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Changes of surface properties of sucrose particles during grinding in a cocoa butter-based suspension and their influence on the macroscopic behavior of the suspension 可可脂基悬浮液研磨过程中蔗糖颗粒表面性质的变化及其对悬浮液宏观行为的影响
IF 3 3区 农林科学 Q2 FOOD SCIENCE & TECHNOLOGY Pub Date : 2024-04-14 DOI: 10.1007/s00217-024-04542-8
Knut Franke, Ute Bindrich, Sarah Schroeder, Volker Heinz, Dana Middendorf

Chocolate mass is a cocoa butter-based suspension, which mainly consists of sugar and cocoa particles dispersed in a continuous lipid phase. During chocolate manufacturing, sugar particles have to be ground to sizes below 25–30 µm. Such a fine grinding is carried out either by five roll refiners or by ball mills. Despite obtaining similar particle size distributions at the end, the grinding procedures result in different chocolate mass properties. The reasons for that are not fully understood, so far. Therefore, changes in particle sizes and surface properties of sucrose particles as well as their interactions with surrounding cocoa butter during the different grinding processes were investigated including atomic force microscopy techniques to characterize local surface states. It was found that especially the alteration of surfaces during continued grinding differed. In the case of roller grinding, surface states became more inhomogeneous and different surfaces states at microscopic level existed in parallel. More homogenous surfaces but with a higher degree of amorphous states were formed during grinding in the ball mill. Variations in macroscopic behavior of the suspension can be explained by the differences in interaction of particles with each other and with the surrounding lipid phase.

巧克力块是一种以可可脂为基础的悬浮液,主要由分散在连续脂相中的糖和可可颗粒组成。在巧克力生产过程中,糖粒子必须研磨到 25-30 微米以下。这种精细研磨是通过五辊精炼机或球磨机进行的。尽管最终得到的颗粒大小分布相似,但研磨程序却导致巧克力的质量特性不同。其原因至今尚未完全明了。因此,我们采用原子力显微镜技术研究了不同研磨过程中蔗糖颗粒的粒度和表面特性的变化,以及它们与周围可可脂的相互作用,以确定局部表面状态的特征。研究发现,在持续研磨过程中,表面的变化尤其不同。在滚筒研磨的情况下,表面状态变得更加不均匀,不同的表面状态在微观层面上平行存在。在球磨机中研磨时,形成的表面更均匀,但无定形状态程度更高。悬浮液宏观行为的变化可以用颗粒之间以及颗粒与周围脂相之间相互作用的差异来解释。
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引用次数: 0
Impact of the reduction or replacement of NaCl during production and ripening of raw cured pork and turkey sausages 在生腌猪肉和火鸡肠的生产和成熟过程中减少或替代氯化钠的影响
IF 3 3区 农林科学 Q2 FOOD SCIENCE & TECHNOLOGY Pub Date : 2024-04-13 DOI: 10.1007/s00217-024-04528-6
Mona Wagner, Madeleine Ploetz, Carsten Krischek

There are health concerns with regard to the consumption of sodium. Excessive consumption of sodium is suspected to cause high blood pressure, among other things. Therefore, sodium should be reduced or replaced during the production of food. In the present study, in the first part, raw fermented sausages from pork and turkey meat, produced with reduced NaCl concentrations, were investigated. In a second part, the salts, potassium chloride, magnesium chloride, and calcium chloride were added to the sausages, replacing 50% of NaCl. To elucidate, if the reduction or replacement influences the quality of the sausages, physicochemical and microbiological parameters of the products were analyzed. The data show that a reduction of sodium chloride partly influences the hardness and water activity results of raw fermented sausages, made from pork and turkey meat, the redness and nitrite content of the pork sausages, and the ripening losses and total viable counts of the turkey products. Raw fermented sausages with potassium, magnesium, and calcium as partial substitutes for sodium had differing water activity, pH, hardness, and microbiological results using pork and differing pH, hardness, and microbiological results using turkey meat. A bactericidal effect was observed in raw fermented sausages with calcium chloride in inoculation tests with Listeria monocytogenes due to the pH reduction due to calcium. The results indicate that reduction and replacement of NaCl can influence the final products. Therefore, the producers should carefully evaluate before alteration the NaCl content, if this change influences the product acceptability.

钠的摄入存在健康问题。过量摄入钠被怀疑会导致高血压等疾病。因此,在食品生产过程中应减少或替代钠的摄入。在本研究中,第一部分调查了用氯化钠浓度降低的猪肉和火鸡肉制作的生发酵香肠。第二部分是在香肠中添加盐、氯化钾、氯化镁和氯化钙,取代 50%的氯化钠。为了弄清减少或替代是否会影响香肠的质量,对产品的理化和微生物参数进行了分析。数据显示,氯化钠的减少会部分影响猪肉和火鸡肉制成的生发酵香肠的硬度和水活性结果、猪肉香肠的红度和亚硝酸盐含量,以及火鸡肉产品的成熟损失和总活菌数。用钾、镁和钙部分替代钠的生发酵香肠,猪肉的水活性、pH 值、硬度和微生物结果不同,火鸡肉的 pH 值、硬度和微生物结果也不同。在单核细胞增生李斯特菌的接种试验中,由于钙降低了 pH 值,在使用氯化钙的生发酵香肠中观察到了杀菌效果。结果表明,减少和替代氯化钠会影响最终产品。因此,生产商在改变氯化钠含量之前,应仔细评估这种改变是否会影响产品的可接受性。
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引用次数: 0
Uncovering changes in mulberry brandy during artificial aging using flavoromics 利用风味组学揭示桑葚白兰地在人工陈酿过程中的变化
IF 3 3区 农林科学 Q2 FOOD SCIENCE & TECHNOLOGY Pub Date : 2024-04-13 DOI: 10.1007/s00217-024-04502-2
Baolin Han, Shulin Tian, Shenhai Zheng, Yuqi Jiang, Minghong Bian

The addition of oak chips is one of the basic techniques for artificial aging of brandy, but its effect on mulberry brandy flavor is unknown. In this study, the effect of oak chips addition on the aging of mulberry brandy and the evolution of volatile compounds during the aging process were investigated using flavoromics techniques. The results showed that the 15 g/l oak chips had the highest ethyl acetate content and the highest sensory scores at 30 °C aging conditions, with the tannin and total phenol contents at 233.7 ± 6.4 mg/l and 15.83 ± 1.18 mg/l, respectively. Through Partial least squares discriminant analysis (PLS-DA) and correlation analysis, 12 essential compounds during aging were identified, among which Ethyl acetate, Whiskey lactone, Furfural, and Vanillin also showed a positive correlation with aroma intensity, positively influencing the quality of mulberry brandy, resulting in a richer brandy flavor. The results of the study provide a theoretical basis and reference for the artificial aging technology of mulberry brandy.

添加橡木片是白兰地人工陈酿的基本技术之一,但其对桑树白兰地风味的影响尚不清楚。本研究采用风味组学技术研究了添加橡木片对桑树白兰地陈酿的影响以及陈酿过程中挥发性化合物的演变。结果表明,在 30 °C 的陈酿条件下,15 g/l 橡木片的乙酸乙酯含量最高,感官评分最高,单宁和总酚含量分别为 233.7 ± 6.4 mg/l 和 15.83 ± 1.18 mg/l。通过偏最小二乘判别分析(PLS-DA)和相关分析,确定了 12 种陈酿过程中的必需化合物,其中乙酸乙酯、威士忌内酯、糠醛和香兰素还与香气强度呈正相关,对桑葚白兰地的品质产生了积极影响,使白兰地的风味更加丰富。研究结果为桑树白兰地的人工陈酿技术提供了理论依据和参考。
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引用次数: 0
Phenolic profile, antioxidant properties, and pollen spectra of Iranian-originated honeys 伊朗原产蜂蜜的酚类概况、抗氧化特性和花粉光谱
IF 3 3区 农林科学 Q2 FOOD SCIENCE & TECHNOLOGY Pub Date : 2024-04-13 DOI: 10.1007/s00217-024-04539-3
Adel Hajian-Tilaki, Reza Esmaeilzadeh Kenari, Razie Razavi, Reza Farahmandfar

This study was intended to determine the melissopalynological characteristics, LAB color, browning index, total phenolic content, antioxidant activity, phenolic profile, and their correlations within Iranian honeys. Ten honey samples were collected from beekeepers in various floristic regions of Iran, along with two commercial multi-floral samples. To determine the antioxidant activity, three methods of 2,2-diphenyl-1-picrylhydrazyl (DPPH) radical scavenging, β-carotene bleaching, and Ferric reducing/antioxidant power (FRAP) were used. Phenolic compounds were analyzed by high-performance liquid chromatography with diode-array detection (HPLC–DAD). Pollen analysis revealed that bees primarily fed on the Fabaceae and Asteraceae families in the Iranian flora. The local samples were taxonomically categorized as multi-floral honey. Besides, the commercial samples demonstrated the lowest levels of total phenolics and relatively poor antioxidant activity across all three methods. Syringic acid and luteolin were the predominant phenolic compounds in all samples. A strong correlation (p < 0.01) was found between color, melanoidin content and antioxidant activity, while no significant correlation existed between phenolic content and antioxidant activity. Overall, the results confirmed that examined multi-floral honeys exhibited inferior antioxidant activity compared to studies conducted in other regions worldwide, possibly due to sugar-fed bees, insufficient levels of potent phenolic constituents, and post-harvest thermal treatments.

本研究旨在确定伊朗蜂蜜的蜜源学特征、LAB 颜色、褐变指数、总酚含量、抗氧化活性、酚类概况及其相关性。研究人员从伊朗不同花卉产区的蜂农那里收集了 10 份蜂蜜样品,以及两份商业多花蜂蜜样品。为测定抗氧化活性,采用了 2,2-二苯基-1-苦基肼(DPPH)自由基清除、β-胡萝卜素漂白和铁还原/抗氧化能力(FRAP)三种方法。酚类化合物采用高效液相色谱-二极管阵列检测法(HPLC-DAD)进行分析。花粉分析表明,蜜蜂主要采食伊朗植物区系中的豆科和菊科花粉。当地样品在分类学上被归类为多花蜜。此外,在所有三种方法中,商品样品的总酚类物质含量最低,抗氧化活性相对较差。丁香酸和木犀草素是所有样品中最主要的酚类化合物。色泽、类黑色素含量和抗氧化活性之间存在很强的相关性(p <0.01),而酚类含量和抗氧化活性之间没有明显的相关性。总之,研究结果证实,与世界其他地区的研究相比,受检的多花蜂蜜的抗氧化活性较低,这可能是由于蜜蜂以糖为食、有效酚类成分含量不足以及采后热处理造成的。
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引用次数: 0
An update on citrus polymethoxyflavones: chemistry, metabolic fate, and relevant bioactivities 柑橘多甲氧基黄酮的最新情况:化学、代谢命运和相关生物活性
IF 3 3区 农林科学 Q2 FOOD SCIENCE & TECHNOLOGY Pub Date : 2024-04-11 DOI: 10.1007/s00217-024-04529-5
Rosa Toledo, María Tomás-Navarro, Jose Enrique Yuste, Pasquale Crupi, Fernando Vallejo

Polymethoxyflavones (PMFs) occur naturally in citrus peels and citrus-derived foods as well as in other plants. Many in vitro and some in vivo studies have shown potentially relevant biological effects of PMFs, including anticancer, anti-inflammatory, anti-atherosclerosis, and neuroprotective activities. These promising biological effects still require further research to establish their impact on human health. This review updates the current clinical trials data. It highlights the limited information available on the bioavailability and metabolism of PMFs (pharmacokinetics, human phase I and II metabolites in biological fluids and tissues, and gut microbiota metabolism).

多甲氧基黄酮(PMFs)天然存在于柑橘皮、柑橘衍生食品以及其他植物中。许多体外研究和一些体内研究表明,多甲氧基黄酮具有潜在的相关生物效应,包括抗癌、抗炎、抗动脉粥样硬化和神经保护活性。这些有前景的生物效应仍需要进一步研究,以确定它们对人类健康的影响。本综述更新了当前的临床试验数据。它强调了有关 PMFs 生物利用率和新陈代谢(药代动力学、生物液体和组织中的人体 I 期和 II 期代谢物以及肠道微生物群新陈代谢)的有限信息。
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引用次数: 0
Comparative study of thermal behavior of mango kernel fat from seven Ivorian varieties related to their chemical composition 与化学成分有关的科特迪瓦七个品种的芒果核脂肪热行为比较研究
IF 3 3区 农林科学 Q2 FOOD SCIENCE & TECHNOLOGY Pub Date : 2024-04-11 DOI: 10.1007/s00217-024-04538-4
Alfred Kouakou Kouassi, Taofic Alabi, Elise Amoin N’guessan, Giorgia Purcaro, Sabrina Moret, Mohamed Cissé, Christophe Blecker, Sabine Danthine

In the present study, the fatty acid composition (FAC), triacylglycerol (TAG) composition, crystallization, and melting behaviors of mango kernel fats (MKFs) extracted from seven Ivorian mango varieties—Amelie (AM), Kent (KT), Palmer (PR), Keitt (KI), Brooks (BR), Dadiani (DI), and Djakoumankoun (DN)—were characterized by complementary techniques: pNMR, DSC, polarized light microscopy, and X-ray diffraction. Regardless of the variety, Ivorian MKF is rich in stearic (St) and oleic (O) fatty acids. (72–84% of the total FA), with three main TAGs: StOSt (23.9–45.8%), StOO (15.5–25.8%), and StLSt (10.4–12.5%). Their crystallization onset temperature (Tco) ranged from 15 to 20 °C. All samples showed complete melting around 35 °C, except DN (~ 38 °C). The β-polymorph appeared to be the most predominant and stable polymorph for the seven MKFs. The thermal properties investigated were linked to monounsaturated and triunsaturated triacylglycerol content, indicating the significant influence of chemical composition. The fine analysis of the results allows the seven Ivorian varieties to be divided into four groups, based on both their physical properties and thermal behavior, and the StOSt wealth: hard high-StOSt fat (DN), half-hard medium-StOSt fat (DI, BR), soft low-StOSt fat (KT, PR, KI), and very-soft very-low-StOSt fat (AM). The seven investigated mango varieties from Ivory Coast might offer a wide range of applications in food, pharmaceutical, and cosmetic industries.

本研究采用互补技术,对从七个科特迪瓦芒果品种--梅莉(AM)、肯特(KT)、帕尔默(PR)、基特(KI)、布鲁克斯(BR)、达迪亚尼(DI)和贾库曼昆(DN)--中提取的芒果核脂肪(MKFs)的脂肪酸组成(FAC)、三酰甘油(TAG)组成、结晶和熔化行为进行了表征:对核磁共振、DSC、偏光显微镜和 X 射线衍射进行了表征。无论品种如何,科特迪瓦 MKF 都富含硬脂酸(St)和油酸(O)。(占总脂肪酸的 72-84%),主要有三种 TAG:StOSt(23.9-45.8%)、StOO(15.5-25.8%)和 StLSt(10.4-12.5%)。它们的结晶起始温度(Tco)在 15 至 20 °C 之间。除 DN(约 38 °C)外,所有样品都在 35 °C左右完全熔化。在七种 MKF 中,β 多晶体似乎是最主要和最稳定的多晶体。所研究的热特性与单不饱和和三不饱和三酰甘油的含量有关,这表明化学成分的影响很大。通过对结果进行精细分析,可以根据物理特性和热行为以及 StOSt 富集程度将七个科特迪瓦品种分为四组:硬质高 StOSt 脂肪(DN)、半硬质中等 StOSt 脂肪(DI、BR)、软质低 StOSt 脂肪(KT、PR、KI)和极软质极低 StOSt 脂肪(AM)。所调查的七个象牙海岸芒果品种可在食品、制药和化妆品行业中广泛应用。
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引用次数: 0
The Mortiño (Vaccinium floribundum Kunth): a review of its suitability as a promissory crop in the Ecuadorian Paramo and its potential uses, environmental role, and health benefits 莫蒂诺(Vaccinium floribundum Kunth):对其作为厄瓜多尔帕拉莫地区前景广阔的作物的适宜性及其潜在用途、环境作用和健康益处的审查
IF 3 3区 农林科学 Q2 FOOD SCIENCE & TECHNOLOGY Pub Date : 2024-04-11 DOI: 10.1007/s00217-024-04546-4
Jorge Caranqui Aldaz, Lucía Andreu-Coll, Rafael Martínez Font, Francisca Hernández García

The mortiño (Vaccinium floribundum Kunth), belonging to the Ericaceae family, is a native species of the Ecuadorian paramos. It has a shrub-like habit and produces edible fruits. In the Neotropics, it is primarily found in the Andes of Colombia and Ecuador, thriving in humid environments up to an elevation of 3700 m above sea level. In this review, a selection of studies was carried out that evaluated the taxonomy, reproduction biology, and nutraceutical, environmental properties, and industrial use of the mortiño (V. floribundum). The data gathered from various bioassays were essential in determining the appropriate techniques for tissue differentiation and assessing the quality of resulting plants. This work aims to generate a deep knowledge of the cultivation of mortiño, as well as the properties of its fruits and the benefits they provide for health. These are rich in compounds with antioxidant activity, so the consumption of V. floribundum fruits is related to health benefits. Besides, the environmental role of V. floribundum and its applications in various industries, especially in the development of nanoparticles contributes to the valorization of this plant. Overall, this research contributes to establishing sustainable methods for the propagation of Vaccinium floribundum, ensuring its successful cultivation and utilization for both commercial purposes and ecological preservation.

莫蒂诺(Vaccinium floribundum Kunth)属于菊科,是厄瓜多尔巴拉莫山脉的原生物种。它的生长习性类似灌木,果实可食用。在新热带地区,它主要分布在哥伦比亚和厄瓜多尔的安第斯山脉,生长在海拔 3700 米以下的潮湿环境中。在这篇综述中,我们选择了一些研究,对莫利诺(V. floribundum)的分类、繁殖生物学、营养保健、环境特性和工业用途进行了评估。从各种生物测定中收集的数据对于确定组织分化的适当技术和评估所产生植物的质量至关重要。这项工作的目的是深入了解毛蕊花的种植、其果实的特性及其对健康的益处。这些果实富含具有抗氧化活性的化合物,因此食用 V. floribundum 果实对健康有益。此外,V. floribundum 的环保作用及其在各行各业的应用,特别是在纳米粒子的开发方面,也有助于提高这种植物的价值。总之,这项研究有助于建立可持续的花叶蔓越橘繁殖方法,确保其成功栽培并用于商业目的和生态保护。
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引用次数: 0
Corn and barley protein concentrates: effects of fractionation and micronization on the chemical, functional, and thermal properties 玉米和大麦浓缩蛋白:分馏和微粉化对化学、功能和热性能的影响
IF 3 3区 农林科学 Q2 FOOD SCIENCE & TECHNOLOGY Pub Date : 2024-04-11 DOI: 10.1007/s00217-024-04544-6
Paola Conte, Maria Paciulli, Marina Mefleh, Fatma Boukid

The present study intends to investigate the impact of fractionation and micronization on the compositional, functional, and thermal characteristics of two protein concentrates derived from corn and barley. Fractionation of protein concentrates (by sieving) resulted in three fractions, i.e., fine (< 100 µm), medium (100–300 µm), and coarse (> 300 µm), while micronization resulted in an average particle size of 30 µm. No specific pattern was observed between particle size and chemical composition of corn and barley protein concentrates due to the complex interplay between particle size, surface area, structural changes, and botanical origin. Protein solubility varied depending on the pH and particle size, showing that the coarse fraction exhibited higher solubility than the fine fraction. For both corn/barley protein concentrates, coarse fraction had higher water-/oil-holding capacity. The barley fine fraction showed high foaming capacity, while all proteins lacked emulsification ability. Across all samples, a trend of increasing enthalpy with decreased particle size was observed, except for micronized barley, where enthalpy decreased, indicating possible protein structural changes. Thus, variations in properties among fractions highlight the importance of particle size in determining the proteins’ functionality for potential applications in food systems.

本研究旨在探讨分馏和微粉化对玉米和大麦两种蛋白质浓缩物的成分、功能和热特性的影响。蛋白质浓缩物的分馏(通过筛分)产生了三种馏分,即细(100 微米)、中(100-300 微米)和粗(300 微米),而微粉化产生的平均粒径为 30 微米。由于粒度、表面积、结构变化和植物来源之间复杂的相互作用,玉米和大麦浓缩蛋白的粒度和化学成分之间没有特定的模式。蛋白质的溶解度随 pH 值和颗粒大小的不同而变化,这表明粗颗粒的溶解度高于细颗粒。玉米/大麦浓缩蛋白中,粗颗粒的持水/持油能力较高。大麦细馏分显示出较高的发泡能力,而所有蛋白质都缺乏乳化能力。在所有样品中,都观察到随着粒度的减小,焓值呈上升趋势,只有微粉大麦的焓值下降,这表明蛋白质结构可能发生了变化。因此,不同馏分之间性质的变化突出表明了粒度在决定蛋白质功能性方面的重要性,这也是蛋白质在食品系统中的潜在应用。
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引用次数: 0
Fourier transform infrared spectroscopy coupled with chemometrics for the monitoring of virgin olive oil quality during storage up to 18 months 傅立叶变换红外光谱法与化学计量学相结合,用于监测初榨橄榄油在长达 18 个月的储存期间的质量
IF 3 3区 农林科学 Q2 FOOD SCIENCE & TECHNOLOGY Pub Date : 2024-04-11 DOI: 10.1007/s00217-024-04505-z
Hicham Zaroual, El Mestafa El Hadrami, Christine Chénè, Romdhane Karoui

This study examines the feasibility of using mid infrared (MIR) spectroscopy for monitoring the quality of 14 Moroccan virgin olive oil samples belonging to three (3) varieties, originated from three (3) geographical origins, extracted with different systems, irrigated and fertilised with different modes.

The application of principal component analysis (PCA) and factorial discriminant analysis (FDA) on MIR spectra data allowed to discriminate perfectly the samples according to their storage time with 96.87% of correct classification.

The obtained results were confirmed following the application of three different multivariate regression tools namely partial least squares regression (PLSR), principal component regression (PCR) and support vector machine regression (SVMR) applied on MIR spectra data, since excellent prediction of R2 = 0.99 and RMSEP = 17.05 days was observed. In addition, the evaluation of the effectiveness of MIR spectroscopy to predict the chemical parameters allowed to obtain excellent validation models with R2 ranging between 0.98 and 0.99 for free acidity, peroxide value, chlorophyll level, k232 and k270.

本研究探讨了使用中红外(MIR)光谱监测 14 个摩洛哥初榨橄榄油样本质量的可行性,这些样本属于三(3)个品种,来自三(3)个地理原产地,使用不同的系统进行提取,并以不同的模式进行灌溉和施肥。在对近红外光谱数据应用了三种不同的多元回归工具,即偏最小二乘法回归(PLSR)、主成分回归(PCR)和支持向量机回归(SVMR)后,所获得的结果得到了证实,因为观察到 R2 = 0.99 和 RMSEP = 17.05 天的出色预测。此外,通过评估近红外光谱对化学参数的预测效果,还获得了极佳的验证模型,游离酸度、过氧化值、叶绿素含量、k232 和 k270 的 R2 在 0.98 和 0.99 之间。
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引用次数: 0
Development and validation of an analytical method for the quantification of capsanthin in chili peppers and products by high-performance liquid chromatography 利用高效液相色谱法开发和验证辣椒及其制品中辣椒素的定量分析方法
IF 3 3区 农林科学 Q2 FOOD SCIENCE & TECHNOLOGY Pub Date : 2024-04-10 DOI: 10.1007/s00217-024-04541-9
Shini Yang, Xue Wang, Xuan Huang, Xiaojun Liao, Zhenzhen Xu

Capsanthin is a natural red–orange pigment present in red paprika and has been proven to have various health benefits. The rising consumption of chili peppers and the global demand of natural color promote the need for capsanthin quantification analysis. In the present study, a high-performance liquid chromatography method was developed for the analysis of capsanthin in chili peppers and their products. The chromatographic and extraction parameters were optimized. The concentration of capsanthin ranged from 0.5 to 200 mg/L which showed good linearity (R2 > 0.99). The LOD and LOQ of samples ranged from 0.014 to 0.092 mg/kg and 0.049–0.12 mg/kg, respectively. The recovery experiment (recovery rate 84.79–103.55%, RSD 1.64–9.27%) and interlaboratory test (the RSD of repeatability and reproducibility was in the range of 3.11–4.06% and 4.66–5.52%, respectively) demonstrated good accuracy, precision, repeatability, and reproducibility of the proposed method. The results indicate that the developed method will be a valuable tool for routine analysis of capsanthin in chili peppers and their products.

辣椒素是一种存在于红辣椒中的天然橙红色色素,已被证实具有多种健康益处。辣椒消费量的增加和全球对天然色素的需求促进了对辣椒素定量分析的需求。本研究开发了一种高效液相色谱法,用于分析辣椒及其制品中的辣椒红色素。对色谱和提取参数进行了优化。辣椒素的浓度范围为 0.5 至 200 mg/L,线性关系良好(R2 为 0.99)。样品的最低检出限(LOD)和最低检测限(LOQ)分别为 0.014 至 0.092 mg/kg 和 0.049-0.12 mg/kg。回收试验(回收率为84.79%~103.55%,RSD为1.64%~9.27%)和实验室间检测(重复性和重现性的RSD分别为3.11%~4.06%和4.66%~5.52%)表明该方法具有良好的准确度、精密度、重复性和重现性。结果表明,所开发的方法将成为辣椒及其制品中辣椒素常规分析的重要工具。
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引用次数: 0
期刊
European Food Research and Technology
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