{"title":"Powder Metallurgy Progress, an international open-access journal with 20 years of publishing history announces the Extension of the Journal`s Scope","authors":"","doi":"10.2478/pmp-2020-0007","DOIUrl":"https://doi.org/10.2478/pmp-2020-0007","url":null,"abstract":"","PeriodicalId":52175,"journal":{"name":"Powder Metallurgy Progress","volume":"436 1","pages":""},"PeriodicalIF":0.0,"publicationDate":"2020-06-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"41291053","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
U. Robert, S. Etuk, O. Agbasi, Ubong A. Iboh, S. Ekpo
Abstract Disc-shaped compacts were fabricated from two mix proportions of calcined eggshell nanopowder and dry cassava starch and then used as test samples. The electrical resistance (R), thermal sensitivity index (β) and electronic activation energy (Ea) of the samples measured over a temperature range from 35 to 75oC were found to decrease non-linearly in values with increasing temperature. It was also observed that the results obtained (R = 3.691E6 Ω – 6.210E7 Ω, β = 3812K – 5316K and Ea = 0.33 eV – 0.46 eV) fulfill market requirements by comparing very well with the established values for NTC thermistors. Hence, from manufacturing viewpoint, recycling of chicken eggshell wastes and cassava effluents can avail electronic industry with promising and alternative materials for fabrication of temperature sensing / monitoring / control devices suitable for engineering applications. This will also help to reduce environmental pollution.
{"title":"Temperature-Dependent Electrical Characteristics of Disc-Shaped Compacts Fabricated using Calcined Eggshell Nano Powder and Dry Cassava Starch","authors":"U. Robert, S. Etuk, O. Agbasi, Ubong A. Iboh, S. Ekpo","doi":"10.2478/pmp-2020-0002","DOIUrl":"https://doi.org/10.2478/pmp-2020-0002","url":null,"abstract":"Abstract Disc-shaped compacts were fabricated from two mix proportions of calcined eggshell nanopowder and dry cassava starch and then used as test samples. The electrical resistance (R), thermal sensitivity index (β) and electronic activation energy (Ea) of the samples measured over a temperature range from 35 to 75oC were found to decrease non-linearly in values with increasing temperature. It was also observed that the results obtained (R = 3.691E6 Ω – 6.210E7 Ω, β = 3812K – 5316K and Ea = 0.33 eV – 0.46 eV) fulfill market requirements by comparing very well with the established values for NTC thermistors. Hence, from manufacturing viewpoint, recycling of chicken eggshell wastes and cassava effluents can avail electronic industry with promising and alternative materials for fabrication of temperature sensing / monitoring / control devices suitable for engineering applications. This will also help to reduce environmental pollution.","PeriodicalId":52175,"journal":{"name":"Powder Metallurgy Progress","volume":"20 1","pages":"12 - 20"},"PeriodicalIF":0.0,"publicationDate":"2020-06-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"49290488","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
C. Gierl-Mayer, M. Huemer, H. Danninger, M. Dlapka, G. Stetina, R. Ratzi
Abstract For powder metallurgy products, high density is an essential requirements to obtain maximum mechanical properties. Here, supersolidus liquid phase sintering (SSPLS) is an effective means to attain high sintered density, as known from PM high speed steels. In the present work it is shown that this technique can also be applied to Cr prealloyed low alloy steel grades. Supersolidus sintering through indirect heating requires precise control of temperature and also the atmosphere, to avoid uncontrolled changes of the carbon level. Higher C contents are beneficial here since they enable lower temperatures and result in wider temperature windows for sintering. The temperatures necessary for SSLPS at moderate C levels are fairly high for standard sintering furnaces, therefore induction sintering was studied in this work. It showed that, as was to be expected, also here precise temperature control is required, but for any carbon level tested a sintering temperature could be identified that yielded high sintered density and good shape retention. The high density attained, in combination with the very high temperatures, results in pronounced grain growth, this process no more being inhibited by the presence of pores, which is undesirable but can however be remedied by suitable heat treatment.
{"title":"Supersolidus Sintering of Cr Prealloyed Steels by Inductive Heating","authors":"C. Gierl-Mayer, M. Huemer, H. Danninger, M. Dlapka, G. Stetina, R. Ratzi","doi":"10.1515/pmp-2019-0006","DOIUrl":"https://doi.org/10.1515/pmp-2019-0006","url":null,"abstract":"Abstract For powder metallurgy products, high density is an essential requirements to obtain maximum mechanical properties. Here, supersolidus liquid phase sintering (SSPLS) is an effective means to attain high sintered density, as known from PM high speed steels. In the present work it is shown that this technique can also be applied to Cr prealloyed low alloy steel grades. Supersolidus sintering through indirect heating requires precise control of temperature and also the atmosphere, to avoid uncontrolled changes of the carbon level. Higher C contents are beneficial here since they enable lower temperatures and result in wider temperature windows for sintering. The temperatures necessary for SSLPS at moderate C levels are fairly high for standard sintering furnaces, therefore induction sintering was studied in this work. It showed that, as was to be expected, also here precise temperature control is required, but for any carbon level tested a sintering temperature could be identified that yielded high sintered density and good shape retention. The high density attained, in combination with the very high temperatures, results in pronounced grain growth, this process no more being inhibited by the presence of pores, which is undesirable but can however be remedied by suitable heat treatment.","PeriodicalId":52175,"journal":{"name":"Powder Metallurgy Progress","volume":"19 1","pages":"53 - 62"},"PeriodicalIF":0.0,"publicationDate":"2019-12-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"42773841","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Abstract Lead is known to be banned in alloy making, highlighting toxicity concerns and environmental legislations. Researchers and scholars around the globe were in immediate search of new lead free solder alloys which could potentially replace the old Sn-Pb alloy. In this comprehensive study, shear strength and impact toughness tests were conducted on Sn-1Cu-1Ni when different amounts of Ag (0.25, 0.5, 0.75 1 % by wt.) is added. Shear strength test is tested using micro force test system. Impact toughness test is analyzed using Charpy impact test set up by calculating the energy difference before and after impact. The study reveals that, Ultimate shear stress increased from 19 MPa to 21.3 MPa. Yield strength increased from 27.4 MPa to 29.7 Mpa. Impact toughness of the alloys increased from 9.4 J to 10.1 J. Thus, Sn-1Cu-1Ni-1Ag is found to have improved shear strength and impact toughness than Sn-1Cu-1Ni.
{"title":"Experimental Investigations on Impact Toughness and Shear Strength of Novel Lead Free Solder Alloy Sn-1Cu-1Ni-XAg","authors":"S. Jayesh, Jacob Elias","doi":"10.1515/pmp-2019-0009","DOIUrl":"https://doi.org/10.1515/pmp-2019-0009","url":null,"abstract":"Abstract Lead is known to be banned in alloy making, highlighting toxicity concerns and environmental legislations. Researchers and scholars around the globe were in immediate search of new lead free solder alloys which could potentially replace the old Sn-Pb alloy. In this comprehensive study, shear strength and impact toughness tests were conducted on Sn-1Cu-1Ni when different amounts of Ag (0.25, 0.5, 0.75 1 % by wt.) is added. Shear strength test is tested using micro force test system. Impact toughness test is analyzed using Charpy impact test set up by calculating the energy difference before and after impact. The study reveals that, Ultimate shear stress increased from 19 MPa to 21.3 MPa. Yield strength increased from 27.4 MPa to 29.7 Mpa. Impact toughness of the alloys increased from 9.4 J to 10.1 J. Thus, Sn-1Cu-1Ni-1Ag is found to have improved shear strength and impact toughness than Sn-1Cu-1Ni.","PeriodicalId":52175,"journal":{"name":"Powder Metallurgy Progress","volume":"19 1","pages":"90 - 96"},"PeriodicalIF":0.0,"publicationDate":"2019-12-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"49316277","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Abstract The customary edged tool for machining is uneconomical for harder and hard to machine materials and furthermore the level of surface finish accomplished is not that great. As of late, a lot of consideration in mechanical engineering has been centered on finishing tasks. Not many investigations have been accounted for till date on the advancement of substitute magnetic abrasive powder (MAP). In this paper, to improve the finishing performance, the abrasive powder were prepared by mechanical alloying of diamond powder and iron (Fe) powder, compacting these with universal testing machine (UTM) and then sintered at different temperature in a sintering machine in an inert gas (H2) atmosphere. These compacts were crushed and sieved to obtain various sizes of MAP. This abrasive powder were micro-structurally examined. The results indicate that the densification increases and porosity decreases with increasing temperature. Moreover, the prepared bonded MAP has potential performance as a new MAP for fine finishing in Magnetic Abrasive Flow Machining (MAFM) process.
{"title":"Preparation, Microstructure Evaluation and Performance Analysis of Diamond-Iron Bonded Magnetic Abrasive Powder","authors":"Palwinder Singh, L. Singh, Sehijpal Singh","doi":"10.1515/pmp-2019-0008","DOIUrl":"https://doi.org/10.1515/pmp-2019-0008","url":null,"abstract":"Abstract The customary edged tool for machining is uneconomical for harder and hard to machine materials and furthermore the level of surface finish accomplished is not that great. As of late, a lot of consideration in mechanical engineering has been centered on finishing tasks. Not many investigations have been accounted for till date on the advancement of substitute magnetic abrasive powder (MAP). In this paper, to improve the finishing performance, the abrasive powder were prepared by mechanical alloying of diamond powder and iron (Fe) powder, compacting these with universal testing machine (UTM) and then sintered at different temperature in a sintering machine in an inert gas (H2) atmosphere. These compacts were crushed and sieved to obtain various sizes of MAP. This abrasive powder were micro-structurally examined. The results indicate that the densification increases and porosity decreases with increasing temperature. Moreover, the prepared bonded MAP has potential performance as a new MAP for fine finishing in Magnetic Abrasive Flow Machining (MAFM) process.","PeriodicalId":52175,"journal":{"name":"Powder Metallurgy Progress","volume":"19 1","pages":"82 - 89"},"PeriodicalIF":0.0,"publicationDate":"2019-12-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"46017557","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
J. Ecker, K. Dobrezberger, J. Gonzalez-Gutierrez, M. Spoerk, C. Gierl-Mayer, Herbert Danninger
Abstract Fused Layer Modelling (FLM) is one out of several material extrusion (ME) additive manufacturing (AM) methods. FLM usually deals with processing of polymeric materials but can also be used to process metal-filled polymeric systems to produce metallic parts. Using FLM for this purpose helps to save costs since the FLM hardware is cheap compared to e.g. direct metal laser processing hardware, and FLM offers an alternative route to the production of metallic components. To produce metallic parts by FLM, the methodology is different from direct metal processing technologies, and several processing steps are required: First, filaments consisting of a special polymer-metal composition are produced. The filament is then transformed into shaped parts by using FLM process technology. Subsequently the polymeric binder is removed (”debinding”) and finally the metallic powder body is sintered. Depending on the metal powder used, the binder composition, the FLM production parameters and also the debinding and sintering processes must be carefully adapted and optimized. The focal points of this study are as following: 1. To confirm that metallic parts can be produced by using FLM plus debinding and sintering as an alternative route to direct metal additive manufacturing. 2. Determination of process parameters, depending on the used metal powders (steel and copper) and optimization of each process step. 3. Comparison of the production paths for the different metal powders and their debinding and sintering behavior as well as the final properties of the produced parts. The results showed that both materials were printable after adjusting the FLM parameters, metallic parts being produced for both metal powder systems. The production method and the sintering process worked out well for both powders. However there are specific challenges in the sintering process that have to be overcome to produce high quality metal parts. This study serves as a fundamental basis for understanding when it comes to the processing of steel and copper powder into metallic parts using FLM processing technology.
{"title":"Additive Manufacturing of Steel and Copper Using Fused Layer Modelling: Material and Process Development","authors":"J. Ecker, K. Dobrezberger, J. Gonzalez-Gutierrez, M. Spoerk, C. Gierl-Mayer, Herbert Danninger","doi":"10.1515/pmp-2019-0007","DOIUrl":"https://doi.org/10.1515/pmp-2019-0007","url":null,"abstract":"Abstract Fused Layer Modelling (FLM) is one out of several material extrusion (ME) additive manufacturing (AM) methods. FLM usually deals with processing of polymeric materials but can also be used to process metal-filled polymeric systems to produce metallic parts. Using FLM for this purpose helps to save costs since the FLM hardware is cheap compared to e.g. direct metal laser processing hardware, and FLM offers an alternative route to the production of metallic components. To produce metallic parts by FLM, the methodology is different from direct metal processing technologies, and several processing steps are required: First, filaments consisting of a special polymer-metal composition are produced. The filament is then transformed into shaped parts by using FLM process technology. Subsequently the polymeric binder is removed (”debinding”) and finally the metallic powder body is sintered. Depending on the metal powder used, the binder composition, the FLM production parameters and also the debinding and sintering processes must be carefully adapted and optimized. The focal points of this study are as following: 1. To confirm that metallic parts can be produced by using FLM plus debinding and sintering as an alternative route to direct metal additive manufacturing. 2. Determination of process parameters, depending on the used metal powders (steel and copper) and optimization of each process step. 3. Comparison of the production paths for the different metal powders and their debinding and sintering behavior as well as the final properties of the produced parts. The results showed that both materials were printable after adjusting the FLM parameters, metallic parts being produced for both metal powder systems. The production method and the sintering process worked out well for both powders. However there are specific challenges in the sintering process that have to be overcome to produce high quality metal parts. This study serves as a fundamental basis for understanding when it comes to the processing of steel and copper powder into metallic parts using FLM processing technology.","PeriodicalId":52175,"journal":{"name":"Powder Metallurgy Progress","volume":"19 1","pages":"63 - 81"},"PeriodicalIF":0.0,"publicationDate":"2019-12-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"41515994","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
H. Brunckova, Ľ. Medvecký, E. Múdra, A. Kovalčíková
Abstract Neodymium niobate NdNbO4 (NNO) and tantalate NdTaO4 (NTO) thin films (~100 nm) were prepared by sol-gel/spin-coating process on Pb(Zr0.52Ti0.48)O3/Al2O3 substrates with annealing at 1000°C. The precursors of films were synthesized using Nb or Ta tartrate complexes. The XRD results of NNO and NTO films confirmed tetragonal T-NdNbO4 and T-NdTaO4 phases, respectively, with traces of monoclinic MNdNbO4 and M´-NdTaO4. The surface morphology and topography were investigated by SEM and AFM analysis. NTO was smoother with roughness 5.24 nm in comparison with NNO (6.95 nm). In the microstructure of NNO, small spherical (~ 20-50 nm) T-NdNbO4 and larger needle-like particles (~100 nm) of M-NdNbO4 phase were observed. The compact clusters composed of fine spherical T-NdTaO4 particles (~ 50 nm) and cuboidal M´-NdTaO4 particles (~ 100 nm) were found in NTO. The results of this work can contribute to formation of different polymorphs of films for the application in environmental electrolytic thin film devices.
{"title":"Polymorphs of Neodymium Niobate and Tantalate Thin Films Prepared by Sol-Gel Method","authors":"H. Brunckova, Ľ. Medvecký, E. Múdra, A. Kovalčíková","doi":"10.1515/pmp-2019-0004","DOIUrl":"https://doi.org/10.1515/pmp-2019-0004","url":null,"abstract":"Abstract Neodymium niobate NdNbO4 (NNO) and tantalate NdTaO4 (NTO) thin films (~100 nm) were prepared by sol-gel/spin-coating process on Pb(Zr0.52Ti0.48)O3/Al2O3 substrates with annealing at 1000°C. The precursors of films were synthesized using Nb or Ta tartrate complexes. The XRD results of NNO and NTO films confirmed tetragonal T-NdNbO4 and T-NdTaO4 phases, respectively, with traces of monoclinic MNdNbO4 and M´-NdTaO4. The surface morphology and topography were investigated by SEM and AFM analysis. NTO was smoother with roughness 5.24 nm in comparison with NNO (6.95 nm). In the microstructure of NNO, small spherical (~ 20-50 nm) T-NdNbO4 and larger needle-like particles (~100 nm) of M-NdNbO4 phase were observed. The compact clusters composed of fine spherical T-NdTaO4 particles (~ 50 nm) and cuboidal M´-NdTaO4 particles (~ 100 nm) were found in NTO. The results of this work can contribute to formation of different polymorphs of films for the application in environmental electrolytic thin film devices.","PeriodicalId":52175,"journal":{"name":"Powder Metallurgy Progress","volume":"19 1","pages":"34 - 43"},"PeriodicalIF":0.0,"publicationDate":"2019-09-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"47653094","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
M. Zadra, L. Girardini, G. Pederzini, G. Patuelli, M. Piva, S. Bordin, L. De Mitri, A. Popolizio, I. Cristofolini, A. Molinari
Abstract The influence of die wall lubrication during warm die compaction on densification, microstructure and mechanical properties of three low alloy ferrous powders was investigated. Specimens were sintered at 1250°C. Die wall lubrication leads to higher green and sintered density and enhances the dimensional stability. It does not affect the microstructure of the matrix, while pores are smaller and more rounded than in bulk lubricated specimens. In TRS tests, both strength and deformation are higher in die wall lubricated specimens than bulk lubricated ones.
{"title":"Die Wall - Vs. Bulk Lubrication in Warm Die Compaction: Density, Microstructure and Mechanical Properties of Three Low Alloyed Steels","authors":"M. Zadra, L. Girardini, G. Pederzini, G. Patuelli, M. Piva, S. Bordin, L. De Mitri, A. Popolizio, I. Cristofolini, A. Molinari","doi":"10.1515/pmp-2019-0005","DOIUrl":"https://doi.org/10.1515/pmp-2019-0005","url":null,"abstract":"Abstract The influence of die wall lubrication during warm die compaction on densification, microstructure and mechanical properties of three low alloy ferrous powders was investigated. Specimens were sintered at 1250°C. Die wall lubrication leads to higher green and sintered density and enhances the dimensional stability. It does not affect the microstructure of the matrix, while pores are smaller and more rounded than in bulk lubricated specimens. In TRS tests, both strength and deformation are higher in die wall lubricated specimens than bulk lubricated ones.","PeriodicalId":52175,"journal":{"name":"Powder Metallurgy Progress","volume":"19 1","pages":"44 - 52"},"PeriodicalIF":0.0,"publicationDate":"2019-09-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"44353235","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
R. Stulajterova, Ľ. Medvecký, M. Giretova, T. Sopčák, J. Briančin
Abstract The tetracalcium phosphate/nanomonetite (TTCPMH) biocements with the addition of sodium alginate were prepared by mechanical homogenization of powder mixture with hardening liquid containing sodium alginate. The effect of various viscosity of different alginates on properties of TTCPMH cement mixture was investigated. The medium viscous (MED) alginate had a more negative effect on setting process and compressive strength than low viscous (LOW) alginate. An approx. 50% decrease in mechanical properties (compressive strengths, Young´s modulus, work of fracture (WOF)) was revealed after an addition of 0.25 wt % with rapid fall above 1 wt % of LOW alginate in biocement. A statistically significant difference in the WOF was found between of 0.25 and 0.5 LOW alginate biocements (p<0.035) whereas no statistical differences were revealed between WOF of 0.5 and 1 LOW alginate biocements (p˃0.357). In the microstructure of composite cements, the increased amounts of granular or finer needle-like nanohydroxyapatite particles arranged into the form of more separated spherical agglomerates were observed. A low cytotoxicity of cement extracts based on measurement of cell proliferation was revealed.
{"title":"Influence of Sodium Alginate on Properties of Tetracalcium Phosphate/Nanomonetite Biocement","authors":"R. Stulajterova, Ľ. Medvecký, M. Giretova, T. Sopčák, J. Briančin","doi":"10.1515/pmp-2019-0001","DOIUrl":"https://doi.org/10.1515/pmp-2019-0001","url":null,"abstract":"Abstract The tetracalcium phosphate/nanomonetite (TTCPMH) biocements with the addition of sodium alginate were prepared by mechanical homogenization of powder mixture with hardening liquid containing sodium alginate. The effect of various viscosity of different alginates on properties of TTCPMH cement mixture was investigated. The medium viscous (MED) alginate had a more negative effect on setting process and compressive strength than low viscous (LOW) alginate. An approx. 50% decrease in mechanical properties (compressive strengths, Young´s modulus, work of fracture (WOF)) was revealed after an addition of 0.25 wt % with rapid fall above 1 wt % of LOW alginate in biocement. A statistically significant difference in the WOF was found between of 0.25 and 0.5 LOW alginate biocements (p<0.035) whereas no statistical differences were revealed between WOF of 0.5 and 1 LOW alginate biocements (p˃0.357). In the microstructure of composite cements, the increased amounts of granular or finer needle-like nanohydroxyapatite particles arranged into the form of more separated spherical agglomerates were observed. A low cytotoxicity of cement extracts based on measurement of cell proliferation was revealed.","PeriodicalId":52175,"journal":{"name":"Powder Metallurgy Progress","volume":"19 1","pages":"1 - 11"},"PeriodicalIF":0.0,"publicationDate":"2019-09-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"45011497","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
L. Emanuelli, A. Molinari, G. Arrighetti, G. Garoli
Abstract The effect of binder content and WC grain size on the mechanical properties is widely investigated in literature. An increase in binder amount and WC grain size leads to a decrease in hardness and an increase in fracture toughness. Actually, these correlations are related to the influence of binder content and WC grain size through the contiguity and mean binder free path, which are the microstructural parameters that affect the mechanical properties. The aim of this study is to verify the dependence of the two microstructural parameters that govern the WCCo mechanical behaviour, namely the contiguity and mean binder free path, on the mechanical properties of an extended range of WC-Co samples, which differ in terms of Co content and tungsten carbide grain size.
{"title":"T Dependence of the Mechanical Properties on the Microstructural Parameters of WC-Co","authors":"L. Emanuelli, A. Molinari, G. Arrighetti, G. Garoli","doi":"10.1515/pmp-2019-0003","DOIUrl":"https://doi.org/10.1515/pmp-2019-0003","url":null,"abstract":"Abstract The effect of binder content and WC grain size on the mechanical properties is widely investigated in literature. An increase in binder amount and WC grain size leads to a decrease in hardness and an increase in fracture toughness. Actually, these correlations are related to the influence of binder content and WC grain size through the contiguity and mean binder free path, which are the microstructural parameters that affect the mechanical properties. The aim of this study is to verify the dependence of the two microstructural parameters that govern the WCCo mechanical behaviour, namely the contiguity and mean binder free path, on the mechanical properties of an extended range of WC-Co samples, which differ in terms of Co content and tungsten carbide grain size.","PeriodicalId":52175,"journal":{"name":"Powder Metallurgy Progress","volume":"19 1","pages":"23 - 33"},"PeriodicalIF":0.0,"publicationDate":"2019-09-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"44700287","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
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