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Optimization and testing of a Mass Spectrometer Leak Detection (MSLD) system 质谱仪泄漏检测(MSLD)系统的优化和测试
IF 0.6 4区 材料科学 Q4 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2023-12-01 DOI: 10.32548/10.32548/2023.me-04345
Guoyun Bai, Xindong Hu, X. Liao, Tao Chen, Rongmin Pan, Yanxia Li, Junlan Chang
A rapid helium mass spectrometry leak detection method is established to respond to problems of low sensitivity and efficiency in detecting leaks in large vessels. The optimized multistage tandem leak detection system improves leak detection sensitivity by increasing the amount of gas entering the analysis chamber. By involving the main pumping system in the detection process, the effective pumping speed is increased, resulting in a significant reduction in system response time. Additionally, the optimal leak detection vacuum required for maximizing the leak velocity indicating gas movement is determined, thereby further decreasing the system’s response time. Our application demonstrates that the optimized leak detection system increases sensitivity by one to two orders of magnitude, reduces system response time by over 90%, and shortens evacuation time by 7 h. Ultimately, the optimized design of the vacuum system developed for large vessels demonstrates greatly improved leak detection efficiency and overall capability.
针对大型容器泄漏检测灵敏度低、效率低的问题,建立了一种快速氦质谱泄漏检测方法。优化的多级串联检漏系统通过增加进入分析室的气体量来提高检漏灵敏度。通过让主抽气系统参与检测过程,提高了有效抽气速度,从而显著缩短了系统响应时间。此外,还确定了泄漏速度最大化所需的最佳泄漏检测真空度,从而进一步缩短了系统的响应时间。我们的应用表明,优化后的检漏系统将灵敏度提高了一到两个数量级,系统响应时间缩短了 90% 以上,排空时间缩短了 7 小时。最终,为大型船舶开发的真空系统优化设计大大提高了检漏效率和整体能力。
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引用次数: 0
Inverse Determination Of Interfacial Properties of a Bonded Structure Using Lamb Waves Generated By Laser Lateral Excitation 利用激光侧向激励产生的 Lamb 波反向确定键合结构的界面特性
IF 0.6 4区 材料科学 Q4 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2023-12-01 DOI: 10.32548/2023.me-04319
Tianming Ye, Wenxiang Hu, Tao Chen, Yanxia Li
Nondestructive testing of the adhesive bond properties of a bonded structure is essential in aviation, automotive, and other industries. In this study, a Lamb wave–based quantitative characterization method is proposed to determine the interfacial stiffness of bonded structures. A theoretical model is established, with which the dispersion relationship of Lamb waves in a bonded structure is investigated. Different interfacial states ranging from a perfect bond to a weak bond are simulated, and the numerical results show the sensitivity of Lamb waves to interfacial stiffness. A lateral excitation method is proposed to enhance the excitation of the interfacial sensitive Lamb wave modes, and laser ultrasonic experiments show the enhancement of the Lamb wave signals on aluminum-epoxy-aluminum samples generated by the lateral excitation method. Then, a rapid construction method of inversion objective function is presented to reconstruct the interfacial stiffness coefficient of a bonded structure, and its functionality is validated via finite element simulations. Finally, the interfacial properties of the samples are reconstructed using the inversion scheme.
在航空、汽车和其他行业中,对粘接结构的粘接性能进行无损检测至关重要。本研究提出了一种基于 Lamb 波的定量表征方法,用于确定粘接结构的界面刚度。研究建立了一个理论模型,通过该模型研究了兰姆波在粘接结构中的弥散关系。模拟了从完全粘接到弱粘接的不同界面状态,数值结果显示了兰姆波对界面刚度的敏感性。提出了一种横向激励方法来增强对界面敏感的 Lamb 波模式的激励,激光超声实验表明横向激励方法产生的 Lamb 波信号增强了铝-环氧-铝样品上的 Lamb 波信号。然后,提出了一种快速构建反演目标函数的方法来重建粘接结构的界面刚度系数,并通过有限元模拟验证了其功能。最后,利用反演方案重建了样品的界面特性。
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引用次数: 0
Experimental Study On Acoustic Emission Characteristics of SAP Mortar Self-Healing Process SAP 砂浆自愈合过程的声发射特性实验研究
IF 0.6 4区 材料科学 Q4 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2023-11-01 DOI: 10.32548/2023.me-04359
Nairan Wang, Yan Wang, Yihui Su, Haitao Zhao
Self-healing properties of super absorbent polymer (SAP) concrete can reduce the harmful effects of concrete cracking in structures. This study examines the self-healing process of mortars with different SAP content under dry and wet conditions through acoustic emission testing (AE) and elastic wave velocity testing. Findings indicate that the SAP mortar healing process has three stages: rapid water absorption, smooth water absorption, and drying. In a dry environment, increasing SAP content enhances AE activity, indicating internal crack self-healing via further hydration of unhydrated cement particles. In a wet environment, AE activity increases with increasing SAP content during the second healing cycle, indicating self-healing of the mortar matrix. These results suggest the use of SAP concrete could potentially mitigate future structural damage.
超强吸水聚合物(SAP)混凝土的自愈合特性可以减少结构中混凝土开裂的有害影响。本研究通过声发射测试(AE)和弹性波速测试,研究了不同 SAP 含量的砂浆在干湿条件下的自愈合过程。研究结果表明,SAP 砂浆的愈合过程分为三个阶段:快速吸水、平稳吸水和干燥。在干燥环境中,SAP 含量的增加会增强声发射活动,这表明内部裂缝会通过未水化水泥颗粒的进一步水化而自我愈合。在潮湿环境中,在第二个愈合周期中,随着 SAP 含量的增加,AE 活性也会增加,这表明砂浆基质具有自愈合能力。这些结果表明,使用 SAP 混凝土有可能减轻未来的结构损坏。
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引用次数: 0
Nondestructive Analysis On 4D-Printed Hygroscopic Actuators Through Optical Flow-Based Displacement Measurements 通过基于光流的位移测量对 4D 印刷吸湿致动器进行无损分析
IF 0.6 4区 材料科学 Q4 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2023-11-01 DOI: 10.32548/2023.me-04311
F. Bianconi, M. Filippucci, G. Pelliccia, G. Rossi, T. Tocci, G. Tribbiani, David Correa
The many advantages of additive manufacturing are particularly noticeable in the fabrication of 4D-printed actuators. Through the selection of specific printing properties and materials, hygroscopic wood polymer composites (WPCs) can be produced and their reaction to humidity can be preprogrammed to achieve the greatest deformations in the shortest time. This responsive behavior makes 4D-printed WPCs suitable for architectural applications, where they can act as passive airflow controllers to improve hygrometric conditions in indoor environments. Image analysis methods have been proven to be reliable to select the best combinations of materials and properties for hygroscopic WPCs but, in some cases, they provide only information on the curvature angles and the instrumentation and software can be expensive. This paper presents an optical flow method for tracking the displacements through a free and open-source software. Starting from a time-lapse video of the sample immersed in water, the analysis returns a matrix composed of the 3D displacement values for each pixel in consecutive frames and the velocity of the displacement, with their visual representation. Such image analysis techniques proved to be suitable to assess the different hygro-responsive behavior under water of 4D-printed WPCs through low-cost equipment without altering their configuration.
增材制造的诸多优势在制造 4D 打印致动器方面尤为明显。通过选择特定的打印特性和材料,可以生产出吸湿性木质聚合物复合材料(WPC),并对其对湿度的反应进行预编程,以便在最短时间内实现最大变形。这种反应行为使 4D 印刷的木塑复合材料适用于建筑应用,它们可以作为被动气流控制器来改善室内环境的湿度条件。图像分析方法已被证明是选择吸湿性木塑材料最佳材料和性能组合的可靠方法,但在某些情况下,这些方法只能提供曲率角度的信息,而且仪器和软件的成本可能很高。本文介绍了一种通过免费开源软件跟踪位移的光流方法。从样品浸入水中的延时视频开始,分析会返回一个由连续帧中每个像素的三维位移值和位移速度组成的矩阵,并给出可视化表示。事实证明,这种图像分析技术适用于通过低成本设备评估 4D 印刷的木塑材料在水中的不同湿气反应行为,而无需改变其构造。
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引用次数: 0
Influence of the Transverse Stress Component of Ferromagnetic Materials on MBN Signals Under Bidirectional Stress Conditions 双向应力条件下铁磁材料横向应力分量对MBN信号的影响
4区 材料科学 Q4 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2023-09-01 DOI: 10.32548/2023.me-04295
Di Jingyu
This paper studies the effect of the transverse stress component of magnetically isotropic ferromagnetic materials on the magnetic Barkhausen noise (MBN) testing signals under planar bidirectional stress states. Based on the logistic distribution function, a model that can be used to describe the effect of the planar bidirectional stress level on MBN characteristic signals is proposed; the formulated model works within the elastic limit of the magnetically isotropic ferromagnetic materials. Then, the characteristics of the proposed regression model are analyzed by computer simulation. Finally, to validate the proposed regression model, the bidirectional stress experimental data extracted from the published paper is used. The results show that there is a high linear correlation between the actual data and the predicted data of the formulated model. Therefore, it can be proved that the proposed planar bidirectional stress regression model based on the logistic distribution function is feasible, applicable, and valuable.
研究了磁性各向同性铁磁材料在平面双向应力状态下,横向应力分量对磁性巴克豪森噪声(MBN)测试信号的影响。基于logistic分布函数,提出了平面双向应力水平对MBN特征信号影响的模型;所建立的模型在磁性各向同性铁磁材料的弹性极限内工作。然后,通过计算机仿真分析了所提出的回归模型的特点。最后,利用从已发表论文中提取的双向应力实验数据验证回归模型。结果表明,所建立模型的实际数据与预测数据具有高度的线性相关性。由此可以证明,所提出的基于logistic分布函数的平面双向应力回归模型是可行的、适用的、有价值的。
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引用次数: 0
Microwave Real-Time and High-Resolution Imaging System Development for NDT Applications: A Chronology 用于无损检测应用的微波实时和高分辨率成像系统开发:年表
4区 材料科学 Q4 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2023-09-01 DOI: 10.32548/2023.me-04349
Zoughi Reza
In the past four decades, microwave imaging has experienced a renaissance. This has happened because of new technology development, improved and robust image reconstruction algorithms, expansion of imaging modalities, and operational friendliness, particularly for nondestructive testing (NDT) applications (e.g., high-resolution, real-time, portable systems). Efforts to push the envelope forward continues. This paper provides a brief background on some of the key works that laid the foundation for these advancements. Next, the focus of the paper shifts to the author’s research group’s contributions to the field since the early 1990s to the present day in developing new imaging methodologies and tools specifically for NDT applications. This paper gives a chronology of these specific developments and illustrates how the desire to address NDT needs and requirements have kept these developmental processes moving forward.
在过去的四十年里,微波成像经历了一次复兴。这是因为新技术的发展,改进和强大的图像重建算法,成像模式的扩展和操作友好性,特别是对于无损检测(NDT)应用(例如,高分辨率,实时,便携式系统)。推动极限向前发展的努力仍在继续。本文简要介绍了为这些进展奠定基础的一些关键工作的背景。接下来,本文的重点转移到作者的研究小组对该领域的贡献,自20世纪90年代初至今,在开发新的成像方法和工具,专门为无损检测应用。本文给出了这些具体发展的年表,并说明了解决无损检测需求和要求的愿望如何使这些发展进程向前发展。
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引用次数: 0
Influence of the Transverse Stress Component of Ferromagnetic Materials on MBN Signals Under Bidirectional Stress Conditions 双向应力条件下铁磁材料横向应力分量对MBN信号的影响
4区 材料科学 Q4 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2023-09-01 DOI: 10.32548/me-04295
Jingyu Di
This paper studies the effect of the transverse stress component of magnetically isotropic ferromagnetic materials on the magnetic Barkhausen noise (MBN) testing signals under planar bidirectional stress states. Based on the logistic distribution function, a model that can be used to describe the effect of the planar bidirectional stress level on MBN characteristic signals is proposed; the formulated model works within the elastic limit of the magnetically isotropic ferromagnetic materials. Then, the characteristics of the proposed regression model are analyzed by computer simulation. Finally, to validate the proposed regression model, the bidirectional stress experimental data extracted from the published paper is used. The results show that there is a high linear correlation between the actual data and the predicted data of the formulated model. Therefore, it can be proved that the proposed planar bidirectional stress regression model based on the logistic distribution function is feasible, applicable, and valuable.
研究了磁性各向同性铁磁材料在平面双向应力状态下,横向应力分量对磁性巴克豪森噪声(MBN)测试信号的影响。基于logistic分布函数,提出了平面双向应力水平对MBN特征信号影响的模型;所建立的模型在磁性各向同性铁磁材料的弹性极限内工作。然后,通过计算机仿真分析了所提出的回归模型的特点。最后,利用从已发表论文中提取的双向应力实验数据验证回归模型。结果表明,所建立模型的实际数据与预测数据具有高度的线性相关性。由此可以证明,所提出的基于logistic分布函数的平面双向应力回归模型是可行的、适用的、有价值的。
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引用次数: 0
Sectorial Plane Wave Imaging for Weld Inspection Studies 用于焊缝检测的扇形平面波成像研究
4区 材料科学 Q4 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2023-09-01 DOI: 10.32548/2023.me-04312
Lalith Sai Srinivas Pillarisetti, Gangadharan Raju, Anandamurugan Subramanian
Advanced ultrasonic array–based imaging techniques that rely on A-scan data acquired through individual parallel reception of array elements and subsequent post-processing have shown promising performance by generating high-resolution images. An advanced array-based imaging algorithm called sectorial plane wave imaging (SPWI) has been recently proposed with multimode imaging and rapid inspection capabilities. In this work, the efficiency of the SPWI algorithm is demonstrated and compared to the total focusing method (TFM) and plane wave imaging (PWI) algorithms in detecting different types of common weld defects: lack of sidewall fusion, slag, porosity, toe crack, centerline crack, and root crack. The full matrix capture data acquired over each weld defect using a 32-element linear array on an angular wedge configuration is converted to the PWI matrix data to perform SPWI. The corner and indirect mode SPWI inspection results are able to detect all the weld defects with image quality comparable to that of TFM and PWI, but at a higher processing speed due to the slight compromise over reception focusing, making SPWI a viable advanced ultrasonic array–based imaging technique for inspecting welds.
先进的超声阵列成像技术依赖于通过单个阵列元素的并行接收和随后的后处理获得的a扫描数据,通过生成高分辨率图像显示出有希望的性能。最近提出了一种先进的基于阵列的成像算法,称为扇形平面波成像(SPWI),具有多模式成像和快速检测能力。在这项工作中,SPWI算法在检测不同类型的常见焊接缺陷方面的效率得到了验证,并与全聚焦法(TFM)和平面波成像(PWI)算法进行了比较,这些缺陷包括:侧壁熔合不足、渣、气孔、趾部裂纹、中心线裂纹和根部裂纹。使用角楔结构上的32元素线性阵列,在每个焊缝缺陷上获得完整的矩阵捕获数据,并将其转换为PWI矩阵数据,以执行SPWI。拐角和间接模式SPWI检测结果能够检测出所有焊缝缺陷,图像质量与TFM和PWI相当,但由于接收聚焦略有妥协,处理速度更高,使SPWI成为一种可行的基于超声阵列的先进焊缝检测成像技术。
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引用次数: 0
Only the Dead Know NDT: Exploring the Critical and Little-Known Nondestructive Testing Business 只有死人才知道无损检测:探索关键和鲜为人知的无损检测业务
4区 材料科学 Q4 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2023-08-01 DOI: 10.32548/2023.me-04365
Jim Treat, Bruce Pellegrino
With over a century of combined nondestructive testing (NDT) experience, the authors of this article would like to pass along some legacy knowledge of the NDT business from the perspective of services, equipment, training, and certification. Over their multi-decade careers, they have held numerous roles in field deployments, sales, marketing, management, mergers and acquisitions, accounting, government relations, and product development. In all cases, they learned that the key to success in NDT was about providing solutions to customer problems. The authors have experienced firsthand the incredible technical and commercial development of the NDT marketplace and desire to share their insights with the readers of Materials Evaluation.
结合一个多世纪的综合无损检测(NDT)经验,本文的作者希望从服务、设备、培训和认证的角度传递一些无损检测业务的遗留知识。在他们几十年的职业生涯中,他们在现场部署、销售、营销、管理、并购、会计、政府关系和产品开发等领域担任过许多职位。在所有情况下,他们了解到无损检测成功的关键是为客户问题提供解决方案。作者亲身体验了无损检测市场令人难以置信的技术和商业发展,并希望与材料评估的读者分享他们的见解。
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引用次数: 0
Performance of a Guided Wave Pipe Monitoring System Over Extended Periods of Field Operation 导波管道监测系统在长时间野外作业中的性能
4区 材料科学 Q4 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2023-08-01 DOI: 10.32548/2023.me-04335
Stephano Mariani, Sebastian Heinlein, Thomas Vogt, Peter Cawley
The performance of a permanently installed guided wave pipe monitoring system over extended periods has been investigated. Other than at a clamped support, the signals obtained in the three installations reported here have been stable to better than 1% (–40 dB) over periods of 12–24 months, even in hostile oil and gas facility environments. The use of baseline subtraction means that the sensitivity to defects is substantially better than that obtained in one-off inspection; in the two site examples reported here, improvements of 7 and 12 dB relative to one-off interpretation of the A-scan signal were obtained, and changes can be flagged automatically. The improvement in sensitivity is even larger at features such as welds and bends, which give significant reflections even in the absence of damage. The permanently installed system combines long-range guided wave monitoring for localized corrosion patches with eight precise thickness measurements around the pipe circumference, making it possible to monitor the general wall loss rate, as well as detect any more severe, localized corrosion. Permanently installed guided wave monitoring systems are therefore found to be a commercially attractive tool for the assessment of current and future piping integrity.
研究了一种永久安装的导波管道监测系统的长期性能。除了固定支架外,即使在恶劣的油气设施环境中,在12-24个月的时间里,从三个装置中获得的信号稳定在1%以上(-40 dB)。基线减法的使用意味着对缺陷的敏感性大大优于一次性检查;在这里报告的两个站点示例中,相对于一次性解释a扫描信号,获得了7和12 dB的改进,并且可以自动标记变化。灵敏度的提高在焊缝和弯道等特征上甚至更大,即使在没有损坏的情况下也会产生明显的反射。永久安装的系统结合了远程导波监测局部腐蚀斑块和8个精确的管道周长厚度测量,从而可以监测总体壁损失率,以及检测任何更严重的局部腐蚀。因此,永久安装的导波监测系统被认为是评估当前和未来管道完整性的商业上有吸引力的工具。
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引用次数: 1
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Materials Evaluation
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