首页 > 最新文献

mjlh pjwhshhy `lwm w Sny` Gdhyy yrn最新文献

英文 中文
Determination of rheological properties of tomato under quasi static loading conditions 准静态加载条件下番茄流变特性的测定
Pub Date : 2017-04-01 DOI: 10.22067/ifstrj.v1395i0.55948
A. Golmohammadi, Davod Kalanatri
Introduction: Mechanical damages in agricultural products cause wastes directly and indirectly. Bruise damage due to quasi static load is one of the most important reasons of fresh fruit quality loss. Agricultural crops undertake many mechanical loads and physical damages during different stages of harvesting and post-harvest such as handling, transport, storage and processing. In many cases imported loads cause mechanical damages and cellular wall rupture and this rupture leads to perturbation of natural cellular interchanges. This object is one of the important problems of modelling and experimental studies in Biosystems engineering sciences. Tomato is one of the most important horticultural products and a widely produced products in the world. Larg amounts of tomato products are destroyed during the different stages of harvesting, transport and packaging. To study the viscoelastic behavior of agricultural crops, rheology science is used which is the science of biological materials deformation and flow ability under affection of loads at different times. For prediction and classification of materials behavior under different conditions of stress and strain, different rheological models are used. These models include different combinations of metallic body (spring) and Newtonian liquid body (dashpot) that illustrate complex behavior of agricultural products. Determining of factors that affect deformation value of tomato, lead to reduction of product waste. Materials and methods: In this study, the effect of some important parameters such as static loading at three levels (2, 6 and 10 N), storage temperature at two levels (4 and 25 ˚C), loading at two directions for two cultivars (Supper-Beta and Petoerly-CH), were studied on deformation value. Samples were handy harvested at approximate ripeness level (reddish pink) from greenhouse and transported to the Lab. Some physical properties (mass, volume, major and minor diameters, height, sphericity coefficient, surface area) were measured. Samples were subjected to compressive loading using university made apparatus. The Experiments were performed in a fifteen-day period, at two different conditions, ones at temperature 4 ˚C and the other at environmental temperature 25 ˚C, using factorial test in form of completely randomized design. The first test was performed under constant load of 6 N in two directions of fruit axials (Z and Y directions), The second test was performed in three levels 2 and 10 N in direction of calyx face. By indicator, deformation value of tomatoes at 2, 4, 7, 10, and 15 days after loading was investigated. The third test was performed under constant loads of 15 N and deformation values of samples were recorded every 10 mins during a 60-minute period. Results and conclusions: The Results showed at temperature 25 ˚C, with increasing load from 2 up to 10 N, deformation value of the product would be increased about 65%. Increase of deformation value indicates the effect of l
简介:农产品的机械损伤直接或间接地造成浪费。准静态载荷引起的损伤是鲜果品质损失的重要原因之一。农业作物在收获和收获后的不同阶段,如搬运、运输、储存和加工,承受着许多机械载荷和物理损伤。在许多情况下,输入荷载会导致机械损伤和蜂窝壁破裂,这种破裂会导致天然蜂窝式立交的扰动。该目标是生物系统工程科学中建模和实验研究的重要问题之一。番茄是世界上最重要的园艺产品之一,也是一种广泛生产的产品。大量番茄产品在收获、运输和包装的不同阶段被销毁。为了研究农作物的粘弹性行为,应用了流变学,即研究生物材料在不同时间荷载作用下的变形和流动能力的科学。为了预测和分类材料在不同应力和应变条件下的行为,使用了不同的流变模型。这些模型包括金属体(弹簧)和牛顿液体体(阻尼器)的不同组合,它们说明了农产品的复杂行为。确定影响番茄变形值的因素,减少产品浪费。材料和方法:研究了三个水平(2、6和10N)的静载荷、两个水平(4和25˚C)的贮藏温度、两个方向(Supper Beta和Petoerly CH)的载荷等重要参数对变形值的影响。从温室中以接近成熟度的水平(红粉色)方便地采集样品,并将其运至实验室。测量了一些物理特性(质量、体积、大直径和小直径、高度、球形系数、表面积)。使用大学制造的仪器对样品进行压缩加载。实验在15天内,在两种不同的条件下进行,一种是在温度4˚C下,另一种是环境温度25˚C,采用完全随机设计的析因检验。第一次试验在果实轴的两个方向(Z和Y方向)上以6N的恒定载荷进行,第二次试验在果面方向上以2和10N的三个水平进行。通过指标,研究了番茄在加载后2、4、7、10和15天的变形值。第三次试验在15N的恒定载荷下进行,在60分钟的时间内每10分钟记录一次样品的变形值。结果和结论:结果表明,在25˚C的温度下,随着载荷从2增加到10N,产品的变形值将增加约65%。变形值的增加表示加载时间对产品(如西红柿)的影响。这种现象可能是产品在储存过程中体积密度比降低的结果,因为生物化学反应在果实成熟过程中有效,在储存、软化和颜色变化过程中激活细胞壁的破坏性酶。保持果实朝着肾盏面的方向与与肾盏成90度的比例相比,变形较小。这种现象是因为番茄的组织,它的组织在花萼方向比正常方向更硬,因为是花。通过将温度从25℃降低到4˚C,在6N的恒定载荷下,变形减少了约40%。随着温度的降低,生物制品的粘度增加,细胞壁变脆,组织硬度增加。因此,产品在较低温度下的变形值降低似乎是合乎逻辑的。与Petoerly CH相比,超级贝塔品种对压缩静态载荷具有更大的耐久性。在恒定载荷条件下,通用Kelvin流变模型被认为适合于估计应变与时间的关系。
{"title":"Determination of rheological properties of tomato under quasi static loading conditions","authors":"A. Golmohammadi, Davod Kalanatri","doi":"10.22067/ifstrj.v1395i0.55948","DOIUrl":"https://doi.org/10.22067/ifstrj.v1395i0.55948","url":null,"abstract":"Introduction: Mechanical damages in agricultural products cause wastes directly and indirectly. Bruise damage due to quasi static load is one of the most important reasons of fresh fruit quality loss. Agricultural crops undertake many mechanical loads and physical damages during different stages of harvesting and post-harvest such as handling, transport, storage and processing. In many cases imported loads cause mechanical damages and cellular wall rupture and this rupture leads to perturbation of natural cellular interchanges. This object is one of the important problems of modelling and experimental studies in Biosystems engineering sciences. Tomato is one of the most important horticultural products and a widely produced products in the world. Larg amounts of tomato products are destroyed during the different stages of harvesting, transport and packaging. To study the viscoelastic behavior of agricultural crops, rheology science is used which is the science of biological materials deformation and flow ability under affection of loads at different times. For prediction and classification of materials behavior under different conditions of stress and strain, different rheological models are used. These models include different combinations of metallic body (spring) and Newtonian liquid body (dashpot) that illustrate complex behavior of agricultural products. Determining of factors that affect deformation value of tomato, lead to reduction of product waste. \u0000 \u0000Materials and methods: In this study, the effect of some important parameters such as static loading at three levels (2, 6 and 10 N), storage temperature at two levels (4 and 25 ˚C), loading at two directions for two cultivars (Supper-Beta and Petoerly-CH), were studied on deformation value. Samples were handy harvested at approximate ripeness level (reddish pink) from greenhouse and transported to the Lab. Some physical properties (mass, volume, major and minor diameters, height, sphericity coefficient, surface area) were measured. Samples were subjected to compressive loading using university made apparatus. The Experiments were performed in a fifteen-day period, at two different conditions, ones at temperature 4 ˚C and the other at environmental temperature 25 ˚C, using factorial test in form of completely randomized design. The first test was performed under constant load of 6 N in two directions of fruit axials (Z and Y directions), The second test was performed in three levels 2 and 10 N in direction of calyx face. By indicator, deformation value of tomatoes at 2, 4, 7, 10, and 15 days after loading was investigated. The third test was performed under constant loads of 15 N and deformation values of samples were recorded every 10 mins during a 60-minute period. \u0000 \u0000Results and conclusions: The Results showed at temperature 25 ˚C, with increasing load from 2 up to 10 N, deformation value of the product would be increased about 65%. Increase of deformation value indicates the effect of l","PeriodicalId":52634,"journal":{"name":"mjlh pjwhshhy `lwm w Sny` Gdhyy yrn","volume":"1396 1","pages":"858-866"},"PeriodicalIF":0.0,"publicationDate":"2017-04-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"46043522","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 1
Investigation of Psychochemical and Functional Properties of Pomegranate (Punica granatum (L.) cv. Rabab) Juice Concentrate During Storage Period at Different Temperatures 石榴浓缩汁在不同温度下贮藏期间的理化性质和功能特性研究
Pub Date : 2017-04-01 DOI: 10.22067/IFSTRJ.V1395I0.55415
M. Farahmand, M. Golmakani, A. Farahnaky, G. Mesbahi
کنسانتره صنعتی آب انار رقم رباب به مدت 20 هفته در دماهای 20- ،4، 20 و 35 درجه سلسیوس نگهداری و شاخص های شکل گیری کدورت ثانویه، رنگ (L*a*b*)، خصوصیات رئولوژیکی، ترکیبات زیست فعال (ترکیبات فنولی و فلاوونوئید ی کل) و خصوصیات آنتی اکسیدانی (روش هایDPPH و FRAP) برای تعیین بهترین شرایط نگهداری مورد ارزیابی قرار گرفت. نمونه های نگهداری شده در دمای 35 درجه سیلسیوس در 4 هفته آخر دوره نگهداری دارای کدورت ثانویه بودند. . اگرچه نمونه های شاهد رفتار رقیق شونده با برش داشتند، اما پس از دوره نگهداری رفتار غلیظ شونده با برش از خود نشان دادند. بین ارزش L* بین نمونه ها نگهداری شده در دماهای 20-، 4و 20 درجه سلسیوس تفاوت معنی داری مشاهده نشد. ارزش a* و b* نمونه های نگهداری شده در دماهای 20- و 4 درجه سلسیوس به مدت 14 هفته روند کاهشی مشابهی را نشان دادند. میزان محتوای فنولی و خصوصیات آنتی اکسیدانی (هر دو روش DPPHو FRAP) با افزایش دما و مدت زمان نگهداری کاهش یافتند اما ترکیبات فلاونوئیدی با افزایش دما و زمان نگهداری به شکل معنی داری افزایش یافتند. به طورکلی، دمای 4 درجه سلسیوس به مدت 14 هفته، بهترین شرایط دمای نگهداری برای حفظ کیفیت و کاهش هزینه های نگهداری محصول می باشد.
在20、4、20和35摄氏度的温度下,RBM水的浓度为20周,并且形成第二个代码、颜色(L*a*b*)、生物特性、活性生物化合物和抗生素。对酸性(DPPH和FRAP方法)进行评估,以确定最佳保存条件。过去四周在35摄氏度的温度下储存的样本是二次储存期。尽管证人有争强好胜的行为,但他们在被拘留后表现出来了。在20、4和20摄氏度的温度下没有观察到样品之间的L*值。a*和b*的值显示在20至4摄氏度的相同温度下降低14周。工艺量和氧气性能(DPPH和FRAP方法)随着温度和储存时间的增加而降低,但氟的组合随着温度和时间的增加。在土耳其,4摄氏度的温度持续14周是提高储存质量和降低储存成本的最佳保护条件。
{"title":"Investigation of Psychochemical and Functional Properties of Pomegranate (Punica granatum (L.) cv. Rabab) Juice Concentrate During Storage Period at Different Temperatures","authors":"M. Farahmand, M. Golmakani, A. Farahnaky, G. Mesbahi","doi":"10.22067/IFSTRJ.V1395I0.55415","DOIUrl":"https://doi.org/10.22067/IFSTRJ.V1395I0.55415","url":null,"abstract":"کنسانتره صنعتی آب انار رقم رباب به مدت 20 هفته در دماهای 20- ،4، 20 و 35 درجه سلسیوس نگهداری و شاخص های شکل گیری کدورت ثانویه، رنگ (L*a*b*)، خصوصیات رئولوژیکی، ترکیبات زیست فعال (ترکیبات فنولی و فلاوونوئید ی کل) و خصوصیات آنتی اکسیدانی (روش هایDPPH و FRAP) برای تعیین بهترین شرایط نگهداری مورد ارزیابی قرار گرفت. نمونه های نگهداری شده در دمای 35 درجه سیلسیوس در 4 هفته آخر دوره نگهداری دارای کدورت ثانویه بودند. . اگرچه نمونه های شاهد رفتار رقیق شونده با برش داشتند، اما پس از دوره نگهداری رفتار غلیظ شونده با برش از خود نشان دادند. بین ارزش L* بین نمونه ها نگهداری شده در دماهای 20-، 4و 20 درجه سلسیوس تفاوت معنی داری مشاهده نشد. ارزش a* و b* نمونه های نگهداری شده در دماهای 20- و 4 درجه سلسیوس به مدت 14 هفته روند کاهشی مشابهی را نشان دادند. میزان محتوای فنولی و خصوصیات آنتی اکسیدانی (هر دو روش DPPHو FRAP) با افزایش دما و مدت زمان نگهداری کاهش یافتند اما ترکیبات فلاونوئیدی با افزایش دما و زمان نگهداری به شکل معنی داری افزایش یافتند. به طورکلی، دمای 4 درجه سلسیوس به مدت 14 هفته، بهترین شرایط دمای نگهداری برای حفظ کیفیت و کاهش هزینه های نگهداری محصول می باشد.","PeriodicalId":52634,"journal":{"name":"mjlh pjwhshhy `lwm w Sny` Gdhyy yrn","volume":"13 1","pages":"820-829"},"PeriodicalIF":0.0,"publicationDate":"2017-04-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"44394675","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
How appearance features of microwave pre-treatment donut influences consumer acceptance? 微波预处理甜甜圈的外观特征如何影响消费者的接受度?
Pub Date : 2017-04-01 DOI: 10.22067/IFSTRJ.V1395I0.55526
M. Nouri, B. Nasehi, V. Samavati, S. S. Mehdizadeh
در این پژوهش از تکنیک‏های ماشین بینایی به منظور بررسی اثر پیش‏فرآیند مایکروویو بر ویژگی‏های ظاهری دونات استفاده شد. آزمایش‌ها بر اساس روش سطح پاسخ با یک طرح باکس-بنکن طراحی شد. متغیرهای مستقل شامل توان مایکروویو (900-300 وات)، مدت‌زمان پیش‏فرآیند مایکروویو (90-30 ثانیه) و مدت‌زمان سرخ کردن (130-70 ثانیه) بود. همچنین متغیرهای وابسته شامل ویژگی‏های بافت سطحی، شاخص‏های رنگ پوسته، ویژگی‏های ساختار مغز و پذیرش مصرف‏کننده بود. نتایج نشان داد افزایش سطح توان مایکروویو، مدت‌زمان پیش‏فرآیند مایکروویو و مدت‌زمان سرخ کردن سبب افزایش قابل‌توجه زبری سطح نمونه‏ها شد. نتایج همچنین نشان داد اثرات مثبت خطی همه متغیرهای مستقل و اثر منفی درجه دوم توان مایکروویو بر ویژگی‏های ساختار مغز دونات معنی‏دار بود. در مورد رنگ نمونه‏ها، نتایج نشان داد که شاخص‏های L* و a* سطح نمونه‏ها با افزایش سطح همه متغیرهای مستقل به‌طور قابل‌توجهی افزایش یافتند. نتایج حاصل از پذیرش مصرف‏کننده حاکی از تأثیر قابل‌توجه مدت‌زمان سرخ کردن بر نمرات حسی بود. بعلاوه نتایج حاصل از آنالیز همبستگی نشان‌دهنده وجود ارتباط خطی قوی بین ویژگی‏های ظاهری و خصوصیات حسی دونات بود. این نتایج به‌خوبی بیان‌کننده تأثیر قابل‌توجه اطلاعات مربوط به ظاهر نمونه‏های دونات پیش‏فرآیند شده با مایکروویو بر پذیرش مصرف‌کننده بود. همچنین نتایج آنالیز همبستگی نشان داد تکنیک‌های ماشین بینایی قادر به پیش‌بینی پذیرش مصرف‏کننده هستند.
在这项研究中,视觉机械技术被用于研究微波预测对甜甜圈外观的影响。آدایبهابراادروةددحپا1740دبا。直接变化包括微波功率(900-300瓦)、微波预测时间(90-30秒)和发红时间(130-70秒)。因变量还包括高水平、肤色、大脑结构特征和可接受的特性。结果表明,微波功率的增加、微波预测的延迟和样品水平的延迟都会增加。研究结果还表明,所有直接变化的积极影响和第二次微波功率对恐龙大脑结构的消极影响。在样本颜色上,结果表明,通过增加所有单个变量的水平,L*和a*部分显著增加。消费者接受的结果是由于长期制冷的影响。此外,协同分析的结果是视觉特征和感官特征之间有很强的联系。这一结果很好地解释了与甜甜圈的预定样品相关的信息对微波接受的影响。协作分析的结果表明,视觉机器能够预测接受度。
{"title":"How appearance features of microwave pre-treatment donut influences consumer acceptance?","authors":"M. Nouri, B. Nasehi, V. Samavati, S. S. Mehdizadeh","doi":"10.22067/IFSTRJ.V1395I0.55526","DOIUrl":"https://doi.org/10.22067/IFSTRJ.V1395I0.55526","url":null,"abstract":"در این پژوهش از تکنیک‏های ماشین بینایی به منظور بررسی اثر پیش‏فرآیند مایکروویو بر ویژگی‏های ظاهری دونات استفاده شد. آزمایش‌ها بر اساس روش سطح پاسخ با یک طرح باکس-بنکن طراحی شد. متغیرهای مستقل شامل توان مایکروویو (900-300 وات)، مدت‌زمان پیش‏فرآیند مایکروویو (90-30 ثانیه) و مدت‌زمان سرخ کردن (130-70 ثانیه) بود. همچنین متغیرهای وابسته شامل ویژگی‏های بافت سطحی، شاخص‏های رنگ پوسته، ویژگی‏های ساختار مغز و پذیرش مصرف‏کننده بود. نتایج نشان داد افزایش سطح توان مایکروویو، مدت‌زمان پیش‏فرآیند مایکروویو و مدت‌زمان سرخ کردن سبب افزایش قابل‌توجه زبری سطح نمونه‏ها شد. نتایج همچنین نشان داد اثرات مثبت خطی همه متغیرهای مستقل و اثر منفی درجه دوم توان مایکروویو بر ویژگی‏های ساختار مغز دونات معنی‏دار بود. در مورد رنگ نمونه‏ها، نتایج نشان داد که شاخص‏های L* و a* سطح نمونه‏ها با افزایش سطح همه متغیرهای مستقل به‌طور قابل‌توجهی افزایش یافتند. نتایج حاصل از پذیرش مصرف‏کننده حاکی از تأثیر قابل‌توجه مدت‌زمان سرخ کردن بر نمرات حسی بود. بعلاوه نتایج حاصل از آنالیز همبستگی نشان‌دهنده وجود ارتباط خطی قوی بین ویژگی‏های ظاهری و خصوصیات حسی دونات بود. این نتایج به‌خوبی بیان‌کننده تأثیر قابل‌توجه اطلاعات مربوط به ظاهر نمونه‏های دونات پیش‏فرآیند شده با مایکروویو بر پذیرش مصرف‌کننده بود. همچنین نتایج آنالیز همبستگی نشان داد تکنیک‌های ماشین بینایی قادر به پیش‌بینی پذیرش مصرف‏کننده هستند.","PeriodicalId":52634,"journal":{"name":"mjlh pjwhshhy `lwm w Sny` Gdhyy yrn","volume":"13 1","pages":"867-879"},"PeriodicalIF":0.0,"publicationDate":"2017-04-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"44151010","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
بررسی ویژگیهای ساختاری، ریختشناسی، ساختمانی و حرارتی نشاسته سورگوم سفید 白色替代品的建筑、工程、施工和热量
Pub Date : 2017-04-01 DOI: 10.22067/IFSTRJ.V1395I0.55234
احمد احتیاطی, فخری شهیدی, آرش کوچکی, سیدمحمدعلی رضوی, مهسا مجذوبی
Introduction: Sorghum (Sorghum bicolor) is a tropical plant and has the fifth ranking of world cereals production. One of the important aspects of sorghum is drought tolerance and little input need during growth which has made that suitable for cultivation in semiarid regions. Due to the presence of tannin compounds in internal part of sorghum grains and low digestion of cooked protein, sorghum flour consumption is limited. Sorghum grain contains more than 70% starch which is an important tasteless ingredient in food formulas, as the main source of energy and thickening and gelling agent. Extraction of starch from sorghum in regarding to its nutritional problems is a good solution for extension of sorghum uses in food industry. Starch is a semi crystalline structure consisted on linear amylose and branched amylopectin molecules packed in granules. Ratio of these two molecules and their molecular short order and macrostructure and size and shape of granules determine functional properties of starch in the final product. Starch properties is depended on genetic residues so that starches from tubers have distinct differences with cereal starches even obvious differences exists between cereal starches and varieties. In this study we have investigated chemical, morphological, structural and thermal properties of starches four white sorghum line. Material and methods: White sorghum grains were prepared from local farms with line numbers KDFGS1, KDFGS6, KDFGS9 and KDFGS20. Starches were extracted sorghum lines using alkaline steeping method and further purified using toluene-water-salt solution. Chemical parameters were determined including protein by Kjeldahl digestion method, lipid by soxhlet extractor, ash by burning in furnace, moisture by oven drying and amylose content by iodine binding colorimitry,. Light microscopy coupled with digital camera was used for granules shape and size determination moreover surface properties and morphology of granules was observed using scanning electron microscopy technique. Color of starches were determined with hunterlab colorimeter. To evaluate crystalline structure of sample i.e. type of crystals and degree of crystallinity, starches first were conditioned in desiccator containing saturated aqueous sodium chloride solution at 25°C for a week then X-ray diffraction of sample in diffraction angels from 4-40° was determined. Thermal properties of crystals melting or gelatinization were measured using differential scanning calorimetry of starch in deionized water in temperatures from 20-120°C with heating rate of 10°C/min .From heat flow changes over temperature, temperature of onset, peak and conclusion points of crystalline structure melting and its required enthalpy were calculated. Functional groups of starches were investigated using FTIR technique to observe. Results & Discussion: Isolated starches had appropriate quality due to low amount of protein (<%0.36), lipid (<%0.11) and ash (<%0.53) and no signi
高粱(Sorghum bicolor)是一种热带植物,世界谷物产量排名第五。高粱的一个重要特点是耐旱性强,生长过程中需要量小,适合半干旱地区栽培。由于高粱籽粒内部存在单宁化合物,并且煮熟的蛋白质消化率低,因此高粱粉的消费量有限。高粱籽粒含有70%以上的淀粉,是食品配方中重要的无味成分,是主要的能量来源和增稠胶凝剂。从高粱中提取淀粉,解决了高粱的营养问题,为扩大高粱在食品工业中的应用提供了良好的解决方案。淀粉是由直链淀粉和支链淀粉组成的半晶体结构。这两种分子的比例及其分子的短序和宏观结构以及颗粒的大小和形状决定了淀粉在最终产品中的功能特性。淀粉的性质取决于遗传残基,因此块茎淀粉与谷物淀粉有明显差异,甚至在谷物淀粉和品种之间也存在明显差异。本研究对淀粉四号白高粱系的化学、形态、结构和热性能进行了研究。材料和方法:选用当地农场制备的白高粱籽粒,品系号为KDFGS1、KDFGS6、KDFGS9和KDFGS20。以高粱品系为研究对象,采用碱浸法提取淀粉,并用甲苯-水-盐溶液提纯淀粉。化学参数包括:蛋白质用凯氏定溶法测定,脂肪用索氏萃取法测定,灰分用炉内燃烧法测定,水分用烘箱干燥法测定,直链淀粉用碘结合比色法测定。采用光学显微镜结合数码相机对颗粒的形状和大小进行了测定,并用扫描电镜技术对颗粒的表面性质和形貌进行了观察。用亨特比色仪测定淀粉的颜色。为了评估样品的晶体结构,即晶体类型和结晶度,首先将淀粉放在含有饱和氯化钠水溶液的干燥器中,在25°C下干燥一周,然后测定样品在4-40°衍射角范围内的x射线衍射。采用差示扫描量热法,在温度为20 ~ 120℃、升温速率为10℃/min的去离子水中测定了淀粉晶体熔化或糊化的热性能,并根据热流随温度的变化,计算了晶体结构熔化的起始温度、峰值和结束点及其所需焓。用FTIR技术对淀粉中的官能团进行了研究。结果与讨论:分离得到的淀粉蛋白(<%0.36)、脂质(<%0.11)、灰分(<%0.53)含量较低,质量适宜,淀粉样品内杂质含量无显著差异,表明提取方法能有效地将淀粉颗粒从周围基质中分离出来。由于表观直链淀粉含量在27.2 ~ 30.7%之间,属于普通淀粉(蜡质或高直链淀粉),而KDFGS6系淀粉的直链淀粉含量明显高于普通淀粉,这是由于遗传多样性的差异导致淀粉合成酶的差异,从而产生线状和支状α葡聚糖的合成活性不同。淀粉呈白色,色相角为103˚,颜色饱和度为3%,与LAB颜色参数无差异。淀粉的颜色与文献中报道的玉米淀粉的值相当。光镜图像显示,淀粉颗粒大小分布几乎相似,但KDFGS9系淀粉颗粒较小(直径小于15µm)。不同品系的淀粉颗粒平均直径在12.07 ~ 12.99µm之间,比小麦淀粉等其他谷物淀粉小。扫描电镜显示高粱淀粉呈球状或不规则状,表面有气孔。x射线衍射分析表明,淀粉结晶度在25-31%之间,在15°、17°、18°和23°衍射角处存在强衍射,所有淀粉均呈现A型衍射模式,部分淀粉在A型衍射模式的同时还呈现v型晶体模式。在谷物淀粉中,由于直链淀粉螺旋内部部分的疏水性,存在内部脂质,主要是磷脂,与直链淀粉分子形成复合物,这些复合物聚集形成衍射图样,称为v型结晶。结晶熔解起始温度为69 ~ 70℃,熔解峰值温度为73 ~ 74℃,熔解焓为8 ~ 10 J/g。 结果表明,起始温度越低的淀粉,由于晶体缺陷,糊化范围越大。所有淀粉的FTIR光谱吸收模式相似,吸收值差异较小。并将800 ~ 1300 cm-1范围内吸光度计算结晶度的新方法应用于淀粉的FTIR光谱,该光谱与x射线衍射光谱数据不相关。结论:总的结论是,从白高粱品系中提取的淀粉,在某些性质上略有不同,与常见的工业原生淀粉相比,根据文献发表的数据,它们与普通玉米淀粉相似
{"title":"بررسی ویژگیهای ساختاری، ریختشناسی، ساختمانی و حرارتی نشاسته سورگوم سفید","authors":"احمد احتیاطی, فخری شهیدی, آرش کوچکی, سیدمحمدعلی رضوی, مهسا مجذوبی","doi":"10.22067/IFSTRJ.V1395I0.55234","DOIUrl":"https://doi.org/10.22067/IFSTRJ.V1395I0.55234","url":null,"abstract":"Introduction: Sorghum (Sorghum bicolor) is a tropical plant and has the fifth ranking of world cereals production. One of the important aspects of sorghum is drought tolerance and little input need during growth which has made that suitable for cultivation in semiarid regions. Due to the presence of tannin compounds in internal part of sorghum grains and low digestion of cooked protein, sorghum flour consumption is limited. Sorghum grain contains more than 70% starch which is an important tasteless ingredient in food formulas, as the main source of energy and thickening and gelling agent. Extraction of starch from sorghum in regarding to its nutritional problems is a good solution for extension of sorghum uses in food industry. Starch is a semi crystalline structure consisted on linear amylose and branched amylopectin molecules packed in granules. Ratio of these two molecules and their molecular short order and macrostructure and size and shape of granules determine functional properties of starch in the final product. Starch properties is depended on genetic residues so that starches from tubers have distinct differences with cereal starches even obvious differences exists between cereal starches and varieties. In this study we have investigated chemical, morphological, structural and thermal properties of starches four white sorghum line. \u0000 \u0000Material and methods: White sorghum grains were prepared from local farms with line numbers KDFGS1, KDFGS6, KDFGS9 and KDFGS20. Starches were extracted sorghum lines using alkaline steeping method and further purified using toluene-water-salt solution. Chemical parameters were determined including protein by Kjeldahl digestion method, lipid by soxhlet extractor, ash by burning in furnace, moisture by oven drying and amylose content by iodine binding colorimitry,. Light microscopy coupled with digital camera was used for granules shape and size determination moreover surface properties and morphology of granules was observed using scanning electron microscopy technique. Color of starches were determined with hunterlab colorimeter. To evaluate crystalline structure of sample i.e. type of crystals and degree of crystallinity, starches first were conditioned in desiccator containing saturated aqueous sodium chloride solution at 25°C for a week then X-ray diffraction of sample in diffraction angels from 4-40° was determined. Thermal properties of crystals melting or gelatinization were measured using differential scanning calorimetry of starch in deionized water in temperatures from 20-120°C with heating rate of 10°C/min .From heat flow changes over temperature, temperature of onset, peak and conclusion points of crystalline structure melting and its required enthalpy were calculated. Functional groups of starches were investigated using FTIR technique to observe. \u0000 \u0000Results & Discussion: Isolated starches had appropriate quality due to low amount of protein (<%0.36), lipid (<%0.11) and ash (<%0.53) and no signi","PeriodicalId":52634,"journal":{"name":"mjlh pjwhshhy `lwm w Sny` Gdhyy yrn","volume":"13 1","pages":"393-404"},"PeriodicalIF":0.0,"publicationDate":"2017-04-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"46711976","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Effect of Hydroxy propyl methyl cellulose gum on qualitative properties of free gluten baguette bread 羟基丙基甲基纤维素胶对无筋法棍面包品质的影响
Pub Date : 2017-04-01 DOI: 10.22067/IFSTRJ.V1395I0.50478
S. Movahhed, E. Kakaei, H. A. Chenarbon
مصرف گلوتن در برخی افراد ازجمله بیماران سلیاکی ایجاد عوارض نامطلوبی می‌کند. مهم‌ترین روش درمان سلیاک، استفاده از رژیم غذایی بدون گلوتن می‌باشد ضمن آن که می‌بایست مشتقات غلاتی نظیر گندم از رژیم غذایی آنها حذف و با آرد سایر غلات بدون گلوتن، جایگزین گردد. هدف از پژوهش حاضر بهبود عملکرد کیفی نان باگت تولید شده از آرد ذرت به همراه آرد سیب زمینی، با افزودن صمغ‌ هیدروکسی پروپیل متیل سلولز در چهار سطح (25/0 ، 5/0 ، 75/0 و 1 درصد وزنی - وزنی بر پایه آرد) بود. با توجه به نتایج، تیمار حاوی1درصد صمغ، از بیشترین و تیمار شاهد(فاقد صمغ مذکور) از کمترین مقدار از لحاظ ویژگی‌های شیمیایی نظیر رطوبت، خاکستر، پروتئین و فیبر برخوردار بودند. همچنین با افزایش صمغ، میزان بازدهی خمیر و حجم نان در تیمارها نسبت به شاهد افزایش اما بازدهی نان کاهش یافت. قابل توجه این‌که بیشترین بازدهی نان در تیمار شاهد مشاهده شد. با توجه به نتایج حاصل از ارزیابی ویژگی‌های حسی نمونه‌های نان باگت بدون گلوتن، تیمارهای حاوی یک درصد صمغHPMC از بهترین امتیاز برخوردار بودند. همچنین با توجه به نتایج آزمون بیاتی به روش حسی و دستگاهی، در فواصل زمانی 24، 48 و 72 ساعت پس از پخت، تیمار حاوی 1 درصد صمغHPMC از کمترین و شاهد از بالاترین میزان بیاتی برخوردار بودند.
在一些人身上使用饕餮,包括西莉亚的病人,会产生意想不到的后果。治疗Celiac最重要的方法是取代无麸质食物制度,同时必须将其从他们的饮食制度中删除,并用一系列其他无麸质奴隶取而代之。这项研究的目的是提高由土豆算法生产的面包袋的质量,使羟丙基金属细胞在四个水平上增加(25/0、5/0、75/0和1%重量基准)。因此,镜片中含有1%的镜片,这是目击者最常见的镜片,不太可能含有转子、土壤、蛋白质和纤维等化学物质。此外,团队中阈值的增加、肝脏的增加和食物供应的增加都有所减少。值得注意的是,计时器中的大部分食物供应都是可见的。با8;نگلو1578; 3;ند。此外,由于测试结果,基本上在烹饪后24、48和72小时,传感器和设备系统包含了1%的HSync容器,并见证了最高的收入率。
{"title":"Effect of Hydroxy propyl methyl cellulose gum on qualitative properties of free gluten baguette bread","authors":"S. Movahhed, E. Kakaei, H. A. Chenarbon","doi":"10.22067/IFSTRJ.V1395I0.50478","DOIUrl":"https://doi.org/10.22067/IFSTRJ.V1395I0.50478","url":null,"abstract":"مصرف گلوتن در برخی افراد ازجمله بیماران سلیاکی ایجاد عوارض نامطلوبی می‌کند. مهم‌ترین روش درمان سلیاک، استفاده از رژیم غذایی بدون گلوتن می‌باشد ضمن آن که می‌بایست مشتقات غلاتی نظیر گندم از رژیم غذایی آنها حذف و با آرد سایر غلات بدون گلوتن، جایگزین گردد. هدف از پژوهش حاضر بهبود عملکرد کیفی نان باگت تولید شده از آرد ذرت به همراه آرد سیب زمینی، با افزودن صمغ‌ هیدروکسی پروپیل متیل سلولز در چهار سطح (25/0 ، 5/0 ، 75/0 و 1 درصد وزنی - وزنی بر پایه آرد) بود. با توجه به نتایج، تیمار حاوی1درصد صمغ، از بیشترین و تیمار شاهد(فاقد صمغ مذکور) از کمترین مقدار از لحاظ ویژگی‌های شیمیایی نظیر رطوبت، خاکستر، پروتئین و فیبر برخوردار بودند. همچنین با افزایش صمغ، میزان بازدهی خمیر و حجم نان در تیمارها نسبت به شاهد افزایش اما بازدهی نان کاهش یافت. قابل توجه این‌که بیشترین بازدهی نان در تیمار شاهد مشاهده شد. با توجه به نتایج حاصل از ارزیابی ویژگی‌های حسی نمونه‌های نان باگت بدون گلوتن، تیمارهای حاوی یک درصد صمغHPMC از بهترین امتیاز برخوردار بودند. همچنین با توجه به نتایج آزمون بیاتی به روش حسی و دستگاهی، در فواصل زمانی 24، 48 و 72 ساعت پس از پخت، تیمار حاوی 1 درصد صمغHPMC از کمترین و شاهد از بالاترین میزان بیاتی برخوردار بودند.","PeriodicalId":52634,"journal":{"name":"mjlh pjwhshhy `lwm w Sny` Gdhyy yrn","volume":" ","pages":""},"PeriodicalIF":0.0,"publicationDate":"2017-04-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"49219390","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Study of oil fatty acid profile, functional properties and antioxidants activity of hydrolyzate produced from rainbow trout (Oncorhynchus mykiss) viscera by application commercial enzymes 应用商业酶法研究虹鳟内脏水解产物的油脂脂肪酸组成、功能特性及抗氧化活性
Pub Date : 2017-04-01 DOI: 10.22067/IFSTRJ.V1395I0.53714
Soheyl Reyhani Poul, S. A. Jafarpour, R. Safari
Introduction: With the growing population and following the efforts of food production industries, more waste is produced which can be recovered by adding value and brought them back into the cycle of production and consumption. The reason behind is firstly the reduction of waste and secondly the economic importance of value added resultant products. Aquaculture sector produces large volume of wastes including the head, tail, fins, spine, and most importantly their viscera. If the waste managed properly, valuable materials such as hydrolyzed protein powder (the resulting waste hydrolysis using proteases enzymes) and fish oil (byproduct of enzymatic hydrolysis) can be produced. In this study rainbow trout waste was chosen, due to its large volume production in the country. The functional properties and antioxidant activity of hydrolysates as well as the oil fatty acid profile are the main factors to be considered. This study was aimed to investigate the hydrolysis of rainbow trout viscera (oncorhynchus mykiss) by protamex and neutrase enzymes individually and compare the functional properties and antioxidants activity of protein hydrolysate as well as analyze the fatty acid profile of fish oil obtained as by-product of enzymatic hydrolysis process. Materials and methods: Rainbow trout viscera (Oncorhynchus mykiss) were obtained from the fish market in Sari and transported in ice containers to the laboratory. Protamex and neutrase enzymes were purchased from Novozymes Company and protein hydrolysates prepared enzymatically according to the method of Guerard et al. (2002). Proximate analysis was carried out according to the procedures outlined by the AOAC (1995). Degree of hydrolysis determined as described by Hoyle and Merritt (1994). Peptide chain length (PCL) was measured using the method of Adler-Nissen and Olsen (1979). Protein recovery (PR) determined using the method used by Ovissipour et al (2009). Protein solubility for hydrolysates was determined using the method of Robinson and Hodgen (1940). Foam stability index was measured according to the method described by Sathe and Salunkhe (1981). Water holding capacity (WHC) was determined using the method of Rodriguez-Ambriz et al. (2005). DPPH radical-scavenging activity was measured using the method of Yen and Wu (1999). Reducing power was determined by the method of Oyaiza (1986).The chelating activity on Fe2+ was determined, using the method of Decker and Welch (1990). Results & Discussion: Protamex leads to the production of protein powder with higher degree of hydrolysis (34.76 ± 2.92%) and protein recovery (68/16 ± 1.98%) compared to neutrase (p 0.05) despite the difference in L* value. The viscera oil contains 34% monounsaturated, 34.49% polyunsaturated and 31.4% saturated fatty acid. Apart from pH 4 (isoelectric point), the solubility of both protein powders in water was remarkable (more than 90%). The foam activity and stability index of hydrolyzate produced by protamex were more
引言:随着人口的增长和食品生产行业的努力,产生了更多的废物,这些废物可以通过增加价值来回收,并将其带回生产和消费循环中。背后的原因首先是减少浪费,其次是增值产品的经济重要性。水产养殖部门产生大量废物,包括头部、尾部、鳍、脊椎,最重要的是内脏。如果废物管理得当,可以生产有价值的材料,如水解蛋白粉(使用蛋白酶水解产生的废物)和鱼油(酶水解的副产品)。在这项研究中,由于虹鳟鱼在该国的产量很大,因此选择了虹鳟废弃物。水解产物的功能特性和抗氧化活性以及油脂脂肪酸的性质是需要考虑的主要因素。本研究旨在研究鱼精蛋白和中性蛋白酶对虹鳟内脏的水解作用,比较蛋白质水解产物的功能特性和抗氧化活性,并分析酶水解过程中副产物鱼油的脂肪酸组成。材料和方法:从萨里的鱼类市场获得虹鳟内脏(Oncorhynchus mykiss),并用冰柜运输到实验室。Protamex和中性酶购自Novozymes公司,蛋白质水解产物根据Guerard等人(2002)的方法酶法制备。根据AOAC(1995)概述的程序进行近似分析。水解度如Hoyle和Merritt(1994)所述测定。使用Adler-Nissen和Olsen(1979)的方法测量肽链长度(PCL)。使用Ovisisspour等人(2009)使用的方法测定蛋白质回收率(PR)。使用Robinson和Hodgen(1940)的方法测定水解产物的蛋白质溶解度。根据Sathe和Salunkhe(1981)描述的方法测量泡沫稳定性指数。持水量(WHC)采用Rodriguez-Ambriz等人(2005)的方法进行测定。使用Yen和Wu(1999)的方法测量DPPH自由基清除活性。还原力采用Oyaiza(1986)的方法测定。对Fe2+的螯合活性采用Decker和Welch(1990)的方法进行测定。结果与讨论:尽管L*值存在差异,但与中性酶相比,Protamex可生产水解度(34.76±2.92%)和蛋白质回收率(68/16±1.98%)更高的蛋白粉(p0.05)。内脏油中含有34%的单不饱和脂肪酸、34.49%的多不饱和脂肪和31.4%的饱和脂肪酸。除了pH 4(等电点)外,两种蛋白粉末在水中的溶解度都很显著(超过90%)。鱼精蛋白水解产物的泡沫活性和稳定性指数比中性酶水解产物更理想,而在pH6时,这些指数分别达到200.13±9.31%和135.6±5.64%的最大值。此外,两种水解产物的持水能力测定为约4.5 ml/g蛋白质(p>0.05)。与中性酶产生的水解产物相比,Protamex导致产生具有更高DPPH自由基清除活性的蛋白质粉末。相反,中性酶产生的水解产物的还原力高于鱼精蛋白(p0.05)。
{"title":"Study of oil fatty acid profile, functional properties and antioxidants activity of hydrolyzate produced from rainbow trout (Oncorhynchus mykiss) viscera by application commercial enzymes","authors":"Soheyl Reyhani Poul, S. A. Jafarpour, R. Safari","doi":"10.22067/IFSTRJ.V1395I0.53714","DOIUrl":"https://doi.org/10.22067/IFSTRJ.V1395I0.53714","url":null,"abstract":"Introduction: With the growing population and following the efforts of food production industries, more waste is produced which can be recovered by adding value and brought them back into the cycle of production and consumption. The reason behind is firstly the reduction of waste and secondly the economic importance of value added resultant products. Aquaculture sector produces large volume of wastes including the head, tail, fins, spine, and most importantly their viscera. If the waste managed properly, valuable materials such as hydrolyzed protein powder (the resulting waste hydrolysis using proteases enzymes) and fish oil (byproduct of enzymatic hydrolysis) can be produced. In this study rainbow trout waste was chosen, due to its large volume production in the country. The functional properties and antioxidant activity of hydrolysates as well as the oil fatty acid profile are the main factors to be considered. This study was aimed to investigate the hydrolysis of rainbow trout viscera (oncorhynchus mykiss) by protamex and neutrase enzymes individually and compare the functional properties and antioxidants activity of protein hydrolysate as well as analyze the fatty acid profile of fish oil obtained as by-product of enzymatic hydrolysis process. \u0000 \u0000Materials and methods: Rainbow trout viscera (Oncorhynchus mykiss) were obtained from the fish market in Sari and transported in ice containers to the laboratory. Protamex and neutrase enzymes were purchased from Novozymes Company and protein hydrolysates prepared enzymatically according to the method of Guerard et al. (2002). Proximate analysis was carried out according to the procedures outlined by the AOAC (1995). Degree of hydrolysis determined as described by Hoyle and Merritt (1994). Peptide chain length (PCL) was measured using the method of Adler-Nissen and Olsen (1979). Protein recovery (PR) determined using the method used by Ovissipour et al (2009). Protein solubility for hydrolysates was determined using the method of Robinson and Hodgen (1940). Foam stability index was measured according to the method described by Sathe and Salunkhe (1981). Water holding capacity (WHC) was determined using the method of Rodriguez-Ambriz et al. (2005). DPPH radical-scavenging activity was measured using the method of Yen and Wu (1999). Reducing power was determined by the method of Oyaiza (1986).The chelating activity on Fe2+ was determined, using the method of Decker and Welch (1990). \u0000 \u0000Results & Discussion: Protamex leads to the production of protein powder with higher degree of hydrolysis (34.76 ± 2.92%) and protein recovery (68/16 ± 1.98%) compared to neutrase (p 0.05) despite the difference in L* value. The viscera oil contains 34% monounsaturated, 34.49% polyunsaturated and 31.4% saturated fatty acid. Apart from pH 4 (isoelectric point), the solubility of both protein powders in water was remarkable (more than 90%). The foam activity and stability index of hydrolyzate produced by protamex were more","PeriodicalId":52634,"journal":{"name":"mjlh pjwhshhy `lwm w Sny` Gdhyy yrn","volume":"14 1","pages":"162-176"},"PeriodicalIF":0.0,"publicationDate":"2017-04-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"47264024","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
EVALUATION THE PHYSICOCHEMICAL AND MECHANICAL PROPERTIES OF BITTERVETCH SEED (VICIAERVILIA) AND THE FUNCTIONAL PROPERTIES OF ITS FLOUR 苦薇子理化力学性能及其面粉功能性能的评价
Pub Date : 2017-03-21 DOI: 10.22067/IFSTRJ.V1395I0.57362
M. Taghizadeh, B. Shokrollahi, F. Hamedi
Due to the need to find new protein sources with considering the fact that the bitter vetch seed has high levels of protein content, physicochemical and mechanical properties of bitter vetch seed and functional properties of its flour were evaluated in this study. The effects of altering the pH on protein solubility, foaming capacity, foaming stability, emulsion capacity and emulsion stability were studied. The average length, width and height of the grains were 3.5638 mm, 3.6197 mm and 3.8365 mm. the arithmetic and the geometric mean diameter, sphericity and the area were 3.6733mm, 3.6701mm, 1. 0318 and 42.405mm2 respectively. The average true density, bulk density and porosity were 1326.6 kg/m3, 0.7962 kg/m3 and 40.2753% respectively. also the average coefficients of static friction of the plywood, glass, rubber, fiberglass and galvanized iron surface layer were 0.4348, 0.1943, 0.4244, 0.3249 and 0.3739 respectively. Flour produced from this seed contains 24% protein and 9% fat. water and oil absorbing capacity were obtained 2.01 ±0.01 and 1.77±0.03 respectively (grams of water or oil per grams of sample). The results also showed that changes in pH, affected the solubility, foaming capacity, foaming stability, emulsion capacity and emulsion stability of bitter vetch flour.
考虑到苦豌豆籽蛋白质含量高,需要寻找新的蛋白质来源,本研究对苦豌豆籽的理化、力学特性及其面粉的功能特性进行了评价。研究了pH变化对蛋白溶解度、发泡能力、发泡稳定性、乳状液容量和乳状液稳定性的影响。晶粒的平均长、宽、高分别为3.5638 mm、3.6197 mm和3.8365 mm,算术和几何平均直径、球度和面积分别为3.6733mm、3.6701mm和3.6701mm。分别为0318和42.405mm2。平均真密度、容重和孔隙度分别为1326.6 kg/m3、0.7962 kg/m3和40.2753%。胶合板、玻璃、橡胶、玻璃纤维和镀锌铁面层的平均静摩擦系数分别为0.4348、0.1943、0.4244、0.3249和0.3739。由这种种子制成的面粉含有24%的蛋白质和9%的脂肪。吸水性和吸油量分别为2.01±0.01和1.77±0.03(每克样品的水或油的克数)。结果还表明,pH的变化对苦豌豆粉的溶解度、发泡能力、发泡稳定性、乳化能力和乳化稳定性都有影响。
{"title":"EVALUATION THE PHYSICOCHEMICAL AND MECHANICAL PROPERTIES OF BITTERVETCH SEED (VICIAERVILIA) AND THE FUNCTIONAL PROPERTIES OF ITS FLOUR","authors":"M. Taghizadeh, B. Shokrollahi, F. Hamedi","doi":"10.22067/IFSTRJ.V1395I0.57362","DOIUrl":"https://doi.org/10.22067/IFSTRJ.V1395I0.57362","url":null,"abstract":"Due to the need to find new protein sources with considering the fact that the bitter vetch seed has high levels of protein content, physicochemical and mechanical properties of bitter vetch seed and functional properties of its flour were evaluated in this study. The effects of altering the pH on protein solubility, foaming capacity, foaming stability, emulsion capacity and emulsion stability were studied. The average length, width and height of the grains were 3.5638 mm, 3.6197 mm and 3.8365 mm. the arithmetic and the geometric mean diameter, sphericity and the area were 3.6733mm, 3.6701mm, 1. 0318 and 42.405mm2 respectively. The average true density, bulk density and porosity were 1326.6 kg/m3, 0.7962 kg/m3 and 40.2753% respectively. also the average coefficients of static friction of the plywood, glass, rubber, fiberglass and galvanized iron surface layer were 0.4348, 0.1943, 0.4244, 0.3249 and 0.3739 respectively. Flour produced from this seed contains 24% protein and 9% fat. water and oil absorbing capacity were obtained 2.01 ±0.01 and 1.77±0.03 respectively (grams of water or oil per grams of sample). The results also showed that changes in pH, affected the solubility, foaming capacity, foaming stability, emulsion capacity and emulsion stability of bitter vetch flour.","PeriodicalId":52634,"journal":{"name":"mjlh pjwhshhy `lwm w Sny` Gdhyy yrn","volume":"13 1","pages":"38-52"},"PeriodicalIF":0.0,"publicationDate":"2017-03-21","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"47943728","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 1
Isolation and identification of antioxidants components From Cumin seed (Cuminum cyminum) 孜然种子抗氧化成分的分离与鉴定
Pub Date : 2017-03-12 DOI: 10.22067/ifstrj.v1395i0.53312
S. Einafshar, H. Poorazarang, R. Farhoosh, J. Asili
Natural materials are complicated compositions; therefore, a rapid screening of the active antioxidants is being challenged in the literature. Different polarity solvents were applied to isolate four fractions (F1, F2, F3 and F4) of methanolic extract of Cuminum cyminum. Their anti-oxidative properties were tested using radical scavenging and FRAP assays. F3 (with IC50=0.006mg/mL and FRAP= 521.95 mmolFe2+/L) was significantly the most active fraction. Guided isolation through bio-autography on TLC using 1, 1- diphenyl- 2 – picryl- hydrazyl radical (DPPH) as a detection reagent led to the isolation of two antioxidant compounds from F3. F3 was injected to a preparative HPLC with the proper mobile phase (acetonitril: methanol/ water) and isolated two main compounds. These compounds were identified as Luteolin 7 glugoside and Apigenin 7 glucoside by means of 1HNMR and 13CNMR and compare them with references.
天然材料是复杂的成分;因此,快速筛选活性抗氧化剂在文献中受到了挑战。采用不同极性溶剂分离苦菊甲醇提取物的四个组分(F1、F2、F3和F4)。使用自由基清除和FRAP测定来测试它们的抗氧化性能。F3(IC50=0.006mg/mL,FRAP=521.95mmol Fe2+/L)是最具活性的组分。以1,1-二苯基-2-苦丁酰肼自由基(DPPH)为检测试剂,在TLC上通过生物自显影进行引导分离,从F3中分离出两种抗氧化化合物。将F3注射到具有适当流动相(乙腈:甲醇/水)的制备型HPLC中,并分离出两种主要化合物。经1HNMR和13CNMR鉴定为木犀草素7糖苷和芹菜素7糖苷,并与文献进行了比较。
{"title":"Isolation and identification of antioxidants components From Cumin seed (Cuminum cyminum)","authors":"S. Einafshar, H. Poorazarang, R. Farhoosh, J. Asili","doi":"10.22067/ifstrj.v1395i0.53312","DOIUrl":"https://doi.org/10.22067/ifstrj.v1395i0.53312","url":null,"abstract":"Natural materials are complicated compositions; therefore, a rapid screening of the active antioxidants is being challenged in the literature. Different polarity solvents were applied to isolate four fractions (F1, F2, F3 and F4) of methanolic extract of Cuminum cyminum. Their anti-oxidative properties were tested using radical scavenging and FRAP assays. F3 (with IC50=0.006mg/mL and FRAP= 521.95 mmolFe2+/L) was significantly the most active fraction. Guided isolation through bio-autography on TLC using 1, 1- diphenyl- 2 – picryl- hydrazyl radical (DPPH) as a detection reagent led to the isolation of two antioxidant compounds from F3. F3 was injected to a preparative HPLC with the proper mobile phase (acetonitril: methanol/ water) and isolated two main compounds. These compounds were identified as Luteolin 7 glugoside and Apigenin 7 glucoside by means of 1HNMR and 13CNMR and compare them with references.","PeriodicalId":52634,"journal":{"name":"mjlh pjwhshhy `lwm w Sny` Gdhyy yrn","volume":"12 1","pages":"742-749"},"PeriodicalIF":0.0,"publicationDate":"2017-03-12","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"42199026","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
THE EFFECT OF DIFFERENT CONCENTRATIONS OF GLYCEROL ON PROPERTIES OF BLEND FILMS BASED ON POLYVINYL ALCOHOL-ALLYSUMHOMOLOCARPUM SEED GUM 研究了不同浓度的甘油对聚乙烯醇-石竹籽胶共混膜性能的影响
Pub Date : 2017-01-12 DOI: 10.22067/IFSTRJ.V12I5.53473
لیلا منجذب مرودشتی, مسعود یاورمنش, آرش کوچکی
Introduction:Packaging is an important factor in food industry and is dominated by petroleum-derived polymers. Therefore, the amount of research involving the production and characterization of biodegradable films has increased substantially, mainly due to interest in minimizing the ecological impact caused by the use of synthetic packaging materials. Several biopolymers have been exploited to develop eco-friendly food packaging materials. Usually, films based on biopolymers are highly sensitive to environmental conditions and generally present low mechanical resistance. As a result, several researchers have developed films based on mixtures of biopolymers and synthetic polymers. In order to increase the workability and flexibility of biodegradable films, various plasticizers, usually poly-ols, have been widely used, glycerol being one of the most preferred and most studied. Plasticizers reduce intermolecular forces, increase the mobility of the biopolymer chains and thereby improve the mechanical properties of the films. Therefore, the aim of the present study were to investigate the effect of different proportions (20e100% w/w) of plasticizer (glycerol) on physicochemical, mechanical, permeability, surface and thermal properties of biodegradable PVA-AHSG blend films. Polymer blending is one of the most effective methods to have new material with desired properties. Films formed by blending of polymers usually results in modified physical and mechanical properties compared to films made of individual components. Since synthetic polymers are easily obtained and have low production cost, blending of natural and synthetic polymers improves the cost performance ratio of the resulting films. Since Alyssum homolocarpumseed gum (AHSG) is environmentally friendly due to its biodegradability and has good film forming properties, it is considered as a very promising biopolymer. Some synthetic polymers from non-renewable sources are also biodegradable, such as polyvinyl alcohol (PVA). PVA is a synthetic, water soluble polymer with excellent film forming, emulsifying, and adhesive properties. It also imparts good tensile strength (TS) and biodegradability and hence has been used in many biomaterial applications. PVA has also been approved for use in packaging meat and poultry products by the USDA (DeMerlis&Schonek, 2003). AHSG contains free hydroxyl and amine groups, and is therefore miscible with PVA due to the formation of hydrogen bonds. Materials and methods: The aim of this study was to investigate the possibility of producing a novel biodegradable blend film from PVA-AHSG with glycerol as plasticizer in the different concentrations. Films were prepared by the casting method using PVA and AHSG (60:40 ratio). Glycerol was used ac plasticizer because it is compatible with PVA-AHSG blend improving film flexibility, facilitating its handling and preventing cracks. The PVA–AHSG blend film was prepared with different glycerol concentration (20–70%, w/w
简介:包装是食品工业的一个重要因素,主要是石油衍生聚合物。因此,涉及可生物降解薄膜的生产和表征的研究数量大幅增加,主要是因为人们对最大限度地减少使用合成包装材料造成的生态影响感兴趣。一些生物聚合物已被用于开发环保食品包装材料。通常,基于生物聚合物的膜对环境条件高度敏感,并且通常表现出低的机械阻力。因此,一些研究人员开发了基于生物聚合物和合成聚合物混合物的薄膜。为了提高可生物降解膜的可加工性和柔韧性,各种增塑剂,通常是聚乙烯醇,已经被广泛使用,甘油是最优选和研究最多的增塑剂之一。增塑剂减少了分子间作用力,增加了生物聚合物链的迁移率,从而提高了薄膜的机械性能。因此,本研究的目的是研究不同比例(20e100%w/w)的增塑剂(甘油)对可生物降解的PVA-AHSG共混膜的物理化学、力学、渗透性、表面和热性能的影响。聚合物共混是获得具有所需性能的新材料的最有效方法之一。与由单个组分制成的膜相比,通过聚合物共混形成的膜通常会导致物理和机械性能的改变。由于合成聚合物易于获得且生产成本低,天然聚合物和合成聚合物的共混提高了所得膜的性价比。由于Alyssum homocarpumseed gum(AHSG)具有良好的生物降解性和成膜性能,因此被认为是一种非常有前途的生物聚合物。一些来自不可再生资源的合成聚合物也是可生物降解的,例如聚乙烯醇(PVA)。PVA是一种合成的水溶性聚合物,具有优异的成膜、乳化和粘合性能。它还具有良好的拉伸强度(TS)和生物降解性,因此已被用于许多生物材料应用中。PVA也已被美国农业部批准用于肉类和家禽产品的包装(DeMerlis&Schonek,2003)。AHSG含有游离的羟基和胺基,因此由于氢键的形成而与PVA混溶。材料和方法:本研究的目的是研究以不同浓度的甘油为增塑剂,由PVA-AHSG制备新型可生物降解共混膜的可能性。使用PVA和AHSG(60:40比例)通过流延法制备薄膜。甘油之所以被用作增塑剂,是因为它与PVA-AHSG共混物相容,提高了薄膜的柔韧性,有助于处理和防止裂纹。制备了不同甘油浓度(20–70%,w/w)的PVA–AHSG共混膜。测量了其不透明度和颜色等光学性能。研究了薄膜的透水性、含水量、水溶性和密度。对薄膜的机械性能和抗毒素性能进行了评估。用DSC、FTIR和扫描电子显微镜对PVA–AHSG共混膜进行了表征。结果与讨论:本研究结果表明,PVA和AHSG的共混物可以作为一种新型的成膜材料。然而,在不向配方中添加甘油作为增塑剂的情况下,不可能制备PVA-AHSG共混膜。使用浓度为20-70%(w/w)的甘油来制备共混膜。在甘油含量为20%(W/W)的情况下,PVA-AHSG共混膜的厚度(0.065 mm)、吸湿性(118.76%)、水蒸气渗透性(WVP)值(4.9 g mm m-2 kPa−1 d-1)、断裂伸长率(EB)(2.1%)、含水量(22.5%)和水溶性(16.6%)最低,拉伸强度(TS)(64.6 MPa)、杨氏模量(YM)(892 MPa)、密度(0.109 g cm-3)最高,不透明度(0.069 A/mm)和水接触角(74.52◦). PVA-AHSG共混膜中甘油浓度的增加导致水蒸气渗透性和伸长率的增加,而拉伸强度和表面疏水性的降低。甘油浓度的增加显著降低了膜的初始水接触角(p<0.05),从74.52◦ 至37.80◦. 研究表明,增塑剂的加入降低了薄膜的水接触角,进而降低了薄膜疏水性。样品的较高亲水性归因于增塑剂的吸湿性(水结合能力)。增塑剂可以减少生物聚合物分子之间的相互作用,并由于其亲水性而增加溶解度,使聚合物分子具有更高的亲和力来吸引水。随着增塑剂含量的增加,水分含量从22.5%显著增加到40.9%(p<0。 05)。由于甘油具有保水剂的作用,随着甘油增塑膜中水分子数的增加,增塑活性增强。WVP由于其亲水性而随着膜中增塑剂含量的增加而增加。WVP可以与分子上OH基团的数量直接相关。此外,环境条件会显著影响WVP。增塑剂浓度的增加降低了聚合物链之间的分子间力,增加了自由体积和节段运动,使水分子更容易扩散,并产生更高的WVP。薄膜的机械强度由于增塑剂的加入而降低,导致拉伸强度降低和伸长率增加。颜色值的测量表明,随着聚合物共混基质中甘油浓度的增加,b和L值增加,而a值降低。此外,甘油的加入通过氢键促进了PVA、AHSG和甘油之间的相互作用,这反映在无甘油膜的主峰向更高波数的移动上,如FTIR光谱所示。显微镜观察表明,加入甘油作为增塑剂后,表面光滑均匀,没有明显的裂纹、断裂或开口。扫描电子显微镜研究表明,PVA-AHSG共混膜的微观结构对其物理力学性能有着至关重要的影响,这在食品包装应用中具有重要意义。
{"title":"THE EFFECT OF DIFFERENT CONCENTRATIONS OF GLYCEROL ON PROPERTIES OF BLEND FILMS BASED ON POLYVINYL ALCOHOL-ALLYSUMHOMOLOCARPUM SEED GUM","authors":"لیلا منجذب مرودشتی, مسعود یاورمنش, آرش کوچکی","doi":"10.22067/IFSTRJ.V12I5.53473","DOIUrl":"https://doi.org/10.22067/IFSTRJ.V12I5.53473","url":null,"abstract":"Introduction:Packaging is an important factor in food industry and is dominated by petroleum-derived polymers. Therefore, the amount of research involving the production and characterization of biodegradable films has increased substantially, mainly due to interest in minimizing the ecological impact caused by the use of synthetic packaging materials. Several biopolymers have been exploited to develop eco-friendly food packaging materials. Usually, films based on biopolymers are highly sensitive to environmental conditions and generally present low mechanical resistance. As a result, several researchers have developed films based on mixtures of biopolymers and synthetic polymers. In order to increase the workability and flexibility of biodegradable films, various plasticizers, usually poly-ols, have been widely used, glycerol being one of the most preferred and most studied. Plasticizers reduce intermolecular forces, increase the mobility of the biopolymer chains and thereby improve the mechanical properties of the films. Therefore, the aim of the present study were to investigate the effect of different proportions (20e100% w/w) of plasticizer (glycerol) on physicochemical, mechanical, permeability, surface and thermal properties of biodegradable PVA-AHSG blend films. \u0000Polymer blending is one of the most effective methods to have new material with desired properties. Films formed by blending of polymers usually results in modified physical and mechanical properties compared to films made of individual components. Since synthetic polymers are easily obtained and have low production cost, blending of natural and synthetic polymers improves the cost performance ratio of the resulting films. \u0000Since Alyssum homolocarpumseed gum (AHSG) is environmentally friendly due to its biodegradability and has good film forming properties, it is considered as a very promising biopolymer. \u0000Some synthetic polymers from non-renewable sources are also biodegradable, such as polyvinyl alcohol (PVA). PVA is a synthetic, water soluble polymer with excellent film forming, emulsifying, and adhesive properties. It also imparts good tensile strength (TS) and biodegradability and hence has been used in many biomaterial applications. PVA has also been approved for use in packaging meat and poultry products by the USDA (DeMerlis&Schonek, 2003). AHSG contains free hydroxyl and amine groups, and is therefore miscible with PVA due to the formation of hydrogen bonds. \u0000 \u0000Materials and methods: The aim of this study was to investigate the possibility of producing a novel biodegradable blend film from PVA-AHSG with glycerol as plasticizer in the different concentrations. Films were prepared by the casting method using PVA and AHSG (60:40 ratio). Glycerol was used ac plasticizer because it is compatible with PVA-AHSG blend improving film flexibility, facilitating its handling and preventing cracks. The PVA–AHSG blend film was prepared with different glycerol concentration (20–70%, w/w","PeriodicalId":52634,"journal":{"name":"mjlh pjwhshhy `lwm w Sny` Gdhyy yrn","volume":"12 1","pages":"663-677"},"PeriodicalIF":0.0,"publicationDate":"2017-01-12","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"48700248","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 8
EXTRACTION OF CRUDE EXTRACT FROM MALVA NEGLECTA LEAVES AND EVALUATION OF ITS FREE RADICAL SCAVENGING ACTIVITIES 玛尔玛叶粗提物的提取及其清除自由基活性的评价
Pub Date : 2017-01-01 DOI: 10.22067/IFSTRJ.V1395I0.47538
H. Jouyandeh, V. Samavati
Introduction: Accumulation of free radicals could lead to permanent oxidative destruction of organisms by attacking macromolecules and organelles of the body, thus causing organism aging, fatigue and degenerative diseases. Therefore, discovering and developing safe and non-toxic natural antioxidants has been an interesting topic in recent decades. Compared to synthetic antioxidants, extracts from plant resources usually have quite stable constructions and great antioxidant activities, and can easily be absorbed without dangerous immunoreactions. Many antioxidant compounds, naturally occurring from plant sources, have been identified as free radicals or active oxygen scavengers. Malva neglecta (MN), which is known as Panirak/Tooleh in Iran is an annual and herbaceous plant. The leaves and flowers of MN are used in traditional phytotheraphy and in treatment of cough, respiratory system and digestive system problems. The objective of this study was to optimize process conditions of extraction in order to obtain the highest yield from crude extract of MN leaves and identify its antioxidant properties. Materials and methods: Three-variable-three-level Box-Behnken design-response surface methodology (BBD-RSM) with five replications at central point was used to optimize the extracting parameters of crude extract from the MN leaves including extraction time (1-8 h), extraction temperature (50-100°C), and the water/solid ratio (3-30). The ability of extracted materials to scavenge the free radicals of DPPH, OH and super oxide was also evaluated by chemical analysis. Results and Discussion: All three independent variables effected the yield of crude extract of MN leaves. The extraction yield of MN crude extract significantly increased from 5.90% to 8.01% with extraction time varying from 1 h to 6 h. However, the yield was not altered meaningfully, as the extraction time was increased from 6 h up to 8 h. This may be due to degradation of the polysaccharides because of the extended extraction time. The extraction process was performed with temperatures from 50 °C to 100 °C, with the other extraction variables such as ratio of water to raw material and extraction time fixed at 13 ml/g and 3.5 h, respectively. The extraction yield of crude extract increased with increasing extraction temperature and peaked at 7.89 at 100 °C. Different ratios of water to raw material have considerable effect on extraction yield. In this study, we used ratios of water to raw material from 3 to 30 ml/g, with fixed parameters (extraction time and extraction temperature at 3.5 h and 75 °C, respectively). Extraction yield increased noticeably from 6.10 to 8.10 with ratio of water to material varying from 3 ml/g to 24 ml/g. As extraction time, at the higher experimental levels, as the ratio of water to raw material was increased (from 24 up to 30 ml/g) the yield of crude extract was not changed considerably. Under the appropriate condition of ratio of water to raw material, th
自由基的积累可以通过攻击机体的大分子和细胞器,导致机体永久性的氧化破坏,从而引起机体衰老、疲劳和退行性疾病。因此,发现和开发安全无毒的天然抗氧化剂已成为近几十年来的热门课题。与人工合成的抗氧化剂相比,植物提取物结构稳定,抗氧化活性高,易于吸收,无危险的免疫反应。从植物中自然产生的许多抗氧化化合物已被确定为自由基或活性氧清除剂。Malva ignorta (MN),在伊朗被称为Panirak/Tooleh,是一种一年生草本植物。锰的叶子和花被用于传统的植物疗法和治疗咳嗽,呼吸系统和消化系统的问题。本研究的目的是优化提取工艺条件,以获得锰叶粗提物的最高得率,并鉴定其抗氧化性能。材料与方法:采用3变量-3水平Box-Behnken设计-响应面法(BBD-RSM),以5个重复为中心优化提取时间(1 ~ 8 h)、提取温度(50 ~ 100℃)、水固比(3 ~ 30)。通过化学分析评价了提取物对DPPH、OH和超氧化物自由基的清除能力。结果与讨论:三个自变量均影响锰叶粗提物的得率。MN粗提物提取率在1 ~ 6 h范围内从5.90%显著提高到8.01%,但在6 ~ 8 h范围内没有明显变化,这可能是由于提取时间延长导致多糖降解所致。提取温度为50 ~ 100℃,水料比为13 ml/g,提取时间为3.5 h。粗提物的提取率随着提取温度的升高而增加,在100℃时达到峰值7.89。不同的水与原料的比例对萃取率有相当大的影响。在本研究中,我们使用水与原料的比例为3 ~ 30 ml/g,固定参数(提取时间为3.5 h,提取温度为75℃)。当水料比从3 ml/g到24 ml/g变化时,提取率从6.10显著提高到8.10。随着提取时间的增加,在较高的实验水平上,随着水料比的增加(从24 ml/g增加到30 ml/g),粗提物的得率没有明显变化。在适当的水料比条件下,粗提物分子可以充分膨胀,更多的化合物可以溶于水,从而提高提取率。决定系数(R2 = 0.9897)表明模型有效,表明拟合模型可以解释98.97%的变异。采用调整后的决定系数评价实验值与预测值的相关性,结果(R2Adj= 0.9794)表明相关性显著。“缺乏拟合”的f值(1.49)表明“缺乏拟合”相对于纯误差不显著(p > 0.05)。MN叶片产量的CV值为0.64%,具有较好的信度。模型的适当精度值为21.61,PRESS为0.42,表明可以设计出合适的模型。在多元回归分析中,自变量和响应变量的二次多项式方程表示为:Y =7.82 + 1.025X1 + 3.241667X2 + 2.031X3 + 0.525X1X2 - 0.7X1X3 + 0.675X2X3 - 0.206X12 - 0.21833X22其中,Y为提取率(%);X1,提取时间(h);X2,萃取温度;X3为水料比(ml/g)。统计分析结果表明,提取时间为6 h,提取温度为90℃,水料比为19时提取率较高。在此条件下,实验产率为9.22%±0.47%,与预测值9.18%吻合较好;实验收率为9.18%。化学分析结果表明,随着MN粗提物浓度的增加,其DPPH、OH和超氧化物清除能力迅速增强。在最大当量浓度(300 ppm)下,粗提物对DPPH的清除率高于BHT标准(89%对78%)。 自由基的积累可以通过攻击机体的大分子和细胞器,导致机体永久性的氧化破坏,从而引起机体衰老、疲劳和退行性疾病。因此,发现和开发安全无毒的天然抗氧化剂已成为近几十年来的热门课题。与人工合成的抗氧化剂相比,植物提取物结构稳定,抗氧化活性高,易于吸收,无危险的免疫反应。从植物中自然产生的许多抗氧化化合物已被确定为自由基或活性氧清除剂。Malva ignorta (MN),在伊朗被称为Panirak/Tooleh,是一种一年生草本植物。锰的叶子和花被用于传统的植物疗法和治疗咳嗽,呼吸系统和消化系统的问题。本研究的目的是优化提取工艺条件,以获得锰叶粗提物的最高得率,并鉴定其抗氧化性能。材料与方法:采用3变量-3水平Box-Behnken设计-响应面法(BBD-RSM),以5个重复为中心优化提取时间(1 ~ 8 h)、提取温度(50 ~ 100℃)、水固比(3 ~ 30)。通过化学分析评价了提取物对DPPH、OH和超氧化物自由基的清除能力。结果与讨论:三个自变量均影响锰叶粗提物的得率。MN粗提物提取率在1 ~ 6 h范围内从5.90%显著提高到8.01%,但在6 ~ 8 h范围内没有明显变化,这可能是由于提取时间延长导致多糖降解所致。提取温度为50 ~ 100℃,水料比为13 ml/g,提取时间为3.5 h。粗提物的提取率随着提取温度的升高而增加,在100℃时达到峰值7.89。不同的水与原料的比例对萃取率有相当大的影响。在本研究中,我们使用水与原料的比例为3 ~ 30 ml/g,固定参数(提取时间为3.5 h,提取温度为75℃)。当水料比从3 ml/g到24 ml/g变化时,提取率从6.10显著提高到8.10。随着提取时间的增加,在较高的实验水平上,随着水料比的增加(从24 ml/g增加到30 ml/g),粗提物的得率没有明显变化。在适当的水料比条件下,粗提物分子可以充分膨胀,更多的化合物可以溶于水,从而提高提取率。决定系数(R2 = 0.9897)表明模型有效,表明拟合模型可以解释98.97%的变异。采用调整后的决定系数评价实验值与预测值的相关性,结果(R2Adj= 0.9794)表明相关性显著。“缺乏拟合”的f值(1.49)表明“缺乏拟合”相对于纯误差不显著(p > 0.05)。MN叶片产量的CV值为0.64%,具有较好的信度。模型的适当精度值为21.61,PRESS为0.42,表明可以设计出合适的模型。在多元回归分析中,自变量和响应变量的二次多项式方程表示为:Y =7.82 + 1.025X1 + 3.241667X2 + 2.031X3 + 0.525X1X2 - 0.7X1X3 + 0.675X2X3 - 0.206X12 - 0.21833X22其中,Y为提取率(%);X1,提取时间(h);X2,萃取温度;X3为水料比(ml/g)。统计分析结果表明,提取时间为6 h,提取温度为90℃,水料比为19时提取率较高。在此条件下,实验产率为9.22%±0.47%,与预测值9.18%吻合较好;实验收率为9.18%。化学分析结果表明,随着MN粗提物浓度的增加,其DPPH、OH和超氧化物清除能力迅速增强。在最大当量浓度(300 ppm)下,粗提物对DPPH的清除率高于BHT标准(89%对78%)。 此外,MN粗提物在最高实验浓度(150 ppm)下对OH和超氧化物的清除能力(分别为87%和91%)显著高于抗坏血酸标准溶液(分别为74%和81%)。结果表明,从马来籽叶中提取的成分可能具有抗氧化和清除自由基的作用。这项研究可以帮助食品工业在不同的食品、化妆品和药品中添加具有一定功能的新水胶体来源作为替代添加剂。 此外,MN粗提物在最高实验浓度(150 ppm)下对OH和超氧化物的清除能力(分别为87%和91%)显著高于抗坏血酸标准溶液(分别为74%和81%)。结果表明,从马来籽叶中提取的成分可能具有抗氧化和清除自由基
{"title":"EXTRACTION OF CRUDE EXTRACT FROM MALVA NEGLECTA LEAVES AND EVALUATION OF ITS FREE RADICAL SCAVENGING ACTIVITIES","authors":"H. Jouyandeh, V. Samavati","doi":"10.22067/IFSTRJ.V1395I0.47538","DOIUrl":"https://doi.org/10.22067/IFSTRJ.V1395I0.47538","url":null,"abstract":"Introduction: Accumulation of free radicals could lead to permanent oxidative destruction of organisms by attacking macromolecules and organelles of the body, thus causing organism aging, fatigue and degenerative diseases. Therefore, discovering and developing safe and non-toxic natural antioxidants has been an interesting topic in recent decades. Compared to synthetic antioxidants, extracts from plant resources usually have quite stable constructions and great antioxidant activities, and can easily be absorbed without dangerous immunoreactions. Many antioxidant compounds, naturally occurring from plant sources, have been identified as free radicals or active oxygen scavengers. Malva neglecta (MN), which is known as Panirak/Tooleh in Iran is an annual and herbaceous plant. The leaves and flowers of MN are used in traditional phytotheraphy and in treatment of cough, respiratory system and digestive system problems. The objective of this study was to optimize process conditions of extraction in order to obtain the highest yield from crude extract of MN leaves and identify its antioxidant properties. Materials and methods: Three-variable-three-level Box-Behnken design-response surface methodology (BBD-RSM) with five replications at central point was used to optimize the extracting parameters of crude extract from the MN leaves including extraction time (1-8 h), extraction temperature (50-100°C), and the water/solid ratio (3-30). The ability of extracted materials to scavenge the free radicals of DPPH, OH and super oxide was also evaluated by chemical analysis. Results and Discussion: All three independent variables effected the yield of crude extract of MN leaves. The extraction yield of MN crude extract significantly increased from 5.90% to 8.01% with extraction time varying from 1 h to 6 h. However, the yield was not altered meaningfully, as the extraction time was increased from 6 h up to 8 h. This may be due to degradation of the polysaccharides because of the extended extraction time. The extraction process was performed with temperatures from 50 °C to 100 °C, with the other extraction variables such as ratio of water to raw material and extraction time fixed at 13 ml/g and 3.5 h, respectively. The extraction yield of crude extract increased with increasing extraction temperature and peaked at 7.89 at 100 °C. Different ratios of water to raw material have considerable effect on extraction yield. In this study, we used ratios of water to raw material from 3 to 30 ml/g, with fixed parameters (extraction time and extraction temperature at 3.5 h and 75 °C, respectively). Extraction yield increased noticeably from 6.10 to 8.10 with ratio of water to material varying from 3 ml/g to 24 ml/g. As extraction time, at the higher experimental levels, as the ratio of water to raw material was increased (from 24 up to 30 ml/g) the yield of crude extract was not changed considerably. Under the appropriate condition of ratio of water to raw material, th","PeriodicalId":52634,"journal":{"name":"mjlh pjwhshhy `lwm w Sny` Gdhyy yrn","volume":"13 1","pages":"167-179"},"PeriodicalIF":0.0,"publicationDate":"2017-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"68574424","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 2
期刊
mjlh pjwhshhy `lwm w Sny` Gdhyy yrn
全部 Acc. Chem. Res. ACS Applied Bio Materials ACS Appl. Electron. Mater. ACS Appl. Energy Mater. ACS Appl. Mater. Interfaces ACS Appl. Nano Mater. ACS Appl. Polym. Mater. ACS BIOMATER-SCI ENG ACS Catal. ACS Cent. Sci. ACS Chem. Biol. ACS Chemical Health & Safety ACS Chem. Neurosci. ACS Comb. Sci. ACS Earth Space Chem. ACS Energy Lett. ACS Infect. Dis. ACS Macro Lett. ACS Mater. Lett. ACS Med. Chem. Lett. ACS Nano ACS Omega ACS Photonics ACS Sens. ACS Sustainable Chem. Eng. ACS Synth. Biol. Anal. Chem. BIOCHEMISTRY-US Bioconjugate Chem. BIOMACROMOLECULES Chem. Res. Toxicol. Chem. Rev. Chem. Mater. CRYST GROWTH DES ENERG FUEL Environ. Sci. Technol. Environ. Sci. Technol. Lett. Eur. J. Inorg. Chem. IND ENG CHEM RES Inorg. Chem. J. Agric. Food. Chem. J. Chem. Eng. Data J. Chem. Educ. J. Chem. Inf. Model. J. Chem. Theory Comput. J. Med. Chem. J. Nat. Prod. J PROTEOME RES J. Am. Chem. Soc. LANGMUIR MACROMOLECULES Mol. Pharmaceutics Nano Lett. Org. Lett. ORG PROCESS RES DEV ORGANOMETALLICS J. Org. Chem. J. Phys. Chem. J. Phys. Chem. A J. Phys. Chem. B J. Phys. Chem. C J. Phys. Chem. Lett. Analyst Anal. Methods Biomater. Sci. Catal. Sci. Technol. Chem. Commun. Chem. Soc. Rev. CHEM EDUC RES PRACT CRYSTENGCOMM Dalton Trans. Energy Environ. Sci. ENVIRON SCI-NANO ENVIRON SCI-PROC IMP ENVIRON SCI-WAT RES Faraday Discuss. Food Funct. Green Chem. Inorg. Chem. Front. Integr. Biol. J. Anal. At. Spectrom. J. Mater. Chem. A J. Mater. Chem. B J. Mater. Chem. C Lab Chip Mater. Chem. Front. Mater. Horiz. MEDCHEMCOMM Metallomics Mol. Biosyst. Mol. Syst. Des. Eng. Nanoscale Nanoscale Horiz. Nat. Prod. Rep. New J. Chem. Org. Biomol. Chem. Org. Chem. Front. PHOTOCH PHOTOBIO SCI PCCP Polym. Chem.
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
0
微信
客服QQ
Book学术公众号 扫码关注我们
反馈
×
意见反馈
请填写您的意见或建议
请填写您的手机或邮箱
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
现在去查看 取消
×
提示
确定
Book学术官方微信
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术
文献互助 智能选刊 最新文献 互助须知 联系我们:info@booksci.cn
Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。
Copyright © 2023 Book学术 All rights reserved.
ghs 京公网安备 11010802042870号 京ICP备2023020795号-1