) milled 3 mol% yttria-stabilized tetragonal zirconia polycrystals (3Y-TZP).

Materials and methods: Forty bar-shaped specimens (45 × 4 × 3 mm) were prepared using two manufacturing technologies: 3D printing (LithaCon 3Y 210, Lithoz GmbH, Vienna, Austria; n = 20) and milling (Initial Zirconia ST, GC, Japan; n = 20) of 3Y-TZP. The chevron-notch beam method was used to assess the fracture toughness according to ISO 24370. Specimens from each 3Y-TZP group were divided into two subgroups (n = 10) based on the artificial aging process (autoclaving): nonaged and aged. Nonaged specimens were stored at room temperature, while aged specimens underwent autoclave aging at 134°C under 2 bar-pressure for 5 h. Subsequently, the specimens were immersed in absolute 99% ethanol using an ultrasonic cleaner for 5 min. Each specimen was preloaded by subjecting it to a 4-point loading test, with a force of up to 200 N applied for three cycles. Further 4-point loading was conducted at a rate of 0.5 mm/min under controlled temperature and humidity conditions until fracture occurred. The maximum force (Fmax) was recorded and the chevron notch was examined at 30 × magnification under an optical microscope for measurements before the fracture toughness (KIc) was calculated. Microhardness testing was also performed to measure the Vickers hardness number (VHN). A scanning electron microscope (SEM) coupled with an energy dispersive X-ray unit (EDX) was used to examine surface topography and chemical composition. X-ray diffraction (XRD) was conducted to identify crystalline structure. Data were statistically analyzed using two-way ANOVA and Student's t-test with a significance level of 0.05.

Results: The nonaged 3D-printed 3Y-TZP group exhibited a significantly higher fracture toughness value (6.07 MPa m1/2) than the milled 3Y-TZP groups (p < 0.001). After autoclave aging, the 3D-printed 3Y-TZP group maintained significantly higher fracture toughness (p < 0.001) compared to the milled 3Y-TZP group. However, no significant differences in hardness values (p = 0.096) were observed between the aged and nonaged groups within each manufacturing process (3D-printed and milled) independently.

Conclusion: The findings revealed that the new 3D-printed 3Y-TZP produced by the lithography-based ceramic manufacturing (LCM) technology exhibited superior fracture toughness after autoclave aging compared to the milled 3Y-TZP. While no significant differences in hardness were observed between the aged groups, the 3D-printed material demonstrated greater resistance to fracture, indicating enhanced mechanical stability.

目的:本研究旨在评估人工老化对三维(3D)打印和计算机辅助设计和计算机辅助制造(CAD-CAM)铣削的 3 mol% 钇稳定四方氧化锆多晶体(3Y-TZP)断裂韧性和硬度的影响:采用两种制造技术制备了 40 个棒状试样(45 × 4 × 3 毫米):3Y-TZP 的三维打印(LithaCon 3Y 210,Lithoz GmbH,奥地利维也纳;n = 20)和铣削(Initial Zirconia ST,GC,日本;n = 20)。根据 ISO 24370 标准,采用切口梁法评估断裂韧性。根据人工老化过程(高压灭菌),每组 3Y-TZP 试样被分为两个亚组(n = 10):非老化和老化。非老化试样在室温下保存,而老化试样则在 134°C、2 巴压力下进行高压灭菌 5 小时。每个试样都通过 4 点加载测试进行预加载,加载力最大为 200 N,循环三次。在温度和湿度受控的条件下,以 0.5 毫米/分钟的速度进一步进行 4 点加载,直至发生断裂。在计算断裂韧性(KIc)之前,记录了最大力(Fmax),并在光学显微镜下以 30 倍的放大率对楔形缺口进行了检查测量。此外,还进行了显微硬度测试,以测量维氏硬度数(VHN)。扫描电子显微镜(SEM)和能量色散 X 射线装置(EDX)用于检查表面形貌和化学成分。X 射线衍射 (XRD) 用于确定晶体结构。数据采用双向方差分析和学生 t 检验进行统计分析,显著性水平为 0.05:未老化的三维打印 3Y-TZP 组的断裂韧性值(6.07 MPa m1/2)明显高于研磨 3Y-TZP 组(p < 0.001)。高压灭菌老化后,三维打印 3Y-TZP 组的断裂韧性值(p < 0.001)明显高于研磨 3Y-TZP 组(p < 0.001)。然而,在每种制造工艺(三维打印和研磨)中,老化组和未老化组之间的硬度值没有明显差异(p = 0.096):研究结果表明,与研磨 3Y-TZP 相比,基于光刻陶瓷制造 (LCM) 技术生产的新型 3D 打印 3Y-TZP 在高压釜老化后表现出更高的断裂韧性。虽然老化组之间的硬度没有明显差异,但三维打印材料表现出更强的抗断裂性,表明其机械稳定性得到增强。
{"title":"Effect of artificial aging on fracture toughness and hardness of 3D-printed and milled 3Y-TZP zirconia.","authors":"Abdulaziz Alhotan, Burak Yilmaz, Anna Weber, Rua Babaier, Christoph Bourauel, Ahmed Mahmoud Fouda","doi":"10.1111/jopr.13943","DOIUrl":"https://doi.org/10.1111/jopr.13943","url":null,"abstract":"<p><strong>Purpose: </strong>This study aimed to evaluate the impact of artificial aging on the fracture toughness and hardness of three-dimensional (3D)-printed and computer-aided design and computer-aided manufacturing (CAD-CAM) milled 3 mol% yttria-stabilized tetragonal zirconia polycrystals (3Y-TZP).</p><p><strong>Materials and methods: </strong>Forty bar-shaped specimens (45 × 4 × 3 mm) were prepared using two manufacturing technologies: 3D printing (LithaCon 3Y 210, Lithoz GmbH, Vienna, Austria; n = 20) and milling (Initial Zirconia ST, GC, Japan; n = 20) of 3Y-TZP. The chevron-notch beam method was used to assess the fracture toughness according to ISO 24370. Specimens from each 3Y-TZP group were divided into two subgroups (n = 10) based on the artificial aging process (autoclaving): nonaged and aged. Nonaged specimens were stored at room temperature, while aged specimens underwent autoclave aging at 134°C under 2 bar-pressure for 5 h. Subsequently, the specimens were immersed in absolute 99% ethanol using an ultrasonic cleaner for 5 min. Each specimen was preloaded by subjecting it to a 4-point loading test, with a force of up to 200 N applied for three cycles. Further 4-point loading was conducted at a rate of 0.5 mm/min under controlled temperature and humidity conditions until fracture occurred. The maximum force (F<sub>max</sub>) was recorded and the chevron notch was examined at 30 × magnification under an optical microscope for measurements before the fracture toughness (K<sub>Ic</sub>) was calculated. Microhardness testing was also performed to measure the Vickers hardness number (VHN). A scanning electron microscope (SEM) coupled with an energy dispersive X-ray unit (EDX) was used to examine surface topography and chemical composition. X-ray diffraction (XRD) was conducted to identify crystalline structure. Data were statistically analyzed using two-way ANOVA and Student's t-test with a significance level of 0.05.</p><p><strong>Results: </strong>The nonaged 3D-printed 3Y-TZP group exhibited a significantly higher fracture toughness value (6.07 MPa m<sup>1/2</sup>) than the milled 3Y-TZP groups (p < 0.001). After autoclave aging, the 3D-printed 3Y-TZP group maintained significantly higher fracture toughness (p < 0.001) compared to the milled 3Y-TZP group. However, no significant differences in hardness values (p = 0.096) were observed between the aged and nonaged groups within each manufacturing process (3D-printed and milled) independently.</p><p><strong>Conclusion: </strong>The findings revealed that the new 3D-printed 3Y-TZP produced by the lithography-based ceramic manufacturing (LCM) technology exhibited superior fracture toughness after autoclave aging compared to the milled 3Y-TZP. While no significant differences in hardness were observed between the aged groups, the 3D-printed material demonstrated greater resistance to fracture, indicating enhanced mechanical stability.</p>","PeriodicalId":49152,"journal":{"name":"Journal of Prosthodontics-Implant Esthetic and Reconstructive Dentistry","volume":" ","pages":""},"PeriodicalIF":3.4,"publicationDate":"2024-09-03","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142127125","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"医学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
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Journal of Prosthodontics-Implant Esthetic and Reconstructive Dentistry
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